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By E. C. Tarpley, H. M. Cooper, R. F. Abernethy

The standard method of employing preliminary air-drying to determine the moisture in coal has been criticized with respect to the loss of heating value from excessive air-drying. By this method, the coal is air-dried at approximately 10-15° above room temperature with the loss in weight being less than 0.1 percent per hour, and then the residual moisture at 105°C is determined. The total moisture is calculated from these two values.

Feb 1, 1948

By E. D. Gordner

U. S. Bureau of Mines

Jan 1, 1923

By H. R. Shell

To obtain a better understanding of the crystallization of fluoride containing amphiboles from melts, an investigation of the range of stability between fluoramphi-boles and other minerals was conducted by the Bureau of Mines. This study has shown that the stability of fluoramphiboles is strongly influenced by both fluoride concentration and isomorphic replacement. Over 150 reactions were made with different compositions and reaction conditions. substitutions attempted and the phases that formed when the composition was crystallized by cooling from the melt are discussed. The attainment of equilibrium in these multicomponent systems is not claimed. Many ions that would be expected to enter the amphibole structure instead resulted in crystallization of phases other than amphibole. Those compositions that resulted in a high yield of acicular fluoramphibole by crystallization from the melts are shown in table 2. The fluoramphiboles obtained from melts typically had an acicular crystal habit and a hardness of 6 to 7 on the Mohs' scale. Although many had relatively high length to cross section ratios, none were fibrous; it was concluded that the possibility of synthesizing a fibrous fluoramphibole from a melt was low. However, many compositions can be crystallized into a tough, hard, impact-resistant mass of interlocking acicular crystals.

Jan 1, 1958

By A. W. Deurbrouck

The Bureau of Mines reviewed available data on the effect of crushing high-sulfur coals for the liberation of impurities in the light of increasingly stringent air pollution regulations. The survey, which provided information on Appalachian region coals only, indicated that such important coal- beds as the Upper and Lower Freeport and the Upper Kittanning show significant sulfur reductions when crushed to 14-mesh top size. For many other coalbeds amenability to sulfur liberation by crushing was indicated, although too few samples were available to draw firm conclusions,

Jan 1, 1966

By A. W. Deurbrouck

The Bureau of Mines reviewed available data on the effect of crushing high-sulfur coals for the liberation of impurities in the light of increasingly stringent air pollution regulations. The survey, which provided information on Appalachian region coals only, indicated that such important coal-beds as the Upper and Lower Freeport and the Upper Kittanning show significant sulfur reductions when crushed to 14-mesh top size. For many other coalbeds amenability to sulfur liberation by crushing was indicated, although too few samples were available to draw firm conclusions,

Jan 1, 1966

"U.S. Bureau of Mines Publications and Articles, 1994 with Subject and Author Index Compiled by Office of Public Information U.S. Bureau of Mines (USBM) Department of the InteriorINTRODUCTIONThe U.S. Bureau of Mines (USBM) was established in 1910 to conduct inquiries and scientific and technological investigations on mining and the preparation, treatment, and use of mineral substances; to promote health and safety in the mineral industries; to conserve material resources; to promote economic development; to increase efficiency in the mining, metallurgical, quarrying, and other mineral industries; and to inquire into the economic conditions affecting those industries. The organic act of the Bureau, as amended by Congress and approved February 25, 1913, made it the province and duty of the Bureau of Mines to ""disseminate information concerning these subjects in such manner as will best carry out the purpose of this Act.""In accordance with this directive, USBM reports the findings of its research and investigations in its own series of publications and also in articles that appear in scientific, technical, and trade journals; in proceedings of conventions and seminars; in reference books; and in other non-USBM publications. This edition describes reports and articles published during calendar year 1994. It supplements the 50-year list of Bureau publications issued from July 1, 1910, to January 1, 1960; 1 the 50-year list of articles by Bureau authors published outside the Bureau from July 1, 1910, to January 1, 1960; 2 andthe 5-year lists of publications and articlesfrom January 1, 1960, to December 31, 1964,3from January 1, 1965, to December 31, 1969,4from January 1,1970, to December 31,1974,5from January 1,1975, to December 31,1979,6from January 1,1980, to December 31,1984/and from January 1, 1985, to December 31,1989.8"

May 1, 1995

By F. S. LOTT

The number of petroleum refineries in the United States decreased from 399 on January 1, 1947, to 390 on January 1, 1948. On the latter date two additional refineries were under construction , a large one in New Jersey and a small one in Texas . This Crude oil charging capacity, based on complete facilities only , increased in 1947 from 5,569,482 barrels to 6,034,252 barrels per day , owing to material gains reported in all of the larger refining districts . great increase in effective capacity is only in part the result of the completion of major new units for crude-oil processing . Much of it is due to rearrangement and minor additions to existing facilities to permit more efficient and complete utilization . Recent experience has apparently demonstrated that many processing units are capable , with greater emphasis upon maintenance and precise controls , of sustained operations at higher volumes than were indicated in their old rated capacities . This situation doubtless has caused some upward revision in capacity data .

Aug 1, 1948

By Anil Mahyera

Towards the goal of achieving uniform-high-tensions in roofbolts to provide superior roof support[1-7] for extended periods, Terra Tek installed mechanical-anchor bolts in a mine in eight different ways -- under torque/thrust control with and without hardened washers, belleville washers and tension equalization; in a conventional manner with and without a hardened washer. The various bolt groups were analyzed in terms of their tension uniformity and mean tension levels. Installing the bolts accurately with ? a hardened washer under the bolthead, and ? proper torque/thrust control resulted in the mast uniformly tensioned bolts -- with a coefficient of variation of only 14%, an improvement of 3 times over a conventional installation. Also, these bolts maintained a high tension level -- 80% of the installation tension, compared to 50% achieved conventionally.

Jan 1, 1982

By John R. Bradley

The available supply of fuel and power is a subject of importance at all times and particularly at this time. The following brief survey of fuel and power in the United States appraises the extent of the several primary sources of energy the approximate monthly demand, 1929-40; the chief centers of production and consumption; and shifts in the principal uses from 1929 to recent years. The period covers the boom year 1929, the years of the great depression, the more normal year 1937, the recession in 1938, the year 1939, and 1940 (which was affected by armament programs). In some instances, the data for 1939 and 1940 are preliminary. The four primary sources of fuel and power are coal, petroleum, natural gas, and water power. Wood fuel, important in some regions, and foreign trade in natural gas and hydroelectricity represent a relatively small part of the energy supply and are not considered in this study. The tonnages shown are in terms of coal, based upon the calorific or B. t. u. equivalents of the several sources of power. In practice, the usable heat or energy varies according to the type of equipment available for its use. For example, the efficiency of turbine water wheels and internal-combustion engines is much higher than that of steam plants and household-heating devices.

Jan 1, 1941

By Richard D. Miller, Geraldine P. Norrell

This publication contains routine analyses and related source data for 295 natural gas samples from 18 States collected during calendar year 1963 as part of a continuous survey of the United States for occurrences of helium in natural gas. This survey has been conducted by the Bureau of Mines since 1917. The analyses published herein were made by mass spectrometer and a special helium analysis apparatus, which are described in Bureau of Mines Bulletins 4863 and 576.4 Five previous publications have been made to present the results of 5,998 gas analyses made by the Bureau of Mines Helium Activity , prior to 1963. The first three , Bulletin 486,5 Bulletin 576,6 and Bulletin 617,7/ contain analyses and source data on 5,214 gas samples collected from 1917 to January 1 , 1961. The fourth and fifth publications , which are published as Information Circulars , supplement the three Bulletins and contain 784 analyses of samples collected during 1961 and 1962. The present Information Circular is the third annual publication supplementing the three Bulletins .

Jan 1, 1965

By J. A. Organiscak

Quartz dust is one of the most significant ongoing health concerns in coal mining today. Since the early 1980's, the U.S. Bureau of Mines has conducted numerous studies in underground and surface coal mines to identify the sources of quartz dust and its fundamental characteristics. This report presents data and conclusions obtained from these studies. The two most significant quartz dust sources were found to be the continuous miner excavating rock and the highwall drill operating in a rock overburden. The percentage of quartz was found to be higher in the smaller size fractions of dust when significant amounts of rock were mined by the continuous miner. Another factor theorized to affect quartz dust generation and size characteristics is the morphology of the quartz-bearing rock. Several laboratory studies were conducted to investigate capture efficiency of water spray technology and flooded-bed scrubbers with respect to the particle size of the dust. Water sprays and flooded-bed scrubbers were both found to be less efficient on smaller dust particles, and the scrubber was particularly less efficient on quartz dust. These results indicate that quartz control technology should be directed at controlling smaller sized dust particles.

Jan 1, 1990

By N. A. C. Smith, E. W. Dean, W. A. Jacobs, H. H. Hill

Fractional distillation is the most important process in the commercial refining of petroleum. The same procedure, conducted on a small scale, is the basis of a number of analytical methods of wide application in the petroleum laboratory. The Bureau of Mines has studied apparatus and procedure for the distillation analysis of petroleum, and this report is presented as a record of developments up to the present time. The work is incomplete, but the extensive information that has been obtained to date is made available as a guide in handling laboratory distillation problems. The analytical distillation of petroleum is commonly made to determine range of boiling points or to separate the oil. into fractions for detailed examination, or both. When only one of these two ends is sought the procedure involved is notably simpler than when, as is more common, information is required regarding both boiling range and properties of fractions. Moreover the degree of minuteness of measurement and the accuracy of the data required from analytical distillations differ considerably. Often the simplest sort of comparative figures are satisfactory; other tests require complicated and highly tedious procedure. No one distillation method is universally applicable, and it is impossible for anyone group of investigators to foresee all the different kinds of requirements that may occur in the industry.

Jan 1, 1922

By Zsuzsanna Zborovszky

Study of the energy transfer from an inductive circuit to the discharge under the conditions of the minimum discharge voltage being smaller than the source voltage. Analysis of the effect of the electrode separation speed on the duration and maximum power amplitude of the discharge. Recommendation for optimal electrode setting. Experimental data on the variation of maximum discharge power required for ignition as a function of volumetric gas content for methane-air and propane-air mixtures. Experimental determination of the ignition limit for discharges derived from a 24, 15, 10 and 6v inductive-resistive circuit in 8.3% methane-air mixture by using the PTB breakflash with Cd disc and W wires, and also with Cu disc and BeCu wires. Method for calculating ignition limits for other source voltages.

Jan 1, 1978

By Frank J. Weibelt

In accordance with provisions of the Strategic Minerals Act of 1939, the Bureau of Mines surveyed the chromite occurrences in California. The Seiad Creek deposit afforded excellent opportunity for developing reserves that could be used by the nation in case of critical shortages of the mineral. Subsequently an exploration and development program was undertaken in April 1941, which was concluded in October of the same year. Work included road construction, diamond drilling, drifting and crosscutting, surface trenching, and sampling.

Jan 1, 1949

By J. K. Whyatt

The U.S. Bureau of Mines conducted an overcore stress measurement on the 5300 level of the Lucky Friday Mine, Mullan, ID, to investigate the stress regime around an experimental stope in a rock-burst-prone mine. The result indicated a stress field with unexpected magnitude and orientation [s 1 ?135 MPa (19,600 psi) oriented S 80° W). An unusual amount of rock-burst activity was encountered during subsequent excavation. A careful review of the overcore data suggested the overcore strain measurements were valid. Moreover, concentrated rock-burst activity suggested that the measured stress field did exist, but was localized and therefore did not represent the far-field in situ stress field.

Jan 1, 2010

By J. Grumer

The Bureau of Mines, under the sponsorship of the Space Nuclear Propulsion Office, conducted a laboratory-scale hydrogen safety study which determined several combustion characteristics of hydrogen diffusion flames. Experiments show that ambient air may enter the top of a hydrogen flare stack when the hydrogen flow is low. A new concept, supported by photographic evidence, predicts that diffusion flames burning in air on a wide, upright pipe (stack) and fed with slow, upward flows of buoyant gas will induce a downward flow of air along the walls of the pipe that can support combustion within the pipe. Predicted flamedip limits agree roughly with experimental values determined on 6-, 12-, and 18-inch-diameter stacks and increase with increasing stack diameter. Measurements were made of the limiting flow at which a hydrogen diffusion flame blows out in still air. By means of an empirical application of the critical boundary 8 velocity gradient concept, these data lead to a blowout limit of about 10 reciprocal seconds for a hydrogen diffusion flame. Burning rates of large hydrogen diffusion flames ranging from about 0.03 to 1 ft/sec were used to predict approximate flame heights on flare stacks. Temperatures of larger hydrogen diffusion flames up to about 3,600° F were observed, but the most representative value appears to be about 2,600° F. It was found that crosswinds do not strip significant amounts of unburned hydrogen from its diffusion flame and that water-cooled flare stacks are not likely to be damaged when flame is blown back into them by opposing winds.

Jan 1, 1970

By William Cochran

Data on the cost and quantity available were developed for rutile (TiO2), which is potentially recoverable as a byproduct at sand-washing plants in the Southeastern States of Alabama, Georgia, North Carolina, and South Carolina. Baaed on 1969 production data, an estimated 4,300 tons of rutile could be recovered annually from plants that process more than 25,000 tons of sand per year. Rutile prices at which this resource would be available ranged upward from $262 per ton, compared with the current market value of $185 per ton.

Jan 1, 1972

By Ralph Husack, J. W. Eckerd, G. A. Brady

The effect of gamma radiation on Pennsylvania anthracite and on reactions between anthracite and other materials was studied using a shielded , selfcontained 23,000 - curie cobalt 60 source . When anthracite was exposed to air at 65° C the reaction with oxygen was greater in the presence of radiation. than in its absence . Although drop- shatter tests indicated that exposure to radiation decreased the resistance to breakage of anthracite , this evidence of structural weakening was not supported by the results of grindability or particle- size studies . Irradiation caused definite changes in the gases evolved from evacuated samples of anthracite ; the percentages of hydrogen and carbon dioxide were increased, and the methane concentration remained unchanged . Carbon monoxide was evolved only from the unirradiated samples . Electron paramagnetic resonance (EPR ) measurements indicated large differences between evacuated samples and those exposed to air . There was little or no difference between irradiated and unirradiated samples , except that the free- radical content of unirradiated samples of anthracite increased progressively with higher temperatures of evacuation , but in the case of irradiated samples , no such behavior was found . Attempts to produce carbon disulfide and calcium carbide by reacting anthracite with sulfur up to 120 ° C , and with calcium oxide up to 400 ° C , were unsuccessful .

Jan 1, 1964

By L. C. George

The Bureau of Mines measured vapor pressures of selected mixtures in the binary system SnCla-ZnC12 by the static pressure method. Equations expressing the vapor pressure) and the heat and free energy of vaporization) as functions of temperature were developed by numerical analysis based on the sigma-plot method. It was found that the vapor pressure of any SnCl2-ZnCl2 mixture) at any temperature within the range of this investigation) could be accurately calculated from the derived values for the heat and free energy of vaporization for the mixture, with a probable error of 0.01 cm Hg or less.

Jan 1, 1967

By William E. Souder

Behavioral accidents are a particular type of accident. They are caused by inappropriate individual behaviors and faulty reactions. Catastrophe theory is a means for mathematically modeling the dynamic processes that underlie behavioral accidents. Based on a comprehensive data base of mining accidents, a computerized catastrophe model has been developed by the Bureau of Mines. This model systematically links individual psychological, group behavioral, and mine environmental variables with other accident causing factors. It answers several longstanding questions about why some normally safe behaving persons may spontaneously engage in unsafe acts that have high risks of serious injury. Field tests with the model indicate that it has three important uses: It can be used as an effective training aid for increasing employee safety consciousness; it can be used as a management laboratory for testing decision alternatives and policies; and it can be used to help design the most effective work teams.