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By K. Negishi, H. Izui, Y. Komiya

"Aluminum has the disadvantage of low strength. In order to obtain the high strength composites, crystals were refined in the composites. Grain refinement was approached at two process points, generating new grains and grain growth. It is important for refinement how to control the grain growth. Spark plasma sintering (SPS) technique and TiB2powder addition prevent grain growth. To investigate effects of strain and additives to the alloy, aluminum powder was sintered at 70 MPa and 80 MPa, changing the content of TiB2additive powder by SPS method. As the results, the crystal grain size was finer in the composite sintered at higher sintering pressure and with larger amount of additive, though over 1.0mass% TiB2addition dissuades grain refining. These grain refinements improve hardness and tensile strength of sintered aluminum alloys.INTRODUCTIONAluminum matrix composites have low density, high specific strength, and low cost. Their applications are growing continuously in the field of automotive and aerospace industries. Recent studies to improve their good mechanical and tribological properties use different ceramic materials such as Al2O3(Das, Munroe, & Bandyopadhyay, 1996; Ashwatha & Anthony Xaviorb, 2014),SiC(Hassani, Bagherpour, & Qods, 2014), B4C(Ehsan, Masoud, Touradj, Amir Hossein, & Ali, 2015),TiC(Ehsan, Ali, Masoud, Kamyar, & Touradj, 2017), and TiB2(Fei & Zhong-Hua, 2013).On the other hand, grain refinement is also an important techniques for improving the properties of aluminum alloys. Finer grains improve the mechanical properties of the alloy. For cast and wrought alloys, addition of grain refiners in molten alloys accelerates generation of nucleus and suppresses grain growth. Al-Ti-B alloy is generally added as grain refiners in the molten aluminum alloys(Easton & Stjohn, 2001). Especially, TiB2has very high melting point, low density, and excellent hardness. Therefore, TiB2was selected as additions into aluminum alloys. Liquids reaction leads to high cost, oxidation, discoloration of molten alloy, and clustering of additive powder as compared with solid reaction such as sintering. However, sintering of aluminum alloy powder with ceramic powders is difficult for oxide layer surface. Recently, we take attention to spark plasma sintering (SPS) as advanced sintering process. SPS process can easily sinter a high quality specimen at a lower sintering temperature and in a shorter time than conventional sintering processes. By SPS process, we have sintered titanium powders that are as difficult to be sintered by any other processes as aluminum powders, and improved mechanical properties by adding hard ceramic powders TiC and TiB(Kamegawa, Izui, Komiya, Kobayashi, & Arimoto, 2015; Sampei, Izui, Komiya, Shigimura, & Suzuki, 2015). Furthermore, it is important to consider not only pure aluminum but alloys for solid-solution or precipitation strengthening. Actually, pure Al does not have enough strength compared with the alloys. Al-Cu alloy and Al-Mg alloy demonstrate adequate strength for industrial and commercial sectors. Al-Mg alloy retains good formability, and has high resistance to corrosion. It is therefore used for many applications. We must consider alloying processes. The most cost effective process is blended elemental technology where alloying elements are added to base powder as elemental or master alloy powder (Smugeresky & Dawson, 1981; Yasue, Radjai, Miwa, & Sakaguchi, 2003; Bolzoni, Esteban, Ruiz-Navas, & Gordo, 2012)."

Jan 1, 2018

By C. Blawert

The corrosion properties of the skin and the bulk of semi-solid processed and high pressure die cast AZ91 alloy were studied in 5% NaCI solution by (a) analysing the corrosion morphology, (b) measuring electrochemical polarization curves, (c) performing electrochemical impedance spectroscopic measurements, and (d) immersion tests at constant pH-values. Using XRD, LM, SEM and EDX to evaluate the microstructure of skin and bulk specimens, the corrosion results were related to the microstructures of the particular alloys. However, microstructure and corrosion performance were found to be similar for both production processes, and only slight but distinct differences were found. Generally, the skin corrosion properties are inferior to those of the bulk, with the exception of the high pressure die cast AZ91 alloy, where the finer microstructure of the skin layer exhibits a better performance as showed by impedance studies and confirmed in long term immersion tests.

Jan 1, 2004

By J. Holtzhausen

"An analysis of operating costs for underground mining operations in the current global economic climate considers the financial burden for a ventilation system to be in vicinity of 30–50%. These operating costs are often overlooked by management teams in the greater scale of things when looking to save money in the procurement phase. This oversight to operational costs can be as little as the effective delivery of ventilating air to the work zone. One of the biggest opportunities for substantial savings and improvements can be realized in the selection of a quality vent duct that is suitable and fit for purpose. The key component to the selection process for quality products is a solid selection criterion that is followed during the tender process. This allows the management team to filter out unsuitable suppliers and products. The case study identifies some of the key components that were considered in the procurement and selection process for lay-flat ducting products. These included the characteristics and strength of the materials. The selection criteria also considered a ducted performance comparison that offers the best aerodynamic performance with some of the following components. • Airflow at Duct Face (m³/s or cfm), Fan Pressure (Pa), Air Power (kW or hp), Assumed Fan Efficiency, Annual Running Costs, K – Factor or Lambda, Leakage Factor, Joining Method and available Duct Lengths with weights. • Critical components considered were the current Testing standards available for: o Bursting Strength AS 4878.5, Mass AS 2001.2.13, Tensile Strength AS 4878.6, Tensile Strength AS 2001.2.3.1, Tear Strength AS 2001.2.10, Tear Strength AS 4878.7 • Other key considerations were: o Warranty Claim, Damage claims, Local storage / operations, community engagement and relationships, current testing data, previous issues, after sales service with technical assistance, etc. Hidden costs associated with product failures and operational stoppages are often not quantified during the tender process. Buyer beware. INTRODUCTION The largest constraint underground mining operations currently face are their operating efficiencies and electrical costs. The overall cost of an operations ventilation system and its components requires more focus to identify what opportunities exist to maximise efficiency and effectiveness. This tender process may not always be clearly understood and it should be broken down into fewer components to achieve quantifiable results."

Jan 1, 2019

By B. Hohenstein, B. McBain, B. de Jong

"The automated fire assay system (Fast In-line Fire Assay or FIFA) has not found acceptance in the Au mining industry as the lower measurable limit of 0.20 ppm did not allow Au tailings to be measured with confidence. The development of arrested cupellation has overcome this hurdle which was a limiting factor in the FIFA 1 process. In the new automated fire assay process, automated sample preparation, fluxing, fusion and separation of a Pb button are essentially similar to the FIFA 1 process, albeit with some improvements. However, the game-changer is the development and incorporation of arrested cupellation into the automated system, now called FIFA 2. The purpose of arrested cupellation is to reduce the 50 g Pb button to a 5 g Pb button by partial cupellation in a specially developed arrested cupellation system thereby concentrating the Au in the Pb by a factor of 10 and in so doing moving them into higher concentration ranges in the mini-button where they can be read on the spark spectrometer. Results show that concentrations down to 0.02 ppm Au in geological materials can now be determined using arrested cupellation in the FIFA 2 process, an order of magnitude improvement over FIFA 1.INTRODUCTION Traditional fire assay for Au has remained virtually unchanged for 3000 years. It has survived for so long because it is accurate, has relatively low detection limits and is relatively inexpensive. However, it is labour intensive, has a long turn-around time (typically at least 7 hours), is environmentally unfriendly and exposes assay operators to potentially unsafe conditions (toxic fumes, toxic dust and extreme heat from furnaces). The NiS collection method is not as effective for the assay of Au as it is for the PGEs. A rapid, accurate, cost-effective method for the determination of Au and the Platinum Group Elements (PGEs) in geological materials would be a tremendous benefit to mining companies. Many of these objectives have been met by the FIFA 1 (Fast In-line Fire Assay) developed some 15 years ago in which automated methods have replaced the manual procedures which are part and parcel of conventional fire assay. However, concentrations below 0.2 ppm have been very difficult to achieve with sufficient reliability."

Jan 1, 2017

By Andrew Matyas

"During the summer of 1968, the author was employed in the Research Department of Dominion Foundries and Steel, Limited, Hamilton, Ontario. Over the years, Dofasco has been conducting a program for developing more efficient control of its basic oxygen steelmaking process. The author was thus able to obtain a variety of viewpoints from both research engineers and furnace operators. He also had access to extensive literature dealing with BOF control schemes underway at other major steel producers. This paper describes the present state of developments in BOF steelmaking control.The necessity for efficient BOF control is pointed out. To appreciate the variables to be controlled, a brief outline of process fundamentals is included. Technical aspects of present methods of practical control are examined in detail; the relative merits of dynamic over static control models are emphasized. Finally, it is shown how an effective dymic-optimizing control scheme serves as the basis for closed-loop computer control of the process."

Jan 1, 1970

By W. T. Sampson

Introduction The Kirkland Lake (Ontario) property of Wright-Hargreaves Mines, Limited, - consists of four claims. The two main shear zones or 'breaks' of the Kirkland Lake camp extend through three of these claims, for a distance of approximately 3,500 feet. These claims are on the northeast side of the original lake. The water in this section of the lake has now been replaced with mill tailings. The degree of success of any completed undertaking, especially in the mining industry, reflects the personnel involved. I state with pleasure that the successful deepening of No. 5 winze from 6,400 feet to 7,272 feet was largely due to the co-operation and skilled workmanship of Shaft Captain J. Myelde and his efficient 'leaders'. This winze was sunk at a time when it was most difficult to obtain experienced shaftmen, with the result that the crews did not wholly consist of experienced men (although their desire to learn shaft sinking soon gave good results). This condition added greatly to the responsibilities and duties of those in charge, whose first consideration was for the safety of those engaged in the work, and I take great pride in recording that the entire sinking programme was completed without a lost-time accident. Location of Winze Due to the information obtained through deep diamond-drill holes collared below the 6,000-foot level being of sufficient importance to warrant further exploration, it was decided to deepen the existing No. 5 winze rather than sink another winze. This decision meant that the sinking must be co-ordinated with and proceed simultaneously with operations in the winze, where mining was being carried on between the 3,900-foot and 5,100-foot horizons, inclusive.

Jan 1, 1948

By Baisheng Nie

The process of gas diffusion through coal particles and the mathematical physical model under the third kind boundary condition was determined to obtain the rules of gas diffusion through coal particles of different sizes. The analytical solution of the equation was obtained by the Method of Mathematical Physics. The parameters of analytical solutions and the implications of parameters were analyzed. The Biot criterion (Bi) and the Fourier criterion (F0) of mass transfer can represent and reflect the features of gas diffusion field of coal particles. Moreover, the measurement method of gas diffusion coefficient and surface mass transfer coefficient is introduced and an example of measurement is given. The achievement can provide the support to prevent disasters related to methane in coal mines.

Aug 1, 2013

By G. Gu, B. Fang, R. W. Revie, M. Elboujdaini

Electrochemical behavior of an X-80 pipeline steel, including frequency-sweep electrochemical-impedance spectroscopy (EIS), time-sweep EIS at a constant frequency and open-circuit potential (OCP) monitor, was investigated using four-point bending specimens subjected to a stress-corrosion cracking (SCC) test in a near-neutral pH environment. The capacitive loop became smaller with test duration, revealing an increase in the corrosion rate. The resistance obtained in the constant-frequency EIS test showed two regions, of which the region with a remarkable decrease in resistance transformed into a region of slow decrease, whereas the capacitance increased with test time indicating that iron dissolution was fast at first, and then a corrosion product or film formed and covered the surface, leading to the pitting formation.

Jan 1, 2005

By T. Donkin, B. Patterson, M. I. Guthrie, J. T. Ross

"The interest in the use of sensor-based particle ore sorting has increased significantly with the recent advances in the sorting technologies and higher capacities per unit. This technology has the potential to provide great value in processing lower grade ores from the mine whilst delivering higher grades to the mill as well as in upgrading waste rock into ore. Typically, the focus is on the amenability of the ore to ore-sorting and associated reductions in the consumption of energy, water and consumables. However, layout has a significant impact on the installed cost of a concentrator and the layout impacts from fitting an ore-sorting circuit into the concentrator plan need to be carefully considered. This paper examines layout considerations that play an important role in ore sorting projects. These include additional crushing and screening requirement, transportation of the rejected material back to the waste stockpile (mine fleet requirements) and effects on concentrator footprints.INRODUCTION Ore sorting has been practiced throughout history with an early report by Agricola in 1556. Metallic and non-metallic minerals were extracted from rocks by laboriously breaking them with hammers and picks and hand-picking selected material with higher grade off a table. The concept has not changed but the sorting technology has evolved significantly over the last 20 years. Ore sorting is usually a dry process in which a portion of the material is rejected based on mineral properties and/or grade. The methods used for sensing ore particles cover a large range of physical properties. A variety of sensors are available that differ on the discrimination technique that is used, which include: photometry, radiometry, conductivity, magnetism, microwave, X-ray transparency: X-ray transparency and luminescence and UV fluorescence (Sivamohan and Forssberg, 1991; Wotruba, 2006). There are two main ore sorting techniques: particle ore sorting and bulk ore sorting. According to Nadolski et al (2018), the potential for sorting is determined though analysis of grade heterogeneity within the orebody (greater heterogeneity represents more opportunity to add value to a project) at the scale of the intended sorting unit size."

Jan 1, 2019

By F. F. Langford

"The Athabasca Basin occupies about 100,000 km2 of the northwest corner of Saskatchewan with its western margin extending about 50 km into Alberta (Fig. 1). The basin is filled with a Helikian sequence of predominantly fluvial sandstones up to 1600 m thick. The sandstone beds are generally flat-lying, and rest unconformably on a crystalline basement which consists mostly of granitic intrusive complexes and quartzfeldspar- biotite gneisses. The basement rocks represent Aphebian sediments and Archaean basement rocks that were metamorphosed and remobilized to varying degrees during the Hudsonian Orogeny (ca 1800 Maj.Since 1968, three mining camps and several substantial unconformity-type uranium deposits have been discovered in the area (Figs. 1 and 2). These deposits lie along the unconformity surface, partially enclosed in sandstones, and partially in the basement rocks. The major deposits have elongate, pencil shaped orebodies that are parallel to the strike of underlying graphitic biotite gneisses. The total tonnage of uranium is in the order of 150,000 to 200,000 tonnes and mining grades range from 0.5 to 2.5 per cent U3O8.IntroductionUranium exploration started in Saskatchewan in 1945 when Jolliffe and Murphy headed field parties to investigate uranium occurrences on the north shore of Lake Athabasca (Kupsch, 1978). Their investigation lead to the development of the Beaverlodge camp in the following years. Some of the early prospectors were impressed by the fact that the uranium occurrences at Beaver lodge were centred on a thick sequence of unmetamorphosed arkosic redbeds which are now called the Martin Group. This sequence was referred to as the Athabasca Series by Christie (1949), and although some occurrences of uranium were found near Stony Rapids and Black Lake, the vast expanse of Athabasca sandstones south of Lake Athabasca was generally regarded as unpromising."

Jan 1, 1986

By Stephen Se

Geological assessment of active mine faces enables ore grade control, geological modelling and exploration planning. Monitoring of the mine advancement at every drill-blast-muck cycle allows for effective production management. However, geological assessments are performed infrequently due to the need to travel to active mine faces, and detailed surveys to map the mine progress are performed at the end of the month. Instant Mine Modeller (iMM) is a portable ruggedized stereo-vision system that creates photo-realistic three-dimensional models of underground mine faces on-site. The 3D models are generated automatically within minutes and can be viewed underground and annotated with geological information. The overall ore percentages of the face are calculated automatically for grade control. Annotated 3D models are located in the mine coordinate system and can be imported into mine management systems. iMM allows for daily monitoring of the mine progress and geology, and for re-visiting the mine virtually as it existed. iMM has been deployed in an underground hard rock mine for 18 months, and it effectively brings the underground work face into mine management offices enabling the right decisions at the right time. iMM has demonstrated benefits to various mine processes including grade control, geological mapping, 3D photo-realistic as-built and production volume.

Oct 1, 2009

By B. R. Maas

Processing material at a consistent rate through the continuous countercurrent decantation (CCD) thickeners presented a major bottle neck to unlocking additional value from one of the post-flotation streams at the Kansanshi processing plant. The manual operation of the thickeners making up the CCD train resulted in frequent imbalances and process upsets across units. The automation of CCD trains is notoriously tricky as the available manipulated variables are outnumbered by the parameters requiring regulation. The implementation of an advanced, auction-based, control philosophy to manage the movement of both slurry and solution inventory through the train addressed this parameter imbalance and lead to the stabilisation of the circuit. Since the commissioning of this control strategy: an additional 7 200 dmt/day (+36% throughput) of material can reliably be processed through the train, the number of monthly downtime events has reduced, and a saving of $354 000/month in reagent cost has been achieved. INTRODUCTION CCD operation Agitated leaching is a common method used in hydrometallurgy to extract a metal from its host ore. The host ore is initially finely ground to liberate the surfaces of the valued minerals and improve the kinetics of the leaching process. The ore is then contacted in an agitated tank with a lixiviant to dissolve the desired metal into the aqueous phase. The resultant slurry from the leaching process comprises of a solution pregnant in the metal salt and a barren ore. The first purification step taken after leaching is to wash the pregnant liquor solution (PLS) from the depleted ore. On the industrial scale, a set of between two to ten thickeners arranged in a countercurrent configuration is often used to carry out this separation (Perry & Chilton, 1973). The slurry is introduced at the head of the train and a wash solution at the tail. The two streams are pumped through each thickener countercurrent to one other. At each stage the residual PLS in the slurry is mixed and diluted down with the countercurrent overflow solution from the downstream thickener. The diluted slurry is fed into the thickener where the solids separate out through gravity sedimentation. The settled solids are channelled towards the underflow of the thickener by a rake mechanism and pumped downstream to the next thickener in the train. The outcome is the recovery of a PLS from the overflow of the lead thickener and a slurry of washed solids from the underflow of the tails thickener.

Jan 1, 2019

By J. H. Pateson, D. C. Comrie, D. J. Ritcey

"Geopolymers are inorganic semi-amorphous three dimensional silico-aluminates of the poly(sialate) type (-Si-O-Al-0-) or of the poly(sialate-siloxo) type (-Si-O-Al-O-Si-0-). Polycondensation occurs at low temperatures with geopolymers being stable up to 12oo0 c. Research, development and application technology pertaining to geopolymers is being undertaken jointly with Dr. Joseph Davidovits of The Institute for Applied Archaeological Sciences of Florida, U.S.A. This joint focused upon the chemical Barry University in Miami Shores, research and development program has stabilization and solidification of various waste products through geopolymerization. Of particular interest is the geopolymerization of mine wastes including tailings and waste rock derived from the processing of base metals, precious metals, potash, coal and uranium deposits.INTRODUCTIOND. Comrie Consulting Ltd., in cooperation and technical liaison with CANMET, Ottawa has been testing the application of geopolymers to mining wastes. Corporate efforts to date have concentrated upon reactive acid tailings, principally from the abandoned Kam-Kotia Mine site, and dewatered paint waste sludges. Test work conducted to date has successfully yielded geopolymer treated materials and wastes with increased chemical and structural stability. Wastes containing heavy metals, cyanides, arsenic and sulphur dioxide have been successfully geopolymerized."

Jan 1, 1988

By I. Thobadi, C. Pawlik, K. Bisaka, S. Mokoena, M. Erwee

The PyEarth™ process developed at Mintek has been demonstrated successfully at pilot scale. Nine tons of ore containing 2.3 mass % of total rare earth oxides (TREO) from a dormant mineralogically complex iron-rich ore deposit, was subjected to a concentrating smelting step in a 200 kW DC open-arc pilot furnace and the rare earths from the resulting slag were extracted via a hydrometallurgical route. This ore deposit is practically not amenable to extraction by conventional methods. The testwork results proved that the PyEarth™ process was able to optimize the extraction of rare earths while minimizing waste through the removal of iron as a saleable iron alloy. Reduction of iron to the alloy in the smelting step was found flexible, efficient, and controllable, while rare earths were left virtually unreduced in the slag phase. The slag chemistry is selected to optimize both the smelting and leaching performances as well as the alloy composition. Leaching of the resulting slag was found possible and most efficient in hydrochloric acid amongst other lixiviants tested.

Jan 1, 2017

By Leroy C. Stewart

Owing mainly to the use of ethylene dibromide in the production of tetraethyl lead for gasoline treatment, there has been a tremendous increase during the past decade in the demand for bromine. In the United States, production, derived mainly as a by-product from the treatment of brines from salt wells, rose steadily from about two million pounds in 1924 to nine million pounds in 1931. In 1936, production amounted to between 20 and 21 million pounds. Much of the increase during the past four or five years has been due to the operation of the Ethyl-Dow Chemical Company's plant, which extracts bromine directly from sea water. The process employed by the Ethyl-Dow Company is somewhat similar to that in use on salt-well brines at their plant at Midland, Michigan, but whereas these brines contain around 1,300 parts per million bromine, sea water contains only 65 to 70 p.p.m.-about as much as the waste effluent in the brine process. By intensive research, however, a process was developed whereby a very considerable percentage of the bromine content of sea water could be recovered, and at a satisfactory operating cost. In its essentials, the process consists in liberating the bromine from the sea water by treat-ment with chlorine, blowing the bromine out of the water by a current of air, and finally absorbing it in a solution of soda-ash.

Jan 1, 1938

By Gobbs C., J. Lam

"The Eagle East project, accessed from the existing and operating Eagle Mine in the Upper Peninsula of Michigan, is an underground base metal project currently in execution by Lundin. This paper will provide an update on several aspects of ventilation including use of a twin-decline access, innovative airflow crossover arrangement and construction ventilation methodology. Integration into existing mine ventilation systems including construction methodology will also be covered. Performance benchmarks and lessons learned are discussed across these topics.INTRODUCTIONLundin has owned and operated the Eagle Mine since 2013. This hard rock underground mine is located in the upper peninsula of Michigan, USA. High-grade nickel ore is mined using sublevel open stoping mining methods and trucked to surface via haul ramp. The mine, having been in production for four years, is nearing the completion of the initial orebody. A satellite orebody 2,000 meters East of the current workings and approximately 900 meters below surface, was identified that could extend operations until 2023. In 2016, Lundin approved the Eagle East project and construction began in 2017 (Lundin Mining Corporation, 2017).Due to proximity to the existing mine, Eagle East will be both accessed and serviced from the existing Eagle Mine. Ventilation at the Eagle Mine uses two fresh air intakes with direct fired combustion heaters; one at the mine portal feeding fresh air into the ramp and one at a fresh air raise located near the Eagle deposit. The primary ventilation circuit is powered on the exhaust air side, with two 700 hp exhaust fans located at a single return air raise. Underground, fresh air is distributed through the main access decline and fresh air raise (FAR) to the production levels and controlled with mechanical regulators on the exhaust side. The exhaust air is collected through return air raises with a collector/transfer drift on 250 Level and then to the surface through a return air raise (RAR)."

Jan 1, 2019

By Jochen Petersen

This paper gives an overview of the various strands of postgraduate and undergraduate training offered in the Department of Chemical Engineering at UCT. Since 2003 the Department is offering a formal postgraduate MSc programme in hydrometallurgical engineering aimed especially at graduate work-based engineers, with 5 weeks of intensive course work plus a research dissertation on a work-related project. This programme has now run 5 times over the years and produced some 20 degrees. The paper reflects on the experiences with running the course, especially the difficulties experienced with supervising industry-based external students. Furthermore, through the Department a graduate training program is offered for all junior metallurgists at a major South African minerals company. This 2-year program, which is currently on its 12th cohort, offers 1 or 2 week intensive blocks of course work alternating with longer stints where the candidates are based at various operations. Although primarily focussed on minerals processing, it has a significant element of hydrometallurgy in it and in recent years an advanced hydrometallurgy stream has been introduced. The paper reflects on the development of the program over the years, the benefits it has provided to the company as well as some of the challenges that remain. Finally the paper gives an overview of hydrometallurgy related undergraduate and research-only postgraduate MSc and PhD projects at the university. Some emphasis is placed on the recently launched South African Minerals and Metals Research Initiative (SAMMRI), a joint government-industry programme to support university-based research in the area of applied metallurgy.

Jan 1, 2014

By Edouard Asselin, Tasawar Javed

The precipitation of hematite from ferric sulphate - cupric sulphate - lithium chloride acidic solutions was studied in a batch reactor. The effect of several variables on the extent of hematite precipitation as well as on its crystallinity and purity was investigated. The variables studied include: initial ferric concentration (1.5 - 30 g/L), retention time (0 - 12 h), initial sulphuric acid concentration (0 - 30 g/L), temperature (150 - 220 °C) and chloride concentration (0 - 25 g/L). The results show that hematite is preferentially precipitated at lower initial iron concentrations. Longer retention times increased the fraction of hematite in the precipitates but did not affect its crystallinity to a significant extent. On the other hand, higher temperatures increased the purity and crystallinity of the hematite. At lower acid concentrations hematite and goethite were precipitated. However, only hematite was precipitated when the initial acid concentration was > 12.5 g/L. Better crystalline hematite was formed at lower acidities. Increasing chloride concentration increased the amount of hematite and decreased the amount of iron sulphate hydroxide phases, but did not affect the crystallinity of the hematite.

Jan 1, 2015

By L. Trytten, S. Bass, P. Nawrocki, J. Mercer

The Sherritt Fort Site nickel refinery and fertilizer plant has been operating continuously since 1954. The ammonia leach process uses ammonia and sulphuric acid, producing nickel and cobalt and an ammonium sulphate byproduct. One of the features of an ammonium sulphate based process is the aggressive nature of ammonium sulphate to concrete and structural steel. After six decades of operation, portions of the structural steel and concrete at the Sherritt facility have become degraded. Infrastructure replacement programs started in earnest more than a decade ago with pipe racks and electrical infrastructure, and have now progressed into building steel. Replacing and repairing this infrastructure within the tight constraints of an operating plant poses several difficult challenges. This paper will outline the approach taken to accomplish this difficult work, and discuss key learnings from the ongoing program.

Jan 1, 2015

By J. B. Mawdsley

Introduction The writer was instructed to visit the Chibougamau region during the field season of 1927 and report on the mineral discoveries that had been made there since 1911. lt was deemed advisable to obtain detailed information regarding the rocks underlying the area in the vicinity of these recent discoveries. Accordingly an area 60 square miles in extent was mapped. The outcrops were studied along the water courses and along bush traverses spaced at half-mile intervals between these water courses. The completion of the rest of the summer's programme allowed only three weeks for this work. lt is from this small, mapped area, and this necessarily cursory survey, that the material for this paper was obtained. Location And Means Of Access The name Chibougamau district is applied loosely to an ill-defined area of about 1,000 square miles lying mostly north and west of Chibougamau lake in the Province of Quebec. The lake is approximately half way between lake St. John and James bay. It lies 150 miles north of the Canadian National railway and 40 miles south of Mistassini?lake.

Jan 1, 1928