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By John W. Frey

This paper presents one of a series of digests of foreign mining legis- lation and court decisions which is being prepared in advance of a general re- port relative to the rights of American citizens to explore for minerals and to own and operate mines in various foreign countries. This interpretation of the laws of Portugal, prepared from the best available information in Washington, has been slightly amplified in accordance with suggestions trans- mitted through the courtesy of the Department of State by Fred Morris Dearing, American Minister at Lisbon.

Nov 1, 1929

By John Durkin, Harry Dobroski

This paper presents a general overview of the Bureau of Mines' programs in the areas of operational and post-disaster communications. These programs encompass both hardware developments and system evaluations. Topics discussed include a new visual paging system compatible with existing pager phone lines, a means of modifying commercially avail able pager phones to permit selective paging and message leaving, a multiplexed telephone system that uses twisted shielded pair and requires no central control, medium frequency hardware developments, and a manual for mine communications. Research has continued in the area of post-disaster location and communications. This research is based on seismic and electro- magnetic techniques. Each has been extensively studied and field tested to better understand its ability to perform effectively. A brief description is given of the post-disaster program. Results are promising and provide insight into future areas of research.

By James P. Bennett

The U.S. Bureau of Mines investigated the role of imported natural flake graphites in dolomite-carbon refractories used in steelmaking processes and evaluated carbon fibers as a potential substitute. Varying quantities (1.5-30 pct) of natural flake graphite and carbon fibers were added to test samples. The effect of the additions on modulus of rupture (75°-2,750° F), deformation under load (2,750° F), and air-slag-metal resistance (3,000° F) was studied. Carbon purity of natural flake graphite additions did not influence hot strength, deformation under load, or air-slag-metal resistance. When the quantity of 90-pct-carbon graphite addition varied between o and 30 wt pct, hot strength was highest, deformation under load lowest, and air-slag-metal wear the least at 10 wt pct. As test temperature increased from 500° to 2,750° F, the hot strength difference became less. Carbon fiber additions were limited to 1.5 pct in dolomite-carbon brick. At this level, physical properties were generally comparable to those obtained with natural flake graphite, but were below values obtained with 10-pet-f1ake graphite additions. Carbon fibers are not considered a satisfactory substitute for natural flake graphite.

Jan 1, 1989

By M. W. Pullen

It is recognized that the determination of electrical resistivity of the earth within a given area may furnish information concerning the location of certain mineralized strata of economic importance. Present knowledge of the electrical resistivity of the various rock formations is almost nil, and the geophysicist who is detailed to make a survey of an area without any data as to the relative resistivity of the underlying rocks is greatly handicapped. Such surveys are usually made within areas known to contain mineral deposits to aid in locating desirable points for drilling. Usually these areas have been prospected by diamond drilling, and drill cores of the various rocks and ores are usually obtainable. Were it possible to make resistivity tests in a laboratory of the drill cores or from pieces of the rocks and ore within an area before attempting a field survey, this would indicate not only the advisability for such a survey but would aid considerably in the interpretation of the results of such a survey. To be of most value a definite method should be used for all such tests, and as yet such a method has not been established.

Jan 1, 1929

By H. W. Wainwright

One phase of the research and development work on synthetic liquid fuels conducted by the Bureau of Mines at Morgantown, W. Va. in cooperation with West Virginia University deals with the purification of synthesis gas.2/ Most of the experimental studies on gas purification have been directed toward the removal of organic sulfur from gas, either catalytically or by adsorption with activated carbon. An important part of the purification program has been the development of suitable analytical methods for determining organic sulfur compounds. As the total sulfur content, organic and inorganic, of purified synthesis gas should not exceed 0.1 grain per 100 cubic feet, the need for accurate analytical methods is apparent. It is also apparent that such methods must be rapid if one wishes to evaluate various processes for removing sulfur from gas. The organic sulfur found in most gas produced from coal is usually present as carbon disulfide, carbon oxysulfide, methyl and ethyl mercaptans, and thiophene, with the exception of thiophene, the remaining organic sulfur compounds respond similarly to catalytic treatment and can be removed effectively. Not only does thiophene resist most catalytic treatment, but it poisons some catalysts, rendering them ineffective in removing the other forms of organic sulfur.

Jan 1, 1950

"There mines are located in out of the way places, where timber is scarce and its price high, the problem of protecting it from fire risk is of considerable practical importance. Scarcity of timber for mining purposes is commonly met with in the more arid parts of the country, where, so, mine timbers are most likely to become dry, and inflammable, and where, therefore, the risk from fire is accentuated. Any effective and cheap method of securing adequate protection of such timber at the lowest possible cost is worthy of careful investigation. The use of magnesite cement has been suggested in this connection.The necessary qualities for any substance for the use suggested above may be summarized as follows: It should be resistant to abrasion, and to impact and structural stresses. It should be durable when subjected to the action of the elements, and stable to any minor derangements of the base on which it is placed. It must be relatively unaffected by changes in temperature, by the action of water, and should adhere to the material on which it is placed, and it should also be free from shrinkage cracks due to setting up the material, Magnesite cement appears to fulfill the various conditions outlined above.The elasticity of such cement is the outstanding quality which makes it desirable for exterior work. It also possesses the ability to adhere to all materials in a marked degree. Its freedom from expansion and contraction after setting is one of the principal reasons for its adhesive quality. It may be applied to old brick or stone walls, even tho they have been repeatedly covered with paint, and the quality of adhearing to wood makes it possible to secure a weather-proof protection to the wooden casings and trim of exterior openings. The quality of adhesion and elasticity is easily proved by applying a 1/2"" layer to a 1"" board which has been first covered with metal lath. Such a board, about 8 feet long, may be repeatedly deflected about 3"" in the center without breaking the bond to the board, or causing any cracks to appear in the magnesia cement. The ability to resist fire as well as the possession of insulating qualities are also desirable characteristics of magnesia cement stucco.Magnesite cement stucco should be applied in two coats, each 1/4"" thick on various surfaces such as wood lath, metal lath, sheathing board, brick, hollow tile, or stone; care being taken as regards the presence of lime, unless the same has been rendered, or become inert as with very old, walls. The first coat made up to a consistency that works easily under the trowel is applied in the usual manner. No water should be added to the liquid chloride as it would alter its density, and injure the work. The second or finishing coat is then applied. The aggregates are different in each, and no other dry material should be added to them as they come to the trade. The cement may be applied in zero weather without damage. Setting is quite slow under such conditions, but the cement ultimately becomes hard. It should always be applied to a dry surface excepting that under certain conditions it is desirable to apply a solution of magnesium chloride before using the stucco."

Dec 1, 1919

By Edward D. Thimons

Because of the high number of accidental methane gas ignitions in metal and nonmetal mines, the Bureau of Mines searched for a simple guideline that would allow mine personnel to evaluate the methane hazard in a given mine. Air samples were collected by the Bureau in 53 metal and nonmetal mines and analyzed for trace evidence of methane gas. Samples were collected in the returns and at the working faces. Those mines classified as gassy by the Mine Safety and Health Administration had a significantly higher average methane concentration than those classified as nongassy. Of the 9 gassy mines sampled, 7 had methane concentrations above 100 ppm, whereas only 1 of the 44 nongassy mines had a concentration above 100 ppm. The 100-ppm concentration may be used as a simple and convenient guideline for forecasting the methane hazard in a mine, whether or not the mine is classified as gassy. There was no consistent correlation between commodity mined and methane concentration, nor was there a correlation between mine depth and methane concentration. Neither of these factors can be considered a guideline for predicting methane hazards.

Jan 1, 1979

By E. F. Ferrell

Gold was recovered from scrap electronic 60-40 (tin-lead) solders by drossing with aluminum or zinc at elevated temperatures. The gold, together with other metallic impurities, collected in the dross phase which could then be separated from the molten solder by skimming or filtering. Drossing upgraded the gold concentration by a factor of 10. Further upgrading was achieved by a combination of steps including an oxidation roast and either a combined cyanidation-amalgamation treatment or an aqua regia leach. The gold was then recovered in highly concentrated form from the aqua regia or cyanide solutions by cementation and from the amalgam by volatilization or dissolution of the mercury. The solder was purified by reaction with NaOH to remove dissolved aluminum or with SnCl2 to remove dissolved zinc.

Jan 1, 1976

By G. Nuñez, M. A. Pathak, C. F. Stanley

"Holographic interferometry is a non-destructive technique to detect small deformations1 of an object. It is a whole-field technique· with an accuracy of a few microns. An adaptation of holographic interferometry is time-averaged holographic interferometry which is particularly useful in detecting small vibration amplitudes of an object under investigation. Its application to biological tissue is especially difficult due to the combination of (a) the high sensitivity of the technique, and (b) the tendency of these objects to deform excessively, or move during the testing period. (This is also compounded by the changing moisture content of the tissue surface.)Ideally, a pulsed laser and fast-acting thermoplastic film camera could be chosen to overcome these difficulties, but the total equipment cost could exceed $75,000. In this paper we describe our relatively economical method to apply time· averaged holographic interferometry to an excised animal lung, utilizing holographic plates and a mechanically-shuttered continuous-wave Argon laser.EXPERIMENTAL METHODThe schematic of the experimental setup is shown in Fig. 1. The holographic equipment, including the laser, is fixed on a 3 ft x 6 ft x 4 in. honeycomb holographic table. This table is functionally similar to one described by Mark and Horsch2 which can be constructed for about one thousand dollars. The holographic table itself rests on six inner tubes to absorb floor vibrations. All unnecessary vibrations must be reduced to preserve the quality of the holograms. A laser beam from a 0.5-watt continuous-wave Argon laser is split by a circular variable beamsplitter (Newport Corporation Model 50GOOAV.1) into two beams, i.e., an object beam and a reference beam. The object beam is again split into two beams of equal intensity by a 50150 beamsplitter (Newport ·Corporation Model BS.1). These beams are optically filtered and expanded by spatial filters (Newport Corporation Model 910) to cover as much area of the object as possible. Soft biological tissues exhibit low reflectives, resulting in a relatively high reference to object beam ratio of roughly 5 : 1 at the holographic plate."

Jan 1, 1989

By Warren D. Longwill

All known resources within the four proposed RARE II additions to the Yolla Bolly-Middle Eel Wilderness in northwestern California occur in the Gig Butte-Shinbone study area (fig. 1). No mineral resources are Figure 1.--NEAR HERE. known in the East Fork, Murphy blade, or Wilderness Contiguous units. About 2,400 tons (2,177 t) of subeconomic manganese resources averaging 9.5 percent manganese have been estimated at the Blue Jay Mine in the Big Butte-Shinbone unit. In addition about 9,700 tons (8,793 t) of subeconomic chromium-nickel-cobalt resources in thin laterite soil at the Grubstake Prospect contain about 1.27 percent chromium oxide, 0.45 percent nickel, and 0.03 percent cobalt. Adjacent Ultramafic rock outcrops have pods averaging 2.5 percent chromium oxide (Cr203); one pod contains about 40 tons (36 t) of indicated subeconomic resources.

Jan 1, 1981

By Hillary W. St. Clair

This report gives the results of an experimental study of the progressive changes that occur in particle size and size distribution when a homogeneous and isotropic mineral is subjected to crushing by impact. The mineral used in the study was uniformly sized quartz, which was crushed in a simple drop¬-weight machine that applied impact energy up to about 100 kg-cm per g. Screen analyses of the crushed products were analyzed by the method of moments to determine the mean size, variance, skewness, and kurtosis. Analysis of the data from these experiments shows that the mean size of the crushed product is a function of the energy input and the initial size. The size distribution is functionally related to the degree of size reduction. As the mean particle size is decreased, at first there is a corresponding increase in the variance and decrease in the skewness, But, as size reduction is carried further, each tends eventually to approach a steady value, and the form of the size distribution becomes stable.

Jan 1, 1972

By Byron S. Gottfried

This Bureau of Mines report presents a method for combining the distribution curves at different specific gravities of separation, for a given piece of coal-cleaning equipment and a given raw coal feed, into a single, generalized distribution curve normalized with respect to specific gravity and, therefore, independent of the specific gravity of separation. Illustrative generalized distribution curves, based upon Bureau of Mines collected data on industrial operations, are presented for five different types of coal-cleaning equipment. The well-known concept of probable error is extended to the generalized distribution curve. It is shown that the conventional probable error is directly proportional to the specific gravity of separation. A number of sample calculations, illustrating the use of the generalized distribution curve and generalized probable error, are presented in the appendix.

Jan 1, 1977

By T. H. Dubaniewicz

Fiber-optic technology is progressing rapidly, including the development of fiber-optic sensors for many applications. These sensors have the advantages of high sensitivity, light weight, small size, high bandwidth, and freedom from electromagnetic influences. The U.S. Bureau of Mines is investigating the use of fiber-optic technology to monitor mine atmospheres. This report describes a methane monitor based on differential absorption of infrared light. The monitor can detect methane concentrations as low as 0.2 vol pct as far away as 2 km via fiber-optic cable. The upper range is 100 vol pct methane. Since the system requires no electrical power within the mine, it is intrinsically safe.

Jan 1, 2010

By Charles A. Kumke

In June 1942 , ' the Bureau of Mines selected the Zonia copper mine , near Kirkland , Yavapai County , Arizona , as a property meriting investigation in connection with its search for supplies of strategic minerals for use in the war . The following month , representatives of the War Production . Board conferred with Bureau officials and requested that the property be explored with the object of determining the tonnage and grade of ore that could be brought into production quickly and mined cheaply by open-pit methods . The work wa's designed to verify information submitted by the owners in support of an application for a Government loan. It was essential that the investigations be completed promptly , so that operations might be planned and copper produced for war needs . The investigations called for surface trenching , diamond drilling , and check sampling of underground workings . Unable to purchase equipment for trenching without considerable delay , the Bureau saved time by borrowing most of the necessary items from the Golden Queen mine of the Gold Fields Development Co. at Mohave , Calif. This company , whose engineers had sampled some of the old trenches , had a tentative agreement with the owners to operate and manage the Zonia mine in event the loan was granted . Additional equipment was borrowed from two Governmental agencies . The exploratory work , completed in 16 weeks , was carried on 7 days a week .

Mar 1, 1947

By George A. Savanick

The U.S. Bureau of Mines has patented and transferred to industry an abrasive-enhanced water-jet rock drill. This drill incorporates three novel components: a collimator, jet deflectors for cutting clearance, and an unpressurized swivel, which rotates at 1,000 rpm while passing 20 gpm of an abrasive slurry flowing at 1,000 ft/s. Drilling occurs through the action of a 10,000-psi, 2O-gpm water jet into which is entrained 72 lb/min of abrasives. The pumps, hoses, and fittings are those commonly used in the water-jet-cleaning industry. Only inexpensive, common sandblasting abrasives are used. This drill can cut through hard rocks with moderate-pressure jets; e.g., rocks with a compressive strength of 73,000 psi can be drilled with a 1O,OOO-psi abrasive jet. In addition to drilling holes, the drill can cut deep, narrow kerfs; collar a hole at any angle; drill through rubble; and chamber holes. The development of the abrasive jet drill is a significant advance in the state of the art of hard-rock drilling. The Government of the United States has licensed the abrasive jet drill patent to Weatherford Water Jetting Systems.

Jan 1, 1989

By Yael Miron

Two recent unplanned detonations occurred during blasting operations in sulfide-bearing ores in a Nevada gold mine. Other premature detonations have also reportedly occurred at other Nevada, California, and Arizona operations within the past few years, with increasing frequency. Unplanned or premature detonations can be extremely hazardous to life and can cause extensive property damage. A miner was injured in one of these occurrences. This report, by the U.S. Bureau of Mines, is intended to acquaint personnel involved in such mining activities with the basic causes for these accidents. These causes include the exothermic oxidation of pyrite (FeS2) and formation of ferrous sulfate (FeS04), the exothermic and energetic reaction of the ferrous sulfate with ammonium nitrate-fuel oil (ANFO)-based explosives, and the associated elevated temperatures that can set off detonators and explosives in the boreholes. Recommendations for safe operation by the Mine Safety and Health Administration, the Bureau, and the mine involved with the recent incidents include monitoring temperatures in the blast holes, analyzing for sulfate and ferrous ions, and limiting the time between loading and firing in accordance with conditions in the blast holes. Other procedures for safe operations should fit specific conditions in, the mines.

Jan 1, 1992

By Raymond B. Ladoo

The uses of talc are many but are not, in general well known or fully developed within the last decade several companies have realized the possibilities of greatly increased use and have intelligently proceeded to develop some of the fields which seemed most promising. This has had a tendency to lift talc from the obscurity in which it had existed for years, but the work is only started and much remains to be done. Considerably more attention has been paid to the technology and utilization of talc in Germany and Austria than in this country, despite the fact that the United States produces 65 of the world's talc and Germany and Austria combined but 5.4%. In the "Bericht,uber die tatigkeit des verbends der talcum-interessenten in Oesterreich-Ungarn" (Proceedings of the Austro-Hungarian Talc Association), for the years 1912 and 1913, many notes upon new uses appeared, together with suggestions as to further development of old uses. Aside from a few notes on the use of tar in paper, little has been published in the English language upon this subject. By recent action of the Talc and Soapstone Producers Association (U.S.A.) funds for research into the properties and uses of talc have been made Available and it is hoped that markets will be materially broadened a a result of this work.

May 1, 1920

By E. P. Youngman

Except possibly by individual natives and Liberians (small specters), is now being carried on in Liberia, according to a late report. definite information is obtainable with respect to the mineral resources of e country, except that iron ores are said to be abundant. Tin, copper, zinc, site, corundum, lead, bitumen or li nite, and diamonds have all been re- parte, but no commercial Geposits are known to have, been found. Gold has been duce, but not in significant amounts, as may be inferred from the customs - rt for Liberia recording the exportation of gold to the value of $4.80 Germany from the port of Cape Mount in 1925. It is not uncommon for atives to come into towns with African gold and valuable minerals, but they e reluctant to sive information concerning then. Some years ago the Liberian Government was seeing a loan in return for oil concessions, but apparently no drilling bea boon don

Jun 1, 1932

By Jack E. Tress

The Bureau of Mines has been involved for several years in the development of processes for the recycling of solid wastes. As part of this program, a project was initiated to determine the feasibility of producing secondary pig iron from auto scrap. During the test period, 86,000 pounds of shredded auto scrap, along with petroleum coke and fluxing agents, was charged to a submerged-arc furnace of 1-ton nominal capacity. Eighty-eight thousand pounds of pig iron, with an average carbon content of 3.90 percent and an average copper content of 0.2 percent, was produced at an electrical consumption of 512 kW-hr per net ton. A cost estimate of the process showed that the pig, iron might be produced at a cost of $57 per ton.

Jan 1, 1973

By A. D. Garman

This paper presents one of a series of digests of foreign mining legislation and court decisions which is being prepared in advance of a general report relative to the right of American citizens to explore for minerals and to own and operate mines in various foreign countries . This interpretation of the laws of Japan has been prepared from the best available information in Washington but is released subject to correction and amplification , if necessary , by the proper American diplomatic and consular officers to whom it is being referred through the courtesy of the Department of State . It is based on the law and regulations of 1905 as revised in December , 1915 , and translated by J. de Becker , LL.B. Occasional words and phrases quoted herein are accordingly taken from this translation and have not been checked against the original . The references are to the law ( as distinguished from the regulations ) unless otherwise stated .

Jul 1, 1930