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By Masakazu Iida

In this article, technologies of unburned Al2O3-MgO (UAM) refractories are demonstrated in terms of microstructure evolution. During operation, Mg2+ diffuses from MgO to Al2O3 through the liquid phase to form spinel (MgAl2O4) network. Molten slag tends to penetrate along the voids in the spinel network structure and spinel dissolves in the penetrated slag. Therefore, maintaining a high degree of spinel saturation in the penetrated molten slag is important. In order to achieve the condition described above, suppression of overall mass transfer through penetrated slag is effective. This is achievable by evolution of complicated spinel network structure with small pore diameter, which increases the flow resistance of molten slag. Thus, optimization of refractory composition and fabricating conditions, with the aim of creating on improved spinel network, is essential. The effectiveness of spinel network improvement was validated by commercial applications. According to the investigation of UAM brick after use, further densification due to heating under restrained conditions was recognized. Hence, it was concluded that the evolution of the spinel network structure in UAM refractories is essential technology needed to improve durability.

Oct 30, 2017

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018

By Roberto Balarini Junior

Tribological behavior of Si3N4 balls sliding against Al2O3 discs in water was investigated by studying the influence of parameters such as initial surface roughness and circular axial run-out of the discs. The objective was to relate these parameters with the occurrence of the phenomenon known as ultra-low friction coefficient (ULFC), which is characterized by µ < 0.01, including the correlation with running-in duration. As a general trend, greater initial surface roughness and circular axial run-out resulted in greater running-in duration. In addition, it was verified that a mixed lubrication regime (hydrodynamic and boundary) is required to guarantee the occurrence of ULFC by comparing the calculated minimum film thickness with the composite roughness of the worn surfaces. Also, ICQ-OES analysis of the water after the tests indicated that a silicon concentration greater than 1.3 mg/l should be fundamental for the occurrence of µ < 0.01.

Jul 31, 2018

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By Pedro Jorge Walburga Keglevich de Buzin

The steel production in mini mills generates several process residues, among them the electric arc furnace dust (EAFD). This residue has as main elements Fe, O, and Zn, being classified as hazardous by the presence of Pb and Cd. In recent years, a rise in the chlorine content of this residue was observed, motivated by the increased use of scrap with impurities bearing this element. In this work, a qualitative assessment of the presence of chlorine in the electric steelmaking process is made. Complementing it, theoretical considerations based on the computational thermodynamics tool FactSage show the effects of the chlorine on the mineral species in EAFD and on gaseous species in the gas phase (HCl and Cl2). For this study, PVC polymer was used as the chlorine carrier substance which contaminates the EAF charge; presence of other minor elements in the system such as K, Na and Pb were also considered.

Aug 7, 2018

By Marcus Weldon

We are at the beginning of an era of profound transformation and human progress — a new industrial revolution. This “Automation of Everything” era will be brought about by digital interfaces, data analysis and control of the physical world through networks employing the Nokia Bell Labs Future X1 architecture — networks to support the digitization and connection of everything and everyone with the goal of automating much of life. The interconnection of robots, machines, drones, sensors, processing platforms and people through Future X networks will provide transformative tools for the automation and optimization of factories and warehouses, ports, electric grids, transportation networks, food, healthcare, construction, logistics and supply chain, emergency response, mining, and other physical industries. To date, the level of automation has been modest at best. Automating these physical industries — industries that account for 70 percent of the US Gross Domestic Product, for example — has the potential to drive significant increases in the world’s economic productivity.2 Realizing the potential of this next industrial revolution will require billions of wirelessly connected endpoints for high fidelity physical-to-digital conversion, millisecond response times to tightly control and coordinate machines and robots, and intelligent analysis to optimize real-time decisions — tasks beyond the reach of current networks. Increased levels of automation are already being achieved through the use of 4G advanced wireless access technologies. The untethering of sensors and actuators in industrial environments through the low-latency, high-bandwidth, high-reliability, and massive scale provided by 5G wireless access will complete this evolution, providing an unprecedented ability to digitize, analyze, comprehend and manipulate the physical world at a scale never previously thought possible. These new capabilities will enable us to create digital models of the physical world with ever higher levels of fidelity, further enhancing our ability to improve operational efficiencies and increase productivity and worker safety. Doing this will require a dramatic evolution in network architecture toward massively distributed cloud control and baseband capacity to achieve the required ultra-low latency and ultra-high bandwidth for industrial and infrastructure automation services — the Future X architecture. In early 2019, Nokia Bell Labs will publish a sequel to “The Future X Network: A Bell Labs Perspective”. “Future X for Industries: A Nokia Bell Labs Perspective” will explore how the Future X architecture will automate many of the world’s physical industries, including chapters devoted to electric power, cities, rail, mining, public safety, manufacturing, ports, logistics and supply chain, and an overarching chapter devoted to securing this highly automated world. To give you a small taste of the feast that’s to come, we’re sharing with you an initial installment — “Future X for Industries: Mining” — the Nokia Bell Labs view of how mining will be transformed through a Future X architecture..

Oct 1, 2019

By Nigel Marx

In order to understand (and ultimately to predict) the friction reduction resulting from the use of polymer solutions, the rheological properties of model polymer solutions have been measured over a wide range of shear rates. Both temporary and permanent shear thinning have been observed. By using base fluids of different viscosities it has been shown that permanent shear thinning depends more closely on the shear stress experienced by the fluid than on the strain rate. Hydrodynamic measurements have been made on the polymer solutions using a compliant ball on flat lubricated contact that operates in isoviscous-elastic conditions. The measured friction values can only be predicted with reasonable accuracy if the measured shear thinning properties of the lubricant are taken into account in the hydrodynamic model.

Jul 31, 2018

By Alessandro Marques

Based on a short overview regarding steel defects in the final product, several refractory approaches to maintain or increase steel cleanliness are reviewed in this publication. By applying a ladle to mold approach, one potential to maintain cleanliness is to reduce the probability of air ingress by selection of a suitable slide gate system. Following this path, also the influence of a special configured impact pot is presented to maintain steel quality. Finally, higher productivity as well as cleanliness can be provided by selection of PROIL as a revolutionary product at the casting machine.

Oct 30, 2017

By Martim Hideki Nakayama Kurauchi

One of the main issues regarding the use of charcoal in metallurgical processes is its mechanical strength, which is much lower than coke. There is no defined standard to determine charcoal compression strength, and the methods described in the literature consist in using a prepared specimen and applying compressing load in the same direction of the charcoal fibres. As charcoal is highly anisotropic, it is proposed a procedure that does not use a specimen and with load applied on a specific direction. Instead, it intends to simulate industrial conditions by randomly dumping charcoal inside a tube, without preferential directional arrangement. This is an attempt to determine charcoal mechanical strength and predict the behaviour of bulk charcoal under a static load, as in a blast furnace. Experiments with controlled loads have been carried out on randomly distributed bulk charcoal with controlled initial size and their effect on the size distribution has been analysed. After compression, charcoal is screened and each size is weighed, determining the particle size distribution of the experiment. This method can therefore be used to evaluate charcoal mechanical strength.

Aug 1, 2018

By Jônatas Venancio Barbosa, Dagoberto Brandão Santos, Túlio Magno Füzessy de Melo

In this work, the mechanical and metallurgical behavior of titanium added ultra-low carbon (ULC-Ti) steel under hot and warm working conditions was studied by means of dilatometer compression tests. Double compression schedules were performed at temperatures between 700°C and 1000°C, inter-pass times of 0.5-100 s, and deformations of 0.5 and 0.3 in the first and second stages, respectively, with strain rate of 1 s-1. The analysis of the flow curves obtained allowed the evaluation of the softening characteristics of the steel. The softening and microstructure features indicate different restoration mechanisms depending on the temperature range. Static recrystallization with rapid microstructure restoration is observed at temperatures within the austenitic and intercritical field. Strain induced boundary motion and recovery mechanisms apparently control the restoration process in the ferrite region. In general, flow stress curves showed dynamic recovery behavior. Only the deformation in the intercritical region produced a peak in the flow stress curves. Isothermal holding tests associated with single hit compression indicated the presence of dynamic strain induced transformation, accelerating the softening kinetics at the intercritical region.

Oct 1, 2019

By Rudolf Lesch

Till date, coke has been produced mainly from coals with a content of volatile matters in the range of 20% to 28% and good coking properties. If such so-called &quot;selfcoking&quot; coals are available, blast furnace coke or foundry coke with the required quality characteristics can be produced in top-charged horizontal ovens. In this case, the possibility of using high-volatile coals and in particular coals with low-caking properties is very restricted. Even if high-volatile coking coals have good coking properties, coke produced from such coal alone will not meet the requirements in terms of coke strength. The mechanical coke properties are influenced by the charge coal blend and the coking conditions. In this context, the bulk density of the oven charge is a decisive factor. Research and development in the field of coke production in horizontal chamber ovens aims at improving the specific oven throughput, increasing the raw material basis and introducing environmental protection technologies. The key factor, however, is to guarantee and further improve the rentability of the coke production. It is very important to reduce the cost of the charge coal to a minimum at the same time maintaining or even improving the coke quality.

Aug 17, 2017

By Douglas Glenn Stalheim

The demands for improved mechanical properties in hot rolled long products are increasing as the expectations of global Standards and construction designer’s increase. Cost constraints limit the excessive use of expensive alloys to meet these expectations. In addition, depending on the mill, equipment can limit what can be realized to meet the increasing expectations. The most effective way to meet the increasing expectations for improved mechanical properties of optimum strength and ductility is through producing steel with as fine as possible uniform cross sectional grain size in the “as-rolled” condition. The best solution to the development of this fine and uniform cross sectional grain size is to develop a cost effective alloy design coupled with proper metallurgical process control implemented into an existing mill’s equipment capability and layout. In other words, properly bringing together alloy, metallurgy, process control and existing equipment capabilities to develop an optimum product that can meet the increasing demands of the construction designer. This paper is designed to give a solid understanding of the production and metallurgical requirements to achieve a grain size in “as-rolled” long products that is as fine as possible within the limitations of the process and production parameters of the individual plant.

Jul 30, 2018

By Pierre Montmitonnet, Yukio Shigaki, Jonatas Mezêncio Silva

A precise roll stack deformation model of a flat rolling mill is crucial for strip profile assessment as it depends strongly on the roll’s deformation. The need for more and more advanced products with stringent both geometrical and mechanical tolerances (e.g., Advanced High Strength Steels – AHSS), with thinner and harder steel strips, demands more advanced simulation models. The present paper addresses assumptions made in Finite Element Method (FEM)-based roll stack models on some important, yet barely discussed features: What is the impact on precision of the simplifications such as symmetry and anti-symmetry? Should roll neck boundary conditions in bearings be considered as fixed or simply supported? In this paper a hybrid model developed by the authors for a general flat rolling mill is used to assess those questions. This model runs much faster (100x in some cases) than a whole-FEM-modeled 6-high rolling mill with the elastoplastic strip deformation, thanks to its simplifications adopted. This model assumes a steady state rolling condition, and the roll stack is modeled with tridimensional finite elements, and the loads are calculated via a slab method adopting a plane strain state for the strip deformation (especially true for thin strips). An industrial 6-high cold rolling mill is modeled and results on the application of symmetries and different boundary conditions on the roll’s necks are presented. It is concluded that the application of symmetries and anti-symmetries for the 6-high rolling mill is possible for thin strips. And the way the necks are modeled does not impact on the final strip shape, though it influences the magnitude of the roll’s displacement. The coupling of the strip with the work roll applied assuming a symmetry plane of the arc of contact has little influence on the strip shape.

Oct 1, 2019

By Andreas Jungbauer

Two Arvedi ESP plants going into operation in 2015 will allow a Chinese steel producer to better serve the extremely attractive local and export markets for high-quality, thin-gauge strip products. The energy consumption and the related costs are reduced by up to 45% compared to conventional casting and rolling processes. This also means a major reduction in CO2 emissions. The new plants are designed for an annual production capacity of 2 x 2.55 million tons of high-quality, ultra-thin, hot-rolled strip products with widths of up to 1,600 mm and thicknesses down to 0.8 mm. The project scope also features a comprehensive training and assistance package for plant start-up and operations by personnel from the existing ESP plant at Acciaieria Arvedi SpA, Italy. The plant setup, the trainings and assistance program as well as latest results from the ESP plant in Italy will be presented. While this project is under execution three further ESP lines have been ordered by the same customer summing up now to five ESP lines at the same location.

Jul 30, 2018

By Leonardo Camilo dos Reis, Edmilson Fernandes Dadomi, Claudio Silva de Paulo

In the hot strip mill production, one of the factors that may affect the productivity is the occurrence of failure due to the geometry of the strip at the exit of the rolling mill, because the tip of the strip can turn-down or turn-up. This study had the objective of evaluating the behavior of the strip when leaving the working rolls, through numerical simulation, aiming to know the influences of the main variables that govern the formation of the turn-down. The methodology consisted in performing the computational simulation of the strip mill and to vary the operational and geometric parameters that could influence the process. The results showed that the rolling of hot strips of HSLA material with final thickness varying between of 3 to 6 mm and a reduction of 6.6% to 11.0% in the last stand of a hot strip mill, tends to bend towards the roll with larger diameter, higher friction coefficient , higher temperature and lower limit of material flow. It was observed that the variation in diameter is the main factor that contributes to the formation of the curvature of the front-end of strip. Based on these results, several measures were implemented in the industrial line, with a significant reduction in the occurrence of turn-down.

Oct 2, 2019

By Edo Engel

Hot Blast Stove Technology has been developed to such an extent that low cost hot metal production for over 30 years without major repairs has become achievable, making the decision for a campaign length between 5 to over 30 years a design choice for the plant owner/operator. Some of the earlier examples of designs capable of such long campaign lengths are currently close to the 50th year of their running campaign. These examples are found especially in Europe and North America. Along the duration of these campaigns, repairs to subsystems such as burners, hot blast outlets etc. may be required. Depending on a plant’s up and down stream production capacities, the repairs may have to take place in the shortest possible time frame to minimize production loss. This article discusses an approach for intermediate repairs, executed while keeping the majority of the system at operating temperature.

Oct 30, 2017

By Paulo Sérgio Moreira, Geraldo Lúcio de Faria, Rhelman Rossano Urzêdo Queiróz, Amanda Aparecida Fátima Arruda, Ana Cecília de Carvalho

O objetivo deste trabalho foi avaliar o desempenho em desgaste de camadas espessas de óxidos formadas na superfície do aço inoxidável ferrítico 410D após a sua submissão a tratamentos isotérmicos em atmosfera oxidante. O aço em questão foi estudado no estado de entrega e tratado isotermicamente nas temperaturas de 900°C e 1000°C por diferentes intervalos de tempo. O método de avaliação empregado foi o teste de desgaste micro-abrasivo do tipo esfera presa em placa. Com o desenvolvimento do estudo, foi possível executar análises qualitativas e quantitativas a respeito do comportamento em desgaste do aço inoxidável 410D em função de sua condição superficial, como oxidada ou não. Alterações microestruturais também foram consideradas na discussão dos resultados. Concluiu-se que a camada superficial de óxidos desenvolvida após os tratamentos isotérmicos possui boa aderência e tem potencial para aplicação como camada protetora do aço em aplicações onde a sua resistência ao desgaste seja requerida.

Oct 9, 2019

By Cláudio Antônio Goulart Valadares

O fluxante para aços baixo carbono, aplicado no lingotamento contínuo de placas, apresenta como características a temperatura de fusão entre 1.030°C e 1.070°C e a tendência a cristalização suprimida. Desta forma, o filme de escória apresenta predominantemente a fase vítrea que facilita a transferência de calor na interface molde de cobre e pele de aço em solidificação. Há uma tendência em retirar ou reduzir o teor de flúor nos fluxantes, com o objetivo de minimizar a erosão da câmara de exaustão do lingotamento contínuo, além de ser um risco potencial para a saúde e segurança e do aumento da taxa de erosão da válvula submersa. Este trabalho apresenta os resultados de análise dos filmes de escória do fluxante referência e a sua versão isenta de flúor via microscópio eletrônico de varredura e microscópio óptico de luz polarizada. Mais resultados como difratometria de raios-X e análises térmicas também complementam esta análise assim como algumas características físico-químicas dos produtos em questão.

Jul 30, 2018

By Luciana Lezira Pereira de Almeida

De forma geral, as ferramentas diamantadas empregadas no corte de rochas ornamentais são compósitos constituídos de partículas de diamante embebidas em uma matriz metálica. Neste trabalho, para a preparação da mistura das pós, foram utilizados dois processos distintos: o processo convencional utilizando um misturador do tipo cônico e um processo alternativo utilizando um moinho do tipo Attritor. Ambos os processos tiveram a duração de uma hora. Após o processo de mistura, os pós foram sinterizados sob as mesmas condições, pressão de 35MPa e Temperatura de 750oC por um período de 6 mim. Foram produzidos corpos de prova com e sem diamantes. Para a caracterização dos compósitos foi utilizada a Microscopia Eletrônica de Varredura (MEV), Difração de Raios X (DRX), Porosimetria e ensaio de desgaste. Após as caracterizações e testes ficou evidente que os compósitos obtidos a partir da mistura utilizando o moinho Attitor exibiram melhores propriedades, inclusive em relação à compósitos industriais.

Aug 16, 2017

By Jorge Luiz Ribeiro de Oliveira

A indústria siderúrgica na América do Sul tem sido desafiada desde a crise econômica mundial do final de 2008, como as demais siderúrgicas ao redor do mundo. O cenário de continua degradação das matérias primas, em especial o minério de ferro e a necessidade de reduzir custos, considerando que cerca de 70% do mesmo está relacionado à produção de gusa, atuando em direção oposta, torna este desafio maior ainda. Operar um Alto Forno com elevadas taxas de injeção de carvão (mais que 180 kg/t de gusa) e baixo taxa de combustíveis (menor que 490 kg/t de gusa), considerando a elevação da taxa de geração de escória devido a matéria prima em degradação (~300 kg/t de gusa) torna-se obrigatório ter estabilidade operacional por meio de boas práticas operacionais suportado por adequado sistema de manutenção centrado em confiabilidade (RCM). Este trabalho objetiva mostrar como a ArcelorMittal planta de Tubarão está enfrentando esta situação, visando atingir os objetivos citados anteriormente.

Aug 16, 2017