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By G. W. Jones

Phthalic anhydride is a solid having the formula C8H4O3. It is an important intermediary in production of anthraquinene, alkyd reins, and plasticizers. The combined annual production of phthalic anhydride reported by 10 major manufacturers for 112,250 tons. The raw materials in the manufacture of phthalic anhydride have been the source of numerous fires and explosions. Consequently, the need was felt to determine the temperature flammability and the ignition temperatures crude basic raw material in most phthalic anhydride production crude phthalic anhydride, and pure phthalic anhydride.

Jan 1, 1950

By L. B. Berger

"Additions to List Published in Information Circular 7444 NEW APPROVALSThe following respiratory protective devices have been approved by the United States Department of the Interior, Bureau of Mines, since Information Circular 7444 was issued (March 1948):Gas Masks Approved Under Schedules 14, 14A, 14B) 11+D, and 14E Type N: Universal Gas MasksUniversal gas masks with filters that afford respiratory protection against smoke from ordinary fires and limited respiratory protection against dusts, fumes, mists, and fogs but do not afford respiratory protection against the toxic smokes of warfare.Willson WUG-Nl universal gas mask. Approval BM-1443, issued to Willson Products, Inc., May 25, 1948.Bullard universal as mask. Extension of approval BM-1443, issued to E. D. Bullard Co., January 12, 19 9.Supplied-air Respirators Approved Under Schedules 19 and 19A Type C: Air-line Respirators4. METCO air-line respirator. Extension of approval BM-1920, issued to Metallizing Engineering Co., Inc., December 8, 1948.Type CE: Abrasive Blasting Helmets, Hoods, or Masks9. M.S.A. abrasive mask. Approval BM-1920, issued to Mine Safety Appliances Co., April 30, 1948."

Apr 1, 1949

By Christopher C. Jobes, Alan G. Mayton, Farid Amirouche

Based on prior mine vehicle studies of operators’ exposure to whole-body vibration, researchers from the National Institute for Occupational Safety and Health (NIOSH) evaluated four seat designs on mine haulage vehicles, with regard to roadway-induced jarring/jolting and operator comfort. Investigators collected objective and subjective data from vehicle operators on two existing and two NIOSH seat designs. This study included time and frequency response data using accelerometers and a data recorder, operator perceptions of jarring/jolting and discomfort levels using a linear visual analogue scale, and data from a questionnaire developed for this study. Results from the analysis of subjective data show that operators generally favoured the NIOSH-designed seats over the existing seats. The results of analyses from the absorbed power method and the threshold limit method, based on ISO 2631-1 (ISO, 1985), support the premise that NIOSH seat designs are superior to the existing vehicle seat designs on both models of mine shuttle cars used in the study. The NIOSH seat designs, featuring viscoelastic foam padding, were more effective in reducing vibration energy for operators exposed to vehicle jarring/jolting. In this paper, the performances of the NIOSH and existing seat designs are compared relative to the operator’s exposure to vehicle vibration (mainly jarring/jolting).

By Fred N. Kissell

A parachute-type stopping intended for changing the course of mine ventilation air during mine emergencies has been designed and tested. Some production uses are also visualized for metal mines. Preliminary tests in the laboratory and underground indicate that the parachute stopping is a workable concept, but further developmental research is required.

Jan 1, 1975

By C. G. Kirkland

An apparatus for determining trace impurities in Grade-A helium by mass spectrometer methods was designed and built by the Federal Bureau of Mines. Grade-A is the designation for helium commercially produced by the Bureau. Its nominal purity is 99.995 percent. The device, following a suggestion by Deaton, concentrates the impurities in the helium by freezing them out in a coil-and-trap assembly cooled by liquid helium. A known volume of helium is passed through the trap, the concentration ratio determined, and samples of the concentrated impurities are analyzed by mass spectrometer methods. The apparatus has been in service for approximately 20 months and has satisfactorily met all requirements. Over 200 analyses were made of helium contained in conventional cylinders, obtained from the Amarillo, Exell, Otis, and Navajo Helium Plants, during the 6-month period ending March I, 1959. Total impurity concentrations, in parts per million, were as follows: Amarillo, 19.1; Exell, 17.1; Otis, 11.3; and Navajo, 6.6. Neon and nitrogen were the major impurities. Complete data are shown in table 4 in the body of this report.

Jan 1, 1960

By S. H. Denny

"As the result of the work of an efficient safety organization, the Midwest Refining Co. at its various operations and particularly in the Salt Creek field has been able to show a definite accident reduction. Lost-time accidents during the past year have been reduced to a small number as compared with previous years, and infection cases have been almost eliminated.The accident-prevention work of the Midwest Refining Co. is in charge of the department of industrial relations, with a director as the administrative head; two safety men handle the work directly at Midwest, Wyo. A competent medical staff with a well-equipped hospital at Midwest is also an important factor in the prompt and proper treatment of injured persons when an employee is injured, he is given first-aid and then taken to the hospital with minimum delay.About 1,450 persons are employed in the 4 departments (production, gas, pipe lines, and electrical) and in the 34 districts of the Midwest Refining Co. The work at Midwest spreads over a considerable area, and new drilling operations, pipe work, and similar activities require the services of many small gangs of workers. Complete supervision, of each job, whether shall or large, is possible through the large number of superintendents, foremen, and gang pushers employed; thus, there are 20 superintendents, 78 foremen, and 115 gang pushers. The largest number of men under any one toss is approximately 15, and it is probable that much of the good safety record is due to this intensive supervision. These company officials, including the gang pushers, have been impressed with the idea that it is their duty to see that the men under them do not get hurt; the responsibility of instructing new employees in safety practices is placed directly upon them. Monthly meetings of the field officials, including superintendents, foremen, and gang pushers, and as far as possible the men, of each district are held with the safety engineer. Both officials and men are encouraged to bring up for discussion any practice or proposals looking to the changing of any conditions that will"

Apr 1, 1928

By R. V. Lundquist

The work described in this report, part of the Bureau of Mines long-range program to develop methods of utilizing submarginal domestic sources of aluminum, was undertaken to investigate the effects of iron in the lime soda sinter process, The approximate Fe2O3 content in a sinter for maximum alumina and soda recovery was 8 to 9 percent. Fe2O3 appears to inhibit gelation, and 15.5 percent Fe2O3 produces effects similar to those produced by 1 percent sucrose. In the lime soda sinter process, aluminum silicates are sintered with limestone and soda ash to yield dicalcium silicate and sodium aluminate. The sodium aluminate is extracted by leaching in caustic solution. The solution is purified by heating in an autoclave with lime to remove silica, and alumina trihydrate is precipitated with carbon dioxide. The reactions involved in sintering and leaching are complex. A number of studies by the Bureau of Mines4-9 and others1 indicate that the iron content of sinters influenced the recovery of alumina and soda and the gelation characteristics.

Jan 1, 1962

By Annie G. Smelley

The Bureau of Mines, U.S. Department of the Interior, as part of its mission to effect pollution abatement, conducted research to devise means for disposing of phosphatic clay wastes and reclaiming mined land. Part of the investigation was performed in a cooperative research project with 10 phosphate companies in Florida. The colloidal properties of the phosphatic clay suspensions, called slimes, make them difficult to dewater and dispose of without impoundment storage aboveground. Various reagents to flocculate and dewater these plant wastes were evaluated, and a polyethylene oxide polymer was found to function in a specialized flocculation dewatering technique. The flocculation dewatering method was investigated in bench-scale batch tests and applied in continuous dewatering tests using standard mineral-processing equipment. In continuous tests at feed rates of up to 58 liters per minute, wastes at 4 percent solids were dewatered to about 20 percent solids. About 0.8 kilogram of polymer was used for each metric ton of dry waste clay solids; processing time was about 4 minutes. Requirements for the treatment system are (1) proper mixing of the clay-waste feed and flocculant, (2) rapid removal of water as it is released, and (3) physical manipulation to promote cohesion of solids.

Jan 1, 1979

By Jr. Taylor

The following heats of solution have been measured in 1.160 molal H2SO4 at 25° C: AH298, kcal./mole Be(c) + 77.44(H2SO4?47.849 H2O) H2(g) + BeSO4 (soln) -92.83 ± 0.11 BeSO4 ?(c) + 77.44 (H2SO4?47.849 H2O) BeSO4(soln) -16.45 ± 0.02 BeSO4?2H2O(c) + 77.44(H2SO4?47.849 H2O) BeSO4?2H2O(soln) -5.395 ± 0.019 BeSO4?4H2O(c) + 77.44 (H2SO4?47.849 H2O) BeSO4?4H2O(soln) 1.513 ± 0.010 Combining these data with other experimental results and data taken from National Bureau of Standards information yielded the following heats of formation at 298° K:

Jan 1, 1966

By C. M. McKinney

Sulfur content data from Bureau of Mines routine analyses of 1,060 United States crude oils were used with crude oil production data for the years 1956-66 to prepare tables and charts that illustrate the volume and percentage distribution according to sulfur content of crude oil produced in 10 geographical areas of the United States. Similar relationships for foreign crude oils based on analyses of 201 crude oils and production during 1966 are illustrated for Africa, Canada, Middle East, and South America. Tables are included giving field name, sulfur content, geologic name and age of producing formation, depth of producing formation, and production during 1966 for 882 United States crude oils and 201 .foreign crude oils. Between 1955 and 1966 the average sulfur content of crude oils produced in the United States decreased from 0.73 to 0.67 percent.

Jan 1, 1967

By V. E. Erwin, W. W. Adams

"INTRODUCTION This report presents statistics of accidents at coke ovens in the United States during the calendar years as 1933, the twenty-first year for which data of this kind are available, 1913 being the first year for which accident reports were collected from the operating companies by the Bureau of Mines. The present report is presented in mimeograph form because insufficient funds are available for printing it. The first report of the Bureau of Mines that contained statistics of accidents for the coke-mining industry in the United States covered the two calendar years, 1913 and 1914. While the figures presented therein related both to beehive and by-product ovens, the original returns from the operating companies were not classified so as to permit the presentation of accident statistics for each class of ovens separately. Beginning with 1915, the accident reports from the operating companies have shown the general type of ovens to which the reports related; therefore, since that year, separate statistics for each of the two classes of ovens have been given in the Bureau's yearly reports of accidents at coke ovens.The coke-making industry in the United States established a safety record in 1933 almost equal in merit to that which it achieved in 1932, when the accident-frequency rate was the lowest and therefore the most favorable that the industry has known. Credit for the achievement is due almost entirely to companies operating byproduct ovens. (See table 8.)"

Mar 1, 1935

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

B 5 Typical Input - Ouput The input data and the printed output for case 8 of the simulations (Section A.4) are shown in the following. The branch, level, node, miner and hoist numbers mentioned in the input and output refer to the corresponding numbers in Figures A-3, A-4 and A -5, The plotted ouput, already shown in Figures A,11 and A-12 is not repeated. The input data shown does not include the following simulation parameters: DTIME = 0, 05 FTIME = 130 JPLT(K) = 1 for K = 1, 2, 3 0 for other K TPLSTR = 0.0 TPLST P = 130

Jan 1, 1976

By J. H. Russell

As part of its efforts to maximize resource recovery, the Bureau of Mines conducted studies to recover valuable byproducts from Western phosphate beneficiation tailings. Potential byproducts include phosphorus, vanadium, and uranium. The objective was to determine roasting and leaching conditions for maximum dissolution of vanadium from tailings containing approximately 13 pct P205 and 0.23 pct V. Sulfuric acid leaching tests were conducted with the tailings either as a dilute suspension dried, or in a roasted condition with or without NaCl added during roasting. More than 90 pct of the vanadium was dissolved by roasting at 850° C for 120 min with 8-pct NaCl and leaching at 75°C for 120 min with an excess of 2N H2S04, By roasting without NaCl and avoiding the difficulties of the chloride impurity, nearly 80-pct vanadium dissolution was achieved with an 800° C roast for 180 min. Quadratic regression equations were derived to relate vanadium dissolution to roasting and leaching conditions.

Jan 1, 1982

By C. K. Rose

A hydraulic scaling rig was placed in operation at the Bureau of Mines oil-shale mine near Rifle, Colo., in 1953. The rig consists of a self-leveling platform mounted on a hydraulic-powered boom. The boom is mounted on the bed of a diesel truck. The equipment provides a movable work platform from which two men can work in safety and comfort while barring loose rock from the backs and walls of the rooms, pillars, and haulageways. INTRODUCTION As a part of its synthetic liquid fuels program the Bureau of Mines has developed a mine in the richer oil-shale beds of the Green River formation near Rifle, Colo. An important part of the work of the Oil-Shale Mining Branch is investigation of techniques for low-cost mining of oil shale on a commercial basis. It is evident that scaling loose rock from the high backs and walls of the mine represents a portion of the direct mining cost. This paper describes the development of a scaling rig for operation in the upper heading of the mine, which is 39 feet high.

Jan 1, 1954

By John H. Scott

At the request of the Mine Safety and Health Administration, U.S. Department of Labor, the Bureau of Mines evaluated the model BT 300 C-D blasting machine tester, manufactured and distributed by Research Energy of Ohio, Inc. (REO), to determine whether the tester performed as stated by the manufacturer and responded satisfactorily to electrical faults introduced into the blasting machine circuit. Tester readings were recorded for 13 blasting machines and for 12 circuits constructed to simulate the electrical parameters of actual machines. The tester readings were acceptable for all of the blasting machines, although the switch position assigned to one machine produced an off-scale reading. The tester responded satisfactorily to the simulated circuits and detected serious voltage or capacitance faults when they were introduced. However, it did not respond accurately to certain resistance faults. Temperature tests were also made, and the tester performed equally well at temperatures of 20°, 42°, and 81° F. This tester was judged a useful accessory for field checking blasting machines for defective batteries and capacitors, despite its limitations. It is recommended that the tester manufacturer specify the lowest acceptable reading at which a blasting machine may be used and below which the blasting machine should be returned to the laboratory or manufacturer for maintenance.

Jan 1, 1981

By S. J. Hussey

The Bureau of Mines investigated the applicability of carbon-in-pulp pro-cess for recovering silver from low-grade ores. The reasons for the research were (1) to illustrate a practical procedure for the process design of carbon-in-pulp adsorption circuits using leach slurries and simple equipment; and (2) to illustrate how equations of adsorption theory relating rate data and equilibrium adsorption curves can be helpful in process design. Carbon-in-pulp silver adsorption tests were made on Banner, Idaho; mine-run ore samples with silver contents ranging from 2.0 to 8.5 oz/ton and variations in cyanide leach extraction from 48 to 93 pet. The lower recoveries were attributed to the presence of complex silver sulfide minerals. Carbon-in-pulp batch adsorption tests provided rate data for the estimation of a silver equilibrium adsorption curve. Process design procedures in which the rate data were related to an equilibrium adsorption curvey by equations of adsorption theory were used to plan a four-stage pilot plant cascade. The pilot plant was successfully operated for 45 hr of countercurrent flow, producing a carbon product containing a mean silver loading of 571 oz/ton from a pregnant solution of 1.7 oz/ton of silver. Virtually all of the dissolved silver was recovered on the carbon.

Jan 1, 1978

By Charles D. Martens

Raw non fuel minerals produced in the United States during 1981 had an estimated value of $25 billion, about the same as that of 1980. In terms of 1980 dollars. the value of minerals produced during 1981 was $23 billion.2 This chapter includes tables for 1980 that were not available for publication in the 1980 Minerals Yearbook, but does not include the corresponding tables for 1981. The underlying causes of the overall decline in U.S. nonfuel mine production during 1981 were varied, but the common factor was the worldwide recession. In some cases the decline was traced to foreign competition. For example, iron ore production was lower in part because of increased imports of steel products such as coiled steel sheet. Another problem experienced by the domestic mining industry was the continuing difficulty in attracting capital. This was due in part to the attractiveness of investments outside the mining industry, such as short-term, high-interest securities. Another reason was the importation of commodities from countries where overall costs were lower because of such factors as high ore grade, lower taxes, lower wages, government subsidies, and less stringent safety and environmental regulations.

Jan 1, 1982

By Francis Crowley

Elementary concepts of seismic wave properties are reviewed to establish a framework for discussing seismic noise and its suppression. A liberal number of references is included for those who wish to pursue the topic in detail. A base motion noise level is established for a single surface seismometer. It is argued that simple array processing and seismometer burial should regularly permit us to approach this base noise level which is found in areas free of conspicuous man-made seismic noise sources. The sensitivity of the base seismic level to a number of common disturbances is presented. Solutions that promise to hold the "effective" seismic noise at a site near the base level are given for acoustic, meteorological and fixed local surface sources. Guidelines are suggested for controlling other local man-made sources, e.g. vehicular traffic, by keeping them at sufficiently large distances away from the seismometers to keep noise at permissible levels. These guidelines are speculative and conservative. They should be the subject of future study. The ability to process against general local activity, drilling, and intra- mine sources is limited. Certainly no dramatic gain is to be expected. When strong man-made and/or intramine noise sources are not controllable, detection may well be impossible to achieve, unless the seismometer can be moved close enough to the suspected miner position, i.e. via very deep holes, to compensate for the likely vast differences in strength of the miner signal and the uncontrollable man-made noise sources. However, many intramine sources, e.g., falling water, rock bursts, explosions, etc., may well preclude the existence of a hale miner in their vicinity, and therefore any need to attempt detection of a miner at such locations. The following recommendations are made to enhance the detection and location of a miner signaling seismically. They are: 1. Seismometer burial in slim holes. 2. Narrow band detection, using multiple narrow band filters to cover the likely signal band. 3. Broadband recording and analysis for time-of-arrival estimation.

Jan 1, 1974

By A. J. Farstad, R. F. Kehrman

Characteristics of metal/non metal mines were evaluated to determine the suitability of applying the U.S. Bureau of Mines electromagnetic location system to the problem of locating trapped driers in metal/non metal mines. Statistical distributions of mine depths and overburden conductivities show that the existing USBM EM system is inadequate for most metal/non metal mines. Alternate approaches to trapped miner location in deep mines were identified and subsequent field tests were conducted at six (6) mines to evaluate their feasibility. The approach considered to be the most promising is one which utilizes the existing manpack transmitting system, modified slightly for a dual frequency output, in conjunction with a sophisticated signal processing receiver on the surface. The main advantage of staying with a "through the earth" approach is that the underground equipment can be kept simple, easily maintained, light- weight and inexpensive.

Jan 1, 1979

By Philip C. Tully

The Bureau of Mines, in a continuing effort to improve processes and methods of helium purification, has developed a differential distillation method for removing helium-3 from helium-4. Differential distillation at 4.2 to 1.6 K was used to reduce the helium-3 in helium-4 from about 200 to less than 1 part per billion. The results from four stills ranging in size from 1 to 25 liters are reported. The method has the potential to be adapted to commercial-scale separations.

Jan 1, 1975