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By J. Hudy

An investigation has been made to determine the applicability of the Cendrex3 X-ray instrument for the measurement of the ash content of washed bituminous coal products. The results obtained for selected products from six preparation plants in the Appalachian region and one preparation plant in the mid-western region are described. Emphasis of the study was placed on low-ash bituminous coal products suitable for utility or metallurgical markets. There was good agreement between the results obtained by conventional ash determination methods and by ash determination using the Cendrex for all products tested.

Jan 1, 1968

Develop and evaluate a mechanical position and heading system (MPHS) that provides information about underground mining machine position and heading to aid in the remote positioning of mining machines during face maneuvers. Background While great improvements have been made in mineworker safety, progressive technology continues to create a safer, better working environment for miners by keeping them away from the dangerous face area. In maintaining such high standards of safety, the Bureau is investigating remote, computer-assisted operation of mining systems for underground, highwall, and surface mining applications. A key component of computer-assisted operation is a guidance system. Since there are no guidance systems on any commercial continuous mining machines, the Bureau itself developed and tested the mechanical position and heading system (MPHS). The MPHS is based on linear position transducers (LPT's), and operates on principles of triangulation to provide machine position (xy coordinate), and orientation in the xy plane (yaw or heading). These data are needed in order to keep the continuous mining machine in proper alignment before and during the cutting cycle. The MPHS theory development is in three parts: characterize the sensors used and their configuration; select and define the navigation reference frames; and derive a closed-form solution for determining the position and beading from sensor information. Application of the MPHS theory required the development of hardware, software, and system interfaces.

Jan 1, 1992

By Charles A. Seitz

This Bureau of Mines report describes an automatic and continuous transducer-drift compensator. The compensator formed a part of the instrumentation used to indicate the saturation by hydrogen of a cryogenic, adsorption column. It has a variable delayed-response characteristic and will respond only to signals having rise times faster than component drift times. Zero drift due to varying ambient conditions and component aging is nullified. Equations relating the output as a function of the input signal are given.

Jan 1, 1981

By James R. FitzSimmons

This report describes an instrument developed by the Bureau of Mines as an improved device for examining roof rock in bolt holes. The unit consists of a commercially available fiberoptic unit adapted for use as a flexible stratascope. Field testing in both metal and coal mines has shown the instrument can be easily transported and used by a single operator. The size and flexibility of the instrument eliminate the need for specially drilled holes.

Jan 1, 1979

By H. H. Lowry

Abstracts of papers on low-temperature tar published since 1942 are included in this selected bibliography. Abstract journals -including Chemical Abstracts, Fuel Abstracts, and B.C.U.R.A. Monthly -have been consulted through 1957. Abstracts of papers on low-temperature carbonization are not included unless information is given on composition, economics, processing, or utilization of the tar; thus, papers reporting only yields of tar from assay tests, pilot plants, and commercial operations are excluded. Listing in the bibliography is alphabetical by authors; arrangement under each individual is chronological. Secondary authors are cross-indexed to the main entry. The subject index uses the main entries: Composition, economics, processing, and utilization with appropriate subheadings. A code letter following the abstract number indicates the country where the paper originated.

Jan 1, 1959

To cool hot working environments in deep mines more efficiently, while substantially reducing the maintenance required by presently used cooling coil heat exchangers. Approach A mine's chilled water supply cools fresh air enroute to hot working areas, in an improved, direct-mixing heat exchanger. How It Works Warm, fresh ventilation air traveling through the mine's ventilation tubing enters the lower portion of the cooler heat exchanger through a large round opening designed to accept the ventilation duct. This air flow is turned upward and evenly distributed by egg-crate lattice and pair guide vans at the bottom of the cooler. On the diagram, warm air enters at the bottom left. As the air moves upward through the cooler, it passes through a plastic or wire mesh pad which is arranged so that it offers the most resistance to upward airflow immediately above the cooler inlet: this more or less equalizes the upward air flow along the length of the cooler. The air next moves through the cold water sprays, and then through a wire-mesh demister pad before exiting from the cooler at the top right. Cooling of the air is accomplished in several stages. As the incoming air passes through the lower plastic or wire mesh pad, it is exposed to water flowing downward through the pad to the water sump. This is water that has fallen from the sprays or dripped from the upper wire-mesh mist eliminator. This water is slightly warmer than the spray water since it has already done some cooling,

Jan 1, 1981

By S. J. Broderick

[The authors gratefully acknowledge the assistance of O. C. Ralston, chief engineer, Nonmetals Division, Bureau of Mines, Who suggested the problem and Gave valuable aid during the course of the work. Thanks axe due also to Will H. Coghill, supervising engineer of the Southern Experiment Station, Bureau of Mines. INTRODUCTION One phase of the general program for utilization of coal-mine waste led to the possibility of making a water softener from the material, as the waste matter contained both coal and clay and. it is known that both these substances can be so activated as to exhibit distinct base-exchange properties. The carbonaceous]

Jan 1, 1941

By Alan R. Buehler

In 1986, at the request of the U.S. Bureau of Land Management, the U.S. Bureau of Mines studied part of the 256,430-acre Alvord Desert and part of the 22,240-acre East Alvord Wilderness Study Area (OR-002-074 and OR-002-073A, respectively), in order to evaluate their identified mineral resources. The study areas are located in Harney and Malheur Counties, OR, about 25 mi northeast of the small village of Fields. There are no mines, prospects, or identified mineral resources inside the study areas. Basalt flows within the study areas contain chalcedony-lined vugs and banded agate which may be of interest to rock hounds. An ignimbrite flow contains perlitic material, but crystalline contaminants make it unsuitable for commercial uses. Lacustrine (lake) sediments contain diatomite and clays, and evaporite crusts contain boron too low grade to profitably mine. Small quantities of common opal and petrified wood occur which might be of possible interest to rock hounds. Some of the petrified wood is black, free of fractures, and polishes well; it may be suitable as backing material for soft, thin, and brittle gemstones, such as precious opal. The lacustrine sediments also contain black, fetid layers which have above background, but economically insignificant concentrations of zinc, cobalt, nickel, barium, iron, manganese, aluminum, and potassium. Large quantities of fine-grained dune sands within the study areas are too far from markets for economic consideration. Ephemeral streams in the study areas contain small amounts of placer gold of no economic interest. The western portions of both study areas are reported to have moderate favorability for occurrences of natural gas, and both study areas are reported to have high favorability for the occurrence of geothermal resources. As of December 1986, oil and gas leases covered 3,100 acres in the study areas.

Jan 1, 1987

By H. R. O'Brien

"During the past year, the Pittsburgh experiment station of the Bureau of Mines has been investigating methods for the quantitative estimation of carbon monoxide in blood. This work was necessary because reliable methods of analysis are of the greatest importance in the bureau's research work on prevention and treatment of carbon monoxide poisoning among workers in mines and metallurgical plants. Two of the methods considered involve color comparisons. In one of these methods, differences in tint can be noted fairly readily, while in the other, they are much more difficult to detect. The latter, however, is otherwise considerably simpler. It was decided, therefore, in studying the possibilities of this second method, to use the most sensitive eyes in the laboratory force.Preliminary trials.The method under investigation was the Haldane carmine determination of carbon monoxide in blood. The plain oxyhamoglobin of the blood in dilute solution is a pale straw color, when exposed to carbon monoxide it becomes a cherry pink. In the analysis dilute indigo carmine is added to oxyhsmoglobin until the solution matches in tint the carbon monoxide hemoglobin. The eye wanted, then, was the one most sensitive to faint pinks. But just how to select the analyst was not clear At first the Williams test scale, used in the Navy, was considered, but on con¬sultation with Dr. L. L. Thurston, bead of the Department of Psychology at Carnegie Institute of Technology, the following procedure was adopted.Instead of standard tests made up of all colors, only those occurring in the analysis were used. Solutions were prepared of the two hemoglobins, from which twenty-four different pairs were made up and placed in test tubes like those expected to be used in the analysis. One of each pair differed from the other in percentage of carbon monoxide hemoglobin by amounts varying from 2-1/2 per cent to 20 per cent. Each pair was compared in a box built in our own shop. This was 20 inches long and 5 inches square in cross section. One end was covered with ground glass. Just inside this glass cover were provided two slots, each the width of the test tubes used. The tubes to be compared were dropped into these slots through two holes in the top of the box. The device was placed before a window away from the sun, and so arranged that the light conditions were the same on each slit or opening. The person to be tested was seated before the box, and as the two tubes were placed before him side by side, he marked whether A (left) or B (right) contained the more cherry pink. This procedure was continued till he had compared all the pairs."

Jul 1, 1921

By S. J. Broderick

[One phase of the general program for utilization of coal-mine waste led to the possibility of making a water softener from the material, as the waste matter contained both coal and clay and it is known that both these substances can be so activated as to exhibit distinct base-exchange properties. The carbonaceous]

Jan 1, 1941

By David E. Emerson

An improved method and apparatus for determining the impurities in helium by preconcentration and subsequent analysis by mass spectrometry are described. Preconcentration of the impurities is accomplished by passing a known volume of helium, at slightly above atmospheric pressure, through a metal coil and trap assembly immersed in liquid helium. The concentrated impurities are then analyzed by mass spectrometry. This method can detect impurities in the range of 0.01 to 600 ppm with an accuracy of better than ±0.05 ppm at the 1-ppm level. One operator can analyze 15 samples in an 8-hour day.

Jan 1, 1970

Provide an accurate, simple, alternative means of evaluating the safety of mine electrical ground systems which has little or no negative impact on mine productivity. The Traditional Evaluation Method The Code of Federal Regulations requires all mines to safely ground their power systems to earth. Effective earth grounding reduces shock hazards to mine workers operating electrical equipment, protects equipment from damage by voltage transients, and provides a means of detecting and locating ground faults. Once an earth ground bed has been constructed, its level of resistance has traditionally been used to gauge the safety of the entire grounding system. Bed resistance measurements are normally performed using a ?fall of potential? technique with a current return electrode placed at a remote location, If the resistance measured is acceptably low, then the bed is assumed safe.

Jan 1, 1985

By Claude W. Sill

In the course of a series of investigations on vanadium deposits of the western United States, the Bureau of Mines collected many hundreds of samples for chemical analysis. As uranium is often associated with these vanadium minerals, they were also analyzed for uranium, which was pound to be absent in a large percentage of the samples. Since the usual methods for determining uranium are laborious and time-consuming it is very desirable to have some simple qualitative test that can be applied prior to a quantitative analysis to determine whether uranium is present or absent and thus save the time and expense of applying the quantitative analysis to the large proportion of samples containing no uranium. To be acceptable, the test should be specific for cranium, sensitive enough to detect small amounts of uranium, and. simple enough to make it worthwhile to apply. The available methods for detecting uranium lacked one or more of the desired characteristics. Eventually, however, a method was worked out that satisfied all the requirements. This method is probably more specific and sensitive than the usual qualitative methods for uranium, and its simplicity and speed of application make it ideal for testing samples prior to quantitative analysis.

Jan 1, 1945

By W. B. Berwald, T. W. Johnson

"The United States Bureau of Mines, in cooperation with the Natural Gas Department of the American Gas Association, has been studying actively for the past several years the flow of natural as through high-pressure pipe lines. 4 This report deals with that part of the study involving the design of pipe-line systems consisting of lines laid parallel to each other. The lines are referred to as the original line and the parallel line. The paralleling lire may or may not extend the entire length &f the original line; however, the parallel line is connected at its two ends to the original line.As a result of the large expansion of the natural-gas industry almost all markets within economic distance, from the developed as fields have at least one pipe line supplying them with natural gas. Small increases in the consumers' demand for natural-gas can be met usually by increasing operating pressures, but any marked increase in demand necessitates paralleling sections of the existing systems. It is believed that to a large extent future expansion in the natural—gas industry will consist of paralleling the present lines. The several formulas given in this report have been developed to aid in the design of such systems. Curves and tables were prepared from these formulas to simplify the calculations materially and to facilitate determination of the sizes of pine to be used in paralleling various diameter lines to give the most economical design. The formulas are presented without detailed derivations, as a complete report on the flow of natural gas through pipe lines is being prepared which will contain the derivations of these formulas. Examples included here show the detail of application of the several formulas to problems of design of parallel lines."

Jun 1, 1934

By D. Harrington

Near the close of the nineteenth century electricity was introduced underground, and the mining industry automatically was confronted with another potential source of fatalities and injuries to mine workers. Electricity has become an increasingly vital factor in the production of goal, particularly in recent years, because of the greatly extended mechanization that has taken place underground. The enlarged use of electrical equipment for cutting, loading, and hauling coal unquestionably increased the potentiality of shock and explosion hazards underground. Electricity may be used in coal mines with minimum danger if electric equipment and power-carrying wires are chosen properly and installed and kept protected by proper safeguards; on the other hand, if vigilance is relaxed in the slightest degree accidents may result. Electrical accidents are caused chiefly by direct contact with electrical equipment or power-carrying wires, by ignition of explosive gas or dust, and by fires of electrical origin. Electricity now ranks fourth as a cause of coal-mine fatalities, not including deaths from explosions or fires of electrical origin.

Jan 1, 1936

By Harry W. Campbell

A mineral survey by Bureau of Mines personnel identified no mineral resources or mineral occurrences with development potential at prospects in the Mecca Hills Wilderness Study Area (WSA). Bentonite occurrences are in Skeleton Canyon and Surprise Canyon. Sand and gravel occurrences are numerous in and near the WSA. Much of the Mecca Hills WSA was leased for oil and gas exploration in 1983. No current mining claims or other leases were found in the study area. The Skeleton Canyon Clay Mine yielded clay to seal irrigation canals, Clay to seal ponds was also mined from the Red Top Clay Mine west of the USA. A sand and gravel pit south of the study area (near Box Canyon Wash) supplied material for local construction projects. A commercial sand and gravel pit was operating in 1983 near the mouth of Thermal Canyon 4 miles west of the WSA.

Jan 1, 1984

By J. C. Franklin

The Bureau of Mines substantially reduced shale degradation in a coal mine by two spray coat applications of a water-base epoxy sealant. More than 12,700 square feet of passageways were treated, and in 18 months only one failure occurred. This failure was due to improper spray application, Material costs averaged 13 cents per square foot, and labor costs were 7 cents per square foot. Labor included moving all materials into the mine, the setup time for each of the areas coated, and application of coatings.

Jan 1, 1977

By N. S. Dalal, X. Shi

"It has been recently suggested that the exceptionally high antitumor and antibacterial activity of natural fredericamycin A (FMA) is related to its ability to spontaneously generate the superoxide anion (02-) and hydroxyl (""OH) radicals in aerobic solutions [Hilton, B. D., Misra, R., & Zweier, J. L. (1986) Biochemistry 25, 5533]. With a view to understand the mechanistic details, attempts were made to reproduce earlier electron spin resonance (ESR) evidence for the oxygenated free radical formation in well-aerated solutions of natural FMA in dimethyl sulfoxide and dilute H 20 2• Little or no evidence was obtained for the formation of the 0 2- and methoxy (""OCH3) radicals, while the detected formation of the 'OH and methyl ('CH3) radicals was attributable largely to mechanisms not involving FMA. These results thus reopen the T question regarding the mechanism of its exceptionally high tumoricidal-bacteriocidal activity. This paper reports on an electron spin resonance (ESR) investigation of the formation of oxygenated free radicals in solutions of natural fredericamycin A (abbreviated as FMA) which has recently been reported to be a highly potent anti¬tumor antibiotic (Pandey et al., 1981; Warnick-Pickle et al., 1981). The impetus for this undertaking was provided by recent reports (Hilton et al., 1986; Stinson, 1986) suggesting that the strong tumoricidal activity with high therapeutic—toxic index of FMA was related to its ability for the spontaneous generation of superoxide anion (02-) and hydroxyl (OH) radicals. For example, the suggested mechanism for the formation of 02- by FMA was (Hilton et al., 1986)FMA-OH + O2 FMA-O + H+ + 02-Here FMA—OH is simply the FMA molecule emphasizing the —OH moiety which becomes FMA-O, the free radical rep¬resenting the oxidized form of the drug. While some other highly effective anticancer drugs in current clinical application, such as bleomycin, are also thought to exert their antitumor effects via the formation of reactive drug-based or oxygenated free radicals (Carmichael et al., 1985; Gianni et al., 1983), FMA was considered unique in that only in this case the free radical formation was thought to be spontaneous, rather than through a metal- or an enzyme-activated process (Hilton et al., 1986; Stinson, 1986). Thus it was suggested (Hilton et al., 1986; Stinson, 1986) that FMA could be the forerunner of a new class of anticancer drugs. However, we noted that while the hypothesis seemed plausible, the reported ESR spectral evidence appeared to be ambiguous. Because of the high significance of the earlier conclusions (Stinson, 1986), we undertook a systematic ESR study of the radical formation in FMA solutions, and as discussed below, our conclusions disagree with those reported earlier."

Jan 1, 1989

By W. E. Miller, John Campbell, W. P. Yant, G. W. Jones

"Because of its interest in accident prevention, the U.S. Bureau of Mines cooperates with city officials and utilities in investigating the causes of explosions in sewers, manholes, and other underground openings and in developing means for preventing such explosions. For several years this Bureau has been cooperating with the Edison Electric Illuminating Co. of Boston and the Boston Consolidated Gas Co. in detecting and eliminating combustibles and physiologically harmful gases in manholes in the city of Boston and adjacent territory.These Bureau of Mines investigations° have shown that combustible gases from the usual sources — leakage from gas—distributing systems and from underground tanks and gasoline wastes — can be located and the dangerous conditions remedied by a well—planned, adequately supervised, systematic, and continuous manhole survey. However, other types of gas, which are termed here ""soil"" gases, also occur in manholes and are more difficult to eliminate because they have no fixed origin and because seasonal and barometric changes affect their production and passage into the manhole space. These gases appear to be produced by bacterial and fermentation or through reactions of entrapped air in the soil. Soil usually abnormally high in carbon dioxide and low in oxygen, and contain varying amounts of methane. They are especially clangorous to men entering manholes because they lack sufficient oxygen to support life. Owing to the difficulty of constructing gastight manholes the most feasible method for eliminating soil gases from manholes is by ventilation. Consequently the Bureau of Mines initiate 4 study of natural ventilation methods for the removal of these gases from manholes and also for taking care of unforeseen accumulations of combustible gases and vapors.The following factors were considered by the Bureau to be important to the natural ventilation of manholes: (1) Relation of area of ventilation opening* to the capacity of the manholes, (2) size and shape of the manhole, (3) design of the ventilation opening (4) and velocity, and (5) weather conditions."

Jun 1, 1936

By J. M. Riley

A fluorometric method using morin in an alkaline-buffered chelating solution has been developed by the Bureau of Mines for determining beryllium in ores and mill products. Apparatus for measuring fluorescence intensities of the beryllium-morin reaction is described. Preparation of the sample for analysis consists essentially of digestion with sulfuric, nitric, and hydrofluoric acids, fusion of the residue with sodium carbonate and sodium borate, Solution of the melt with sulfuric acid, and proper dilution. Chemical separation of other ions is usually unnecessary. The method rave reliable beryllium determinations on samples in the 0.01- to 0.37-percent BeO range. The method is particularly applicable to low-grade beryllium ores; however, semiquantitative beryllium determinations have been made on beryl containing 12.0 percent BeO.

Jan 1, 1956