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By Jacques Eksteen, Sharif Jahanshahi, Neill J. Bartie, Shouyi Sun

The gradual increase in Cr2O3 levels of UG-2 ores has become a matter of concern for platinum producers in South Africa due to the formation of chromite spinels in melters. The effect of bulk FeOx/MgO ratio, Cr2O3, temperature and oxygen partial pressure on phase stability and composition in the system FeOx-MgO-SiO2-Cr2O3-Al2O3-CaO has been studied between 1400°C and 1600°C using the drop-quench technique. An increase in temperature was found to result in a decrease in [Fe/Cr]spinel. This effect is shown in Figure 1 for the six slag compositions investigated.

Jan 1, 2003

By Yimin Zhu, Dezhou Wei, Haijun Liang, Zhifu Zhou

Pyrite is one of sulfide minerals most widely distributed in the earth. During the flotating separation of metal sulfide and the floating desulfation of coal, it is often requaired to restrain pyrite. However, the result is not very satisfactory because of the little difference of floatability of minerals to be separated. The problem is extremely outstanding for the floating desulfation of coal. Researchers carried out a number of experiments with T. ferrooxidans (Yang et al, 2001; Zhou et al, 2000; Zhou et al, 2001; Wei et al, 2001) for an enhanced restraint to pyrite. The results showed that the T. ferrooxidans after being cultured works the best in restraining pyrite. After 10 min pretreatment, the removal rate of pyrite from coal is up to 80%~90%. The research results by Yuan Xin et al (Yuan et al, 2000) show that T. ferrooxidans can restrain effectively the floatability of pyrite and can reduce the recovery of pyrite from 95% to 8%. Though the restraining properties of T. ferrooxidans to pyrite have been proved by many tests and experiments, there are very limited reports on its restraining mechanism. Thus, a systematic experimental research is carried out in this paper.

Jan 1, 2003

By K. C. Corin

It is well known that the grinding circuit plays a crucial role in flotation. The effect of pulp chemistry during grinding is often overlooked. It is believed that the surface properties of the minerals can be adjusted during flotation rather than during grinding. However, recent development in surface analysis techniques (TOF-SIMS, XPS, and AES etc.) have proven that the hydrophilic iron hydroxides formed at the mineral surface during grinding make it difficult for collector adsorption, which may result in poor grades and recoveries of the valuable minerals. This study investigated the effect of the pulp chemistry conditions during milling and the subsequent effects on flotation performance of an Nkomati ore. The results have shown that there was approximately 10 % increase in Ni recovery, when the ore was ground at a dissolved oxygen (DO) concentration of 0 ppm (DO-0) in comparison to no gas control during the grinding stage. However, when the pH was changed from 9 to 11, no gas control resulted in a 20 % decrease in the Ni recovery compared to only 5 % decrease in the Ni recovery at DO-0. A noteworthy observation is that controlling a combination of DO and pH during grinding is of critical importance for better floatability and selectivity for such a system. It also became clear from this study that the presence of oxygen is critical to the consumption of xanthate, which is consistent with the general literature. It has been established that grinding at lower DO levels/redox potentials (Eh) in the presence of xanthate significantly improves the flotation performance of the valuable minerals.

Sep 1, 2012

By Alejandro Rubio-Lopetegui, Gonzalo Montes-Atenas

The occurrence of Enargite (Cu3AsS4) in hydrometallurgical plants bears a number of challenges. One question lies on how Copper and Arsenic can be selectively extracted from the solid surface structure when immersed in aqueous solution. The leaching of Enargite in ambient conditions has been extensively studied; nevertheless, challenges regarding the process kinetics and surface structures enabling the extraction process remain ill-understood. Prior knowledge indicates that different conditions of pH, Eh, temperature, speciation of the aqueous phase or variations of these parameters defines the overall rate at which metals and other elements will be transferred to the solution. One aspect that the research studies have seldom addressed involves studying the main features of the surface structures formed during the leaching process at the outmost surface atomic layer. Such structures will mediate between the solid bulk and the solution to undertake subsequent stages of leaching process. The aim of this research work is to critically analyze the state of the art of Enargite electrochemistry from the mediator formation-dissolution mechanisms standpoint occurring at the mineral-solution interface. The most probable mediator species reported in the literature were found to be: Arsenolite and Sulfur (acidic media), Covellite (acidic and alkaline media) and Tenorite (alkaline media). As a result of this analysis, it was observed that the surface speciation was not in full agreement with the previous knowledge suggested to explain Enargite leaching reactions and, therefore, modified Eh-pH diagrams are presented. The acquired insights on the surface structures rising from the Enargite-aqueous solution interactions is further revised to provide new experimental protocols towards selectively separating Copper and Arsenic through hydrometallurgical paths.

Jan 1, 2014

By Xingshi Yang, Ghislain Bournival, Seher Ata

"Particle-laden interfaces are a fundamental research topic in froth flotation since the process involves particle-coated bubbles in both the pulp and the froth phase. In most experimental studies the characteristics of the particle layer in multi-bubble systems are poorly defined. An experimental setup has been developed based on a Langmuir-Blodgett (L-B) trough. The modified trough allowed introducing an air bubble beneath the particle monolayer formed at the air-water interface which made the study of the interaction between the bubble and the monolayer under various pH values possible. The monolayer characteristics of the particles were also studied and compared in terms of surface pressure (?-A) isotherms and packing factor. On compression, the particles formed branched structure at high pH whereas a uniform monolayer was formed at lower pH. Observations related to the behavior of particles during compression and expansion cycles, and the coalescence of a bare bubble with the flat particle laden interface were provided and the implication of the results for flotation process was discussed.INTRODUCTIONFroth flotation is known for its versatility and ability to concentrate low-grade, complex ores. It is considered a physico-chemical process in which particles attach to air bubbles, depending on their hydrophobicity as well as other factors, and are carried to the surface to form a froth layer. Reagents are used to stabilize bubbles and the froth layer (Pugh, 1996). However, particles, which are carried by the bubbles or entrained, significantly contribute to the stability of the froth phase (Ata et al., 2003; Zanin et al., 2009; Bournival et al., 2015a). Their relevance in mineral processing has led to a number of fundamental studies on the effect of particles and their properties on the process of froth flotation.Flotation systems are particularly difficult to characterize due to the broad range of properties of particles (e.g. size, liberation, hydrophobicity, etc.) and inconsistent operational conditions (e.g. changes in water quality, reagent addition, etc.). Several studies have made the use of well characterized particles in laboratory conditions. Such studies allowed the finding of an optimal contact angle for the stabilization of the froth phase (Johansson and Pugh, 1992; Ata et al., 2002). Froths have a large number of bubbles so that individual interactions are not observed. The study of two bubbles allows to determine the stability of the bubbles, with particles, and to some extend the stability of the bubble-particle aggregate (Gourram-Badri et al., 1997; Bournival et al., 2015b). The removing of particles between two bubbles may also be studied from a Scheludko cell (Johansson and Pugh, 1992) or by observing a bubble with a flat interface (Sethumadhavan et al., 2002). However, these systems provide limited information on the arrangement of the particles."

Jan 1, 2018

By P. C. Beuria

Iron ore concentrate contains different mineral phases viz. hematite, magnetite, goethite, kaolinite, and gibbsite. Presence of some of these phases like goethite, kaolinite, and gibbsite contribute to the loss on ignition (LOI) content of the sample. Iron ore fines (pellet feed) are pelletized for utilization in DRI & BF processes. In the present pelletization technology i.e., straight grate and grate kiln processes, the LOI in the ore should be within the range of 2.0-2.5%. LOI content in the iron ore concentrate is found to be more than 4% after beneficiation of low-grade iron ore. It is therefore difficult to produce good quality pellet because of high LOI content. The LOI content of the sample is a detrimental factor in the pellet making. For effective pelletization, the LOI content in iron ore fines needs to be reduced before pelletization. It can be reduced by fluidized bed roasting. The objective of present work is to understand the kinetics of removal of LOI from iron ore fines. The effects of bed depth, temperature, and residence time on reduction of LOI content in iron ore fines were studied using muffle furnace. The process of roasting was carried out at four different temperatures varying from 400 to 950 °C with a variable residence time of 30, 45, 60 & 75 minutes and at bed depths of 16, 32, 48 & 64 mm. In all instance of experiments carried out, one of the parameters was kept constant. It was observed that at 850 °C and 30 minutes of residence time, there was sufficient removal of LOI in static bed condition even at a high bed depth of 64 mm. Keywords: LOI, pellet feed, fluidized bed roasting, goethite

Sep 1, 2012

By Kazutoshi Haga, Atsushi Shibayama, Altansukh Batnasan

The objectives of this study were to propose a viable alternative method for recovery of precious metals such as gold (Au), silver (Ag) and palladium (Pd) from waste printed circuit boards (WPCBs) and to regenerate the spent lixiviant solution for reuse. The proposed method generally consists of several steps as follows: 1). iodine-iodide leaching for metals extraction; 2). separation and recovery of precious metals and metal impurities from a pregnant leach solution; 3). regeneration of the spent iodine-iodide solution/lixiviant. In this method, more than 99% of Au leaching was achieved in the iodine-iodide solution from the solid residue of WPCBs that was obtained via sequential processes including incineration at 800 ?C and high pressure oxidative leaching with a diluted sulfuric acid at 120 ?C, while the leaching of Ag and Pd was less than 1%, respectively. Besides Ca, Cu, Ni, Co and Zn as main metal impurities, leaching efficiency of other metals did not exceed 1%. The precious metals and base metals as metal impurities present in the pregnant leach solution were separated and recovered by precipitation using L-AA and NaOH solutions. About 99.8% Au, 81.7% Ag and 72.8% Pd were recovered from the pregnant solution at pH of 2 with the addition of 0.1 M L-AA as precipitating agent. The remained small amounts of precious metals and metal impurities were precipitated at pH 13 using 1 M NaOH. The spent lixiviant after sequential precipitation was regenerated in the presence of hydrogen peroxide, hydrochloric acid and potassium iodide. It was revealed that over 90% of gold could be extracted from the residue of WPCBs with the regenerated lixiviant solution.

Jan 1, 2018

By S. Banisi, E. Arghavani, Gh. Parsapour, S. Mousavi

Maximization of water recovery in thickeners is an essential step in the mineral processing industries. The Gol-E-Gohar iorn ore processing plant uses a center pier thickener with a diameter of 38 m and depth of 4 m. The feed rate is 50 t/h solids with a concentration of 5% (w/w), and it has been designed to provide an underflow containing 50% solids. The performance of the thickener was not as expected judged by the overflow stream containing 0.6% solids and water loss of 52 m3/h in the underflow. A criterion called the index of flocculation incorporating the perimeter-based fractal dimension of flocs, floc size, and settling velocities was proposed and used to determine the optimum flocculant dosage which was found to be 20 g/t. The fractal dimension of flocs in a pulp containing 5% solids was found to be between 1.16 (no flocculant) and 1.56 (40 g/t flocculant) which indicated highly branched and loosely bound structures for the flocs as flocculant dosage increased. At these conditions, the size of the flocs which was recorded by a digital microscope increased from 93 µm to 403 µm. A new feedwell with a special design with the aim of preventing flocs breakage and maximizing energy dissipation of pulp was constructed and installed. These modifications led to an increase in the thickener drivehead torque from 5% to 18% of the rated torque, indicating a higher bed depth. Finally, installation of a PID controller reduced the drivehead torque relative oscillation from 52.0% to 12.7%. These changes increased the solids concentration of the underflow from 49.0% to 56.9%, decreased the overflow solids concentration from 0.6 % to values smaller than 0.01% and resulted in a reduction of 27% in water loss in the thickener underflow.

Jan 1, 2014

By N. I. Tyushkova

On the basis of detailed studying of mineral structure of ore and treatment products it is established that the given ore refers to oxidized Pb-Zn vein-disseminated ores. Technological special features of the basic ore minerals and the reasons causing their obstinateness that is defined by following features are revealed, presence at dominating quantity difficult to float lead minerals: mimetesite (9.67%), green lead ore(0.48%); non float: bindheimite (2.16%) and plumbojarosite (0.36%) and high assay of oxides and hydrous ferric oxides; also thin, emulsive and submicroscopic segregations of the defined minerals in swamp ore. As a result of researches the scheme of gravitational-flotation treatment was conducted in semi-industrial scale. It allows to receive two concentrates from ore: a lead gravitational concentrate of mark ??-4 with the assay of 55.5 % of Pb and 0.77 % of Zn; and a Pb concentrate of mark ??-7 with assay of Pb of 40.97 % and Zn of 1.39 %. The total assay of Pb in concentrates makes 81 %. The efficiency offered by gravitational-flotation schemes is defined by possibility for recovery of big impregnated lead minerals under gravitation. The use of this method of gravitation has allowed to recover such mineral as beudantide and to exclude irrevocable losses of lead in tails which are connected with this mineral. Scientific value of the presented researches is connected with the fact the problem of extraction of the oxidized minerals of Bb and Zn is rather difficult and insufficiently studied. Keywords: flotation, oxidized forms of Pb and Zn

Sep 1, 2012

By Lj. D. Andric

By the micronization-milling of the material, the size and the structure of its particles are changed and it comes to the increasing of the potential energy of the system as well as to the chem-ical activity of the material what is the result of an increased free surface and of the concentration of the grate defects, that is of the internal energy of the system. All these changes that are reached, show that new characteristics of treated materials are got by micronization process. Controlling the process of the micronization and by purpose directing of the new characteristics of the activated materials, we can have the positive effects and use them in more technologies. Talc is important nonmetallic mineral raw material that is widely used as either the basic raw material, or as filler. This has stimulated its technological investigation, as well as the investigation of its physical-chemical characteristics. In this paper are shown experimentally reached results of the physical-chemical characteristics of the talc during the process of the micronization in high energetic mill. In this paper, the optimum conditions of miconization of talc in high-energy-speed rotary mill and its influence micronization on a degree of Fe2O3recovery by hydrometallurgical methodes, are presented. The X-ray analysis of the obtained products showed that high quality talc with low content of can be obtained by these physical-chemical processes In this paper, the principles and application or fine and ultra-fine grinding high-energy attriton mill with small balls, enabling fast, efficient grinding, low energy consumption, short grinding time and easy handling will be described.

Jan 1, 2014

By Kal Sastry, Anshuman Prasad

This paper presents a population balance model (PBM) for describing the agglomeration process and select a suitable coalescence kernel that can simultaneously describe nucleation, layering and coalescence mechanisms. The PBM is solved numerically by making use of a size discretization procedure in order to simulate iron ore agglomeration in rotating drums where moist feed is added to preformed seeds. Subsequently, a comparison of computer simulation results with the previously published experimental data is provided. Finally, the paper discusses how the current approach can be further extended to the simulation of industrial iron ore agglomeration circuits operated in closed circuit.

Jan 1, 2003

By Weiran Zuo, Emmy Manlapig, Fengnian Shi

The effect of metalliferous grains on electrical comminution efficiency was investigated by comparative experiments using natural rocks and synthetic samples. The result indicated that the existence of metalliferous grains affects the breakage probability and product size distribution of electrical comminution. On average, metalliferous grains increased the breakage probability of particle in the first pulse discharge by 55% and generated finer product at the coarse end. As a result, particles with metalliferous grains exhibited higher energy efficiency than that without metalliferous grain in electrical comminution. A positive linear relation between product fineness and specific energy in electrical comminution was observed. With the assistance of numerical simulation on the electrical field distribution of ore particle, the role of metalliferous grains in electrical comminution is confirmed and the mechanism of metalliferous grains effect is elucidated. Understanding of the effect of metalliferous grains on electrical comminution is important to evaluate the feasibility of applying electrical comminution to ores with different mineral composition, and to understand the breakage behavior in electrical comminution.

Jan 1, 2014

By Nicolus Rotich, Ritva Tuunila, Louhi-Kultanen. Marjatta

Most minerals, their ores, and gangue require sorting in order to maximize the recovery of the primary product during concentration. Gravity separation though old, is not obsolete and is continually playing an important role in mineral processing and many other industries, especially where plant energy efficiency is of concern. Screen designs e.g. material of construction, deck angle of inclination, the feed throughput, and physical as well as chemical properties of the particles, are critical factors to consider when using gravity for solid separation. Solids loading and screen geometry are significant, and easily manipulated operational parameters that affect both the screening rate and efficiency to a large extent. In this paper we applied nonlinear least squares optimization technique, and response surface methodology first, to assess the significance of the two factors, and secondly to select the best mathematical models that optimize both capacity and efficiency of the screening process. Initial experiments and confirmation tests were conducted on a prototype screen of 846.51cm2 effective area, (2100 cm2 total area). For glass beads of sizes 0.75-3mm, with feed loads of 10g up to 160g, and inclination angles from 5-20o, a maximum efficiency of 66.7%, and a screening rate of 22g/s was achieved with a screen loading of 86.5g, and an inclination angle of 12.43o. These results were then subjected to nonlinear least squares optimization, in which afterwards an optimum theoretical efficiency of 72% and screening rate of 31.2g/s were achieved at a loading of up to 104g. There was excellent performance at angles 12.5=?=17.5, but poor at the angles outside this range. The screening efficiency did not seem to respond significantly to changes in screen loading. Confirmation tests conducted at selected optimum parameters achieved an efficiency of 72.1% (at 17.5o with 88g load), and a rate of 27g/s at 16.5o with 104g.

Jan 1, 2014

By Lucy van de Ruit, Megan Becker, Aubrey Mainza, Jenny Wiese

"UG2 chromitite ore is a complex, highly disseminated platinum ore from the Bushveld Complex in South Africa, with typical platinum group mineral (PGM) grain sizes below 15µm. The introduction of stirred mills to the platinum industry has enabled grinding to finer product sizes, which has improved liberation and recovery of the finely grained PGMs. However, reduction in particle size leads to an increase in chromite entrainment in the flotation concentrate, which has a negative impact on the subsequent smelting process. Factors such as particle size, froth structure, solids concentration and water recovery have all been identified as impacting entrainment, but whether particle shape also has a significant effect is unclear. The purpose of this study was to determine whether the recovery of chromite particles by entrainment during the flotation of UG2 ore is affected by particle morphology. A laboratory vertical stirred mill with inert ceramic media was used for grinding UG2 ore which was then floated in a batch flotation cell. Flotation feed and concentrate samples were analyzed using QEMSCAN to quantify the angularity and aspect ratio distributions of the particles. The stirred mill product was found to have relatively broad aspect ratio and angularity distributions, with the major mineral components (chromite and silicates) having very similar shape characteristics. Analysis of flotation feed and concentrate samples suggested that particle shape does not have a significant effect on chromite entrainment."

Jan 1, 2014

By A. V. Bogdanovich, S. A. Urnysheva

"Gravity and X-ray luminescent separation methods are generally used in processing of diamond ores. X-ray luminescent separators are applied for separation of diamonds from feed ore size fractions from 100 to 10-15 mm size and for final treatment of gravity concentrates over 1 mm size. Gravity separation machines used for diamond ores separation are heavy medium cyclones and pneumatic jigs. One of the most important parameters, to a large extent affecting diamonds recovery from ore, as well as processing costs and specific energy costs, is size of dumped final tailings. That was exactly the purpose of the studies, the results of which are described in this paper. The studies performed on different ores showed that in order to achieve high recovery results, it is necessary to dump heavy medium separation tailings below 3 mm size. Separation of final tailings of -6+1 mm size by jigging is also possible. However, with a view to exclude extra diamond losses, it is necessary to maintain jigging concentrate yield approximately at 25% from starting feed, with its subsequent cleaning in heavy medium cyclones. In addition to that, it is necessary to separate 20-25% of middling with diamonds content at feed ore level and subject it to grinding. This will complicate flow sheet, but reduce load on heavy medium cyclones. In order to develop optimal flow sheet for gravity concentration of a specific diamond ore, large-scale investigations are required, including technical-and-economic assessment of separation alternatives. INTRODUCTION In processing of diamond ores, gravity and X-ray luminescent separation methods are generally used. It is common practice to apply X-ray luminescent separators for separation of diamonds from feed ore size fractions from 50 (100) to 20 (10) mm size and for final treatment of gravity concentrates over 1 mm size. With that, X-ray luminescent separation tailings larger than 3-6 mm size are reground and delivered to gravity concentration processing stage. Middling products circulation volumes are large, not infrequently necessitating decrease in concentrating plants capacity, especially with mining in deep workings of deposits, where ore strength is higher (Goryachev, 2010; Vaginov, 2000; William, 1988). Diamond ores preparation before processing is accomplished by means of roll-screw crushers and autogenous grinding mills, minimizing probability of free diamonds damage in liberation from barren rock. In re-crushing of size fractions that are “difficult” in autogenous grinding, high pressure grinding rollers are applied (Burchardt, 2014; Fedotov, 2011a, 2006b)."

Jan 1, 2018

By Camilo Uribe, Williams Calderón, Gonzalo Montes-Atenas

In industrial hydrometallurgical operations, the leaching process is often implemented via heap or dump leaching operations. During the pile up of these massive amounts particles a porous material is then formed. The manner it is constructed is crucial since it will define the permeability and other parameters determining the flowrate of leaching solution across the material. This study aims to estimate how the unsaturated permeability of the staked porous structure confined in a column-like geometry varies with and without particle size segregation. The piling up will be modeled using the Rocky® software. Different disposals of particle size distributions across the column will be simulated and their effect onto the overall column unsaturated permeability will be estimated. It was found that when the belt speed increased, the particle segregation in the column also increased. This condition is expected to improve the permeability of the porous structure in the column, probably due to the smaller compaction of larger particles when they are located at the base of the column and maintain a suitable porosity to permit leaching flowrates relatively high, suggesting better extraction results. The opposite was observed when small particles were preferentially located at the bottom of the column. These results are expected to provide an insight towards what is the best way to construct heaps and dumps.

Jan 1, 2014

By Peter Rubie, John Russell

"For many years, optimizing the relining of hard rock grinding mills has been complicated by the large number of variables, the low frequency of relines (resulting in a slow relining experience assessment and review cycle), and the potential economic risk associated with some changes to relining equipment or work practices. A technology that has its roots in the automotive manufacturing industry is being utilized to construct a statistically accurate, configurable, and dynamic simulation of the mill relining process. The detailed effects of various mechanization and process changes can be rapidly modeled and compared. Application of this discrete event analysis technology in the mineral processing industry delivers a range of benefits to many industry stakeholders. For example, mill maintenance managers and contract relining companies can embrace the opportunity to benchmark current performance against world’s best practice. Concentrator plant designers and mill manufacturers, informed by this technology’s scientifically defensible data set, can accurately plan for maximum plant efficiency when designing an infrastructure and equipment combination that truly maximizes annual plant availability. Time-motion studies of grinding mill reline data at mills of varying dimensions, liner configurations, mill relining equipment, operator and tool variables, have been integral to the development of this dynamic simulation tool and its associated data set. Access to mill relining simulation technology will enable mineral processing industry professionals to take advantage of an increased capacity to develop mineral concentrator performance optimisation initiatives within the given financial, physical and technological constraints of the individual concentrator plant."

Jan 1, 2014

By Manuel Diaz

"In these difficult times for the mining world, mainly due to the global uncertainty about metal prices and the increased activity of opponents to the mining industry, it is essential that mining companies focus on efforts and strategies that will give them the most flexibility to succeed under the fury of these phenomena. The careful management of systems to control costs, and indicators to measure with great precision actual variations in costs and cash flows, are essential to adequately manage the uncertainty. Similarly, clear corporate and regional strategies designed to maximize cash flow and operating margin will allow the company to be better prepared to face any negative situations caused by declining metals prices, stricter government regulations and increasing social pressure. Gold Fields Limited, a corporation of South African origin and with more than 100 years in the gold mining business, has developed the ability to adapt to large changes generated by different global crisis throughout its history. This occasion will be no different. Given the critical situation of the mining industry in the world today, Gold Fields has embarked on a re-structuring plan at global level that will allow much closer control and real efficiency of production costs. This plan includes the creation of regional business units that allow greater independence for each region while still preserving the standards and cultural values of the Corporation. This presentation will explain why we believe that this approach combines the best aspects of the two styles of business, and what are the expected results. In the Americas Region, Gold Fields currently operates Cerro Corona, in Peru. In addition, the company is considering opportunities for growth in Chile, Brazil, Mexico and Canada."

Jan 1, 2014

By G. Venkateswara Rao

The jigging of ferrous ore to produce higher-grade products has been practiced for many decades. This is due to easy separation, a beneficial trade- off between operating cost and reduced yield relative to Dense Media Separation (DMS). Jigging becomes prominent for beneficiation of iron ores in the coarser size range. At present drive is towards the use of under bed air pulsed jigs for the beneficiation of ferrous ores. The main advantage is that the under bed air pulsed jigs are capable of generating the large pulse of amplitudes required to fluidize a deep bed of heavy ores particularly lump iron ore up to 40mm size. The major jig parameters effecting the jigging operation are bed height, shape of the pulse, residence time, operating pressure, valve cycle time and water flow rate. With the pulse shape set correctly for optimum stratification rate, even it is still necessary to provide enough residence time, to ensure the difficult material will take time to migrate to the expected layer in the bed. In order to find the Jig Stratification Index (JIS) parameters like bed height, operating pressure, water flow rate, cycle valve time and shape of the pulse were optimized first by conducting various tests. Typical Iron ore samples from Odisha (both lump and fines) were subjected to stratification studies at residence time of 1, 5 and 15 minutes. Jig Stratification Index (JSI) for both lump (0.30) and fines (0.20) were determined by using APIC Jig. The maximum possible JSI was calculated by using heavy liquid separation test (0.42 for lump and 0.24 for fines). It is found that the jig bed JSI is less than the Heavy liquid JSI for both lump and fines. The ratio of Jig bed JSI to the heavy liquid JSI is 0.83 for lump and 0.71 for fines. The JSI and ratio of Jig bed JSI to Heavy liquid JSI are low for fines due to fluid turbulences causing some degree of remixing in the jig bed. The fluid turbulences are more for fines than lump, hence jigging of fines is difficult and challenging. Keywords: sub grade iron ore, gravity separation, jigging, apic jig, stratification, residence time, jig stratification index

Sep 1, 2012

By R. Chowdhury

Axis House manufactures and supplies alkylhydroxamate reagent of various carbon chain lengths for application in flotation of oxide copper and other minerals. As part of reagent performance improvement the structural factors of hydroxamate are examined by various analytical tools in particular with X-ray diffraction of single crystals. In a recent publication, the structure of n-octylhydroxamic acid and its corresponding potassium salt are presented with findings of hydroxamic functional group geometric preference, H-bonding, keto-enol tautomerisation, acid-salt aggregation and alignment of carbon chain. In this paper an example of branched alkylhydroxamate 3, 5, 5-trimethylhexylhydroxamate will be presented and compared with the result of linear alkylhydroxamate.

Sep 1, 2012