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By John Zetterstrom

Increased activity in the beneficiation of taconite, particularly the magnetic variety, has shown the need for more information on the rate of oxidation of magnetite to hematite. This oxidation occurs in the pelletizing step of the beneficiation process. Magnetic taconite is an intimate association of magnetite and a siliceous gangue. It must be ground to approximately 70 to 30 percent minus 325 mesh to liberate the magnetite from the gangue. With sufficient liberation, magnetic concentration will yield a product high enough in iron and low enough in silica for blast-furnace use. The magnetic concentrate must be agglomerated before it can be used in a blast furnace. Agglomeration is the general term applied to all methods of compacting or consolidating fine iron-oxide materials, sintering and pelletizing being the two most common methods. Sintering is clone on a Dwight-Lloyd or Greenawalt sintering machine. Pelletizing consists of balling fine, moist oxide in a rotating drum, followed by baking at .a temperature below that of incipient fusion to develop a permanent bond within each pellet. The magnetic concentrate from taconite is too fine for good sintering practice but fine enough for good pelletizing practice.

Jan 1, 1950

By Robert P. Vinson

The U.S. Bureau of Mines evaluated a light-scattering technique for discriminating between spherical and nonspherical particles. This evaluation was a three-step procedure. The first step required collecting light-scattering data for a variety of particles. This was accomplished with a particle analyzer called the DAWN-A. The DAWN-A measured the scattered light intensities of individual particles at a forward scattering angle of 40°. These DAWN-A measurements of individual particles are called scattering signatures by the Bureau researchers. The second step in this evaluation was to calculate a sphericity index number using the scattering signatures produced by the DAWN-A. The sphericity index number can range from 0 to 1. A calculated sphericity index of 1 would show that based on the intensity of scattered light, the particle was a perfect sphere. The third and final step of this evaluation was the comparison of the calculated sphericity indices of the various particles. Comparing these indices made it possible to discriminate between the nearly spherical waterdrops and the nonspherical coal and rock dust particles.

Jan 1, 1993

By J. T. McCartney

"INTRODUCTION The surface areas of the finest fractions of a pulverized material are disproportionately larger than their weights. For instance, Pesrott and Kinney 3/ showed that, in a sample of minus 200-mesh coal, particles that are about 2 microns in diameter represent 15 percent of the entire surface area but only 1.5 percent of the total weight. Because the sur- face area is the dominating factor in the behavior of finely divided materials in many practical processes, the role of the finest particles is of great importance. The oxidation and combustion of pulverized coal, both in the dry form and in suspension in oils, and the hydrogenation to fluid hydrocarbons of mixtures of pulverized coal and heavy oil are reactions in which the surface area of the coal particles has considerable influence. This investigation of the size distribution of fine coal particles was conducted with the hope that such processes would thereby be better understood. The results should also be of value in the study of the crushing and fracture of coal."

Sep 1, 1945

By Earl R. McMillan

"Coal washing commands the thoughtful attention of a steadily incre in number of people. Clean coal is not merely a luxury but is rapidly becoming a necessity in some industrial operations.Coal seams in the Northeast are rarely free from ""bone"" and shale or clay partings which vary from a fraction of an inch to several feet in thickness. Nearly all of the coal measures are folded and faulted, the coal seams dip at various angles, and in some cases are badly broken. In mining these seams fragments of the roof and floor, as well as partings of impur-ities within the seams, unavoidably become mixed with the coal, so that the raw coal as it comes to the surface often contains as much as 50 per cent, by weight of waste.At the Bureau of Mines experiment station at Seattle, the washing of this coal in order to improve it for commercial use has been studied. Since the process of coal-washing depends upon differences in specific gravity between the clean coal and, its associated impurities, the first problem undertaken was that of determining the specific gravity of the clean coal and of each parting of impurity contained in a large number of representative seams.It was found that the freshly-mined coal is practically saturated with water, this being observed in determining the effect of moisture content upon the specific gravity of the coal particles, selected from samples of coal varying from low-grade subbituminous up to semianthracite, all of which are found in the State of Washington. The specific gravity values determined for the cleanest particles varied from 1.28 to 1.35; in general, the higher the rank of the coal the hither the specific gravity."

Nov 1, 1920

By R. L. Hopkins

Some typical thiacyclopentanes and thiacyclohexanes were synthesized to provide reference compounds needed for the identification of sulfur compounds in crude oils. Two general methods of synthesis were employed: (1) cleavage of 2-alkyltetrahydropyrans with hydrogen bromide followed by the reaction of the resulting dibromoalkanes with sodium sulfide and (2) the catlyzed reaction of cyclic ethers or 1)4-or 1)5-alkanediols with hydrogen sulfide. Both methods produced mixtures of 2-alkylthiacyclopentanes and 2-alkylthiacyclohexanes with 2-alkyltetrahydropyran as the starting material. The structures of the reaction products were established by analysis for sulfur; desulfurization; gas-liquid chromatography (GLC); mass, infrared, and nuclear magnetic resonance (NMR) spectra; and an alternate synthesis. The synthesis of the cyclic sulfides contributed substantially to the identification of 10 members of this class of sulfur compounds in crude oil.

Jan 1, 1967

By Thomas C. Ruhe

The Bureau of Mines conducted research to determine the safe operating conditions for using recycled (used) lubricating oil from mining equipment as a partial replacement for diesel fuel to make ANFO-type blasting agents. The use of recycled oil (RO) saves energy, reduces oil imports, and reduces mining costs. Low ambient temperatures may cause these recycled oils to become too viscous for proper absorption by ammonium nitrate (AN) prills and result in poor blast performance, safety hazards, and environmental problems. To help quantify and resolve these issues, viscosity, mixing, and performance tests were conducted at various temperatures. Diesel fuels No. 1 and No. 2 were studied separately and in blends with 25,50, and 75% RO. Good quality ANFO mixes (94-6) were produced with dry absorbent prills and blended fuel (No. 1 diesel plus RO) at temperatures as low as -40°F (-40°C) with 75% No. 1/25% RO, and at -20°F (-29°C) with 50/50. Diesel fuel No. 2 also made good mixes as low as -30" F (-34°C) with 75% No. 2/25% RO, and at 0°F (-18°C) with 50/50.

Jan 1, 2008

By Oliver W. Keener

This paper describing the methods and costs of mining at the Hartley-Grantham mine of the Century Zinc Co. in the Tri-State Lead and Zinc district is one of a series being prepared by the United States Bureau of Mines can mining practices, methods, and costs in the various mining districts of the United States. LOCATION, HISTORY, AND GEOLOGY The Hartley-Grantham Mine is located just outside the city limits of Baxter Springs, Kans., as shown in Figure 1. A plan of the mine is given in Figure 2, and Figure is a cross section through A - A of Figure 2.

Jan 1, 1930

By H. B. Freaman, C. L. Colburn, C. M. Bouton

"The mine telephone has been perfected to such an extent that it is giving satisfaction in most mines were the wiring is well insulated. Very often the telephone cannot be depended upon on account of falls of rock, grounding due to worn insulation or extreme dampness. In the event of a disaster it frequently happens that the mine telephone system is put out of commission by the agency that causes the disaster, at the time when it is most urgently needed. On this account the mining industry is interested in any kind of telephone system that can be counted upon in an emergency. Many requests have been received by the Bureau of Mines to devise means of utilizing wireless methods for this purpose.The results of some preliminary experiments conducted by the writers at the Bureau of Mines experimental mine at Bruceton, Pennsylvania, in the ordinary sending and receiving of radio waves through earth strata are described below. The experiments were made in cooperation with the Westinghouse Electric end Manufacturing Co., which assigned to this work three of its radio engineers, C. A, Boddie, E. C. Douglas, and F. D. Fessler,The preliminary experiments consisted first in receiving signals from without the mine by means of a receiver located inside the mina, and second, both sending and receiving messages underground through the strata. It was found that with a receiving instrument set at a point 100 feet underground, signals from KDKA station, of the Westinghouse Electric and Manufacturing Co. East Pittsburgh, Pa., could be heard distinctly. Station KDKA is at a distance of about 18 miles from the experimental mine. About 50 feet from the receiving station used in this test was a 6-inch bore-hole from the surface, lined with iron pipe and containing electric light wires which extended therefrom through-out the mine. The presence of these wires evidently assisted greatly in the reception, for when the receiving set was carried to another point in the mine removed from wires and tracks the signals were barely audible through 50 feet of cover. The fact that signals were detected, however, even though faintly, is sufficient evidence of transmission through the ground to encourage further experimenting.In sending waves underground the Westinghouse 20-watt B.T. model T.F. transmitter was used in such a manner as to send out continuous waves of 200 to 300 meters length."

Oct 1, 1922

By Robert L. Thorne

Cassiterite deposits on Sullivan Creek in central Alaska were investigated by the Bureau of Mines in the spring of 1943. Gold miners in the area have been recovering cassitorite each season as a byproduct of gold placer operations. Approximately 300 tons of tin concentrates have been shipped from the district. The deposits were sampled though trenches and small shafts. An average tin content of 0.28 pound per cubic yard was indicated. A detailed description of sampling methods and sample analyses is presented in this report.

Jan 1, 1948

By Wilbur I. Duvall

This paper presents arguments which show that a velocity seismograph should be used to measure building and ground vibrations produced by blasting . However , portable velocity seismographs suitable for this type of measurement are not commercially available . The paper describes how a velocity seismograph can be assembled from commercially available velocity gages , amplifiers , and recorders . Also , specifications are given which could be used in the design and manufacture of a portable velocity seismograph suitable for measuring vibrations from blasting .

Jan 1, 1964

By Miller, ALEX U, Edward Thomas

In March 1937 the entire country was shocked by news of an explosion of gas in a New London (Tex.) schoolhouse, which resulted in the death of 280 pupils and 14 t eachers. The Government investigators of this disaster believed that the cause was the ignition and explosion of a large volume of explosive natural gas-air mixture that had accumulated in a poorly ventilated space beneath the first floor of the main school building and that this accumulation was due to leakage from gas lin suspended underneath the floor to carry the gas supply to the school.!i/ For some years there has been a potential explosion hazard in school houses and other buildings that are supplied with water from deep wells in certain parts of Illinois. Notwi thstand.ing the disaster at New London, Tex., and the fact that there had been gas ignitions at four water wells in different parts of the State, the explosion hazard in schools and other buildings was not fully recognized until a few months after the disaster in Texas, when an explosion occurred in the settling basin of the municipal water works of Clinton, Ill., and another in a pump house of the municipal water works in Normal, Ill, The explosion in the settling tank of the municipal water works in Clinton, Ill., occurred on August 12, 1937, and a.id considerable damage to the settling tank, but fortunately no one was injured. At the time of this explosion rapairs'and aJ.terations to the water plant were in progress, and 10 men were employed in the immediate vicinity of the settling tank. Two of these men were enlarging a hole in the concrete side with an air hammer for the installation of a larger discharge line.

Aug 1, 1938

The performance of two large-capacity ventilation systems was compared through tests conducted in a large dead-end heading at a pilot oil shale mine in Colorado. Sulfur hexafluoride (SF6) tracer gas was used to measure the performance of the two systems: a free-standing jet fan and a reversible fan with rigid duct. The tracer gas was used to simulate the production of mine air pollut-ants, including blasting pollutants, hot diesel emissions, free methane from surrounding strata, and methane desorbing from muck piles. The test room was 55 ft wide, 30 ft high, and 320 ft long. The performance of the two fans was similar, but the jet fan used less power. The tests showed that either system could provide effective ventilation during oil shale mining.

Jan 1, 1986

By John J. Henn

Two lime sinter processes for recovering alumina from clay, the double-leach process and the single-leach process, are evaluated in this Bureau of Mines report. In both processes, clay and limestone are mixed and sintered to form calcium aluminate from which alumina is extracted as sodium aluminate by leaching with a dilute solution of sodium carbonate. The pregnant liquor is desilicated, then carbonated to precipitate alumina trihydrate which is recovered and calcined to a,-alumina. The fixed capital costs for plants producing 1,000 tons per day of alumina are $85 million for the double-leach process and $86 million for the single-leach process based on a Marshall and Stevens chemical equipment index of 240.0. Because plant locations are variable with respect to the proximity of clay and limestone deposits, a nomograph is included to determine operating costs at various delivered costs of clay and limestone. For plants at which the delivered cost of clay containing 30 percent A1203 is $2 per ton and the delivered cost of limestone is $1 per ton, the operating costs are $81.04 and $89.87 per ton of alumina for the double-leach process and single-leach pro-cess, respectively.

Jan 1, 1969

By F. C. Houghten, R. R. Sayers, C. P. Yalaglou

"Introduction.Atmospheric conditions relative to high temperature and humidity are of great importance in mining, as well as in such allied fields as railroad and vehicular tunnels. An extended investigation into the effect of these factors on men has been in progress for some time, both in the field under actual working conditions, and at the Pittsburgh experiment station of the bureau in cooperation with the American Society of Heating and Ventilating Engineers and the U. S. Public Health Service.For several years one of the writers (Dr. Sayers) and L. Harrington, supervising mining engineer of the bureau, have been studying the effects of hot humid atmosphere in metal mines on the comfort and efficiency of the workers. Some of the reactions experienced in still and in moving saturated mine air at temperatures of 90 to 100°F., with men at rest are presented in a recent paper.****The present paper is based on experiments made under carefully controlled conditions to determine the relative feeling of warmth experienced by men in atmospheres of various degrees of temperature and humidity. The work was conducted by the research laboratory of the American society of Heating and Ventilating Engineers, at the Pittsburgh experiment station of the Bureau of Mines, in special physchrometric chambers built for this purpose. It was carried on under the direction of F. Paul Anderson, director of the laboratory, Dr. R. R. Sayers and A. C. Fieldner of the Bureau of Mines. The results given in this paper are for still air only. Investigations of the effects of moving air are being continued, and will be reported later."

Jan 1, 1924

By Lars Osen

This investigation was undertaken to contribute to the understanding of underground pull tests by conducting laboratory tests under closely controlled conditions. Steel bolts, instrumented with electrical resistance strain gages, were anchored in an aluminum block, a granite block, and a steel sleeve, and were subjected to pull tests. The bearing plates used were either flat7 dished, or embossed. In pull testing a bolt that is prestressed, there is a range of loading during which bolt load is greater than the jack-applied load, This study showed that preload, the size, shape, and type of bearing plate; and the geometry of the system determine the point at which bolt load and applied load become equal. The effects on bolt load of both a theoretical solution and actual pull tests were analogous and led to similar results.

Jan 1, 1965

By Stanton L. Tainter

"As an adjunct to its minerals-investigation program, the Bureau of Mines has developed a number of operating devices and techniques worthy of note. This paper, prepared under the supervision of J. H. Hedges, chief, Tucson Branch Mining Division, and under the general supervision of Lowell B. Moon, chief, Mining Division, reports upon certain methods devised to overcome difficulties encountered in cementing of diamond-drill holes at a Bureau of Mines project at Christmas, Gila County, Ariz.Pressure grouting was employed to recondition a caved hole it was desired to reopen and deepen. The hole, which had boon stopped 7 months previously at a depth of 488 feet, was caved below 449 feet in a contact zone of claylike, altered diorite and crumbly metamorphosed limestone. As other means of obtaining moderate pressure were not available, carbon dioxide gas, drawn from tank of liquid carbon dioxide through a pressure reducing and regulating valve, was used. The hole was reopened successfully with 12 grouting jobs.Another hole, where cawing from several water-bearing fractures between 202 and 232 feet gave trouble, was successfully cemented by the use of a grouting plug. An attempt to cement through the rods had failed, owing probably to agitation caused by water currents. Pressure grouting through the caning set above the cave could not be need, because water was forced up outside the casing when pressure was applied. The problem was solved by using a wooden plug 1-13/16 inches in diameter, which, when soaked in water, expanded to a tight fit in an AX hole. A hole was drilled through the plug, and a rubber flap valve was nailed to the lower end. In the upper end of the plug the hole was enlarged to fit loosely over an EX rod coupling finished smooth. The plug was lowered on the end of the drill rods to a point about 10 feet above the cave, where it was allowed to expand tightly to the hole. Cement grout was then pumped through the rods, and the rods were removed from the hole. After allowing time for the cement to set, the wooden plug was chopped out and drilling van resumed.Over 300 tests were made to determine the type of cement most suitable for use on the Christmas job, and the effect of cement-water ratio, temperature, and various admixtures on workability, setting time, and strength. The results of these tests, described in detail in the body of this report, indicate the desirability of thoroughly testing available cements when it is necessary to drill holes under difficult conditions that may cause failure.When it became desirable to reopen and deepen a caved drill hole, it was considered easiest to recondition the hole by pressure grouting, As other mans for obtaining moderate pressure were not available, a method utilizing carbon dioxide gas was employed. The hole was reconditioned successfully with 12 grouting jobs."

Nov 1, 1949

By L. E. Dalverny

This Bureau of Mines report describes the deployment, 5-month operation, and lessons gained from a continuous gas monitoring system using sampling-tube bundles at an underground mine fire in West Virginia. Research information gained indicates the utility of relating certain gas concentration ratios to events during fire development, mine reventilation, and mine recovery. In addition to monitoring the quality of remote fly ash seals, the system provided timely warning of dangerous gas concentrations which developed during surface and underground recovery activities. An evaluation of system components is supplemented by recommendations for improvements.

Jan 1, 1975

By Keith G. Wallace

Coal mine ventilation systems are often subject to high leakage rates. As a result, changes in airflow resistance will strongly affect the efficiency with which air is delivered to the working place. One major source of airflow resistance is the line brattice used to direct air from the last open crosscut to the working face. Because it is a great distance from the fan, the resistance of the line brattice can result in more overall leakage than an equivalent resistance closer to the fan. Substituting auxiliary fans for brattice eliminates this source of resistance, with improvements in system efficiency and cost. Also, in some mines, the leakage that leads to spontaneous combustion can be reduced. The benefits obtained by several different brattice and fan substitutions have been studied by Mine Ventilation Services, Inc., Lafayette, CA, under contract to the U.S. Bureau of Mines. Changes in main fan duty were compared with additional costs associated with auxiliary fans. Results indicate that in some circumstances, considerable leakage reductions and cost savings are possible.

Jan 1, 1990

By D. Harrington

Springing or chambering of deep drill holes is common practice in some quarries. It involves definite hazards from premature explosion during placing of the springing charges or the final charge due chiefly to heating of the bottom of the holes by the successive exploding of the springing charges or, in some instances, from burning of paper or other material following detonation of the explosives The danger is either unknown or disregarded in many instances by those who place the charges in the holes. Disregard of this hazard probably is, at least in part, responsible for the far too high fatality and injury rate due to charging explosives and premature slots in quarry work. Awareness of the danger' should result in elimination or at least of material decrease in injuries from this cause.

Jan 1, 1941

By Benjamin W. Haynes

Materials from phosphate rock mining and processing were analyzed for fluorine and uranium content as part of the Bureau of Mines program to more effectively recover resources from mining and mineral processing reject materials. The analysis of both feed and waste materials generated in the beneficiation and acidulation of phosphate rock was performed to obtain information on the disposition and concentration of these elements in phosphate rock processing streams. Fluorine was determined by a distillation-titration method and by ion chromatography. Uranium was determined by the dibenzoylmethane (DBM) method, the reliability being confirmed by roundrobin analysis of samples within Bureau of Mines research centers. National Bureau of Standards (NBS) Standard Reference Material (SRM) 120b-Phosphate Rock was also analyzed for fluorine and uranium to verify procedures and results. Fluorine values ranged from 0.3 wt-pct in gypsum filter cake to 3.7 wt-pct in phosphate rock concentrate. Uranium ranged from less than 5 µg/g in gypsum filter cake to 200 µg/g in a dried clay slime.

Jan 1, 1981