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By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Satish V. Kailas

For product sustainability “closing the cycle” is the first requirement. If the materials used in making the product is not replenished at the rate at which it is being extracted, the cycle is open and the product would not be sustainable. This includes the materials used in generating the energy used to make the product, the transportation, use and disposal. If the materials used in a product, that includes lubricants, is one that cannot be replenished, it has to be recycled for the product to be sustainable. The other basic condition for sustainability is the eco-friendliness of the product. It is argued that the present lubricants do not fall in this category. Using the example of cutting oil emulsions we have shown that it is possible to meet the conditions of sustainability in terms of both the material extraction-replenishment cycle and eco-toxicity. Cutting oil emulsions made from coconut oil and natural additives are shown to have superior cutting properties and are completely eco-friendly. It is concluded that products made using these conditions are possible and is a necessity for man to lead a sustainable life. Closing the cycle, with respect to the energy used in the cycle will make the product completely eco-friendly.

Jul 31, 2018

By Dyego Monteiro de Souza

This study compares the wear resistance of specimens lubricated with biofluids or mineral oil. Tribological studies were performed by ball-cratering test. In these tests were used as lubricants epoxidized soybean oil, castor oil and mineral oil. The specimens used were untreated and nitrided AISI 4140, while a steel ball AISI 52100 was used as a counterbody. In order to analyze the results obtained, the worn volume was calculated and the characterization of the crater, after the test, was made using optical microscopy and SEM. Wettability was also measured for the different surface condition and lubricants. As expected both specimens showed a smaller volume worn when lubricated with mineral oil due to inherent properties of this type of lubricant. Among the vegetable oils studied, the castor oil showed a better performance in the lubrication of the specimens untreated while on the nitrided specimen have shown less wear when lubricated with epoxidized soybean oil, indicating a difference in the efficiency of oils, as lubricants, depending on the surface conditions of the mechanical components.

Jul 31, 2018

By Elizaveta Cheremisina

In steelmaking process lime serves as flux. Rapid lime assimilation and slag formation of the desired composition have a significant effect on the refining reactions. It is important to know the rate limiting step of lime dissolution to control and improve the converter process. Kinetics of pure CaO and industrial lime dissolution in model slag has been studied in the range of temperatures 1300 –1600°C. Lime samples were prepared in cylinder form and immersed in the melt for predetermined time. Considering the total mass balance of CaO in the slag and linear dimensions of lime samples, mass transfer coefficients were derived. Diffusion coefficients were calculated under conditions of non-stationary diffusion. The derived activation energy of less than 200 kJ/mol indicates that diffusion is the limiting step in the process of lime-dissolution in slag.

Oct 30, 2017

By G. Martino, F. Silva, Emmanuel Marchal

The definition of the chemical specification at multiple steps of the steelmaking process is very common in the industry. Among all elements and compounds, the Sulphur content has a special control over several stages, from the coal blend to the final products. Coke, iron and steelmaking specialists usually agree on a static specification for each intermediate product according to their local operation capacity and production cost. However, local decisions have major impacts on the whole production chain and many global factors should be considered in order to make the best decision. In this study, we will exemplify focusing on Sulphur content concepts and techniques that could be applied to many decisions in an integrated carbon steel plant. The variation of coal and coke prices, the desulphurization cost and time, the processes operating points, the hot metal rate at converters, prices and demands of low and ultra-low Sulphur steel grades are some of the integrated factors that are usually disregarded during the specification process. Mathematical modeling presents itself as a proper option into dealing with all the complexity that emerges from integrating all these processes' trade-offs and decisions. This study presents the results of a mathematical model that encompasses economic, thermal, chemical, and mass balances, physical quality of materials and productivity constraints of all processes of a hypothetical integrated carbon steel plant. It optimizes the iron and steelmaking process on a global and unique objective, dynamically defining targets for product quality to achieve the lowest steel production cost. This study details multiple market-plant scenarios in order to compare economic and operating results of a static vs dynamic specification practice.

Oct 1, 2019

By Eduardo Dominguez Trindade

Lubricant oils are subjected to reciprocating movement in the piston ring/cylinder tribocouple of automotive engines. In this kind of movement, the relative speed oscillates between zero and a maximum, and therefore the lubrication regime goes from boundary to hydrodynamic. Tribotests are widely used in laboratories to hint at the friction developed in these systems. In the present work, a SRV tribometer was used to evaluate the friction behaviour of lubricant oils under reciprocating movement up to 60 Hz. A high acquisition rate allowed the analysis of data inside each reciprocating cycle. Both a pure base oil and a fully formulated lubricant were used. Changes in the contact pressure, viscosity and speed were seen to influence friction, which was correlated to the relative thickness predicted by Hamrock-Dowson equation. While some observed characteristics were typical consequences of the Stribeck curve, other effects were also observed, such as the occurrence of seizure at high reciprocating frequency. A lower boundary coefficient of friction due to additive package in the formulated oil was also observed. The results allow a better understanding of friction in reciprocating cycles and can be used to evaluate the performance of oils and surfaces in laboratory prior to engine testing.

Jul 31, 2018

By Vinícius da Silva Madruga

Os processos de lingotamento contínuo e de lingotamento convencional apresentam diferenças na solidificação dos aços, esse fato tem impacto na distribuição, quantidade e forma de inclusões de óxidos e sulfetos. O objetivo desse trabalho é verificar de que maneira tais diferenças influenciam na distribuição dos sulfetos ao longo do aço solidificado de qualidade SAE 1050. Para isso, 20 amostras foram retiradas de eixos forjados e barras laminadas, produtos conformados de origem do lingotamento convencional e do lingotamento contínuo, respectivamente. As amostras foram analisadas em microscópio ótico e microscópio eletrônico de varredura no modo de análise automatizada de partículas. Através das imagens e de dados numéricos obtidos, foi visto que nas amostras de barra laminada há grande quantidade de sulfetos, se analisada na seção longitudinal, em relação às amostras de eixo forjado. Analisando na seção transversal, foram detectados menos sulfetos devido ao alinhamento dos mesmos. Entre as amostras de eixo forjado, a área ocupada pelos sulfetos é maior no pé do lingote, reduzindo em direção à cabeça, apesar de a cabeça apresentar mais sulfetos. Tais diferenças foram atribuídas à taxa de resfriamento, à seção transversal do produto e ao processo, que variam entre os dois tipos de lingotamento.

Oct 30, 2017

By Gabriel Oliveira Glória

Due to growing concern about the ambient impacts, lignocellulosic fibers are been investigated to replace the synthetic ones in polymer composites The giant bamboo fiber, a relatively unknown lignocellulosic fiber with potential for composite reinforcement, still needs to characterize for possible engineer applications. However the giant bamboo fiber has low adhesion with the polymeric matrix. In order to understand the interaction that occurs between the bamboo fiber and the polymer matrix is necessary to evaluate its physical and chemical characteristics. Therefore, the present work analyzed the giant bamboo fiber by means of Fourier Transform Infrared (FTIR) spectroscopy. The spectrum revealed main absorption bands typical of giant bamboo fiber specific molecular interactions.

Aug 16, 2017

By Boryong Lee, Heedong Sung, Minho Park, Sunyoung Choi

Recently, the demand for ultra-thin steel plate with high hardness and strength has been increasing in various industries. In order to satisfy this requirement, steel company designs the chemistry with low CEQ and obtains the required characteristics through quenching and tempering process. Especially, these steels are accompanied by low temperature tempering as a necessary process. Unlike ordinary high temperature tempering steels, it is impossible to improve the flatness after low temperature tempering. Therefore, shape control in the quenching process is very important for securing the excellent quality flatness. In order to obtain flatness in the quenching process, uniform cooling inside the plate should be accompanied. However, the quenching process has limitations in estimating the temperature behavior during cooling because the plate temperature is lowered to room temperature. In this study, a thermocouple was installed inside the actual quenching plate to measure the temperature behavior during cooling and to establish the manufacturing conditions of the quenching plate to ensure excellent flatness quality.

Oct 1, 2019

By Adriano Gonçalves dos Reis

In the development of the structural materials for the advanced applications, as in the aerospace industry, there is a constant strive to increase both strength and toughness. Maraging steels are iron-nickel alloys designed to combine both properties that are achieved through the age-hardening of low carbon martensite. This alloy have a metastable martensitic structure that can revert to austenite when heated in temperatures close to the aging temperature, and this effect can be enhanced with the temperature increasing and time of treatment. Therefore, the study of creep behavior in elevated temperatures has technological importance to the development of this material. In this work the creep behavior of a maraging 300 steel solution annealed is evaluated by carrying out creep tests at 650ºC and in a stress of 200, 300 and 500 MPa. Creep parameters, such as steady state creep rate (?????), final creep time (tf), and stress exponent from secondary creep (n) are determined, considering that they are important to evaluate the creep resistance of the material.

Aug 7, 2018

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Jorge Madias

Durante la laminación de barras y alambrones para construcción civil; perfiles y ángulos estructurales y barras redondas y hexagonales de aceros de corte libre puede presentarse la apertura de la punta o la cola y el estallido central, con la consiguiente parada y caída de la productividad, y pérdida de rendimiento metálico. En este trabajo se analizan las diversas causas que confluyen para que este problema ocurra. Se analiza la influencia de posibles defectos en las palanquillas, las características del corte de las mismas y otros problemas de calidad. Se revisa el rol del precalentamiento previo a la laminación, la refrigeración de los cilindros, el diseño de pasadas y la respuesta del material en función de su ductilidad. Se presentan diversos casos industriales para ilustrar las diferentes razones detrás del problema de la apertura de punta.

Jul 30, 2018

By Michael Windhager, Karl H. Ziehenberger

ULTIMA® are high performance, centrifugal cast, double poured (CC duplex) work rolls. This paper describes the principle of the ULTIMA® roll concept and its wide range of usability. The ULTIMA® concept provides a solution for rod and bar mills to increase performance and output, even under harsh rolling conditions. The main focus is on highly loaded mill stands that require both high wear resistance and resistance against thermal fatigue, like pre-dog bone, dog bone, slitter. Specific case studies of quite different mill configurations and rolled product mix prove the positive impact on production yield, mill and roll shop operations, and profitability in terms of TCO (total cost of ownership).

Oct 1, 2019

By Rogério Felício dos Santos

Nitriding of metallic materials using electric discharges generated during electric discharge machining (EDM) is a recently developed technique. The aim of this paper was to correlate mechanical properties of a nitrided layer produced in AISI 4140 steel by EDM nitriding with the type and amount of nitrides. A conventional die-sinking EDM equipment and electrolytic copper electrodes were used to generate the electric discharges. The electrolyte was a solution of urea in deionized water. Knoop microhardness profiles assessed the variation of hardness along the nitrided layer, whereas the elastic modulus of this layer was measured using nanoindentation tests. Optical microscopy and X-ray diffraction (XRD) were used to characterize the nitrided surface. The results showed the formation of a nitrided layer containing iron nitrides with average thickness of around 25 µm. The amount of nitrides reduced from the surface towards the centre and these results correlated well with microhardness profiles obtained.

Jul 31, 2018

By Fernando Ruiz Díaz

En aplicaciones a elevadas temperaturas como por ejemplo en cámaras de combustión y toberas de vehículos aeroespaciales se requiere el uso de aleaciones que permitan una elevada extracción de calor y buenas propiedades mecánicas. En este trabajo se realiza un análisis comparativo de las aleaciones Cu-Cr-Zr y Cu-Ag-Zr. Las mismas fueron sometidas a ensayos de resistividad eléctrica entre 25ºC y 700ºC y de tracción a 150ºC, 450ºC y 700ºC. Los resultados de los ensayos de resistividad eléctrica fueron convertidos a conductividad térmica mediante la relación de Wiedemann- Franz. A través de este análisis se observa que la aleación con mejor conductividad térmica es la de Cu-Ag-Zr presentando además un cambio de fase que no es observado en la aleación Cu-Cr-Zr. Respecto al ensayo de tracción la aleación Cu-Cr-Zr presenta mayores valores de resistencia a la tracción y tensión de fluencia a las temperaturas estudiadas.

Aug 16, 2017

By Peter Grawenhof

Universal joint shafts and slipper spindles are commonly used in rolling mills to compensate the design- and process-related offset between the motors and work rolls. Although both types of shafts exhibit on the same kinematic principle, there are basic differences regarding the design concepts. These differences become noticeable on many levels and may become very distinct in terms of Life-Cycle-Costs (LCC). In this respect, a critical comparison between universal joint shafts and slipper spindles can be made.

Aug 16, 2017

By Wan-sub Kim, Joon-Tae Lee, Seongkyu See, Yong-Kyu Park

Softening heat treatment of CHQ alloy steel (Cr-Mo Steel) is a bottleneck process that requires 90% or more of the entire manufacturing process. In order to reduce the property deviation between edge and center and remove the low-temperature structure problems, CHQ products is heat treated by customers. This technology comes from the idea to solve the problem by applying the concept of “In-line isothermal transformation through initial quenching + heat source addition. Consider the stability of field operations, durability from high ambient temperature and fall of scale, Instantaneous heating and cooling control was required for the conversion of slow cooling and rapid cooling products. An electric heating system was applied to the underside of Stelmor air-cooling nozzle. Using the Scan Pyrometer, the feedback control was performed and fine temperature control was performed through the thermocouple by zone. Through the this technology, it is possible to develop and expand products that can be shortened or omitted by the heat treatment process of customers.

Oct 1, 2019

By Wolfgang Linden

One of the most important factors in successful electric steelmaking is the continuous observation of the process and the reaction to it. Traditional electric arc furnace control uses mainly direct controls which are based on the electric power input. Not considering the furnace conditions will necessarily lead to suboptimal operation in terms of energy consumption and productivity not fully utilized.The ARCCESS FEOS (Furnace Energy Optimization System) includes the simultaneous control of the transformer tap, impedance operating point, reactor tap, burner and carbon injection, and DRI charging control. FEOS has proven in practical operation benefits of high melting yields, no interruptions through switch offs in borderline temperature area, rapid reaction, reproducible and efficient electrical energy input and short power-on times.

Jul 30, 2018

By Ivan César Lopes Diniz, César Romero Afonso Goulart Júnior

Mandrels are tools applied to manufacturing seamless tubes. In VSB plants (Vallourec Soluções Tubulares do Brasil), it is used in two mills. Mandrel and PQF Mills. This is an expensive tool due its alloy (hot work tool steel – AISI H13) and lengh (between 12 meters and 22,5 meters). An opportunity to apply mandrels from PQF in Mandrel Mill has been identified. However, mechanical properties of PQF mandrels must be improved. This work presents the heat treatment process of Quenching and Tempering developed internally at VSB to improve PQF mandrel properties aiming to achieve Mandrel Mill requirements. Hardness and metallography tests were performed before and after some steps of the heat treatment to characterize and validate the process.

Oct 5, 2019

By Mario Andres Albuja Ribadeneira

El presente trabajo pretende encontrar la ruta para incrementar la productividad y reducir el costo de transformación en una acería eléctrica, mediante el uso de la tecnología disponible en el mercado. El método para alcanzar los resultados se enfocan en una drástica reducción de los tiempos de transformador conectado (power-on), los tiempos de transformador apagado (power-off) asi como la reducción en los consumos de las materias primas e insumos para la fabricación de acero por la ruta del horno eléctrico. La experiencia de Adelca arroja resultados que sobrepasan el 100% de productividad y 30% de reducción en el costo de transformación de la palanquilla. Los resultados obtenidos sin duda alguna servirán de una guía probada para quienes buscan un mejor desempeño en el negocio del acero.

Aug 16, 2017