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By J. Douglas Causey

In 1987, at the request of the Bureau of Land Management, the U.S. Bureau of Mines studied 11,069-acres of the 12,290-acre Eldorado Wilderness Study Area (NV-050-423) in order to evaluate its identified mineral resources. The study area is located in Clark County, NV, adjacent to and northeast of the town of Nelson. There are inferred subeconomic resources on the Paul (gold, silver), Bel (gold, silver), Big Horn-Inez (silver, copper, lead, zinc) claims, and Montezuma (gold, silver, copper, lead, zinc) patented claim group in the Eldorado study area. Because of lack of exposures, tonnage and grade on these properties could not be determined. No resources were identified for the other five properties examined in the area. The southern two-thirds of the area is in the Eldorado mining district, a base- and precious-metal district which has been intensely explored for over 100 years. Nine claim groups were examined in the study area. Eight claim groups are within the Eldorado district and include the Montezuma (patented -M.S. 3966), Bel, Eldorado, VAR, SINJUN, Paul, Rusty Bit, and Big Horn-Inez. One property, the Flintstone claim group, is north of the Eldorado mining district at the north end of the study area.

Jan 1, 1988

By Carl E. Norman

An investigation of geologic structure on macroscopic, mesoscopic, and microscopic scales was conducted on near-surface igneous and metamorphic rocks in which the existing stress field was determined by in situ methods. A consistent NE-SW orientation of the maximum compressive stress in the horizontal plane at four of five test localities appears due to the intrusion of NW-trending diabase dikes. Structural features at the mesoscopic scale show no consistent directional relationship to determined stress directions. Petrofabric diagrams of open microfractures show preferred orientations, but these are not consistently related to the orientations of larger structural features, such as joints, foliation, or mineralized shear zones. However, at five of six test sites the preferred direction of microfractures occurs nearly perpendicular to the maximum principal stress directions; an anomalous parallel relationship exists at a test site in an intrusive rock body. The results suggest that the open microfracture subfabric may provide a means for gaining information on the directional properties of stress fields. Such information can be obtained from oriented cores taken from holes which exceed the approximate 100-foot depth to which other in situ methods are presently limited.

Jan 1, 1970

By Maria I. De Rosa, Charles D. Litton

The U.S. Bureau of Mines conducted experiments for predicting materials' ease of combustion (smoldering onset, smoldering, flaming, and decomposition rates) by means of submicrometer smoke particle characteristics for the development of a simple test method. The experiments were carried out in an approximately 20-L furnace, with a 10-L/min airflow through the furnace for a 14-min duration, at set furnace temperatures of 150°, 250°, and 1,000°C. The variables studied as a function of time were the onset time of smoke particles, time and duration of maximum smoke particle generation, average concentration of smoke particles, and particles' average diameter, mass weight loss, and furnace temperatures. Results show that the onset time of smoke particles is predictive of materials' ease of smoldering, and the time of maximum smoke particle generation and its duration, coupled with mass weight loss, are predictive of materials' ease of smoldering and flaming (depending on the experimental temperatures), and decomposition rates.

Jan 1, 1992

By R. V. Thurston, Edmund S. Leaver

"During the development of the sulphur dioxide leaching process for the treatment of ""mixed"" copper ores at the Southwest experiment station of the Bureau of Mines*** the pulp from treatment of roasted cupriferous pyrite with sulphur dioxide gases and water showed an unexpected amount of sulphuric acid. After following out several false premises it was found that this was due to iron in the solution, and also that this iron tended to oxidize to the ferric state if the concentration of sulphur dioxide in the roaster gases used did not rise above a certain figure. While the percentage of iron present was email it was enough to cause an entirely different set of conditions from those of the original sulphur dioxide leaching process and to promise a much wider application of the general idea. Sulphurous acid dissolves only certain copper minerals, sulphuric acid solutions certain additional minerals and ferric sulphate solutions certain further additional copper minerals, so this observation was of importance in connection with possibilities in the hydrometallurgy of the so-called ""mixed"" or partly oxidized copper ores.The work has been carried along by a number of experimenters. L. R. Eckman, junior chemist of the Southwest station, contributed largely to the early developments. L. Roberts, W. D. Bonner and C. G. Maier each in turn physical chemists at the Pacific Experiment station, (Berkeley, Calif.) have studied the reactions involved. A complete report of all the work on this process will be prepared later under the direction of O. C. Rolston. The purpose of the present paper is to place a summary of the more practical phases of this seemingly important piece of work before those interested."

Dec 1, 1923

By John S. Berber

Bureau of Mines research on the production of phthalic anhydride by vapor phase oxidation of hydrocarbons began at Morgantown, W. Va., in October 1960. For these preliminary studies, a known solution containing naphthalene and 1-methylnaphthalene was used. In another series of tests, pure naphthalene was dissolved in different solvents. A series of investigations was conducted with the neutral oil fraction (210° to 270° C) of a low-temperature tar obtained from the Texas Power and Light Company's low-temperature carbonization unit. The neutral oil fraction was first dealkylated, and then the product was distilled into 210° to 250° C and 250° to 270° C fractions. These two fractions were then subjected to catalytic vapor phase oxidation. Although a number of catalysts was tested, most of the experiments were made using 9 percent vanadium pentoxide on inert alumina. The activity of this catalyst did not decrease after 162 hours at 1,030° F. Studies were conducted over a temperature range from 610° to 1,180° F. An operating temperature of 1,030° F yielded 47.50 percent of phthalic anhydride from a synthetic mixture of naphthalene and 1-methylnaphthalene. The highest yield (84.40 percent phthalic anhydride) was obtained with naphthalene dissolved in toluene and also with naphthalene dissolved in methyl ethyl ketone. With a 210° to 250° C fraction the highest yield of phthalic anhydride obtained was 12.32 percent at a temperature of 900° F, and, with a 250° to 270° C fraction, it was 15.80 percent at a temperature of 875° F.

Jan 1, 1963

Aid mine operators as well as mine inspectors in making quick but sufficiently accurate measurements of the rock dust content of coal/rock dust mixtures. The Problem Past research has shown that accumulations of volatile coal dust in underground coal mines can be rendered non-explosive by dilution with chemically inert rock dust (usually limestone). Consequently, rock dusting is required by law in U.S. underground coal mines. However, mine officials and inspectors have no quick and reliable means to determine whether enough rock dust has been applied to achieve a mixture that is in compliance with the law. Even the compliance tests used by the Mine Safety and Health Administration (MSHA) are slow and involved. MSHA assures that a mine has been rock dusted adequately by collecting samples from rock dusted areas of the mine and sending the samples to a laboratory for analyses of the inert-dust content. The analyses may not be completed for more than two weeks, during which time the mine in question might be inadequately protected against coal dust explosions. To solve this problem, the Bureau of Mines devised a quick, simple and reliable device that can immediately determine the rock-dust content of a mixture of coal and rock dust.

Jan 1, 1985

By M. M. Tilman

The Federal Bureau of Mines developed a rolling method that improves creep resistance and yield strengths of lead alloys containing up to 5 wt-pct Sb. The 0.69-inch-thick slab-cast alloys were breakdown-rolled to 0.226 inch and finish-rolled to 0.063 inch at 5-or 20-pct reduction per pass. Rolling was at room temperature to simulate conventional cold rolling, and at 75°, 125°, and 175° C. Two alternative methods evaluated consisted of (1) a single cold final pass followed by annealing and (2) a single hot final pass. Two additional processing methods involving percipitation strengthening were included for comparison. Compared with conventional cold rolling, hot rolling at 125° and 175° C with multiple light passes vastly improves creep resistance and raises yield strengths. Tensile strengths are less affected. The other treatments also improve creep resistance significantly and generally improve tensile properties; magnitudes vary with treatment and composition.

Jan 1, 1975

By James J. Olson

The Bureau of Mines recorded both particle accelerations and velocities from one-stick and production blasts at Eagle-Picher Industries' Shullsburg mine, Shullsburg, Wis., to test the effectiveness of square root scaling in grouping underground blast vibrations and to determine the effects of rock type and mine geometry on blast vibrations. Although the charge weights of subsequent delay periods sometimes exceeded the charge weight of the zero-delay period, both acceleration and velocity records showed that the zero-delay portion of the Shullsburg production blasts produced the highest vibration amplitudes. Because of the restricted range of charge weights in the Shullsburg experiments, no statistical determination of an appropriate scaling factor could be made. However, the square root scaled peak particle velocity data from the Shullsburg production blasts grouped well within the approximate band-width of vibration data obtained by the Bureau from quarry blasts in many different rock types. This indicates that scaling by some factor, perhaps the square root or cube root of the charge weight, may be an effective way to group and study vibration data from underground blasts. Further research is needed to determine which scaling factor is best for underground blasting.

Jan 1, 1970

By W. Bruce Montgomery

Manganese oxides occur, with some iron oxides, in small scattered lenses on property controlled by the Columbia Manganese Co. (1943) near Evington, Campbell County, Va. The company mined some manganese ore during 1917 and 1918. A preliminary examination in May 1942 indicated the possibility of finding additional ore. On August 21, 1942, the Bureau of Mines began prospecting to verify the continuity of the ore exposures. Work on this project continued until February 5, 1943. Prospecting and development work included shaft sinking, crosscutting, drifting, trenching, and test-pitting in six separate areas indicating two types of deposits. The most predominant type is a wide brecciated area in which occur lenses or pockets of nodular manganese oxides. The other type is characterized by more of a vein structure, including thin layers of manganese oxides.

Jan 1, 1949

By H. C. Loesche

The problem of signaling to the hoisting engineer from the cage in a shaft mine has been given considerable thought and attention by engineers and mine operators seeking to Increase the safety and efficiency of hoisting. HISTORY R. L. Rutherford,3/ an employee of the Magma Copper Co., Superior Ariz., realizing the need for a simple and practical moving-cage signaling system, began a serious of experiments early in 1937, Available electrical moving-cage signal in operation at this date required that signal wires be installed in the shaft to make a simple, positive signal without wires, the first experiments used the pipe lines in the shaft for carrying the signal current, but these experiments were not successful.

Jan 1, 1945

By James J. Olson

Previous Bureau of Mines studies of vibrations from quarry blasts have shown that the square root of the charge-weight may be used to group particle velocity data from various charge sizes, and that empirical propagation equations may be used to estimate vibration amplitudes. Particle accelerations of the sandstone roof of the White Pine Copper mine, Michigan, were measured to determine whether similar propagation equations may be developed for underground mine blasts. Vibration data from White Pine blasts were best grouped by scaling with the square root of the charge weight. Cube root scaling did not effectively group the data. The empirical propagation equation AW1/2 = 50,000 (R/W1/2)-2.21 where A is peak-to-peak acceleration in g's, W is the zero-delay charge-weight in pounds, and R is the distance from the blast in feet, may be used to estimate maximum vibration amplitudes from production sized blasts. Vibration differences among headings and types of explosive charge (AN-FO and dynamite), while statistically significant, were not a major factor in the estimation of maximum vibration amplitudes with an empirical propagation equation. Vibration differences between types of explosive charge were larger than the differences among headings, indicating that some reduction of vibration amplitude might be gained by using AN-FO rather than dynamite. Acceleration records from both White Pine's AN-FO and dynamite production blasts show that high intensity vibrations from the delayed portions of the blast (each delay interval = 25 milliseconds) were separate events, and that the zero-delay portion of the blast produced the maximum vibration amplitudes. If the pull of the underground blast round can be maintained, a reduction of the zero-delay charge-weight may effectively reduce the maximum vibration amplitude of the blast.

Jan 1, 1970

By Oliver C. Ralston, Foster Fraas

"INTRODUCTION The predominant characteristic of powdered mica is the thin -plate shape of the particulars, and the thinner the plates, the more enhanced is this characteristic. Consequently, it is frequently desirable to grade mica according to the thickness of the plates. Concerning the various possible methods for grading mica, very little has been published. There is also no information on the relative quantities of mica per given range of plate thickness. This paper presents a graphical method that shows how these quantities are distributed and how the different methods of grading compare.CUMULATIVE BULK DENSITYBulk density, which is an indirect measure of the plate thickness, was determined in a small cylindrical cup of 3.37 cubic centimeters volume. The mica was placed in the cup under a standard procedure. The densities thus measured checked these determined in a 273 cubic centi¬meter cup with less than a 2 percent error.In calculating cumulative densities it is important to know how they are averaged. In any grading operation the bulk density of a series of fractions is determined. Starting with the lowest density fraction, the cumulative percent under-density can be calculated through the various fractions. It is possible that quantity may be measured by volume or weight and that the averaging may be done by a number of methods. However, experimentally it has been shown that the quantity must be by volume and that the averaging must be arithmetic. This is illustrated in table 1, in which the calculated and actual bulk densities are listed."

Sep 1, 1942

By A. May

Florida has accumulated about 400 million tons of phosphogypsum, a mineral process waste generated in the production of fertilizer, and is adding 30 million tons to this annually. To minimize storage of this waste and reduce potential environmental effects, the Bureau of Mines conducted research into utilizing the phosphogypsum, by identifying and developing high-volume uses for this material. Admixtures of phosphogypsum, fly ash, and lime that could produce a coarse aggregate suitable for road construction were investigated. Using phosphogypsum with asphalt, cement, cement-kiln dust, silica, clays, and oxychlorides to pro-duce aggregate was also examined.

Jan 1, 1985

By J. N. Van Sant

Lignite mining in North Dakota was begun about 1884 to supply the domestic needs of settlers. Annual production has grown rather slowly but steadily, exceeding 3 million tons in 1950. The western part of the State has lignite reserves, amounting to 351 billion tons, underlying an area of 28,000 square miles. Contour strip mining has almost completely replaced underground mining as the method of production. Lignite is often found under rather shallow and easily removed overburden, and this is the primary reason for the change in mining practice. Current mining operations are conducted where the overburden is 30 to 70 feet thick. Contour strip mining results in high production rates, at present 27 to 56 tons per man-day. These high production rates result in relatively low production costs.

Jan 1, 1959

By Joseph J. Wallace

1. The Pocahontas No. 3 and Pocahontas No. 6 ere the two most important beds in Mercer County from the standpoint of present production and recoverable reserves. 2. Known measured and indicated reserves in all beds, based on a minimum thickness of 14 inches and 1,800 tons per acre-foot of coal in place, are estimated at 188 million short tons as of January l, 1953. Of this total, 80 million short tons are in beds 28 inches and more thick. Areas in each bed were omitted from the estimate because available data relative to the bed characteristics are too meager to make an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these areas, such reserves should be added to the total estimated reserves.

Jan 1, 1954

By D. E. Hirsch

The types of compounds present in aromatic concentrates derived from high-boiling petroleum distillates can be estimated from a gel permeation chromato-graphic (GPC) analysis by the use of tables developed from extensive GPC and mass-spectral analyses on fractions from four crude oils. For a fraction from the GPC analysis, the retention volume and the molecular weights (from mass spectrometer) suffice to indicate the types of compounds which predominate. The tables which show these qualitative analyses were developed through the use of pure compounds as well as the extensive analyses on Prudhoe Bay (Alaska), Gach Saran (Iran), Swan Hills (Canada), and Wilmington (California) crude oils. These tables provide a rapid method for determining which types of compounds are present in a GPC fraction before attempting to develop quantitative data.

Jan 1, 1974

By C. A. Wilson

The Bureau of Mines started a continuing program to investigate and evaluate analytical techniques to assist governmental agencies to select simple, rapid, reliable methods for crude oil spill identification. Six crude oil samples were analyzed to evaluate gas-liquid chromatography, atomic absorption spectrophotometry, infrared spectoscopy, sulfur and nitrogren determinations, mass spectrometry, nuclear magnetic resonance spectroscopy, and ultraviolet spectrophotometry. Samples were studied from the following selected fields: El Morgan, Egypt; Duri, Indonesia; Minagish, Kuwait; Bachaquero, Venezuela; Gach Saran, Iran; and Prudhoe Bay, Alaska. These samples were chosen to represent high-production fields that are likely to be involved in oceanic transport. Over 50 years of Bureau of Mines analytical research on petroleum served as the basis for evaluation of the experimental results to determine which of the methods are effective techniques to identify crude oil spills. Gas-liquid chromatographic analysis, atomic absorption spectrophotometric analysis, and sulfur-nitrogen determinations are recommended as the most useful of the techniques investigated.

Jan 1, 1975

By Ronald D. Hill, Elmore C. Grim

The cost of reclamation can vary widely, depending on the primary objectives of the restoration activities. statistics in this study originated from State files, publications, and personal communications relating to restoration and pollution control measures for previously mined lands (orphan lands) and active mines. Reclamation of orphan lands is generally considered a public burden and constitutes an economic problem. All work reported here was completed under government contract, by the lowest bidder, with money coming from State and/or Federal funds. Cost would have been substantially lower had the reclamation been concurrent with mining. Several persons connected with some of the projects have observed that costs could probably be reduced by at least one half, if the reclamation had been conducted along with the mining. The expense of clearing and grubbing of volunteer vegetation, disposal of buried trees and brush, loosing of compacted spoil, and re-establishing access to areas could be saved. In addition, a contracting firm doing the work for a government agency would have mobilization costs and receive a profit. Mining companies also are profit conscious and would consider these costs in anticipating their profits (e.g., overhead would be less if reclamation is integrated with mining). The data presented here should serve as a guide for estimating and determining cost ranges, however, it should be recognized that variations exist. Adjustments may be necessary from the standpoint of physical conditions, economic conditions, price changes, and more restrictive requirements of recent surface mining laws. Reclamation conditions, procedures and successes in the eastern United States, particularly in Appalachia, have no bearing on conditions to be expected in the western United States. The situations are wholly different. Reclamation in the West differs from th t in the East, primarily because of aridity especially a during the summer months 1). Because of the many variables and differences between reclamation in eastern and western areas, they will be discussed separately.

Jan 1, 1974

By Thomas A. Gray, Lynn M. Crayne, Michael A. Trevits, Phil Glogowski

Mine seals can be remotely constructed in underground coal mines, through vertical boreholes, when direct access to a fire is impossible or considered to be too dangerous. This method has great merit because boreholes can be drilled to specific mine areas and seals can be positioned close to a fire zone. The technology however, can be largely ineffective if the constructed seals do not provide effective barriers to airflow or cannot be used to impound water and other inert materials. Unfortunately, no viable alternatives exist to sealing the entire mine at the ground surface. Full-scale remote mine seal construction research is being conducted at the National Institute for Occupational Safety and Health’s (NIOSH) Lake Lynn Laboratory (LLL). Under this effort, Howard Concrete Pumping Company and GAI Consultants, Inc. have joined forces to evaluate a potentially significant improvement to the current state-of-the-art. This paper will cover development of novel technology for remote mine seal construction, evaluation of the materials used, construction practice, and follow-up testing.

By W. Blake, J. K. Whyatt, T. J. Williams

Researchers at the U.S. Bureau of Mines collected and analyzed over core measurements and other indicators of in situ stress characteristics at the Lucky Friday Mine, Mullan, ID. An analysis of these data revealed that significant local variations in in situ stress are present in this mine and that these variations existed prior to mining. High stresses were found to be associated with the most competent strata and a locked section of a fault. An estimate of the predominant stress field was developed for mine-wide modeling. The estimate shows that the greatest principal stress was oriented north of northwest. This information should provide a basis for mine-wide structural modeling of the Lucky Friday Mine and should generate important insights into localized stress conditions, which may significantly affect both local and mine-to-mine variations in seismicity induced by excavation.

Jan 1, 1995