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By T. Christos

The explosive oils, nitroglycerin (NG) and ethylene glycol dinitrate (EGDN), were extracted from dynamites by a halocarbon solvent and were then determined by high-pressure liquid chromatography. Separation was achieved by liquid-liquid chromatography on a column packed with Durapak-Carbowax 400/Corasil II and the eluted NG and EGDN were detected with a double-beam ultraviolet detector.

Jan 1, 1973

By R. L. Grayson, S. S. Peng

"Research has been conducted during the past year on a study to correlate respirable coal mine dust characteristics with worker positions and coal seams. The first characteristic of respirable coal mine dust which has been addressed in the correlation study is respirable dust mass concentration. In fulfillment of this objective, two mines operating in different coal seams have been selected for respirable dust mass sampling on both longwall panels and continuous mining sections. At present, sampling has been completed on the longwall panel operating in the first mine, and one half of the planned sampling has been accomplished on the continuous mining section.The first mine sampled is operating in the Pittsburgh coal seam. The average mining height is approximately 78"" with an average of 8"" of bottom shale being mined. The mine is primarily a longwall mine, and continuous mining machines are used to support the longwall.Figure 1 shows the layout of the longwall panel which was sampled. Intake air is coursed via the track heading up to the headgate area. The air splits at the headgate. Approximately 20,000-30,000 cubic feet of air per minute (CFM) is used to ventilate the longwall face and about 5,000-10,000 CFM is routed down the belt entry. Substantial leakage across the gob was noted during the sampling period. An average of 1800 CFM per 100 feet of face leaked through the shields into the gob from #1 shield to #112 shield. A substantial amount of leakage also occurred between the #1 shield and the solid rib of the headgate development panel. The path of the air used to ventilate the panel is shown with arrows in Figure 1. Direction of air flow was opposite to the coal moving direction on the armored face conveyor.A double-drum ranging shearer is used on the face to cut a 30-inch web of coal. Normal practice is to cut from the tailgate to headgate with the leading drum raised and the tail drum lowered for cutting bottom. After reaching the headgate, the shearer is reversed and both drums are lowered for a clean-up pass. The last 40 feet of face on the tailgate is cut on the clean-up pass.The shearer is equipped with 2 banks of 4 water sprays each and 2 large sprays on the headgate end and 1 bank of 4 sprays on the tailgate end. Additionally, sprays are located above bits on the cutting drums. Actual cutting speed was approximately 14-18 feet per minute, depending on conditions.The cross sectional area for air flow on the face was approximately 60 square feet before a pass was mined and 80 square feet after a pass was mined but before the shields were advanced. The cross sectional area at the shearer was about 35 square feet.The condition of both the tailgate and headgate of the panel was good with no signs of significant roof problems. The roof conditions along the face during the sampling period were variable. At times, as much as 3 feet of drawslate fell from the roof for a span of as much as 40 shields. Generally, however, relatively local areas of falling roof were encoun-tered, usually limited to a 10-20 shield span when appearing.Ten days were spent gathering respirable dust samples on the longwall panel. Mine Safety Appliance (MSA) sampling units equipped with 10-mm nylon cyclones, pre-weighed MSA PVC filters, and constant-flow DuPont pumps were used to obtain thesamples. The pumps were calibrated at a 2 liters-per-minute flow rate. The 10-mm cyclone was selected for classifying total dust into the desired respirable fraction in order to obtain ""legally defined"" respirable dust samples for detailed physical characterization."

Jan 1, 1988

By U. E. Brown

This papery describing the mining methods employed by the Bunker Hill and Sullivan Mining and Concentrating Co. at Kellogg, Idaho, is one of a series being prepared by the United States Bureau of Mines on mining practices, methods, and costs in the United States. The Bunker Hill and Sullivan mines are situated in the western part of the Coeur d'Alene district at Kellogg, Shoshone County, Idaho. The mines were discovered during the summer of 1885 and except for two short periods of labor trouble, between 1890 and 1900, have been in continuous operation. About 575 men are employed at the mine. The production is about 1,400 tons of lead-silver ore per day. This is treated in the company's concentrator and smelter at Kellogg.

Jan 1, 1931

By A. L. Pierce

This paper describing the mining practice at the Spring Hill mine of the Montana Mines Corporation, Helena, Mont., is one of a series issued by the Bureau of Mines on mining methods and costs in various districts. Its purpose is to summarize improved methods whereby lower costs have recently been obtained. These improvements are principally the adoption of a modified sublevel stoping method of mining the use of grizzlies underground improvements in haulage, and rage bonuses. The Sprint Hill, Trine is situated in Grizzly Gulch, 3 miles southwest of the city of Helena. Helena is on the links of the Northern Pacific and the Great Northern Railways; and the East Helena smelter of the American Smelting and Refining Co. to which the concentrates from the mine are shipped, is but 6 miles east of Helena. The mine is probing 150 to 200 tons of gold ore per day, with an underground crew of about 40 men.

Jan 1, 1931

By R. V. Ramani, P. M. T. White, D. Sutton

3.1 Criteria for Selection A coal deposit has the following major characteristics: i) wide distribution as a flat-lying, thin, bedded deposit ii) stable nature of its major components and ranking characteristics such as carbon, heat content, volatile components, specific gravity, etc. iii) number of constituents and characteristics which under present regulations limit usage, such as content of ash, sulphur, sodium, etc. iv) effect of characteristics of over- and under- lying host rocks including porosity and permeability, lithology and general geology v) low value, high bulk nature. Because of the relative stability of its major components and its low unit price, coal does not require the same attention to detail as do the metal deposits. However, new regulations combined with social pressures make it imperative that more accurate information be made available concerning factors which affect the quality of coal and which may have an adverse effect on the environment when the coal is mined or burnt. The method selected for the evaluation of a coal deposit must, therefore, be flexible and sensitive enough to be used to interpolate stable parameters whose general distribution character-

Jan 1, 1974

This report was limited to a search of available literature on under- ground methods to combat acid water pollution. From this review it is evident that very little work has been done in this specific area. It is also evident that there are specific areas of mining engineering and mining related hydrology and geology that need further research efforts to solve the many water problems. They are: (A) Composition, variation and availability for oxidation of sulfur in strata. (B) Rate of oxidation of sulfuritic materials. (C) In situ limestone and its influence on underground acid drainage. (D) Structural, stratigraphic and hydrologic character of old mining areas as a basis to make decisions about adjacent new mining areas. (E) Operational changes in mining methods to prevent pollution. (F) Sealants for underground coating to exclude water from contact with pyrite to inhibit formation of the contaminants. Such a program has been initiated on refuse piles. The prime purpose of this report is to investigate those practices which have been used to regulate or control water accumulation and prevent harmful mine drainage. A supplemental purpose is to indicate those areas which need further research to prevent underground mine water pollution.

Jan 1, 1970

By Victor Himel

This report documents a systematic approach towards implementing an improved ensemble for the mine rescue team system that will protect against the hazards of mine rescue and recovery and will also afford improved performance through increased comfort and maneuverability, lighter burdens, and improved human engineering designs. In the first part (Task 1) the mine rescue team's protective needs were defined along with the test methods required to evaluate whether a particular piece of gear met these needs. Task 2 assessed existing gear against performance criteria and standards developed in Task 1. Task 3 consisted of the conceptual design and construction phases of the MRPE program. Special consideration was given to advanced concepts, materials, and equipment.

Jan 1, 1982

By Ralph L. Windrow

This paper is one of a series being prepared for and published by the United States Bureau of Mines describing methods and costs of mining and preparing sand and gravel for market at various plants throughout the United States. These papers are designed to disseminate technical information regarding the methods used. The cost tabulations represent operating expenditures only and not total costs. It is recognized that publication of total costs might in many instances cause embarrassment to individual producers as well as to the industry as a whole. On the other hand, operating costs are essential to the technical discussion and study of the methods employed. The attention of the reader is specifically called to this differentiation in order that no misunderstanding of the scope of the cost tabulations shall ensue. The Clowdy plant, with which this paper deals, is located 7 miles west of Dallas, Tex., and has a rail connection with the Texas and Pacific Railway. In addition to the rail outlet there is a paved road over which materials produced at this plant can be moved into Dallas by truck.

Jan 1, 1932

By Oliver A. Dibble

This paper it one of a series being prepared for and published by the United States Bureau of Mines, describing mining methods and costs at clay pits throughout the United States. These papers are designed to disseminate technical information regarding the methods used. The cost tabulations represent operating expenditures only and not total costs. It is recognized that publication of total costs might in many instances cause embarrassment to individual operators as well as to the industry as a whole. On the other hand, operating costs are essential to the technical discussion and study of the methods employed. The attention of the reader is specifically called to this differentiation in order that no misunderstanding of the scope of the cost tabulations shall ensue. The open-pit recovery of clay for cement plants is a comparatively simple operation in comparison with underground mining of clays; nevertheless, it represents an appreciable factor in the cost of cement manufacture. The following report deals specifically with the methods employed by the Aetna Portland Cement Co., which operates cement mills at Fenton and Bay City, Mich., in recovering clay from their pit at Corunna, Mich., on the Grand Trunk Western Railway.

Jan 1, 1932

By Robert S. Sanford

The Broughton and Ring magnetite deposits in Essex County, N. Y., are thought to be in a mineralized belt that extends from the Lake Sanford mining district to Lake Champlain and passes through the Mineville district. The country rook is syenite-gneiss, similar to that in the Mineville area. The Bureau of Mines conducted a vertical magnetometer survey of the area. On the Broughton properties there are no indications, magnetically, of magnetite in any degree of concentration. 'On the ding properties a number of sharp, localized magnetic anomalies were observed. One core-drill hole was bored to a, depth of 48.3 feet, also, to test one of the strongest anomalies. The field work was in progress from December 1943 to July 1944. Although no iron ore was intersected by' the drill hole, it showed that the amphibolite rook, at a depth of 6 to 100 feet below the surface, contained enough magnetite and iron sulfides to account for the anomalies recorded by the magnetometer survey.

Jan 1, 1949

By W. M. Myers

The U. S. Bureau of Mines conducted an investigation to determine the cause of the deterioration of Portland cement during storage and transportation , and to discover a means of preventing it . All available printed sources of information on this subject have been examined and a bibliography has been compiled . The subject has also been discussed with the leaders in the cement industry ; the present report is the result of their cooperation , and is based principally on information thus obtained . Deterioration of Portland cement during storage over any considerable period of time has long been noted ; closely related to it is deterioration of cement during transportation, which involves not only the time factor of storage but also exposure to varied climatic conditions . Deterioration in both cases is due to hydration of the cement by absorption of moisture from a humid atmosphere , or by exposure to actual rain-fall . After hydration cement possesses no cohesive power ; the degree of deterioration is directly proportional to the degree of hydration . The amount of deterioration of Portland cement during storage has been accurately determined in an investigation by the Structural Materials Research Laboratory , in cooperation with the Portland Cement Association . Cement stored in a shed in cloth sacks retained 80 per cent of its original strength after three months storage ; 71 per cent after six months ; 61 per cent after one year ; and 40 per cent after two years . The deterioration of Portland cement during storage and transportation was noted particularly in France during the World War . Information concerning cement used by the American Expeditionary Forces was furnished by Lt. Col. H. S. Spackman and Major E. C. Eckel , U. S. R. , who had charge of practically all matters concerning cement used by the A. E. F. The cement used by the A. E. F. came from the following sources : 42,000 tons was French , Swiss , and Spanish cements ; 120,000 tons was English cement ; 55,000 tons made in plants operated by the A.E.F .; 500 tons ( Not over) from America . Deterioration was most marked in cement from the first source .

Jun 1, 1922

By D. D. Bolstad

This report describes the construction and use of a direct-reading azimuth protractor (DRAP) by the Bureau of Mines for measuring fracture orientations in mines, tunnels, or other excavations having a magnetic environment. The DRAP allows a rapid and simultaneous measurement of dip and azimuth of dip of a fracture plane. The instrument is rugged, lightweight, and easily constructible from standard hardware items. The DRAP can measure dip to within ±0.5° and azimuth of dip to within ±5° of corresponding values obtained with a Brunton compass.

Jan 1, 1974

By V. A. Nieberlein

Problems of design involving the high-temperature characteristics of materials of construction have focused attention on tungsten, the metal with the highest melting point. To study the properties of this metal a method was needed to produce tungsten of high purity easily and consistently. The Bureau of Mines has made tungsten metal in massive form on a laboratory scale by hydrogen reduction of tungsten hexafluoride (WF6). Metal made in this manner had a purity of 99.99 percent or better, with reference to all detectable impurities, including gases. The process tolerated a wide variation in operating conditions, and the results with respect to total impurities as low as 0.01 percent were reproducible.

Jan 1, 1959

By V. Castranova, K. VanDyke

"INTRODUCTION A soluble mediator has been described which is released from activated rabbit leukocytes and induces histamine secretion from rabbit platelets (Barbaro and Zvaifler, 1966; Siraganian and Osler, 1971). This factor has been isolated, characterized and named platelet activating factor, PAF (Bcnveniste et. al., 1972). PAF has since been chemically identified as l-0-alkyl-2-acetyl-sn-glyceryl-3-phosphocholine (Benveniste et. al., 1979; Demopoulous et. al., 1979).PAF is a lipid mediator of broad biological activity. It causes smooth muscle contraction, contraction of lung tissue and decreased FEV 1; while enhancing capillary permeability thus causing edema (Pinkard, 1983). In addition, PAF is a chemoattractant and can lead to inflammation.PAF has been reported to stimulate the release of lysosomal enzymes, leukotriene B,, and lipid metabolites from neutrophils (Smith et. al., 1983; Shaw et. al., 1981; Lin et. al., 1982; O'Flaherty et. al., 1984). The objective of the present investigation was to further characterize PAP-induced stimulation of granulocytes and to develop a bioassay, i.e. chemiluminescence, for screening PAF receptor antagonists and inhibitors of PAP-induced activation of granulocytes. The possible use of the chemiluminescence assay to monitor PAF synthesis by human granulocytes is also described.METHODSBlood was drawn from healthy volunteers into a blood storage bag containing CPD anticoagulant. Granulocytes were partially purified by dextran sedimentation and further purified by centrifugal elutriation as described previously (Jones et. al., 1980). Granulocytes obtained by this procedure were approximately 95 percent pure. The number of granulocytes in this preparation was determined using an electronic cell counter (Coulter Model Z1, Coulter Instrument Co., Hialeah, FL). Isolated granulocytes were used to monitor membrane potential, hydrogen peroxide and superoxide release, oxygen consumption, calcium uptake and, in some cases, chemiluminescence. Studies of PAF receptor antagonists were conducted using neutrophils isolated by density centrifugation. Briefly, blood was layered onto Mono-Poly-Resolving Medium (Flow Laboratories, McLean, VA) and centrifuged at 22 °C and 300 g for 30 min. Neutrophils collected from the second band of this gradient were at least 90 percent pure."

Jan 1, 1989

This bibliography lists publications issued by the Bureau of Mines concerned with investigations on petroleum and natural gas. The items included are chosen for their continuing interest and value. It was recognized early that a list of petroleum and natural gas publications was needed for the Bureau's work, and unofficial publication of a ?straight forward? listing was begun. It was at first a chronological list; however, suggestions submitted by its users prompted a format change to show publications under broad, general topics. Author and subject indexes were developed, becoming more detailed with each new edition. This present list supersedes the ones compiled in 1949, 1952, and 1957, and several supplements, which were aside available to the public by the Library Of the Bureau?s Bartlesville Petroleum Research Center. The unofficial field publication came to be widely known nail in considerable demand by those who are primarily interested in the Bureau's publications on petroleum and natural gas so that it became, desirable to have it published as an Information Circular. It is hoped drat, this official publications will result in a wider and more effective use of the Bureau's research results which are reported in its publications.

Jan 1, 1964

[THIS bibliography lists publications issued by the Bureau of Mines concerned with investigations on petroleum and natural gas. The items included are chosen for their continuing interest and value. It was recognized early that a list of petroleum and natural gas publications was needed for the Bureau's work, and unofficial publication of a ?straight forward listing? was begun. It was at first a chronological list; however, suggestions submitted by its users prompted a formed change to show publications under broad, general topics. Author and subject indexes were developed, becoming more detailed with each new edition. This present list supersedes the ones compiled in 1949, 1952, and 1957, and several supplements, which were aside available to the public by the Library Of the Bureau?s Bartlesville Petroleum Research Center. The unofficial field publication came to be widely known and in considerable demand by those who are primarily interested in the Bureau's publications on petroleum and natural gas so that it became, desirable to have it published as an Information Circular. It is hoped that this official publication will result in a wider and more effective use of the Bureau's research results which are reported in its publications.]

Jan 1, 1964

By Robert A. Jankowski

Through laboratory and underground studies, the Bureau of Mines has evaluated the use of passive barriers (dust shields) to help confine dust generated by longwall shearers to the face area. Laboratory studies focused first on selection of the optimum barrier design, which proved to be a simple, gobside barrier (made of conveyor belting), coupled with a headgate splitter arm, which was found necessary to prevent the dust cloud from entering the walkway at the headgate end of the shearer when cutting tail to head. Further laboratory testing was done to determine whether using passive barriers in combination with different water-spray dust-reduction methods, including the shearer-clearer system developed by the Bureau, would improve dust reduction over that from using the water sprays alone. It was found that the combination of gobs ide passive barriers plus the full shearer-clearer system was most effective, and surmised that this would be especially useful in thicker seams. However, underground testing revealed that the shearer-clearer system alone was 35 pct more effective in reducing dust contamination than when used with the gobside passive barriers, and far more effective than using passive barriers with a conventional water spray system. For such an effective system as the shearer-clearer; the reduction in avail-able space over the top of the machine actually impeded system performance; this was shom1 in both eastern and western mines. But when used with comparatively inefficient water spray systems, the passive barriers, used in combination with a headgate splitter arm, provide consider-able help in reducing dust levels in the walkway.

Jan 1, 1986

By John L. Ellenberger

The Bureau of Mines investigated the occurrence of slickensides in mine roof in the Pittsburgh coalbed in a portion of the Valley Camp No.3 mine in southwestern Pennsylvania to improve the potential for prediction of slicken-sided zones and determine the orientations of the most prominent slickensided planes. Two distinct types of slickensides were identified; those which were associated with clay veins observed in the coalbed (genetic), and those which were unrelated to any visible structure (nongenetic). The study draws three conclusions: (1) Nongenetic slickensides are not the result of tectonic forces, (2) both genetic and nongenetic slickensides tend to dip at an angle of 30°, and (3) genetic slickensides tend to be alined parallel to the trend of the clay vein and usually dip toward the center of the clay vein. A schematic roof bolting plan is presented that may provide improved roof support where slickensides are present. Roof stability could be improved by supplemental bolting in the direction normal to the plane of slickensides.

Jan 1, 1979

By R. L. Grant, R. W. Van Dolah, N. E. Hanna

An experimental investigation was conducted to assay the relation between natural gas concentration and ignitibility of the gallery atmosphere . Both the gas concentration representing maximum ignitibility and the relationship between certain properties of the explosives and their incendivity are discussed . The data show that variation in the natural gas content in the gallery can have a highly significant effect on ignitibility of the gallery atmosphere ; maximum ignitibility of the atmosphere by permissible explosives occurs with approximately 8.1 percent natural gas . The study also shows that incendivity of a permissible explosive cannot be determined only by its detonation velocity , oxygen balance , or ballistic mortar strength . However , for similar type explosives , trends observed indicate that their incendivity increases with detonation velocity or bulk strength . Additionally , for underoxidized explosives studied here , the more negative the oxygen balance the less incendive was the explosive within a class defined by salt content .

Jan 1, 1963

By John C. Edwards

Carbon monoxide (CO) sensors are used in mine fire early-warning systems. Experiments were conducted by the U.S. Bureau of Mines with six diffusion-type CO sensors to determine their response to a reference CO concentration under both static and dynamic flow conditions. Static experiments were conducted with 0.5 L/min flow of 16 ppm CO in N2 through 8-and 12-L chambers. Dynamic flow experiments were conducted in two environmental chambers: One had directional flow capability of 1 m/s, and the second provided moderately nondirectional flow as high as 1.8 m/s. Reference CO concentrations of 13.5 to 19 ppm in air were used for the dynamic experiments. The results of the static experiments demonstrated that the sensors consistently underestimated the reference gas concentration. The dynamic experiment results showed the sensors provided reasonable agreement with the reference gas concentration when directional flow effects were not considered. Directional flow effects were evaluated for two sensors. One of the sensors showed a strong dependence upon the relative orientation of the diffusion tube with respect to flow direction. The second sensor did not show a dependence upon flow direction. The sensors' directional flow effect is significant for their proper in-mine utilization.

Jan 1, 2010