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By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Eduardo Vitral

The present study focuses in the simulation of pattern formation by ion beam sputtering on a material surface. This process is responsible for the appearance of unexpectedly organized patterns, such as ripples, nanodots and hexagonal arrays of nanoholes. A numerical analysis of preexisting patterns is proposed to investigate surface dynamics, based on a model derived from a Kuramoto-Sivashinsky anisotropic equation, in a two dimensional surface with periodic boundary conditions. While deterministic, its highly nonlinear character gives a rich range of results, making it possible to describe accurately different patterns. A finite-difference semi-implicit splitting scheme is employed on the discretization of the governing equation. Simulations were conducted with realistic coefficients related to physical parameters (anisotropies, beam orientation, diffusion). The study dealt with a random and a monomode 1D structure initial condition in order to understand how the shape and wavelength of the initial pattern evolve with time. Ripples and hexagonal patterns were observed in the results, being physically consistent with the phenomenon. Moreover, the Method of Manufactured Solution has been used as verification of the developed numerical scheme.

Aug 16, 2017

By Dalila Chaves Sicupira

A pitting corrosion study of welded joints of lean duplex stainless steel (LDSS) UNS S32304 has been performed. LDSS S32304 thick plates were welded by different processes commonly employed in equipment and piping construction: SMAW (Shielded metal arc welding), GMAW (Gas metal arc welding) and FCAW (Flux cored arc welding). The electrochemical behavior of different weldment zones (fusion zone (FZ), base metal (BM) and heat affected zone (HAZ)) was characterized both independently using an electrochemical microcell and together through whole sample analysis. The electrochemical method applied was performed in acidified glycerin, a process fluid of the biodiesel industry. The results were correlated to the microstructural features of the materials. Based on the results, is possible to conclude that the breakdown potential (Eb) of the fusion zone (FZ) was higher than the Eb obtained for the heat affected zone (HAZ). In general, top samples show higher breakdown potential than root samples and also the samples welded using filler metal 2209 has a better anodic behavior than the filler metal 2307. According to the results, GMAW welding process with 2209 as filler metal was revealed as the optimum chosen for application of 2304 duplex stainless steels in this case.

Jan 16, 2018

By Ramon Augusto Moretti, Henrique da Rocha Severino, Renato Nascimento de Castro, Fernando Cesar Sousa

Rolling stand 12 (LTx) of long steel, installed in the company A, Piracicaba - SP unit, had presented high levels of vibration, which affected its internal components, such as: shaft, gears and bearings, generating downtime. To evaluate this equipment a study was proposed by the following engineering techniques: Conventional Vibration Analysis, Operational Deflection Shape (ODS) and numerical simulation by the Finite Element Method (FEM). In the Conventional Vibration Analysis, high levels of vibration were observed during manufacturing process, especially when the material reaches the equipment. Impacts generate high values in acceleration, on average 80 m/s² peak to peak. In the moment of impact, misalignment of internal components was observed by ODS. Field results were correlated to those obtained by the Finite Element Method, which allowed to calibrate FEM model. Thus, the most effective structural modification already numerically evaluated was implemented in the system. Afterwards, new measurements by vibration and ODS techniques were performed, and attenuation of vibrational levels and operational mode, which overloaded the internal components rolling stand, were verified.

Oct 1, 2019

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Peter Fajfa, Heinz Palkowski, Jakob Kraner, Matjaž Godec

The study of asymmetric rolling on the AA 5454 aluminium alloy plates was carried out. The plates were taken directly from the industrial hot rolled sheet. They were cold rolled on the laboratory mill with different rotation speed of the upper and the lower work roller with the strains around 33 % and 44 %. To get closer to the industrial conditions the maximal dimensions of the rolled plates for laboratory rolling mill and the special industrial lubricant were used. After deformation the plates were annealed to the soft condition. This research was focused on all possible effects of asymmetric rolling: The reduction of rolling force, the increase of strain at same set roll gap, bending of workpiece, finer microstructure, more heterogeneous textures and as a consequence of that better mechanical properties. The asymmetric rolling with favourable mechanisms in the deformation zone has created the material with the homogeneous hardness in the cross section and with lower anisotropy, which is crucial for improvement of formability properties of aluminium work hardened alloys and to get closer to properties of steels. In the presented paper the general impact and different effects of speed difference of rollers was investigated on cold rolled aluminium alloy. Obtained and analysed results explain the function of asymmetry in rolling process and the options to implement the asymmetric rolling in industrial plant.

Oct 1, 2019

By Boryong Lee, Heedong Sung, Minho Park, Sunyoung Choi

Recently, the demand for ultra-thin steel plate with high hardness and strength has been increasing in various industries. In order to satisfy this requirement, steel company designs the chemistry with low CEQ and obtains the required characteristics through quenching and tempering process. Especially, these steels are accompanied by low temperature tempering as a necessary process. Unlike ordinary high temperature tempering steels, it is impossible to improve the flatness after low temperature tempering. Therefore, shape control in the quenching process is very important for securing the excellent quality flatness. In order to obtain flatness in the quenching process, uniform cooling inside the plate should be accompanied. However, the quenching process has limitations in estimating the temperature behavior during cooling because the plate temperature is lowered to room temperature. In this study, a thermocouple was installed inside the actual quenching plate to measure the temperature behavior during cooling and to establish the manufacturing conditions of the quenching plate to ensure excellent flatness quality.

Oct 1, 2019

By Rafael Abreu Fraga, Carlos Noberto Paula da Silva, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Since 2016 Gerdau Ouro Branco has been producing steel plates of various qualities and grades. However, it was not until 2018 that the first plates produced by accelerated cooling process were made available for external testing, in this case for large diameter UOE pipes manufacturing. Recent line pipe and OCTG specifications are showing that the oil and gas market still consumes regular API grades, such as X60, X65 and X70, however with increasing wall thicknesses, reaching values up to 1.5 inches. These specifications also demand longitudinal and transverse tensile guarantees and drop weight tear tests in temperatures as low as -40°C. Projects with these types of mechanical properties present process requirements as challenging as those necessary for higher API grades in lower thicknesses. This paper shows the steel design concepts and rolling routes for achieving the necessary properties for X70 steel plates in 28.15 mm. The microstructural features were also investigated and associated with the production process and the tensile and toughness results. Finally, challenges such as tensile anisotropy and DWTT abnormal fracture are presented.

Oct 1, 2019

By Osvaldo Guilherme Comineli

While the hot cracking of Cu-containing steels is a serious and widely known problem for the industry, the literature reports that copper only slightly impairs the hot-ductility measured in laboratory. A distinction is drawn between hot ductility and hot shortness and the respective cracking operating mechanism involved at the respective range of temperature. The representability of the laboratory assessment of hot cracking of Cu-containing steels by hot tensile tests compared with actual results in industrial practice is discussed. The effectiveness of the variable affecting in each cracking mechanism and respective temperature range, focused in improving the hot cracking assessment of Cu-steels and the relative importance of oxidation will also be discussed. It is concluded that the hot tensile test in argon might be a good simulation if properly interpreted and that the role of oxidation is secondary in causing hot shortness. A schematic diagram for the hot tensile test is proposed.

Oct 30, 2017

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By John Hinton

Electromagnetic based (EM) sensor technology has been shown to detect changes in the magnetic permeability of steel strip travelling down the run out table after rolling. Measuring below the Curie temperature, these changes can be interpreted in terms of the phase transformation from austenite (paramagnetic) to ferrite (ferromagnetic). These real time measurements provide a detailed insight into the changes in the structure at high temperature providing the steel producer with feedback on quality control, product consistency and product development. However unlike mill microstructure models, the sensor measurement provides a point reading at a distance through the cooling course. To map the transformation in more detail, a sensor array is required along the length of the Run Out Table i.e. to measure points on the austenite to ferrite transformation curve. This paper describes the process and metallurgical factors that should be considered in the optimum design of a sensor array, i.e. the number and location of the sensor heads. Examples of cooling strategies for different steel grades e.g. low carbon, structural and dual phase steels are used to demonstrate the importance of sensor location. In addition, the effect of variability within typical industrial parameters e.g. cooling speed, on the sensitivity of sensor output and location will be considered.

Oct 1, 2019

By Mirko Jurkovic, Thomas Hueper, Jens Kempken

The high competition scenario pushes the steel producers business. Zero defect requirements from customers force the operators for additional efforts in process control and quality management. PQA® has been developed as an advanced process and quality management assurance solution. It is focusing on the analysis of process data, equipment information, inline quality measurement devices and trend analysis. The paper describes the structure of the advanced process and quality management assurance solution PQA®; it gives insights on the expert know-how, process and quality evaluation and points out the benefits like cost reduction, improvement yield and customer satisfaction increase.

Oct 1, 2019

By Luiz Bruno de Oliveira Araujo, Luciano Morais Teixeira, Luiz Gustavo Pedrosa de Melo, Altair Lúcio de Souza

The off-line simulation of the metallurgical process in an industrial line brings several benefits such as: evaluation of the influence of the main parameters that affect the results of the process, comparison between different set ups, greater assertiveness in operational adjustments, process optimization and reduction tests for development of new products. With this objective, a software for offline simulation of the hot strip mill process of Gerdau Ouro Branco was developed based on the logic of calculations implemented in the online model. The software results in important process variables such as mill pass scale, load, torque, and power at each pass, temperature and the hot mean flow stress of the simulated material. During rolling mill process the strip presents different temperatures and time between passes for different points along the length, which directly influences the hot strength of the product and consequently in the calculated variables, thus the calculations executed by the software were divided to three points of the strip, head, body and tail bringing the individual results to each of these positions.

Oct 1, 2019

By Evan Thomas

It has been shown before that liquids can slip at a solid boundary, which prompted the idea that parallel-surface bearings can be obtained by the use of alternating slip and non-slip regions in the direction of fluid flow. The amount of slip at the wall depends upon the surface tension at the liquid - solid interface, which in turn depends on the chemical composition of the surface and its roughness. In the present study a heterogeneous surface was created by coating half of a circular glass disc with a coating repellent to glycerol. A rotating glass disc was placed at a known distance above the coated stationary surface and the gap was filled with glycerol. With the top surface moving in the direction of slip to non-slip region, a pressure build up can be theoretically predicted. The pressure gradient in the two regions is constant, similar to that in a Rayleigh step bearing, with the maximum pressure at the boundary. In order to accurately measure the force generated by the pressure increase, a load cell was attached to the heterogeneous disc. Experiments were conducted by varying both sliding speed and distance, and the resultant load carrying capacity was measured and compared with theoretical calculations. This allowed the slip coefficient of the coated surface to be evaluated.

Jul 31, 2018

By Jose Maria Rodriguez-Ibabe, Ronaldo Antonio Neves Marques Barbosa, Douglas Glenn Stalheim

Major costs in the production of both flat and long commodity grade structural steel products include alloy, labor and energy. Flat and long commodity grade structural steels such as ASTM A36, ASTM A527Gr50, S235, S275, S355 and other equivalent world societal standards represent over 500 million annual tons worldwide. These simple commodity grades consist of a minimum of three base common alloying elements, carbon, manganese, silicon and then can be supplemented with microalloying elements of either vanadium or niobium. Since 2016 raw material costs for two of the five alloying elements in these commodity grade structural steels, FeMn and FeV, have risen significantly and/or have become volatile making it difficult to maintain stability in profitability for these commodity grades. For steel plants producing hundreds of thousands and in some cases over a million tons annually of these common structural steel grades because of the significant alloy cost increase for Mn and V alloy additions has squeezed profitability of these grades. These grades typically represent the base loading for cost controls in most all steel plants and hence a significant cost increase or volatility in two of the five elements used for these grades having a negative effect on overall production costs. However, with a proper strategy for alloy designs working in conjunction with the mills existing processing capabilities to achieve the desired end metallurgy/mechanical properties, alloy costs and operational efficiencies can be realized.

Oct 1, 2019

By Jan Knobloch

Inter Stand Cooling (ISC) can increase productivity of a HSM and improve final mechanical properties of the strip. Constant Target Exit Temperature can be ensured for the whole strip length eliminating skid marks and other temperature oscillations of the transfer bar. The paper deals with advanced control module of ISC. Essential mathematical models of the control system is introduced and basic functionality is explained. Temperature model is based on FEM. Mechanical and thermal properties of the strip are calculated from chemical composition using neural network. Further on an experimental possibilities for investigation and design of ISC cooling headers will be shown. In conclusion practical experience with ISC on various HSM will be discussed.

Jul 30, 2018

By Antonio Adel dos Santos, Carmos Antonio Gandra, Fabricio Mazola da Silva Paiva, Vicente Tadeu Lopes Buono

Abstract Usiminas Steel Plant in Ipatinga installed an accelerated cooling device named CLC (Continuous On-Line Control) in 2010, enabling it to supply steels produced by TMCP (Thermo Mechanical Control Process) technology. This technology complements the TMCR (Thermo Mechanical Control Rolling), with the inclusion of the accelerated cooling process after controlled rolling. There are various gains in terms of quality and productivity associated to the application of such technology. However, the flatness control for API steel becomes crucial because large thermal stresses may be generated due to thermal heterogeneity during the fast cooling when the austenite phase decomposes mostly into ferrite and bainite. In literature, there is lack of knowledge regarding a full understanding of the relation among cooling conditions and plate flatness. Therefore, this work has focused on the effect of the cooling strategy for API steels, aiming at optimizing flatness and keeping the mechanical properties within the specified ranges. The starting point was dilatometer simulation, where cooling conditions such as start cooling temperature, SCT, finish rolling temperature, FRT, and cooling rate, CR, were changed in order to evaluate their effect on microstructure. Those laboratory conditions supposed to give the best results were transposed to industrial scale, so as to produce experimental lots of plates with five different cooling strategies. It was shown the possibility to find a cooling profile that guarantees the balance between mechanical properties and flatness requirements. The influence of cooling strategy on flatness was explained by the varied heat transfer regimes occurring from hot steel surface to the ambient

Oct 1, 2019

By Bruno Kneipel Neto, Mylena Inaiê Correia, Fabricio Cerqueira, José Francisco da Silva Filho

The automotive industry, when aiming to increase the resistance to corrosion, uses in the Body in White (BIW) concept the galvanized steels. The hot-dip galvanized steels that stand out most are known as GI steels. They are formed by the zinc element and by phases of intermetallic intermediate iron-aluminum-zinc compounds. The characteristic properties of the GI coating are directly related to the formation of the intermetallic layer, which is responsible for providing the connection between the metal substrate and the coating layer. In this context, two different types of steel (SAE1005 and TRIP780 steel) were used for laboratory characterization of their intermetallic layers through metallographic techniques. The results of the tests showed that the inclined section metallographic inlay technique allows obtaining a larger region of analysis of the intermetallic layer. For the surface analysis, it was observed that the chemical solution used in the preparation of the samples was effective, making possible an analysis more specific about the intermetallic layer formation, distribution and morphology.

Oct 12, 2019

By Henara Lillian Costa

This paper aims to investigate the effects of a possible incorporation of ethanol to the lubricant during engine use on friction and lubricant film thickness, by adding small amounts of ethanol to Group I base (with and without an organic friction modifier) and to formulated oils. Film thickness was measured using ultrathin film interferometry. Friction tests were carried out using a mini-traction machine to obtain Stribeck curves. The film thickness measurements showed that in the region of low speeds, where the elastohydrodynamic film is very thin and therefore boundary lubrication may prevail, the addition of ethanol produced some boundary film, which was not present for the base oils. For the base oil with an organic friction modifier, the presence of ethanol increased the thickness of the low friction boundary film. For the formulated oil, the addition of ethanol reduced film thickness in all lubrication regimes. The friction tests showed some friction reduction due to addition of ethanol to the base oil, in particular at low speeds. For the formulated oil, the addition of ethanol reduced friction at high speeds, which was associated to a reduction in the viscosity of the lubricant, but at low speeds, the presence of ethanol reduced the formation of a boundary layer, increasing friction. For the base oil containing an organic friction modifier, the presence of ethanol increased the range of speeds for which low boundary friction occurred.

Jul 31, 2018

By Hiago Antunes Amador de Oliveira, William Pratt Rogers, Aaron Young

Monitoring systems are highly critical components in the safety of tailings storage facilities (TSF). Internet of things (IoT) platforms present a unique way to improve TSF monitoring systems. Since there are so many available IoT technologies, this conference paper aims to create a focused list of IoT options for improving TSF safety. To achieve this aim, a brief qualitative review of available literature and state of the art technologies is presented in Section 2. The article further assists this aim by summarizing the benefits of IoT platforms which have been found in the literature. With respect to findings, literature suggests that while sensor technologies have existed as solutions for tailings dams for many years, IoT greatly reduces the cost of deploying, monitoring, maintaining, and gaining insight from these sensors. Additionally, IoT removes the need for manual data collection from sensors, enabling the monitoring of tailings dams from miles away and the use of new sensor technologies. Therefore, as a conclusion, this article recommends that IoT capable monitoring systems be considered for use in TSF monitoring.

Oct 3, 2019