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By Esteban Ruisanchez Rodriguez

In this paper we will discuss the process of the grain size customization of the EBT filler sand in relationship to the technical characteristics of the furnace and its tap hole. By customizing the grain size distribution, the glassy area formed on the top of the tap hole varies and supports differently the metallurgical pressure of the molten steel providing increased free opening speeds. Taylor made sand improves therefore the free opening rate, reduces the tap to tap time and increases the lifespan of the tap

Aug 16, 2017

By John Anthony Vasquez

During the last years Riva Acciaio Verona has taken the decision to invest in the route of a fully automated meltshop. The aim is to reduce at the minimum the operator's intervention from the bucket preparation till the ladle transfer to the continuous casting bay. The foundation for achieving the goal is the introduction of innovative technological solutions (fully automated cranes for bucket charge in the EAF, robots for sampling, etc. The paper underlines how the different solutions are based on the best practices to improve operator's safety and describes the different steps of the project, the different solutions adopted and the results in terms of production, energy savings, cost reduction and improved safety. Details are presented for: scrap yard management and bucket preparation, EAFs centralized controls and related robots for auxiliary operations (sampling, EBT cleaning, scraper for slag door automation, complete mass & energy balance based on process control), LFs centralized controls and process integration.

Aug 16, 2017

By Jean-Philippe Houde

The Blast Furnace Campaign lifetime is highly depending on the wear progress of the hearth lining. This progress is monitored in general through single and double thermocouples at the cold side of the lining. This type of monitoring becomes ineffective as soon as heat resistance will be formed in the refractory lining. Paul Wurth’s monitoring system, consisting of MTP-Sensor and Heat Flux Probes, is able to identify such heat resistances to give a true hearth lining wear. Since last year Paul Wurth is also able to install safely those MTP-Sensor and Heat Flux Probes on running blast furnace without salamander tapping, thanks to a newly developed cooled core drilling device. Blast Furnaces that are equipped with Paul Wurth’s monitoring system have optimized their campaign lifetime as they received right information upon the true wear lining such as detection of heat flux transfer failure, detection and monitoring of brittle layer or detection of hot spot.

Aug 16, 2017

By Mery-Cecilia Gómez-Marroquín

O presente trabalho trata da formação da ferrita de zinco a partir da mistura e posterior reação solido-solido entre o óxido de zinco e óxido de ferro - Fe2O3 puros em proporções equimolares. A faixa de temperatura onde teve lugar a formação foi entre 1073 e 1373 K. Testes de redução da ferrita da zinco sintética-ZF e pós de aciaria elétrica–EAFD foram realizadas usando misturas de CO e CO2 que variaram entre 50 e 100% CO. Ambos os testes (formação e redução de ZF e EAFD) foram suportados usando técnicas de caracterização física, química, estrutural e microscópica. No caso da redução, foi observado que tanto a temperatura como a percentagem de CO, foram os fatores que, mais afetarem a redução de ferrita de zinco contida no EAFD. A máxima percentagem de redução da ZF foi 85%, para 100% CO, 1373K e 105 min, e 52%, para 50% CO, 1373K e 105 min. Por outro lado, atingiu o 100% para 100% CO, 1273K, em 80.75 min, 60%, para 50% CO a 1373K durante 105 min. no caso da redução do EAFD

Aug 17, 2017

By Mery-Cecilia Gómez-Marroquín

O presente trabalho trata da formação da ferrita de zinco a partir da mistura e posterior reação solido-solido entre o óxido de zinco e óxido de ferro - Fe2O3 puros em proporções equimolares. A faixa de temperatura onde teve lugar a formação foi entre 1073 e 1373 K. Testes de redução da ferrita de zinco sintética-ZF e pós de aciaria elétrica–EAFD foram realizadas usando misturas de CO e CO2 que variaram entre 50 e 100% CO. Ambos os testes (formação e redução de ZF e EAFD) foram suportados usando técnicas de caracterização física, química, estrutural e microscópica. No caso da redução, foi observado que tanto a temperatura como a percentagem de CO, foram os fatores que, mais afetaram a redução de ferrita de zinco contida no EAFD. A máxima percentagem de redução foi 85%, para 100% CO, 1373 K e 105 min, e 52%, para 50% CO, 1373 K e 105 min. Por outro lado, atingiu o 100% para 100% CO, 1273K, em 80.75 min, 60%, para 50% CO a 1373 K durante 105 min.

Aug 16, 2017

By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Boryong Lee, Heedong Sung, Minho Park, Sunyoung Choi

Recently, the demand for ultra-thin steel plate with high hardness and strength has been increasing in various industries. In order to satisfy this requirement, steel company designs the chemistry with low CEQ and obtains the required characteristics through quenching and tempering process. Especially, these steels are accompanied by low temperature tempering as a necessary process. Unlike ordinary high temperature tempering steels, it is impossible to improve the flatness after low temperature tempering. Therefore, shape control in the quenching process is very important for securing the excellent quality flatness. In order to obtain flatness in the quenching process, uniform cooling inside the plate should be accompanied. However, the quenching process has limitations in estimating the temperature behavior during cooling because the plate temperature is lowered to room temperature. In this study, a thermocouple was installed inside the actual quenching plate to measure the temperature behavior during cooling and to establish the manufacturing conditions of the quenching plate to ensure excellent flatness quality.

Oct 1, 2019

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Eduardo Dominguez Trindade

Lubricant oils are subjected to reciprocating movement in the piston ring/cylinder tribocouple of automotive engines. In this kind of movement, the relative speed oscillates between zero and a maximum, and therefore the lubrication regime goes from boundary to hydrodynamic. Tribotests are widely used in laboratories to hint at the friction developed in these systems. In the present work, a SRV tribometer was used to evaluate the friction behaviour of lubricant oils under reciprocating movement up to 60 Hz. A high acquisition rate allowed the analysis of data inside each reciprocating cycle. Both a pure base oil and a fully formulated lubricant were used. Changes in the contact pressure, viscosity and speed were seen to influence friction, which was correlated to the relative thickness predicted by Hamrock-Dowson equation. While some observed characteristics were typical consequences of the Stribeck curve, other effects were also observed, such as the occurrence of seizure at high reciprocating frequency. A lower boundary coefficient of friction due to additive package in the formulated oil was also observed. The results allow a better understanding of friction in reciprocating cycles and can be used to evaluate the performance of oils and surfaces in laboratory prior to engine testing.

Jul 31, 2018

By Peter Grawenhof

Universal joint shafts and slipper spindles are commonly used in rolling mills to compensate the design- and process-related offset between the motors and work rolls. Although both types of shafts exhibit on the same kinematic principle, there are basic differences regarding the design concepts. These differences become noticeable on many levels and may become very distinct in terms of Life-Cycle-Costs (LCC). In this respect, a critical comparison between universal joint shafts and slipper spindles can be made.

Aug 16, 2017

By Gabriel Oliveira Glória

Due to growing concern about the ambient impacts, lignocellulosic fibers are been investigated to replace the synthetic ones in polymer composites The giant bamboo fiber, a relatively unknown lignocellulosic fiber with potential for composite reinforcement, still needs to characterize for possible engineer applications. However the giant bamboo fiber has low adhesion with the polymeric matrix. In order to understand the interaction that occurs between the bamboo fiber and the polymer matrix is necessary to evaluate its physical and chemical characteristics. Therefore, the present work analyzed the giant bamboo fiber by means of Fourier Transform Infrared (FTIR) spectroscopy. The spectrum revealed main absorption bands typical of giant bamboo fiber specific molecular interactions.

Aug 16, 2017

By Guilherme Corrêa Soares

Deeper understanding about the strain hardening behavior of steels has become necessary due to its importance in industrial processes such as mechanical cold forming, rolling and drawing. In this work, the strain hardening behavior of AISI 304, non-grain oriented electrical (NGO) and dual phase steels was investigated. Tensile tests were performed and the strain hardening behavior of each steel was studied by the Hollomon’s equation. X-ray diffraction measurements and hardness tests were also carried out in order to characterize the specimens. Different work hardening stages were observed in each steel during the deformation process. The results obtained are discussed in terms of the relationship among the instantaneous strain hardening coefficient, hardness and eventual phase transformations. The instantaneous strain hardening coefficient of dual phase and NGO increases after the yield point, rapidly reaching its maximum and then steadily decreases until tensile strength is reached. In AISI 304’s case, the strain hardening coefficient keeps raising to high values in response to a large strain and then rapidly decreases before reaching the tensile strength. In comparison to the other steels, AISI 304 shows higher instantaneous strain hardening coefficient value, which persists even in large strains. This is a consequence of its strain hardening mechanism based on stress-induced martensite transformation.

Aug 16, 2017

By Thierno FALL

This paper describes the study of the work-roll during the hot rolling process thanks to a 3D model built with the Finite Element Method (FEM). In terms of computational cost, that method needs high resources compared to 1D model which are mostly used. However, the 3D model is built to have a better understanding of the work-roll thermal and mechanical behavior during the hot rolling process. The thermal model shows that the highest temperature reached during rolling are within the range of 500°C and 600°C. The thermal field input used to simulate the mechanical behavior of the work-roll shows a biaxial thermal stress state, in the circumferential and axial planes. However, a peak of radial stress is observed in the backup zone. It did not generate plastic strain but could influence the fatigue behavior of the work-roll.

Oct 1, 2019

By Osvaldo Guilherme Comineli

An extensive investigation into the role of low copper contents on the hot ductility of C-Mn-Al steels has been carried out in order to better understanding the problem of “hot shortness”. Previous work has suggested that this problem results from the build up of Cu that occurs at the surface of the steel as a consequence of the preferential oxidation of iron. This causes the formation of a Cu-rich film of low melting point. A nickel addition has been reported as a solution to the problem, since it increases the solubility of copper in the austenite. After hot tensile testing to failure, samples of Cu-containing steels have been examined using optical, scanning and transmission electron microscopes. Recently published results indicate that copper, in addition to precipitating out as CuS, also segregates to MnS inclusions forming a shell around them. This does not seem to impair the hot ductility under an inert atmosphere, but may have serious consequences under an oxidising environment and lead to “hot shortness”. The influence of nickel in improving the hot ductility seems to be due to it forming a higher melting point alloy with the segregated copper. Data from this incomplete work also suggests that Ni reduces the precipitation of CuS particles. Current investigation carried out using confocal microscopy still to be completed will improve the understanding of the role of copper and nickel on the problem of “hot shortness”.

Aug 8, 2018

By Fernando Ruiz Díaz

En aplicaciones a elevadas temperaturas como por ejemplo en cámaras de combustión y toberas de vehículos aeroespaciales se requiere el uso de aleaciones que permitan una elevada extracción de calor y buenas propiedades mecánicas. En este trabajo se realiza un análisis comparativo de las aleaciones Cu-Cr-Zr y Cu-Ag-Zr. Las mismas fueron sometidas a ensayos de resistividad eléctrica entre 25ºC y 700ºC y de tracción a 150ºC, 450ºC y 700ºC. Los resultados de los ensayos de resistividad eléctrica fueron convertidos a conductividad térmica mediante la relación de Wiedemann- Franz. A través de este análisis se observa que la aleación con mejor conductividad térmica es la de Cu-Ag-Zr presentando además un cambio de fase que no es observado en la aleación Cu-Cr-Zr. Respecto al ensayo de tracción la aleación Cu-Cr-Zr presenta mayores valores de resistencia a la tracción y tensión de fluencia a las temperaturas estudiadas.

Aug 16, 2017

By Mathias Woydt

The tribological and mechanical properties of binderless and metal-bonded niobium carbides (8 or 12 vol.-% of Cobalt, 12 vol.-% of Fe3Al) are presented. Rotating disks made of niobium carbide bearing hard metals were mated against alumina (99.7%) under unlubricated (dry) unidirectional sliding tests (0,1 m/s to 12,0 m/s; 22°C and 400°C) as well as in oscillation tests (f= 20 Hz, ?x= 0,2 mm, 2/50/98% rel. humidity, n= 105/106 cycles). Microstructure and phase compositions were determined as well. The tribological data obtained were benchmarked with different ceramics, cermets, hard metals and thermally sprayed coatings, where NbC bonded with 8% and 12% Co presented above 8 m/s the lowest wear rates so far in such a benchmark. Binderless NbC (HP-NbC1) and the metal bonded NbCs exhibited low wear rates under dry sliding associated with high P?V load carrying capacities. NbC-based hard metal bonded with 12 vol.-% of Fe3Al resulted in a higher hardness level than for 12 vol.-% cobalt. The tribological profile established revealed a strong position of NbC bearing materials under tribological considerations and for closed tribosystems against established reference tribo-couples.

Jul 31, 2018