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By John Ward Smith

Methods for estimating the amounts of nahcolite, dawsonite, and the sum of these two sodium carbonate minerals from oil-yield assay data are developed and evaluated for Green River Formation oil shales from the saline section of Colorado's Piceance Creek Basin. Derived statistically, these estimation methods depend on the fact that these minerals yield water and gas measured during oil-yield assay. The estimation procedures yield values for nahcolite and nahcolite-plus-dawsonite of sufficient accuracy for stratigraphic plotting and correlation, whereas estimates for dawsonite are more generalized. However, resource estimates and reserve computations for both nahcolite and dawsonite accurate within 10 percent of the real value are readily available by summing the mineral amounts calculated by the procedures presented. These estimation procedures are applicable to oil-yield assay data on core samples from more than 30 coreholes which have penetrated the saline section of the Green River Formation in Colorado.

Jan 1, 1972

By J. G. Groetsch

Municipal solid waste (MSW) contains about 8 pct ferrous metallics which are typically recovered by magnetic separators at municipal resource recovery facilities. At present, only about 182,500 ton/yr of MSW magnetics are being processed for remelting out of the -11 MMton/yr discarded. The Sn in MSW magnetics makes this material difficult to recycle to the steel industry. An electrolytic method using stannous fluoborate-fluoboric acid for removing Sn was evaluated. Optimum concentrations of Sn in the electrolyte and the effects of impurities such as Al, Cu, Fe, and Pb on Sn recovery from the electrolyte were evaluated. Operating parameters were 60 to 65 g/L fluoboric acid and 20 to 30 g/L Sn using stainless steel electrodes at a current density of 60 A/ft2. Tests were run with postconsumer scrap4 and MSW magnetics. Good results were obtained with MSW magnetics, after pretreatment by reshredding, magnetic separation, and air classification. The final Sn content of the MSW magnetics scrap was reduced from 0.18 to 0.017 wt pct. Heat and solvent treatments of MSW magnetics to remove coatings did not significantly improve Sn removal beyond that obtained with material that had only been mechanically pretreated.

Jan 1, 1984

By Wm. W. Odell

A study of certain gas making and fuel problems peculiar to the gas industry of California has been made by the Bureau of Mines. The work was done at the request of, and in cooperation with The California Gas Research Council 2, for the purpose of obtaining basic information on the gas-making fuels available to California, and their applicability to the present and future needs of the gas industry in that State. The data obtained have been applied in outlining a construction program, and indicate the possibilities in efficiently utilizing fuels in making gas by other than the oil-gas process. This paper presents an outline of the study and a summary of the principal results obtained, with some of the more important conclusions and recommendations based on this data. Gas is produced in California by processes which are both unique and different from those common to other parts of the United States. The bulk of the manufactured gas is made in and distributed from two main districts which are centers of population - namely, the Los Angeles district and the San Francisco Bay district. The gas manufactured in the Bay district is, almost exclusively oil-gas, whereas that produced in the southern part of the State, where natural gas is available, is mostly mixed natural gas and reformed-gas, but oil-gas is the chief product when the supply of natural gas is inadequate. Practically all of the gas companies are equipped with oil-gas generating apparatus, and anticipate using it in the future. As the continued use of the oil-gas process to the exclusion of all other processes, depends upon a continued supply of oil at a low cost, and the prospect of obtaining such low-priced oil in the future is somewhat uncertain, the questions have arisen: What will the future gas-making process or processes be? When will it be necessary to make plans for the installation of different gas generating equipment, and what will that equipment comprise?

Jan 1, 1926

By D. E. Hirsch

The Bureau of Mines has developed a systematic procedure for separation, characterization, and semiquantitative analysis of high-boiling (350° to 550° C) distillates of crude oils. Isothermal and molecular distillation were used to prepare the 370° to 530° C distillate of Recluse, Wyo., crude oil. The distillate was separated into fractions by chemical treatment, silica-alumina gel adsorption, and gel permeation chromatography (GPC). The fractions were analyzed by use of GPC correlations and mass and nuclear magnetic resonance (NMR) spectrometry. The increased knowledge of petroleum composition obtained from the data will contribute to improved petroleum processing and utilization and energy conservation.

Jan 1, 1974

By Jon C. Volkwein

Advances in mining technology have enabled deeper seams of coal to be mined from the surface. Highwall mining is frequently used to mine areas at the perimeters of a surface mine when removal of the overburden becomes uneconomical or threatens environmentally sensitive surface features. At the same time, advances in materials and technology have enabled highwall mining of coal that create blind headings over 300 meters in length. Deeper surface mining and deeper highwall penetration depths have lead to more frequent encounters with methane gas. While this coal is remotely mined from the surface, underground ignitions of methane have propagated to the surface and injured miners. Methods described in this paper show how this hazard can be correctly monitored and controlled for auger type highwall mining machines. Research indicates that small quantities of gas liberated during mining migrate to the face, creating higher gas concentrations than would otherwise be expected. Using the same principles that cause the gas to migrate to the face, researchers have shown that inert gas introduced at the collar of the hole can inert the entire hole, thus ensuring safe conditions for mining.

By R. W. Watson

This Bureau of Mines report summarizes some recent results on the sensitivity of various experimental explosive systems using ammonium nitrate (AN) as the oxidizing agent. The sensitivity survey included drop-weight and friction testing and sensitivity to initiation by projectile impact and a No.8 blasting cap. It was found that certain types of AN prills can result in cap-sensitive mixtures when combined with No.2 diesel fuel (Fa); prilled AN mixed with nitromethane also result in cap-sensitive mixtures. Mixtures of AN prills and neat 1-and 2-nitropropane were not cap-sensitive, and the use of powdered or grained aluminum in AN-FO did not adversely affect the sensitivity except possibly to increase its sensitivity to friction.

Jan 1, 1974

By D. R. Mathews

The Bureau of Mines investigated the effects of tungsten and chromium, separately and combined, on improving the mechanical properties and oxidation resistance of vanadium. Binary and ternary vanadium-base alloys were prepared and tested for oxidation resistance and tensile strength. Softening occurred with less than 1 weight-percent of either tungsten or chromium, followed by strengthening with higher alloying contents. Vanadium alloys containing up to 9.8 weight-percent chromium or 14.1 weight-percent tungsten were more resistant to oxidation in air at 600° C than unalloyed vanadium. For the alloys with 12.20 weight-percent chromium or 14.56 weight-percent: tungsten, the maximum concentrations used, the lower yield strengths were about twice that of 38,600 psi for the unalloyed vanadium. Recrystallization temperatures for these alloys were 100 and 150° C higher, respectively. Alloys containing both chromium and tungsten had properties similar to those of the vanadium-tungsten alloys.

Jan 1, 1967

By F. N. Kissell

The applicability of the "direct method" for determining the methane content of virgin coalbeds was tested. Preliminary results indicate that the direct method, when applied to exploration cores, can be successfully used to estimate coalbed gas content and also approximately predict the total gas emission from a prospective mine located in the coalbed at the exploration site.

Jan 1, 1973

By D. T. Couillard

Video technology is becoming an important tool for many designers of industrial training programs. This report describes how trainers at the Minntac Mine, Mt. Iron, MN, have developed videocassettes of safe job procedures (SJP's) for training miners assigned to perform unfamiliar work tasks. All steps necessary for videocassette production, from idea to finished product, as well as the required equipment and prices, are listed and/or briefly explained. Minntac officials believe that the SJP videocassettes have contributed significantly to a reduction in mine accidents.

Jan 1, 1985

By H. E. Blake

An evaluation was made to determine the economics of utilizing waste fluosilicic acid for production of (1) calcium fluoride, and (2) anhydrous hydro-gen fluoride. Two versions of each process were considered and compared. The evaluation showed that both products could be produced and marketed competitively. Lowest estimated product sales prices required to yield a 25-percent return on investment before taxes (discounted cash flow basis) was $339.34 per ton of hydrogen fluoride and $48.64 per ton of calcium fluoride.

Jan 1, 1971

By R. A. Beall

A series of 45 zirconium ingots has been cast by the consumable electrode arc melting process with the object of analyzing the effects of power input from 50 to 230 kilowatts and reduced pressure furnace atmosphere to improve the quality of regular 8-inch-diameter production ingots made thereby. Electrode consumption rate, molten pool volume, melting efficiency, sidewall quality, arc stability, and yield efficiency are considered. The use of direct current and alternating current is studied. In conclusion, reduced pressure furnace operation is shown to promote electrical efficiency, ingot homogeneity, high metal yield, and are stability. INTRODUCTION Zirconium is a particularly difficult metal to melt because of its affinity for atmospheric gases and its solvent properties when molten. In addition, zirconium sponge as produced by the boll process contains minor amounts of magnesium chloride, which cause severe spattering luring melting, because of these difficulties with zirconium, and its sister metal titanium, near techniques have been developed to permit production of commercial size ingots. Among the more promising is the consumable electrode arc melting method.

Jan 1, 1955

By S. J. Davenport

[The tremendous increase in mine mechanization since 1929 has increased markedly the application of electric power in and about the coal mines of the United States. Cutting, drilling, and leading machines have replaced hand-mining methods in nary mines. As a result, expansion of the gathering haulage has necessitated introduction of extensive feeder, trolley, grid other power wires. (1)3/ In spite of this vast mechanization the fatality rate from electric shock has been on the decline. However, there are still too many accidents, and efforts to eliminate electrical hazards cannot be relaxed. It is hoped that an acquaintance with the physiological aspects of electrical accidents will make workers end management aware of the lurking dangers of this very common and extremely dangerous form of energy.]

Jan 1, 1951

By Nicholas Kyriazi, John P. Shubilla

The National Institute for Occupational Safety and Health, National Personal Protective Technology Laboratory, has undertaken a study to determine how well self-contained self-rescuers (SCSRs), deployed in accordance with Federal regulations (30 CFR 75.1714), hold up in the underground environment with regard to both physical damage and aging. This report presents findings regarding laboratory-tested SCSRs in the seventh phase of testing from May 1999 to August 2000. The SCSRs were tested on human subjects and on a breathing and metabolic simulator. The results indicate that most of the apparatus, if they pass their approved inspection criteria, perform satisfactorily. The deployed CSE SR-100s, however, exhibited significantly higher inhaled carbon dioxide (CO2) levels than new units, as they did in the previous two phases. Several Draeger OXY K-Pluses that rattled when shaken were found to have potassium superoxide (KO2) particles throughout the breathing circuit, including the mouthpiece. Draeger investigated the problem and developed a shake test to detect damaged units. The durations of new Ocenco M-20s were statistically significantly longer than those of deployed units, although only by 2 min.

Jan 3, 2002

By Oliver Bowles

"Rhodesian asbestos is of high quality and is much in demand by American consumers. Production in Rhodesia was first reported in 1909. The production for this and each succeeding year is shown in the following table:The serious curtailment in production for the years 1912 and 1913 was occasioned by transportation difficulties. In 1914 a railway was projected to Victoria and thereafter production increased greatly. Up to 1916 asbestos was obtained,from the Victoria district only, but thereafter the Bulwayo district became an important,producer with minor quantities from Gwelo.In the Bulawayo district the productive area is about 2 1/2 miles long, with Shebanie mine at the north-west end, the Nil Desperandum at the south end, and the Birthday claims between them."

Oct 1, 1920

By Joan T. May

Anhydrous methods were tested for the extraction of beryllium from low-grade source materials. The purpose of the investigations was to find new extraction processes that are applicable to domestic ores. Beryl, helvite, and phenacite materials containing from 0.1 to 2.8 percent BeO were used as starting materials for direct halogenation tests and pretreatment followed by halogenation. The results of the investigations showed that direct fluorination and carbide-chlorination are two practicable methods that can be applied to low-grade concentrates. Treatment of concentrate-carbon mixtures with anhydrous hydrogen fluoride extracted 99 percent of the beryllium in the concentrate; the soluble fluoride product, converted to an oxide, contained 70 percent BeO. Chlorination of beryllium-silicon carbide, prepared from low-grade concentrates, extracted beryllium into the volatile chloride product.

Jan 1, 1962

By Lippe D. Sadwin

A high-speed streak camera method for making equation of state measurements (shock and particle velocities) on samples of rock under dynamic load conditions is described. Experimental data are given for tests on 12 samples representing 5 rock types. Analysis of these data shows that the method is practical and that good reproducibility of results can be obtained. The pressure range covered in the tests was from 1 to 50 kilobars.

Jan 1, 1966

Multiple-seam interactions are a major ground control hazard in many U.S. underground coal mines. In some U.S. coalfields, particularly in central Appalachia and the West, the majority of today’s mines are operating above and/or beneath previously mined seams. The effects of multiple-seam interactions can include roof falls, rib spalling, and floor heave. These can seriously disrupt mining operations and threaten the safety of miners. In early 2006, a West Virginia coal miner was killed by rib roll that occurred in a high-stress zone beneath a remnant structure in an overlying mine. Fortunately, not every multiple-seam situation results in hazardous conditions. Indeed, the vast majority do not. For the past several years, the National Institute for Occupational Safety and Health has been conducting research to develop better techniques for predicting the location and severity of multiple-seam interactions. During this investigation, more than 50 mines were visited across the U.S. coalfields. Nearly 300 case histories were collected and analyzed using multivariate statistical techniques. The study also employed the numerical model LaM2D to estimate the multiple-seam stress, the Analysis of Longwall Pillar Stability (ALPS) and the Analysis of Retreat Mining Pillar Stability (ARMPS) programs to determine pillar stability factors (SFs), and the Coal Mine Roof Rating to measure roof quality. The study focused on the two most common types of multiple-seam interactions: • Undermining, where stress concentrations caused by previous full extraction in an overlying seam is the main concern; and • Overmining, where previous full extraction in an underlying seam can result in stress concentrations and rock damage from subsidence. The study confirmed that overmining is much more difficult than undermining, and isolated remnant pillars cause more problems than gob-solid boundaries. For the first time, however, it was possible to quantify these effects in terms of the equivalent thickness of interburden needed to compensate for them. The study also found that pillar design is a critical component of multiple-seam mine planning. Many of the failed cases involved pillars whose SF seemed inadequate once the multiple-seam stresses were accounted for. Weaker roof was also found to significantly increase the risk of multiple-seam interactions. The most important result of the study is an equation that predicts the critical thickness of the interburden required to minimize the likelihood of a multiple-seam interaction. This equation was incorporated into a step-by-step methodology that allows mine planners to evaluate each potential interaction and take steps to reduce the risk of ground control failure. Such measures could include installing cable bolts or other supplemental support, increasing the pillar size, or changing the mine layout to avoid the remnant structure entirely. These Proceedings also contain several previously published papers that cover other facets of multiple-seam mining research. Two papers describe the LaModel family of software developed by Professor Keith A. Heasley of West Virginia University. The LaModel programs were designed for calculating the stresses and displacements in coal mines or other thin, tabular seams in layered media. The original three-dimensional version of LaModel is essential for detailed analyses of complex multiple-seam scenarios. LaM2D, by contrast, implements a simplified two-dimensional model that is suitable for quick approximations of the multiple-seam stresses and strains. Three additional papers in these Proceedings describe the extensive multiple-seam experience of the Harris Mine, examples of extreme multiple-seam mining from the central Appalachian coalfields, and longwall mine experiences in Pennsylvania, West Virginia, and Utah. The final paper reports on a numerical modeling study that provided some insight into the mechanics of multiple-seam mining.

Jan 5, 2007

By L. C. IlsLey

As part of its work for the improvement of safety conditions in mines , the Bureau of Mines has undertaken to establish a list of permissible storage - battery locomotives for use in gaseous mines , and , to this end , has issued Schedule 15 , "Procedure for Establishing a List of Permissible Storage -Battery Locomotives for Use in Gaseous Mines . " Up to the present time , two approvals * have been issued under this Schedule , and considerable testing work done on four other applications which have been made for approval . Prior to the publication of Schedule 15 , the Bureau conducted both field and laboratory investigations to determine the hazard from the batteries used in mine locomotives . ** These investigations indicated that the safety of the locomotive would depend largely on proper care of the battery , also on the use of a battery as mechanically rugged as possible . For this reason the Bureau staff , in testing locomotives submitted for approval , considered it advisable to subject the batteries to a jarring or bumping test to prove their adequacy as regards mechanical endurance and ruggedness . These tests on the batteries of the locomotives are described below.

May 1, 1922

Control the release of ground-water into active underground coal workings by short-term pumping from dewatering wells sited on fractures. Approach The sudden release of fracture-stored groundwater into underground coal workings often occurs when mine workings are developed beneath fracture valleys, Pumping from fracture trace-sited dewatering wells, prior to development of the underlying workings, can be an efficient means of intercepting fracture-stored groundwater before it is released into the mine. Dewatering operations are discontinued once the underlying mine workings have been fully developed, and the maximum possible reduction in fracture storage has been achieved through pumping. How It Works An aerial photographic technique known as fracture trace analysis is used to site dewatering wells on rock fractures in a valley bottom. Downhole caliper and temperature logs are used to assess the fracture flow potential of each dewatering well drilled.

Jan 1, 1987

By J. W. Holcomb

Many mines are opened into the coal beds by shafts; and, at some of these operations, the same cages or skips that are used for hoisting coal also are used for transporting men into and out of the mines. At some mines, separate man-and-material shafts are maintained, and the cages in these are utilized for transporting men and supplies only. In most instances, these cages are operated either singly or in pairs by a hoisting engine installed in a building near the shaft. Single ropes from the tops of the cages pass over bull wheels on the head frame to either electrically or steam-driven hoisting engines that require engineers to operate them. There are records of several instances where hoisting engineers have become incapacitated suddenly while hoisting men, and the passengers on the cages were killed or injured. Where the same cages are used for hoisting cars of coal and for lowering and hoisting men, especially where self-dumping cages or skips are used, safety pre¬cautions must be taken, such as providing steel bonnets for the cage deck, enclosed sides, adequate handholds, gates for closing the end openings, safety catches, and locking devices to prevent accidental dumping. Some of the newer hoisting installations are of the elevator type; where an operator rides in the cage in the same manner as an elevator operator in a building. These cages have single or multiple decks and are primarily for transporting men; but, in some instances, supplies also are transported. They are a great improvement over the installations where the same cages are used for hoisting cars of coal and transporting men.

Jan 1, 1952