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By C. Pohlandt

A literature survey of methods suitable for the determination of cyanides in process streams and effluents is presented. Of the large number of methods published, 92 are examined in detail, emphasis being placed on the selectivity of the methods, i.e. the extent to which they enable one to distinguish between ionic cyanide and metal-cyanide complexes. Methods designed for the determination of 'total cyanide' (i.e. ionic cyanide as well as coordinated cyanide) are evaluated critically. Other aspects of the methods are also considered, such as sensitivity, accuracy, speed, and freedom from interferences.

Jan 1, 1983

By R. P. King

The University of the Witwatersrand (Wits) and the minerals industry of South Africa have grown with the city of Johannesburg. The former has provided teaching and research in mining and metallurgy, while the latter has been responsible for the practical training of metallurgists and for the testing and implementation of innovative ideas proposed by the academics. This interplay between inventiveness and industrial application is illustrated by three examples: the establishment of the iron and steel industry as a result of the persistent experimentation undertaken by Professor G. H. Stanley, the first Professor of Metallurgy and Assaying at the South African School of Mines, which later became Wits; the establishment of the research organization that eventually became the Council for Mineral Technology (Mintek) - again through Professor Stanley's faith in the role of research; and the establishment at Wits of physical metallurgy as a discipline in its own right, as first suggested by Professor C. E. Mavrocordatos of Wits against the opinion of his colleagues in the industry. The Department of Metallurgy at Wits has been well supported by the minerals industry. Not only does the industry provide grants for the financial support of students, but it supplements the salaries of personnel in the Department, making possible the recruitment of top-class academic staff. At present the greatest problem is the lack of interest shown by matriculants in the metallurgical industry as a career. However, an enormous effort is being made by the Chamber of Mines, The South African Institute of Mining and Metallurgy, and the Wits Department of Metallurgy to ensure that matriculants receive appropriate information about the career prospects in the minerals industry.

Jan 1, 1983

By G. H. Grange

Details are given of three legal controls for the pollution of the air, the water, and the land, together with brief histories of the developments leading up to these controls. Attention is drawn to the fact that legal action may be instituted against a mine under common or other laws where pollution causes proveable damage or loss. It is suggested that an international conference should be held to define the philosophies and principles on which to base not only the necessary legislation for environmental control but also the machinery by which the controls can be administered.

Jan 1, 1978

By L. J. Park, A. D. Thomas

Gladstone Pacific Nickel Limited (GPNL) is proposing to develop the Marlborough nickel deposit in central Queensland and the Yarwun Refinery in Gladstone, Australia. The project proposes to connect the two sites with a DN 500, single pump station slurry pipeline, transporting up to 4 Mtpa of nickel laterite ore as slurry 180 km from Marlborough to Gladstone. Slurry viscosity is a key parameter influencing pipeline design. Not only is the slurry viscosity relatively high, requiring pumping at low concentrations, around 30% by weight, but the viscosity (yield stress and plastic viscosity) increases with shearing or agitation. It is argued that the viscosity changes can be analysed in terms of total energy input, including energy input during grinding. The slurry viscosity is therefore expected to increase along the pipeline and the pumping concentration must be low enough such that the increase in yield stress does not cause transition to laminar flow towards the end of the pipeline. The base viscosity of two ore types is determined using a rotational viscometer for minus 212 micron slurries. Viscosity variations with ore particle sizes of d99 212, 425 and 600microns are investigated. For each of these particle sizes the expected increase in viscosity during pipeline transport is simulated on a laboratory scale by agitation with a turbine mixer in a baffled container to give the same equivalent unit energy input as will occur in the pipeline. Tests were also conducted on the d99425 micron slurry in a 2.7 metre diameter DN 200Wheelstand, rotated for the 23 hour transit time and at a similar relative velocity as in the pipeline. Based on the Wheel stand test results the yield stress is expected to increase by a factor of 3.1during pipeline transit. The preliminary design allows for a reduced pumping concentration to accommodate this increase in yield stress towards the end of the pipeline.

Jan 1, 2007

By M. F. Dawson, S. B. Davis

SYNOPSIS This paper describes the size reduction of limestone smaller than 1 mm by attrition grinding, using quartz (1 to 3 mm) as the grinding medium in a laboratory rig. The ore and grinding medium were closely sized fractions, and the particle size of the grinding medium was at least three sizes larger than that of the ore. Batch tests showed that the size reduction of the feed followed two first-order rate processes: one for an apparently fast-breaking ore fraction, and a slower one for most of the ore (86 per cent). The production of fines (material smaller than 10 µm) followed a zero-order rate equation. Continuous runs showed that the process could be modelled as a perfectly mixed system provided that the discharge screen did not selectively retain coarser particles of ore. The ratio of medium to ore (both by mass and by volume) was found to have a significant effect, the most energy¬efficient grinding occurring at ratios between 1 and 2. The solids content of the slurry also had a significant effect, the greatest efficiency being obtained at 50 to 65 per cent solids (by mass). Within these energy-efficient ranges of medium-to-ore and solids content, the lower values resulted in maximum feed breakage and the higher values in maximum fines production. The most important factor in the breakage of feed was the difference in the particle size of the grinding medium and the ore; the amount of ore broken out of the feed size for a given energy input was found to increase linearly with the difference between the size of the grinding medium and that of the ore up to 2 mm. The production of fines increased similarly, but only up to a difference of about 1,2 mm, when it levelled off at about 5 kg/kW ? h. The mechanism proposed for attritioning is mainly the abrasion of 1 µm planes of limestone along the crystal axes, with some fracturing along existing lines of weakness. The energy consumption of nearly 200 kW ? h per ton of product smaller than 10 µm appears to be higher than that in other types of milling. It is concluded that the value of attrition milling lies in its selectivity; in this work, only the softer limestone and virtually none of the hard quartz grinding medium was comminuted.

Jan 1, 1989

By P. R. Jochens, D. D. Howat, R. B. Atmore

INTRODUCTION The Miller chlorination process has assumed a preeminent position in the refining of gold bullion, a position it has maintained for over half a century. In the early sixties considerable interest was aroused by the idea of producing a consistently high grade bullion at the mine smelthouses themselves. However, as the use of chlorine in industrial plants is associated with considerable hazards, oxygen was considered a natural alternative, apart from bing less expensive than chlorine. Partial refining at the mine smelthouses would considerably decrease the requirements made on Rand Refinery Limited as well as indicating the possibility of reducing final refining costs. An added factor would be the purer silver chloride obtainable, after prior removal of the base metals by oxygen injection, which would facilitate the production of high-purity silver. The free energies of formation of the oxides of the metals;- silver, copper, lead, zinc, iron and bismuth indicate that, with the exception of silver, these metals should be capable of removal as oxides by oxygen injection. Rose1 had shown that during injection of gold bullion, considerable loss of silver to the boraxsilver slag occurred and, furthermore, that copper removal was not efficient and oxide attack on the refractories was severe. Plant test work2 had confirmed the difficulty of copper removal, but had shown that zinc and lead were almost completely removed. The difficulty of copper removal by oxygen injection warranted further investigation. Also, the high decomposition pressure of silver oxide suggested that by suitable control of the slag composition it might be possible to reduce to very small proportions the silver carried into the slag as oxide. The oxidation of copper by oxygen injection and subsequent dissolution of the oxide in a slag may occur according to the following reactions; Reactions 4 and 5 were considered because of the relatively high solubility of oxygen in molten silver and silver alloys. Thermodynamic data indicate that there is little possibility of any reaction involving the formation of CuO occurring at temperatures above 1 000 °C. To ensure that the operative reactions 1 and 4 take place to the maximum extent, the following factors He significant. (a) an increase in the activity of the copper in the bullion, (b) an increase in the partial pressure of oxygen in the system, (c) an increase in the activity of the oxygen in solution in the metal, (d) a decrease in the activity of cuprous oxide in the slag. From practical considerations, the operative variable most easily susceptible to control is the composition of the slag. SOLUBILITY OF COPPER OXIDES IN BOROSILICATE SLAGS Very scanty information exists on systems containing copper oxides but the indications are that slags containing considerable amounts of boric oxide would possibly prove to be the best solvents for cuprous and cupric oxides. This is attributed to the fact that the activities of copper oxides are much lower in boric oxide slags than in slags in which silica is the main network former. The number of possible slags containing boric oxide was limited by consideration of liquidus temperature, viscosity, corrosive action on refractories, volatilization, and ultimately cost (for industrial application). Slags in the systems soda-boric oxide-silica and lime-boric oxide-silica were selected paying due attention to the above limitations. Additions of 5, 10 and 15 per cent cupric oxide were made to the finely ground, premelted slags. These mixtures were then reground and 2g quantities held in re crystallized alumina crucibles at temperatures of 1150°C and 1 250°C respectively for 30 minutes. The crucibles were removed from the furnace, rapidly cooled, cut in half longitudinally, and a thin section taken from one half was subjected to microscopic examination.

Report M48 Tracer tests on furnaces at M etalloys Limited. Report M52 A high-speed, multi-input serial-interfacing system for a computer with simultaneous back-1lP recording on magnetic tape. Report M53 The development of an automatic sample-changer and control instrumentation for isotope-source neutron-activation analysis. Report M69 The determination, by X-ray-fluorescence spectrometry,of tin and tungsten in ores, concentrates, and residues of scheelite, wolframite, and cassiterite. Report M77 Analysis of the results of a marked-ball test in relation to theories of ball wear in rotary mills.

Jan 1, 1983

By G. A. Brown

A colloquium on industrial minerals entitled' A Strategy for Growth in the Industrial Minerals Sector' was held at Mintek on 5th November, 1991, under the auspices of the Extractive Metallurgy Sub-Committee of the SAIMM. The SAIMM had not been previously active in the field of industrial minerals, and the programme was designed to appeal to the middle management of mining and manufacturing companies in the industrial-minerals field. A total of 86 registered for the Colloquium, a predominance of the delegates (65 per cent) being non-members of the SAIMM. Two overseas delegates were registered after announcements

Jan 1, 1992

By K. C. Wilson

Recent experiments and analyses have provided greater understanding of friction losses for the size distribution of the particles forming the slurry. Wilson and Sellgren (2001), Wilson et al. (2006) and Sellgren and Wilson(2006) have proposed a multi-component model consisting of carrier fluid and pseudo-homogeneous, heterogeneous and fully stratified solids. The technique presented here was found to estimate friction losses well when compared to reported experimental results with pipelines with diameters mainly from 0.2 to 0.5 m for various mixtures of fine sand to coarse gravel and products from mineral processing and phosphate mining.

Jan 1, 2007

Discussion of the above paper by G. J. van JAARSVELDt Mr Ortlepp's paper is important, and deals with a subject towards which much controversy and insufficient basic scientific logic, in my opinion, have been directed. He attempts to remedy some of our unscientific popular misconceptions, and for this we thank him. However, I regret to say that experience has shown that some of his statements cannot be allowed to pass unchallenged. Author's reply Mr Van Jaarsveld's contribution is welcome because it provides an opportunity for me to clarify certain points that were perhaps not adequately explained in the paper.

Jan 1, 1979

By H. Wagner

The paper points out that bord-and-pillar mining is the most important method of coal extraction in South African underground coal mines, and advocates that pillar design procedures should be refined to make more rational allowance for the differences in strength properties between various coal seams and roof and floor strata. However, any deviations from well-established design procedures must be based on sound engineering principles and reliable data on the strength properties of the seams and strata concerned. Recent information indicates that practices for the protection of surface structures against underground mining should be revised.

Jan 1, 1980

By J. A. Ryder, M. U. Ozbay

An ERR-based methodology is presented for use in the re-assessment of the performance of stabilizing pillars, taking into account the effects of fracturing that can occur in pillar foundations under conditions of high stress. It is shown that the damage in the foundations of under-designed pillars can cause up to 30 per cent increases in ERR compared with the ERR for pillars with unfractured foundations. Despite this reduction in assessed performance, stabilizing pillars are still generally found to result in substantially lower ERR levels than alternative methods of reducing ERR, such as the use of stiff backfill or backfill ribs.

Jan 1, 1990

By J. A. Wates

Stope backfilling in South African gold mines uses the coarser cyclone fraction of the gold tailings. The disposal of the overflow from the cyclones, which is finer and of higher moisture content than normal gold tailings, presents some problems. This paper describes an investigation undertaken to define the parameters that are required for a quantitative and qualitative assessment of the operation and stability of slimes dams built of such material. However, seeing the investigation was conducted on the slimes from only one mine, it is recommended that, until a wider range of data becomes available, tests should be conducted for each individual mine.

Jan 1, 1988

NIM reports Report No. 1615 Fluorspar pellets. A survey of the world market and an assessment of future South African production. Report No. 1621 Correction for matrix effects in the analysis of solutions by X-ray-fiuorescence spectrometry. Notices Questionnaire on Technicians The Department of National Education's committee of enquiry into the education, training, utilization, and status of engineering technicians in the Republic of South Africa was established as a result of Resolution 6.3 taken at the Sixth Conference on Engineering Education: The Education and Training of Engineering Technicians. Vraelys oor Tegnici Die Departement van Nasionale Opvoeding se komitee wat ondersoek instel na die opleiding, gebruik en status van ingenieurstegnici in die Republiek van Suid-Afrika is gestig as gevolg van Besluit 6.3 wat geneem is tydens die Sesde Konferensie oor Ingenieursopleiding: Die Opleiding van Ingenieurstegnici. Competition for Student Members of the South African Institute of Mining and Metallurgy Each year the Institute offers a prize (or prizes should the entries warrant it) of up to R100 for the best paper or dissertation on a topic appropriate to the interests of the Institute. The competition is open to all Student Members of the Institute.

Jan 8, 1974

The First International Symposium on Seismicity in Mines, organized by the South African National Group on Rock Mechanics in collaboration with the South African Institute of Mining and Metallurgy, was held in Randburg (near Johannesburg) from 13th to 17th September, 1982. It was the first attempt to provide an international forum for the consideration of seismic problems specifically affecting mines or associated with mining. Numerical mathematics The South African Society for Numerical Mathematics and the Computer Science Department of the University of Natal are organizing the Ninth Symposium on Numerical Mathematics to be held in Durban from 18th to 20th July, 1983.

Jan 1, 1983

Crossroads for Students Students in their matriculation year, whatever their background, have reached a crossroads in their lives: behind them lie the relatively carefree years of childhood; ahead lies the whole of their working lives. Whether those working lives will be rewarding and interesting depends to considerable extent on whether they get 'a good matric' and carry on to some form of further education. IPMI awards 1985 Nominations for the 1985 Awards are now being accepted by the Awards Committee of the International Precious Metals Institute. THE DISTINGUISHED ACHIEVEMENT AWARD was established to recognize important career contributions to the advancement of precious metals, be it technological, economic, or business.

Jan 1, 1984

By P. H. Botha

An account is given of the procedures used by the South African Iron and Steel Industrial Corporation (Iscor) for tests on the flotation of coal fines, and some of the beneficiation problems encountered with coal from Durnacol, Grootegeluk, and the Soutpansberg area are discussed. These, and other South African coals differ from overseas coals in that they contain a high percentage of fixed ash, which means that they have to be crushed more finely for liberation and that they then contain more fine material (smaller than 0,84 mm). In addition, the coal from the three areas mentioned occurs in fine layers and seams, and contains many intergrown particles.

Jan 1, 1980

By R. H. C. Andrew

With the advent in recent years qf mechanization in deep-level gold and platinum mines, large quantities of rubber was are being used on both production and support vehicles. Conditions in these types of mines are extremely harsh and, as a result, we performance is significantly lower than in other types of mining such as open-cast base metal mining, where more favourable conditions prevail. Various options are available to the user to reduce tyre costs, including the use of retreads, the filing of tyres, and the repair of damaged tyres. While these methods may be generally successful in open-cast conditions, their use in deep-level mining needs to be carefully evaluated for each particular set of conditions. A basic requirement for any evaluation of we costs is the availability of reliable data on tyre performance and, for this reason, it is essential that proper tyre records are maintained This paper reviews the performance of tyres in deep-level gold and platinum mines in Johannesburg Consolidated Investment Company, Limited (JCI) over a period of about 8 years, and shows how the costs of retreading and tyre filing can be evaluated in practice. It also discusses the cost implications of repairing damaged tyres.

Jan 1, 1994

By J. D. Flint

The geological conditions in the Vierfontein area ~re such that conventional pillar extraction ~stooping) cannot be practised safely or efficiently. Both the open-end lift and the pocket-and-fender methods of pillar extraction have been tried with little success because of problems with roof control and ground stability. The main reasons for the difficulties are the coarse-grained sandstone roof, local weaknesses in the coal seam, and the rate at which the pillars were extracted. The mine has practised bord-and-pillar mining since it started production in 1952, and considerable reserves of coal are contained in the pillars. As an alternative to total pillar extraction, in which hand-loading methods were practised, a system of partial pillar extraction using mechanized-mining methods ~11"modified goaf-line support has been evolved. These remnant coal pillars (snooks) remaining after partial extraction ofthe pillar, together with the installation of 1,2 m" matpacks and a double line of fullcolumn resin roofbolts, ensure control of the edge of the area that has been mined out (goaf). Where roof conditions preclude the use of conventional pillar-extraction methods, this method holds promise as a safe and efficient alternative for the recovery of coal from pillars and for an increase in the volumetric extraction of the reserves within a mining panel.

Jan 1, 1984

Advances in extractive metallurgy, 1977. Proceedings of the third symposium organised by the Institution of Mining and Metallurgy held from 18-20th April 1977. London, the Institution of Mining and Metallurgy, 1977. 244 pp. £18,50. Coal preparation A meeting of the Organising Committee of the Eighth International Coal Preparation Congress took place in Moscow on 24th and 25th May, 1977. Representatives NIM reports Report no. 1906 An automated instrument for measuring the effects of impurities on cathodic-current efficiency during the electrowinning of zinc. (2nd Sep., 1977). Report no. 1908 An analysis of the replies to a questionnaire on materials of construction for ore hoppers. (16th Sep., 1977). Report no. 1913 The mechanism and rate of reduction of Mamatwan manganese-ore fines by carbon. (2nd Sep., 1977). Report no. 1914 The thermodynamics of the formation of sulphate complexes of iron (111), cobalt (11), iron (11), manganese (11), and copper (11) in perchlorate medium. (15th Sep., 1977). Report no. 1924 The composition of chromite grains from varwUB Witwatersrand reefs. (23rd Sep., 1977). Atomic absorption The Perkin-Elmer Corporation of South Africa is planning to hold an Atomic Absorption Autumn School in Cape Town from 10th to 13th April, 1978. Travel bursaries Two Atlas Cop co travel bursaries for study tours of Swedish mines may be awarded annually to young mining graduates. Stability in coal mining The First International Symposium on the above subject is to be held in Vancouver (Canada) on 5th to 7th April, 1978.

Jan 1, 1978