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By John E. Pahlman

The Bureau of Mines has conducted research on a dual leaching method that offers the potential for the economic recovery of the silver, as well as of the manganese, contained in some domestic manganiferous silver deposits. The method consists of an initial leach of manganese with aqueous sulfur dioxide (S02) followed first by a neutralization rinse, and then by a second leach with cyanide solution for the extraction of silver. Refractory silver in these ores was either (1) intimately associated with the manganese, (2) chemically resistant to cyanide leaching, or (3) rendered inaccessible to cyanide leach solution by the surrounding manganese mineralization. Less than 10 pct of the silver was extracted when minus 2.5-plus 1.3-cm ore pieces were leached directly with cyanide. However, extractions of 25 to 82 pct of the silver and 65 to 96 pet of the manganese were attained in laboratory column-leach tests using the dual leaching method on equivalent-sized ore pieces from seven domestic deposits.

Jan 1, 1987

By S. H. Ash

As part of the work done at the Washington coal mines during the year 1929 , a study was made of the safety practices in and about the mines . Inasmuch as electrical blasting has made considerable headway it is interesting to note the manner in which it is done and the reasons why it was discarded at some of the mines . Blasting is done at the mines in the State by means of capped fuse , electric blasting " caps , " and in some instances by electric delay detonators . Black blasting powder with fuse is used at most of the open- light mines . The use of squibs was discontinued several years ago because the coal operators , without exception , recognized the dangers incidental to their use . Permissible explosive and dynamite are also used at some of the open- light mines . With the exception of some rock work and the driving of level work in gangways and air courses the explosive is detonated by means of capped fuse .

Apr 1, 1930

By J. B. Janus

This report continues a series of analyses of coal samples made by the Bureau of Mines in connection with the yearly purchase of several million tons of coal for various Government agencies. Listed are the analytical data on the composition and quality of tipple and de livered samples of coal collected during fiscal year 1974.

Jan 1, 1975

By Ani Chitaley

A new method has been developed for handling supplies in underground bituminous coal mines. A survey indicates industry wide implementation potential for the proposed method. Reduction of supply handling accidents' by as much as 73% and improvements in the productivity of face operations by at least 3% are anticipated benefits. The new method is based on the palletization of daily supplies and the use of a forklift for carrying out the handling tasks at the underground section. A prototype of the forklift has been delivered to the U.S. Bureau of Mines. The forklift has demonstrated several important features necessary for underground supply handling such as compactness, maneuverability, visibility, ease of control and auxiliary attachments for hoisting, carrying timber and pulling. Design improvements are recommended for future generation underground forklifts. These relate to higher speed, increased battery duty cycle, higher payload and modified traction/steering to eliminate plowing of soft mine floors.

Jan 1, 1983

By E. J. Kloos

Bureau of Mines-approved self-contained breathing apparatus of the compressed air demand type were evaluated for performance at low temperature. Apparatus durations, breathing resistances, and airflow rates were measured on machine tests at room temperature and -25° F. Man tests under actual wearing conditions verified the machine test results. Many serious functional changes in apparatus performance occurred at low temperature. Pressure regulators malfunctioned when diaphragms lost flexibility. Under certain conditions frozen condensed moisture sealed exhalation valves and fogged eyepieces. High-pressure leaks, not encountered at ordinary temperature, developed at low temperature. Tests results are discussed generally and specifically for each apparatus. Recommendations are given to obtain optimum performance from demand type breathing apparatus at low temperatures.

Jan 1, 1968

By Steven A. Fechner

In 1984 the Bureau of Mines cunducted mineral investigations of specific sites within the Yentna Mining District. One hundred eight placer and rock samples were taken. Reconnaissance placer samples were collected from drainages in the Talkeetna, Susitna, and Yentna River basins. The highest placer gold values were found in the historic placer gold producing creeks of the Cache-Peters Creek area. Samples taken from an outcrop in the Middle Fork of Iron Creek in the Talkeetna Mountains contained previously unreported high lead, zinc, and silver values.

Jan 1, 2011

By John Nagy, Austin R. Cooper

Information is presented on the pressure and rate of pressure development during a dust explosion . The data were obtained in laboratory studies in a 75- cubic inch vessel with mineral , agricultural and chemical dusts . The factors investigated include dust concentration , oxygen concentration of the atmosphere , admixed inert powder , and admixed moisture . Information is given also on the effects of these factors on the composition of the atmosphere after the explosion .

Jan 1, 1964

By H. P. Hermance

The Ely mine, which at one time was the largest producer of copper in the United States, has been idle for the past 30 years. A remarkably continuous ore shoot probably averaging 100 feet wide and 19 feet thick was mined on about a 25° slope for 3,400 feet on the incline. The ore was massive sulfides containing chalcopyrite, pyrrhotite, pyrite, and sphalerite. The estimated production of the Ely mine is 400,000 tons of ore averaging 3.3 percent copper. Because of the critical position of copper during the recent war, a search for extensions and recurrences of parallel ore shoots at the Ely deposit seemed warranted. The Bureau of Mines surveyed selected areas by geophysical methods, diamond-drilled nine holes, and sampled mine dumps during its investigations, which began in 1942 and terminated in 1946. The diamond drilling totaled 5,229 feet. The logs of the holes include chemical analyses of mineralized sections.

Jan 1, 1949

By M. K. Larson, J. K. Whyatt, F. M. Jenkins

The U.S. Bureau of Mines conducted an overcore stress measurement on the 5300 level of the Lucky Friday Mine, Mullan, ID, to investigate the stress regime around an experimental stope in a rock-burst-prone mine. The result indicated a stress field with unexpected magnitude and orientation [F . 135 MPa (19,600 psi) oriented S 80E1W]. An unusual amount of rock-burst activity was encountered during subsequent excavation. A careful review of the overcore data suggested the overcore strain measurements were valid. Moreover, concentrated rock-burst activity suggested that the measured stress field did exist, but was localized and therefore did not represent the far-field in situ stress field.

Jan 1, 1995

By L. B. Pankratz

The heat contents of the sesquioxides of erbium, holmium, thulium, and ytterbium (Er203, Ho203, Tm203, and Yb203) in the cubic crystalline form were measured over the temperature range from 298° to 1,800° K. The erbium and holmium sesquioxides gave regular heat content-temperature curves. Thulium sesquioxide had a minor thermal anomaly near 1,680° K, with a heat absorption of 310 cal/mole; similarly, ytterbium sesquioxide had a minor anomaly near 1,365° K, with a heat absorption of 150 cal/mole. The heat content results are presented in both tabular form (at 100° intervals) and in algebraic form. Entropy increments, corresponding to the tabulated heat content results, also are listed.

Jan 1, 1963

By Herbert R. Appell

Urban refuse, cellulosic wastes, and sewage sludge have been converted to heavy oil by heating under pressure with carbon monoxide and steam. Conversions of the organic matter to oil, water, and gas have averaged near 90 percent at temperatures of 250° to 400° C and pressures of 1,500 to 5,000 psi. The yield of oil, based on the dry organic matter of the waste materials, is usually near 40 percent. This is the equivalent of more than 2 barrels of oil per ton of dry, ash-free waste material. The oil from urban refuse and cellulosic wastes has a sulfur content near 0.1 percent. This low sulfur content makes the oil from refuse a desirable source of fuel oil.

Jan 1, 1970

By Ludwig Schmidt

Investigations conducted by the Bureau of Dines pertaining to the reduction of evaporation losses of petroleum have shown that such losses may be reduced 70 to 80 per cent by the use of vapor-tight tanks equipped with vacuum and pressure relief valves, and vapor-tight thief hitches. Additional studies have shown that it is often economical to supplement this type of construction with other measures that will reduce evaporation losses still further. Water-cooling systems, insulation, and light colored paints are the measures most often used in connection with vapor-tight tanks. Painting with light colored paints probably is employed in the greater number of cases. On account of the cost of insulation, or of installing water cooling systems, the use of these methods are restricted to tanks containing gasoline or crude petroleum with a very large content of low-boiling fractions. The effect of cooling systems has been discussed in a previous report.2 In choosing paints for tanks many factors must be considered. Probably the three most important are cost, protective value, and color. Many companies have adopted a standard color for all of their tanks in this way they reduce the initial cost of paint by buying in large quantities. The tank farms of such companies usually have a neat appearance, resulting from the uniform painting of all tanks. This procedure also has advertising value. Unfortunately, most of the paints used to protect steel are of the darker colors, usually red or black. These colors accelerate the rate of evaporation. Several companies have solved this difficulty by using a dark colored metal-protective paint as a primer coat, and a paint of any desired color for the final coat. Special metal-protective primers to be used under light-colored cover coats have been placed on the market by several paint manufacturing companies.

Jan 1, 1925

By Jan M. Mutmansky, Christopher J. Rise

"One of the most serious long term health problems associated with underground,mining is Coal Workers Pneumoconiosis (CWI'), more commonly known as Black Lung Disease. It occurs in some coal workers, normally after 15 or more years of exposure to coal mine dust, and leads to a variety of respiratory problems. Two types of pneumoconiosis are recognized simple CWP, which has been estimated to affect 6.9 percent of miners and is a condition that does not impair the miner's ability to work nor reduce life expectancy; and a more severe form of black lung (called progressive massive fibrosis) that occurs in about one percent of the cases and results in severe lung damage.Although the relationship between coal dust and CWP has long been recognized, detailed knowledge of the relationship is insufficient for setting up authoritative guidelines to reduce the health risks for those employed in dusty,underground environments. CWP is not only a health problem for workers that causes considerable distress, it is also a very expensive problem the total annual costs associated with CWP approach two billion dollars.As part of its efforts to combat CWP, the U.S. Bureau of Mines in 1983 established a Generic Mineral Technology Center to carry out basic research into all aspects of respirable coal dust:— control of dust generation — the behavior of dust in the mine — characterization of dust particles interaction of dust and lung— the relationships among dust generation and mobility and the mine environment, geology, and seam characteristics,Penn State, West Virginia University, the University of Minnesota, and the Massachusetts Institute of Technology are involved in this research, which is administered from the Department of Mineral Engineering at Penn State.Our work is one of the seven projects to be conducted at Penn Slate. We are concerned particularly with the characterization of dust and its relationships with the mine environment, and our main goal is to establish standard procedures for describing and measuring these variables.Coal DustCoal dust is a very complex material that varies greatly in chemical and mineralogical properties. Moreover, it is not the only constituent of respirable dust in the mine. When a coal seam is mined, it is inevitable that rock particles other than coal are included in the material. This rock comes from the mine roof, the floor, and the partings and inclusions within the coal scams. Since the roof and floor strata, the partings and inclusions are often stronger than the coal, mining them frequently causes more dust than mining the coal itself. One of the objectives of our research is to find the relationships between a specific coal's characteristics before it is mined and the respirable dust characteristics after it is mined. We are particularly interested in the size distribution of particles, the chemical properties, and the mineralogical properties."

Jun 1, 1988

By R. R. Wells

An important activity of the Bureau of Mines is the continual search for new sources of minerals. As a part of the investigation of strategic mineral deposits in the United States, samples of mercury ores were submitted to the Ore Dressing sections of the Salt Lake City and Albany stations for metallurgical testing. This paper gives data summarizing the results obtained from laboratory beneficiation studies of mercury ore samples submitted during the period 1941 to 1947. Ores tested included three from Jackson County, Oreg., one from Valley County, Idaho, one from Storey County, Nev., and one from Sonoma County, Calif. In general, the ores from Oregon were not amenable to concentration by flotation because of intimate association of cinnabar with other minerals or because of extremely low grade. One Oregon ore was amenable to direct distillation provided lime was added to reduce corrosion of the retort.

Jan 1, 1950

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Jan 1, 2012

By C. W. Vierrether

Tailings from the Pea Ridge iron mine contain significant amounts of apatite, which has rare-earth element values associated with it. In association with the recovery of rare-earth minerals as a secondary resource, the U.S. Bureau of Mines conducted an investigation on the recover ability of the rare-earth minerals from these tailings. The mill tailings were subjected to a phosphate flotation to separate the apatite from other constituents. More than 70-pct recovery of the rare-earth values was achieved. Based on mineralogical characterization and prior analysis of rare-earth-bearing breccia pipe material at Pea Ridge, it is proposed that processing this phosphate concentrate on a vanner table would yield up to a 95-pct recovery of the rare earths in the concentrate, with the apatite reporting to the tailings. Intensive ore microscopy studies of the original tailings to the flotation products led to the identification of monazite, xenotime, and rare-earth-enriched apatite as the major rare-earth-bearing minerals in the tailings.

Jan 1, 2010

By H. R. Babitzke

The purpose of this Bureau of Mine- investigation was to develop columbium and tantalum alloys suitable or u at elevated temperatures. Columbium and tantalum were combined with tungsten, hafnium, zirconium, molybdenum, vanadium, and titanium, and the resulting alloys were evaluated with respect to workability, hardness, electrical resistivity, strength at elevated temperatures, oxidation resistance, and weldability. Cb-33Hf-10W-10Ti, Cb-20111-5Mo, and Cb-30Hf-5Mo exhibited superior high temperature properties. Cb-33Hf-10W-10Ti had tensile strength values of 44,300 psi at 1,200° C and 16,500 psi at 1,400° C, Cb-20Hf-5Mo had values of 35,700 and 20,700 psi, respectively. The corresponding values for Cb-30Hf-5Mo were 38,900 and 17,800 psi. These alloys are fabricable by conventional methods with excellent strength at temperatures up to and including 1,400° C. An oxidation rate of 7 to 21 mg/cm2/hr was observed up to 1,000° C.

Jan 1, 1967

By F. W. Lane

Some months ago the Bureau of Mines began research of a fundamental character on sulphur in petroleum. In the course of this work, the usual qualitative test for sulphur in organic compounds1 was applied to certain oils that were believed to contain approximately 0.5 percent sulphur. No sulphur was found, and, as a check on the qualitative test, the oils were subjected to quantitative determination of this element by the oxygen-bomb method.2 The sulphur content of the oils ranged from 0.10 per cent to 0.50 per cent. This experience led to further trial of the qualitative test for organic sulphur, both on the oils mentioned above, and on common sulphur-containing organic substances. No difficulty was experienced in detecting the element in the latter, but with the petroleum oils the test, as usually performed, could not be relied upon to detect less than 0.60 per cent of sulphur consistently. The use of mechanically polished pure sheet copper for the detection of free sulphur, hydrogen sulphide, and perhaps other sulphur compounds has been recommended.3

Jan 1, 1927

By C. J. Chindgren

Two air classification systems were built and tested as separatory devices for recovering the nonferrous metal values from shredded automotive nonmagnetic reject scrap. A horizontal air system with a capacity up to 16 tons per hour was used to obtain preliminary separations, and a smaller capacity vertical system was used as a cleaning device. Shredded automobile reject material containing aluminum, copper, and zinc values of about $55 per ton were air-classified in the horizontal elutriator. Ninety-six percent of the metal was recovered in a 74-percent metal concentrate. Tandem operation of both classifiers recovered 92 percent of the metal in an 80-percent concentrate while rejecting 87 percent of the nonmetallics. Heavy media separation of the air-classified concentrate produced an overall recovery of 91 percent of the metal in the form of a 99-percent metal concentrate.

Jan 1, 1971

By Murray Weintraub

The Bureau of Mines investigated the aerodynamic factors that control the functioning of the blowcase devices used in pneumatic processes for dispersing solids. Alumina powder of 8-micron mass-mean diameter was placed in 0.75- inch-diameter by 10-inch-long cylinders} and a blowcase technique was employed. It was determined that dimensions and gas rates for discharging the powder from the cylinder by a stream of gas may be calculated by assuming a fluidization mechanism and extrapolating residues to a desired finite quantity or to zero at the terminal velocity. The state of agglomeration of a powder at discharge may be determined from measurements of the velocity required for zero residue.

Jan 1, 1967