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By R. T. Johansen

The wettability of petroleum reservoir materials by water and crude oil has been recognized as an important factor in determining waterflood behavior. The problem of simulating and studying reservoir conditions and characteristics, to produce laboratory results congruous with field experience, has been examined by many methods. (1, 2, 3, 4).4/ The most generally accepted approach to this problem is determining wettability of the porous medium by imbibition methods; or, after solvent extraction, predetermining the wettability of the samples by coating the surface of the medium to render it preferentially oil-or water-wet (3, 5). The emphasis of wettability studies has been placed on the characteristics of the reservoir materials with little consideration being given to the fluids themselves. Therefore, the wetting tendencies of crude oils have been investigated by a recently developed method (6). Imbibition and the more general phenomena of capillary pressure are the most direct ways to measure wettability. The simplest type of capillary pressure observations involves the use of an interfacial-tension capillarimeter, which does not produce as separate values either interfacial tension or contact angle. Actually, these quantities do not have independent significance in reservoir engineering, and the property of wettability they are intended to evaluate is given, immediately by capillarimetric measurements.

Jan 1, 1961

By O. E. Traubert, E. G. Meiter

"The daily sulphur dioxide content of the air at the Pittsburgh Experiment Station of the Bureau of Mines was determined by the bureau at the request of Committee D-14 on Screen Wire Cloth of the American Society for Testing Materials. The purpose of the investigation was to obtain data for use in interpreting screen-corrosion tests, which were conducted simultaneously and jointly by the committee4 and the Bureau of Mines.The plan of this investigation was to vale a single daily determination, except on Sundays and holidays, of the SO2 content of the atmosphere at the exposed test screens, for a period of one year. No attempt was made to determine the variation during the day, except on the morning of October 15, 1927, when the atmosphere was unusually foggy and smoky. Several successive determinations were made on that date to ascertain changes in the SO2 as the morning haze disappeared. The SO2 determinations were begun on August 11, 1927, and continued until August 11, 1923.The Pittsburgh Experiment Station of the Bureau of Mines is in a residential section about 3 miles east of the central or main business district of Pittsburgh. The air samples were taken on the roof above the auditorium, or the center rear of the building. This was also the place where the pieces of screen were placed for corrosion tests. The height was about 40 feet above ground level. Several sources of considerable smoke and SO2 are in the immediate vicinity. On the west side of the building is a double-track railroad. At this point the line runs through a cat below the level of the building. The horizontal distance between the air-sampling position and the railroad tracks is about 400 feet, and the vertical distance about 70 feet. The power plant for the Bureau of Mines building is about 250 feet south of the sampling position. About 1000 feet farther to the south are the engineering building and power plant of Carnegie Institute of Technology, and 1/4 mile to the southwest is the power and heating plant for the Carnegie Library and Museum. About 1 to 2 miles farther south and also southwest"

Jun 1, 1930

By G. J. Slavens

The Bureau of Mines has devised technology to recover cobalt, nickel, and byproduct copper from domestic lateritic material using an oxidative, ammoniacal ammonium sulfate leach. Nickel, cobalt, and copper were recovered by solvent extraction and electrowinning. To reduce the cost and complexity of cobalt recovery, an alternate method using lig-nite to extract Co3+ was investigated as reported herein. In the first 25 BV (bed volumes) of solution contacted with lignite, 97 wt pct of the Co3+ was extracted in & downflow column at pH 9.3. After 85 BV, the lignite was loaded to 1.5 wt pct Co3+ and further ex-traction was minimal. The lignite extracted cobaltic ammine complexes rather than cobalt ions and was nonselective as to other -metal cations and ammonium ions. Deleterious cations and 80 wt pct of the nonammine ammonium ions were removed prior to acid elution of the lignite. The removal of the ammines prior to elution to produce an ammonium-ion-freeCo3+ eluate was only partially successful. Thus Co3+ removal from ammoniacal solutions by lignite is technically difficult and economically unfeasible. It was also determined that reduction of Co3+ to Co2+ occurred during the extraction-elution process.

Jan 1, 1984

By Karl C. Dean

The Bureau of Mines stabilized 10 acres of windblown copper mill tailings at McGill, Nev., by a combination chemical-vegetative procedure. Legumes, winter wheat, wheat-grasses, and wild rye were seeded, and the area was subsequently sprayed with a resinous adhesive chemical to stabilize the sands until the vegetation could grow. During the year since treatment, the area has been well stabilized against wind erosion. The established vegetation appears to be capable of self-perpetuation and renewal without irrigation. The cost of stabilizing the area was $135.50 per acre.

Jan 1, 1969

By J. E. Gebhardt

External control of the electrochemical potential of a bed of mineral particles has been investigated by the Bureau of Mines as a method for controlling particle inter-action with organic collectors and thus, flotation response. A cylindrically shaped, 200-to 300-g bed of sulfide mineral particles was used as the working electrode to examine the potential distribution in the bed. The dissolved oxygen concentration of the electrolyte had a significant effect on the potential profile across the mineral bed. Low oxygen levels were necessary to achieve uniform electrochemical potential distributions. Flotation separation of a chalcocite-pyrite mineral mixture by controlled potential was achieved using ethylxanthate, but the flotation behavior of chalcocite and pyrite from the mixture does not follow the flotation behavior of the individual minerals. That is, the presence of another sulfide mineral alters the flotation behavior with ethylxan-thate. Galvanic interaction due to mineral-to-mineral contact between chalcocite and pyrite contributes to differences in the recovery. Chalcocite dissolution products had a deleterious effect on pyrite flotation by activating flotation below -0.1 V (saturated calomel electrode) and depressing flotation above -0.1 V. Pyrite dissolution products had no effect on chalcocite flotation.

Jan 1, 1985

By Richard L. Unger

The U.S. Bureau of Mines has designed, fabricated, and tested a prototype track maintenance vehicle for underground coal mines. The vehicle uses a stiff rotating brush to clean the track so that a visual inspection is possible. It is also equipped to measure track gauge and cross-level. The objective of this report was to describe the track maintenance vehicle and detail the results of investigations into present underground track inspection procedures and cleaning technologies, which led to the development of the prototype. Recommendations are made concerning the integration of components of this prototype vehicle into current track cleaning and inspection systems used in underground mines.

Jan 1, 1984

By Errol D. Sehnke

This U.S. Bureau of Mines report provides detailed information on worldwide bauxite production capacity by mine and country, including bauxite substitute materials in countries of the former Soviet Union, The information was compiled from a variety of domestic and international sources and was based on information available to the Bureau through December 31, 1994. Capacity data represent announced installed and planned capacities and do not necessarily reflect a U.S. Bureau of Mines judgment of actual mine operating levels or timing of planned expansions. The year-end capacity is the ?in place? capacity or estimated production capacity, whichever is larger.

Jan 1, 1994

By B. K. Shibler

During the investigation of the occurrence of manganese deposits in the Western United States, examining engineers of the Bureau of Mines collected 2-ton samples from five manganese properties near Golconda, Nev. Extensive laboratory tests were made to determine the amenability of these ores to standard ore-dressing methods of concentration. The Tom Major property, one of those sampled, is situated 12-1/2 miles south of Golconda, Humboldt County, Nev. The deposit is described as a bed about 5 feet thick in a thinly bedded shale and dolomite formation. The sample tested was obtained from the manganese bed, but the examining engineer reported: "The mining of an appreciable tonnage at reasonable cost would perhaps cut in half the grade represented by the sample."

Jan 1, 1951

By Earl R. McMillan

"Coal washing commands the thoughtful attention of a steadily incre in number of people. Clean coal is not merely a luxury but is rapidly becoming a necessity in some industrial operations.Coal seams in the Northeast are rarely free from ""bone"" and shale or clay partings which vary from a fraction of an inch to several feet in thickness. Nearly all of the coal measures are folded and faulted, the coal seams dip at various angles, and in some cases are badly broken. In mining these seams fragments of the roof and floor, as well as partings of impur-ities within the seams, unavoidably become mixed with the coal, so that the raw coal as it comes to the surface often contains as much as 50 per cent, by weight of waste.At the Bureau of Mines experiment station at Seattle, the washing of this coal in order to improve it for commercial use has been studied. Since the process of coal-washing depends upon differences in specific gravity between the clean coal and, its associated impurities, the first problem undertaken was that of determining the specific gravity of the clean coal and of each parting of impurity contained in a large number of representative seams.It was found that the freshly-mined coal is practically saturated with water, this being observed in determining the effect of moisture content upon the specific gravity of the coal particles, selected from samples of coal varying from low-grade subbituminous up to semianthracite, all of which are found in the State of Washington. The specific gravity values determined for the cleanest particles varied from 1.28 to 1.35; in general, the higher the rank of the coal the hither the specific gravity."

Nov 1, 1920

By Roy H. Poston

The following paper is one of a series on mining methods and practices being published by the United States Bureau of Mines, and deals with the sinking of the Pim shaft (No. 7) of the St. Louis Smelting and Refining Works of the National Lead Co. in the southeast Missouri lead belt. The shaft was sunk in 1922 and 1923 on a tract several miles south of the company's main plant located at St. Francois, Mo., in St. Francois County. The author is indebted to W. H. Comins, local manager of the company, with whose permission this article has been written, for his helpful criticism; and to E. T. Campbell, geologist, and M. Cross, underground shop foreman; and to W. A. Cole, manager of the E. J. Longyear Development Co., who had general supervision of the work and supplied detailed performance and cost data.

Jan 1, 1932

By M. Hertzberg

This Bureau of Mines report proposes a new methodology for estimating industrial dust explosion hazards in terms of three probabilities or co-factors: The dispersion of the dust, the existence of a flammable dust concentration, and the presence of an effective source of ignition. This method or rationale is proposed as a replacement for the "explosibility index" that was first suggested 25 yr ago, but which, by consen-sus among leading researchers in the field, is now outdated. This report presents a detailed critique of the deficiencies of that old, material-oriented index, and develops the logical rationale for its re-placement by an approach that is better suited for quantitative hazard evaluations. A variety of such evaluations are illustrated, which show how a quantitative prediction of explosion frequencies can be obtained from laboratory measurements and operating conditions in a given indus-trial facility. The method has some pitfalls, particularly as they re-late to the correlation of events or their randomness. These are discussed, as well as the method's other limitations and uncertainties. This work is intended to provide a beginning to a quantitative approach to explosion hazard assessment. To that end, a new method is proposed for estimating thermal ignition probabilities in terms of the measured laboratory autoignition temperature of a dust, its relationship to the operating temperature, and its distribution within a given industrial system.

Jan 1, 1987

By Edward D. Thimons, Jay F. Colinet

Underground coal mining operations in the United States continue to increase productivity as mining equipment and practices are improved. Unfortunately, increased production also results in the potential for increased respirable dust generation and worker exposure. In response, US operations are applying basic controls at elevated levels and looking to emerging technologies in an effort to better control respirable dust levels. Ventilating air and water sprays remain the basis of dust control strategies for both longwall and continuous mining operations, and the level of application for these controls continues to increase. In addition, new technologies are emerging that have the potential to further reduce dust levels. The National Institute for Occupational Safety and Health (NIOSH) has been conducting research into methods to optimize existing control technologies and evaluate emerging control technologies. This paper will summarize control technologies routinely being used in underground coal mine operations, as well as provide a review of new controls that are being pursued.

The National Institute for Occupational Safety and Health (NIOSH) National Personal Protec-tive Technology Laboratory (NPPTL) and the Mine Safety and Health Administration (MSHA) conduct a Long Term Field Evaluation (LTFE) program to evaluate deployed self-contained self-rescuers (SCSRs). The objective of the program is to evaluate how well SCSRs endure the under-ground coal mining environment with regard to both physical damage and aging when they are deployed in accordance with Federal regulations (30 CFR 75.1714). This report presents ?ndings of the combined eighth and ninth phases of the LTFE. For these phases, over four hundred SCSRs were evaluated. The units tested include the CSE SR-100, Draeger Oxy K-Plus, MSA Life-saver 60, and the OCENCO EBA 6.5. The OCENCO M-20 was evaluated only in Phase 9. Testing was per-formed between December 2000 and April 2004. Results of the evaluation indicate that all SCSRs experience some performance degradation due to the mining environment. Observed degrada-tion varies from elevated levels of carbon dioxide, high breathing resistance, and reduced capacity. Mechanical degradation to the SCSR components included breathing hoses, chemical beds, outer cases and seals. The LTFE tests discussed in this report are different from tests performed for SCSR certi?cation to the requirements of 42 Code of Federal Regulations, Part 84 (42 CFR, Part 84). LTFE tests reported here are conducted to an end point, oxygen depletion, to enable comparison of the duration of new and deployed SCSRs. The method for obtaining deployed SCSRs for this evalua-tion was not a random selection from the deployed population of SCSRs. Although the results of these tests are useful for observing performance of the tested SCSRs, they are not representative of all deployed SCSRs. A new evaluation protocol, with revised sampling strategies, test methods, and reporting procedures, is currently being designed to enhance the generalizability of the results. This program will be implemented following completion of Phase 10 of the current LTFE protocol.

Jan 10, 2006

By John Paul Gries

During World War II, when the curtailment of imports led to an unprecedented demand for domestically produced mica, beryl, and other pegmatitic minerals, the Bureau of Mines and the Geological Survey entered upon a program designed to expedite the production of these minerals from the Black Hills area of South Dakota. The program involved mapping, sampling and drilling many pegmatite dikes found in the southern portion of the area and beneficiation tests in the field and in the Bureau of Mines laboratories at Rapid. City, S. Dak., Rolla, Mo., Salt Lake City, Utah, and College Park, Md. This paper describes the mode of occurrence and the sampling and beneficiation tests on one dike, the Helen Beryl pegmatite, which was investigated as part of the general pegmatite study in South Dakota. Investigation of the Helen Beryl Pegmatite by the Bureau began in August 1943 and was terminated in April 1944. During this period the Bureau took a series of bulk samples from pits for beneficiation tests, drove an adit through the center of the dike to obtain feed for a bulk-sampling plant operation, and finally drilled a series of long holes to sample the deposit further. Geologists of the Federal Geological Survey mapped the deposit and the faces of all excavations and logged drill holes from sludge samples recovered from long-hole drilling.

Jan 1, 1949

By J. T. McCartney

"INTRODUCTION The surface areas of the finest fractions of a pulverized material are disproportionately larger than their weights. For instance, Pesrott and Kinney 3/ showed that, in a sample of minus 200-mesh coal, particles that are about 2 microns in diameter represent 15 percent of the entire surface area but only 1.5 percent of the total weight. Because the sur- face area is the dominating factor in the behavior of finely divided materials in many practical processes, the role of the finest particles is of great importance. The oxidation and combustion of pulverized coal, both in the dry form and in suspension in oils, and the hydrogenation to fluid hydrocarbons of mixtures of pulverized coal and heavy oil are reactions in which the surface area of the coal particles has considerable influence. This investigation of the size distribution of fine coal particles was conducted with the hope that such processes would thereby be better understood. The results should also be of value in the study of the crushing and fracture of coal."

Sep 1, 1945

By R. V. Higgins

Many contributions to methods of forecasting the performance of waterfloods of a five-spot pattern have been made by investigators. In most of these forecasting methods, a previously selected sweep efficiency is used, and other simplifying assumptions are employed to obtain the objective. In this paper the calculated oil recoveries from several five-spot single- and multiple-layer stratified reservoirs were made with a minimum of assumptions, and because of the techniques used, no previously selected sweep efficiency was required. As a result, the accuracy of the forecast is increased. Permeability curves and continuously changing saturation gradients are used in every section of the pattern. By means of a potentiometric model, the flood pattern is divided into channels, the centers of which are the streamlines. The channels are divided into cells. As flood water enters, the permeability and saturation of each cell change with time. In this study the production from multiple-sand layers of different absolute permeability but with the same relative permeability-saturation relations are combined. The results are shown for a single- and 10-layer reservoir with a permeability variation of 0.60. The oil rate, water-oil ratio, and recovery are shown as functions of time for a 2- and 20-centipoise oil starting in primary phase and after fill-up.

Jan 1, 1962

By R. J. Fantel

To determine the availability of phosphate rock from domestic re- sources, the Bureau of Mines evaluated the potential production of phosphate rock from the demonstrated resources of 130 mines and deposits. The evaluation included an estimation of resources, engineering methods, and capital and operating costs, and an economic analysis to determine each operation's average total cost of production over the life of the mine, including a 15-pct discounted-cash-flow rate of return on all investments. Quantified but not evaluated in this report are substantial phosphate resources at the inferred and hypothetical resource levels. The 130 mines and deposits contain 6.4 billion tons of recoverable phosphate rock product, about 20 pct from producing mines. At total production costs of under $30 per ton in January 1981 dollars, about 1.3 billion tons of phosphate rock product is potentially available, over 90 pct from producing mines. This study suggests that production from low- cost, high-grade phosphate mines now in operation will decline during the next decade, and new higher cost, Lower grade mines will have to be developed to satisfy demand into the next century, In addition to the demonstrated resources evaluated in this study, 7 billion tons of inferred-level and 24 billion tans of hypothetical- level phosphate rock are potentially recoverable, which, in part, includes material containing high amounts of magnesium, Much of this material could likely become available in the near future.

Jan 1, 1983

By H. D. Pallister

A review of? reports and literature on the pyrite deposits at Pyriton, Ala., indicated that a large tonnage of pyrite, some of which contained a small amount of copper, had been mined and shipped to fertilizer plants throughout the South. The information contained in this literature tended to demonstrate that the ore occurred in separate lenses of greater or less extent and of varying thickness and richness in pyrite as well as in copper. The outcrop being parallel with the Atlantic Coastline Railroad and just south of it makes the deposits readily accessible for shipment. Slopes could be sunk as they were in the past in the ore body if it were of sufficient grade and thickness, and the ore could be hoisted up the slope and milled close to the slope mouth with an ample supply of water from Talladega Creek, which follows the outcrop closely.

Jan 1, 1949

By M. F. Dunn

A handbook to provide a quick reference guide for selecting and using jet fans in a variety of conditions was prepared. The document is intended for use by front-line supervision, ventilation engineers, and mine planners. Included are discussions of jet fan characteristics, selection and use critieria, and do's and don't's for easier operation, safety, and performance. The handbook is based on research at three underground metal/nonmetal mines having cross-sectional areas of 900 to 2,000 ft2.

Jan 1, 1983

By Murray Jacobson

The respirable dust standard in the Federal Coal Mine Health and Safety Act of 1969 is designed to prevent disability and death from coal workers' pneumoconiosis. Beginning June 30, 1970, the operators of coal mines were required to maintain the average concentration of respirable dust in the active workings at or below 3.0 milligrams of dust per cubic meter of air. The standard is reduced to 2.0 milligrams per cubic meter after Dec. 30, 1972. This paper presents the equipment and procedures used by the coal mine operators in implementing the respirable dust sampling program established by the Secretary of the Interior and the Secretary of Health, Education, and Welfare and shows the effect of the law, during the first year, on the reduction of dust levels in selected mines. The system employed by the Bureau of Mines for analyzing and processing the dust samples is also presented.

Jan 1, 1971