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By Llewellyn A. Rubin

Under Bureau of Mines Contract H0122007, Telcom, Inc., with the assistance of Fenix & Scisson, Inc., conducted a 17-month research and development project aimed at provid¬ing a field-test model of a guidance system for use with the Bureau of Mines Probe Drill. The Probe Drill is a part of the Bureau's Mine Rescue System developed under Contract H0101262. Volume I of this report is subdivided into seven sections. Volume II consists of a number of supporting appendices. In addition, there were delivered under the Contract, a number of other documents which are referenced in the text. Section 1 deals with essential contract information, Program Background, and a general system description. Section 2 covers the project chronology in brief. Section 3 is a digest of design considerations and implementation related to the requirements of the Contract. Section 4 is a description of the System, including illustrations of the hardware, and software. Section 5 is devoted to Operation and Maintenance. Para. 5.1 describes step-by-step field assembly and disassembly of the downhole unit. Para. 5.2 covers Operation. Para. 5.3 covers various aspects of maintenance from the lowest field echelon possible. Higher level maintenance must be accomplished in the laboratory, for the present field-test model. Para. 5.4 covers system calibration. Para. 5.5 covers detailed step-by-step operational sequences. Section 6 covers the results of the field testing, post-test evaluation, and recommendations. Essentially, we conclude that the present hardware (field-test model) has proven every aspect of system performance, but failed to provide reliable assurance of an operationally ready system. Telcom, therefore, recommends a three-phase continuing effort devised to provide the operationally-ready model of the system.

Jan 1, 1973

By Paul W. Johnson, Ralph C. Kirby, Frank A. Peters

A series of economic evaluations of processes for producing metallurgicalgrade alumina from low- grade aluminous materials is being conducted by the Bureau of Mines to determine the relative processing costs . The two processes considered in this evaluation are concerned with the recovery of alumina from clay through the formation of ammonium alum . In the first process , dehydrated clay is leached with ammonium bisulfate solution ; in the second process , clay is baked with ammonium sulfate and then leached with water containing a small quantity of sulfuric acid . After the alumina is dissolved by either of these methods , the iron is reduced to the ferrous state to avoid crystallization of ferric sulfate with the alum . The recovery of pure alum requires two crystallization steps . The alum crystals are then redissolved and precipitated with ammonia to produce alumina hydrate , which is calcined to a - alumina . These evaluations are based on published work , and the proposed plants are designed for a capacity of 1,000 tons of alumina per day . The estimated operating cost per ton of alumina for the bisulfate leaching process is $ 117.06 , and for the sulfate baking process , $ 109.26 . Using a Marshall and Stevens chemical equipment index basis of 240.0 , the estimated fixed capital costs , in the same order , are $ 158 million and $ 146 million . Under current economic conditions , these two processes are not competitive with the Bayer process for the production of alumina from bauxite . Since small improvements will not reduce costs sufficiently to approach competitive costs , future research work with these processes should be confined to areas likely to result in major cost reductions .

Jan 1, 1965

By K. K. Kelley

Thermodynamics data for silicates have applications in the fields of extractive metallurgy, ceramics, and geochemistry. To facilitate these applications, up-to-date tables of heats and free energies of formation are needed. It is the purpose of this report to supply such tables for anhydrous silicates. During the last 15 years the heats of formation of a substantial number of anhydrous silicates have been reliably determined at or near room temperature. This resulted from the development (first by the Bureau of Mines and later by the Geophysical Laboratory of the Carnegie Institution of Washington, by the Institute of Geology of the University of Helsinki, Finland, and by the Department of Geology of the University of Chicago) of accurate solution calorimeters, employing hydrofluoric acid as the reaction medium. Specific references to work of these laboratories will be made in the next section of this report. Also, entropy data at 298.150 K. and high-temperature heat-content values are available for many of these silicates, mainly owing to work of the Bureau of Mines. Most of these entropy and heat-content data have been compiled in Bureau of Mines Bulletins (13, 15).3

Jan 1, 1962

By O. C. Blade

This report on the properties of burner-fuel oils produced during 1956 was issued under a cooperative agreement between the American Petroleum Institute and the Bureau of Mines, United States Department of the Interior, at the request of the Oil-Heat Institute of America and the petroleum industry. This survey is the second for this type of fuel, the first being made in 1955. 2/ The surveys are conducted to provide information on the characteristics of burner-fuel oils now manufactured for sale. They are similar in pattern to the diesel-fuel surveys, conducted since 1950, 3/ and are not intended to conflict with but rather to supplement them. The importance of fuel oil has resulted in the need for more information by the petroleum industry, manufacturers of heating appliances, and consumers regarding the types and qualities of the fuels currently being marketed. Samples of burner-fuel oil typical of their manufacture during the early part of 1956 were analyzed by the refiners in accordance with instructions from the subcommittee on fuel surveys of the Automotive Research Committee of the American Petroleum Institute, Results of the analyses were transmitted to the Bureau of Mines where the data were studied and compiled as shown in the tables of this report.

Jan 1, 1956

By D. A. Wilson

A cyclic leaching process was developed for selectively leaching and recovering cadmium from nickel-cadmium scrap battery waste. The six major steps in the process are the following: (1) washing the plates to remove KOH electrolyte, (2) roasting at 550° to 600° C to oxidize metallic cadmium and decompose cadmium and nickel salts, (3) leaching with an ammonium nitrate solution, (4) precipitation of the leached cadmium from solution as cadmium carbonate using CO2 gas, (5) removal of CO2 from the lixiviator by adjusting to pH 4.5, heating, and evacuating the system, and (6) removal of small amounts of leached nickel from the lixiviator using a solvent extraction technique. The regenerated lixiviator is then recycled to leach additional plates. Cadmium extraction was 94 percent and the cadmium carbonate product contained 0.14 percent nickel and 0.12 percent cobalt impurity. The leached plates were smelted to a high nickel-low iron alloy with no detectable amounts of cadmium.

Jan 1, 1971

By R. Pallini

The Franklin Research Center (FRO, a Division of The Franklin Institute was contracted by the U.S. Department of Energy to investigate the application of elastomeric materials for the purpose of smoothing loads on dragline thrust rollers. This report covers the design, fabrication, and demonstration of a portable- device for measuring roller circle track deviations and roller loadings. The results of this work are documented in this report. During December 1981, a field test group visited the Falkirk Mine, Underwood, North Dakota for the purpose of demonstrating the use of the designed and built device. The data collected indicates the practicality and usefulness of such a device for determining actual dragline roller circle roller loads, while the dragline is in service. The device was useful in determining roller load peaking that may be a contributing Factor in the premature failure of these thrust rollers. The device could be used for field evaluation of elastomeric cushioning materials used to eliminate these load peaks.

Jan 1, 1982

By H. P. Rue

The Bureau of Mines has recently collected two samples of crude oil from wells in the Greasewood Flat area of northeastern Colorado. Sample 31310 was taken from the Continental Oil Co.'s well Briggs No. 1 which care in or September 27, 1931, with a maximum production of 940 barrels per day. Sample 31311 was taken from tie Reiter-Foster Oil Co. Is well Ida Johnson No. 1 which came in on August 24, 1931 with a maximum production of approximately 1000 barrels per day.

Jan 1, 1932

By R. K. Koch

The vapor pressures of liquid titanium and liquid platinum were studied under the Bureau of Mines program for the determination of thermochemical data on the transition elements. Beating was done in a 2-kw electron-beam furnace with a water-cooled copper crucible to contain the melt. Temperature was measured with a disappearing-filament brightness pyrometer. The vapor pressure data for liquid titanium in the range 2,008° to 2,379° K are represented by the least-squares derived equation [log p (atm) = 6.268 - 22, T] Two series of determinations were made on liquid platinum. Results of the first series are expressed by the least-squares derived equation [log p (atm) = 8.240 - 30,460T] for the range 2,0860 to 2,4200 K. Results of the second series are expressed by the least-squares derived equation [log p (atm) = 7.795 - 29,580 T] in the range 2,045° to 2,442° K. Third-law evaluations of each series gave mean standard heats of sublimation of 112.4 kcal/mole, 133.3 kcal/mole, and 133.8 kcal/mole for titanium first series on platinum, and second series on platinum, respectively. Second-law heats of sublimation and equations for heats, free energies, and entropies of vaporization were obtained from sigma plots of each data set.

Jan 1, 1969

By L. A. Panek, A. J. Barry, John A. McCormick

"INTRODUCTION During recent years, roof bolting has become widely accepted as a systematic method of supporting both coal- and metal-mine roofs. Today, over 2 million roof bolts are installed monthly. Most of the information on bolt installation procedure reported to date (1,2,3,4,5,6) 3/ has been obtained by trial and error by individual groups or operators. To insure good roof control, experience and field tests have indicated that roof bolts should be installed immediately after the exposure of new roof, and they should be preloaded enough to minimize sag of the roof over the opening. The question of the proper initial preload for roof bolts is under study, although it is a general practice to impose an initial load on a bolt of approximately 10,000 pounds. This created a problem of measuring bolt loads at installations in underground mines, which was partly solved by using a commercial-type torque wrench; a device that permits a direct reading of the torque applied to the nut on a roof-bolt assembly from which the corresponding load can be determined by referring to specifications furnished by the manufacturers. However, considerable apprehension was expressed regarding the accuracy of this measuring procedure because of variations in the manufacture of roof-bolting materials and the degree of care exercised in making bolt installations. In the process of loading a bolt, only a small part of the effort is expended in producing strain in the bolt - the larger part of the effort is used in overcoming frictional effects in the nut-bolt-washer assembly. These frictional effects are subject to many factors, such as condition of threads, type of lubrication, if any, the finish on the nut and bearing plate, and the alinement of the bearing plate on the bolt. The object of this investigation was to determine the accuracy with which the load developed in a slotted-type roof bolt installed in a conventional manner in shale or sandstone roof rock can be determined from the torque applied to the nut.This report is the first of a series relating to basic research in roof bolting in underground mines. A future report will cover results obtained using expansion-type bolts under similar conditions. Other reports will consider the efficiency of bolt anchorages, the long period stability of bolts, and the design of safe and efficient roof-bolting systems."

May 1, 1953

By S. S. Dean, B. Silkes

"INTRODUCTION The metallurgical-research program of the Bureau of Mines .for the past 15 years has emphasized the production of high-purity nonferreus metals through the utilization of our available resources, ores, reducing agents, fuel, and power.Ore dressing or concentration, has always been a vitally important part of nonferrous metallurgy, and the Bureau continues to give most of its attention to it. In the field of the traditional nonferrous metals, the Bureau staff has developed natural-gas reduction of zinc, the application of glomerule technique to preparing high-grade lead concentrates for Scotch-hearth smelting, the production of electrolytic antimony from precious metal-bearing ores, and the recovery of nickel from nickel-chrome-iron ores.In the field of light metals, the Bureau staff has developed several improvements in both magnesium and aluminum production and in alloys of these metals. In the so-called ""rare-metal"" field, Bureau activities have included the production of pure ductile titanium on a larger scale than heretofore attempted, the electrolytic production of cobalt, chromium, and manganese which may now take their proper places as bases for nonferrous alloys as well -as ingredients of special steels. The Bureau staff has investigated many of these new alloys. Investigations of methods of recovering vanadium from its low-grade domestic ores have given promising results. Methods for the preparation of metallic zirconium have been improved."

May 1, 1947

The Bureau of Mines found sulfur hexafluoride (SF6), released from a lecture bottle, to be an ideal gaseous tracer for studying mine ventilation systems. Air samples were collected in glass syringes and analyzed by electron-capture gas chromatography. In these studies, the lower limit of detection was about I part per billion by volume (ppb) of SF6 per part of air. Experiments conducted in a Pennsylvania limestone mine showed this technique useful in evaluating the effectiveness of auxiliary fans, measuring low flow velocities, probing the air circulating near a working face region where ventilation appeared to be poor, and estimating volumetric flow rates in airways of large cross-sectional area and having low flow velocities. This technique was also used in a western vein-type metal mine to measure the amount of return air being recirculated into the intake air due to leakage through old stoped areas.

Jan 1, 1974

By T. A. Raczek

Materials for stronger ventilation tubing for underground use in hardrock mines were developed. The new material composites were evaluated in performance characteristics and compared to currently used materials. The materials were compared on tear, tensile, puncture and flammability properties. Based on cost versus performance data, a polyester film bonded to a polyester fabric was selected as the candidate material for field testing. Ventilation tubing fabricated from the selected material was field tested in two underground uranium mines for four-month periods. The test results indicated that the new composite showed an increase in useful life in the majority of applications, However, the cost performance ratio was not significantly improved to warrant commercialization of the product. When connected directly to some blowers, the material in close proximity to the blower deteriorated. However, material which was punctured or torn by mechanical means did not have further propagation of the tear. The high tear strength of the material prevented further damage. Improved methods of repairing inflated ventilation tubing were investigated and developed. All the repair methods were portable and self-contained. Repair kits based on adhesives, pressure sensitive tapes, and mechanical means were evaluated. Plier staplers and patch systems based on pressure sensitive adhesive proved to be most functional.

Jan 1, 1980

By Paul H. Lu

This Bureau of Mines report summarizes the analysis and eveluation of the field measurement results of a comprehensive ground control study conducted in a mechanized longwall coal mine in West Virginia. Emphasis is placed on the three basic ground control parameters: ground pressure, ground movement, and geomechanical properties. Specific topics include premining ground pressures, front-abutment pressure in the longwall panel, histories of pillar loading, differential roof-strata movement and bed separation, differential floor strata movement, entry roof-to-floor convergence, in situ moduli of rigidity of coal seam and roof and floor strata, and mechanical properties of coal and coal measures rocks.

Jan 1, 1985

By L. A. Haas

In this Bureau of Mines investigation, conditions were determined to form an iron sulfide adherent coating with a metallic golden luster on steel upon anaerobic heat treatment with sulfur. The sulfide formation rate was determined in the temperature range of 105° to 500° C with reaction times up to 68 hours. The optimum temperature and time to form an adhering decorative coating on mild steel was in the range of 105° C for about 70 hours to 285° C for 1 hour. The golden coating consisted of an inner layer of pyrrhotite and an outer layer of pyrite. At temperatures higher than about 300° C, the outer layer thickness decreased owing to the decomposition of pyrite to pyrrhotite.. Small quantities (<0.5 wt-pct) of petroleum oil accelerated the sulfide growth rate. The sulfide coating decreased the corrosion rate of steel in a neutral aqueous medium by a factor of two. The dissolution of pyrite in water was dependent on particle size and surface area with the flat pyrite coatings exhibiting the lowest dissolution rate.

Jan 1, 1974

Large quantities of combustible materials are often found in underground metal and nonmetal mines, with support timber most often the predominant combustible material. Oils, lubricants, paper, cartons, and rags are additional combustible materials and are commonly found in maintenance shop areas. Welding and cuting, shorted or overloaded electrical cables, spontaneous combustion, and careless smoking are some of the common fire ignition sources. Inexpensive, reliable fire detection and suppression systems are available to provide early warning of such fires and to isolate and extinguish fires that originate in underground maintenance shop areas. Technology developed and demonstrated under Bureau of Mines Contract H024216, Mine Shaft Fire and Smoke Protection System, may be applied to protect underground maintenance shop areas. The mine area described in this report is a representative ex-ample only; the fire protection system described considers costs, benefits, equipment performance and includes the concepts of: ? Early warning and alarm ? Isolation ? Extinguishment ? Control. Each fire protection system application requires analysis of numerous variables including total mine profile (depth, personnel, escape routes, hazards, etc.).

Jan 1, 2011

By Raymond B. Ladoo

"The name bentonite has been applied to a group or series of clay-like materials characterized by an alkaline oxide and alkaline earth content of 5 to 10 per cent, fine grain Giza, high absorptive powers, and usually very strong colloidal properties.Bentonite probably represents no mineral of fixed composition, and its physical properties vary considerably. The type material from Wyoming is light yellow or greenish yellow in color, but from other localities it may be cream colored, white, gray, pink, dark brown or even black. It is exceedingly fine grained, very plastic and highly absorbent. The appearance may be dull or powdeay, but a freshly cut surface usually has a waxy luster. Some varieties have the appearance of wax and may be cut into very thin, translucent shavings. The fracture of the type material is roughly conchoidal, that of other varieties is platey and shale-like, while still others have no typical fracture. Bentonite is highly absorbent; .hen wetted it will absorb more than three times its weight or seven times its volume of water. Some varieties when wetted with water expand to more than six times (some experimenters report eight times) their original volume. The wetted material is exceedingly smooth and soft and feels like soft soap. Unlike most clays, bentonite is easily fusible at a comparatively low temperature.Under a high-power microscope bentonite seems to consist of extremely small, more or less rounded, grains of uniform size, but the texture of most varieties is so fine that individual grains can not be distinguished.Some varieties when finely ground and thoroughly agitated with water will stay in suspension indefinitely, forming a translucent gelatinous mass. The addition of small amounts of acids or sodium chloride seems to have little or no tendency to raid coagulation or settling. Other varieties of similar analysis and appearance go into suspension more easily, but settle out again in a comparatively short time. It has been suggested that the material which stays in suspension indefinitely is a true colloid of the emulsion or lyophilic type."

Oct 1, 1921

By J. Douglas Causey

In 1988, at the request of the Bureau of Land Management, the U.S. Bureau of Mines studied part of the 12,740-acre Blue Canyon Wilderness Study Area (OR-003-073) in order to evaluate its identified mineral resources. The study area is in Malheur County, OR, about 27 miles northwest of Jordan Valley. The study area is underlain by Tertiary welded tuff, tuff, perlite and tuffaceous sedimentary rocks capped by basalt. Jasper has been mined from several localities. Some mining has been done by hobbyists. However, the area has been covered by mining claims since 1964, with mining done by commercial operators. This region has been a source of "Owyhee picture" and other similar jaspers. More recent exploration has focused on the gold potential of nearby areas such as Quartz Mountain and Red Butte.

Jan 1, 1989

This study was conducted to determine the feasibility of using large tractor dozers in land reclamation of strip-mined areas. The procedures used are patterned after engineering models developed for evaluation of military ground vehicles in cross-country operations. Tractor dozer manufacturers furnished information on capabilities of existing equipment and ideas on the practicability of using dozers larger than those currently available Generally, they believe that current dozers in the 500? to 700-horsepower range are about as large as can be built and remain economically feasible. However, one manufacturer has a wheeled dozer rated at 1200 horsepower, and another is testing a tracked dozer of about the same horse-power.

Jan 1, 1975

By Sabri Ergun

NEW theoretical data are presented for the intensity of X-rays diffracted from randomly oriented aromatic and alicyclic molecules and diamondlike structures such as are found in coals, cokes, and carbonaceous materials. Data have been computed using the Debye interference function. Computations for the smaller molecules have been made with the Univac 1204 computer: those for large structures, with either the IBM 704 or Bendix G-20 computer. A brief theoretical introduction of the Dobye interference function is given, and an outline is made of the treatment of experimental data so that the experimental interference function can be obtained.

Jan 1, 1965

By Francis Church Lincoln

"INTRODUCTION During the period from September 18 to November 27, 1944, the Bureau of Mines conducted an investigation and exploratory churn-drilling program in an area immediately north of the Crow Branch Diggings, a district lying approximately 2 1/2 miles southwest of the town of Livingston in Grant County, Wisconsin.The work was undertaken as part of a general Bureau of Mines investigation of the zinc-producing area of southwestern Wisconsin at a time when all effort was being made to increase the production of metals important to the Nation's war prrgram.Although no mining has been done in the district in recent years the Crow Branch Diggings were an important source of galena and may be found today in the dumps remaining from old surface-mining operations.The Bureau of Mines undertook an exploratory churn-drilling program on the northwestern projection of the general strike of the digging in a zone where subsurface,lead and zinc mineralization had been reported from drilling done in the early 1900's."

Feb 1, 1947