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By W. G. Matteson

THE Oklahoma legislature recently passed a bill providing for "the creation of an oil and gas department under the jurisdiction of the Corporation Commission, authorizing the. Corporation Commission to appoint a chief oil and gas conservation agent, and conferring exclusive jurisdiction on the Corporation Commission in reference to the conservation of oil and gas, and the inspection of gasoline and oil, the product of crude petroleum, and repealing all acts or parts of acts in conflict therewith and declaring an emergency." Some of the functions of the new bureau include the receiving and filing of all well logs and the direction and supervision of plugging all abandoned oil and gas wells under rules prescribed by the Corporation Commission. The two leading petroleum-producing States of the country, Oklahoma and California, have now established oil and gas bureaus with a staff of inspectors to see that the important rules relating to the conservation of oil and gas are thoroughly enforced. The economic significance and the value of well logs in the conservation work has been recognized and the necessary legal action taken to insure and procure them. William B. Heroy, of the Government Land Classification Board, in a personal communication to the writer, says that the drilling of wells is also regulated by public authority in the Roswell artesian basin in southeastern New Mexico, where a permit must be obtained for the drilling of any well and a certified log of the well recorded with a county official. The method is said to give fairly satisfactory results. In a recent article 1 a National instead of a State Bureau was suggested for collecting and filing well logs. In discussing the paper, L. L. Hutchison characterized such a plan as impractical because the average driller or contractor will often juggle or guess at the log and will not keep the record sufficiently close or accurate, making it necessary to maintain a special man at each well for the sole purpose of obtaining

Jan 6, 1917

Grad, the abbreviation for Graduate Resume Accumulation and Distribution, is a computerized information retrieval system operated on behalf of college placement officers around the country by the non- profit College Placement Council, Inc. Grad is free to all engineering candidates (regardless of the number of years of experience) and is a means of getting together college alumni who are seeking new employment and prospective employers. Who is Qualified? Candidates must have at least a bachelor's degree from a four-year college or university, or. in lieu of this, be accredited by a professional institute such as AIME as a full Member.

Jan 1, 1970

The University of Idaho Mining Society held a meeting on Oct. 23, and elected the following officers: President, Sam Bloom; Vice-President, Lloyd McDougall; Secty Treas, Jess W. Wade. Regular meetings are held on the first and third .Tuesdays of each month, for informal lectures and reports on technical subjects. The Mining Club of the University of Wisconsin has held four recent meetings On Oct. 17, sixteen new members were inducted, and a committee was appointed to buy a Liberty Bond. The second meeting, Oct. 31, was devoted to general entertainment, at the home of Professor McCaffery.

Jan 1, 1918

By W. Tovote

THIS paper is based upon 12 years' experience in the Southwest, including three years that were spent in constant traveling as examining engineer for the Phelps-Dodge Corporation. The material was gathered during rather extensive work in Bisbee, Clifton-Morenci, Globe, and Tombstone, and also on short and rapid trips into most of the mining camps and prospect fields of New Mexico, Arizona, the desert country of California, and as much of Sonora as was safe at the time. My methods of observation and my deductions are not put forward as new or scientific; they are simply rough field methods, based upon short notes, rough sketches, and largely upon memory, which I have found useful for coordinating geological data for the purpose of passing quick judgment on mining possibilities in certain districts exhibiting uniform characteristics. The opportunities for observation have been better these last few years than ever before, clue to the unprecedented activity in mining, which has caused the reopening of hundreds of old mines and the starting of even more numerous prospects all over the mining States. POSSIBLE SYSTEMS OF CLASSIFICATION By Geological Provinces There are a number of well defined geological provinces in the territory under discussion, and a study of their individual features is of interest. The following are a few of those that axe most striking in their uniformity. 1. The "Desert province," extending roughly from. Wickenburg, Ariz., to and beyond Barstow, Cal. In its north-south extent it reaches up to the Colorado River and clown into Sonora, but overlaps other provinces. It is characterized by a worn-down basement of schistose and granitic rocks, on which rest remnants of Paleozoic and pre-Paleozoic sediments, including very old limestones. The sediments are disrupted and contorted. Alteration in the mineralized areas is very prominent, especially in the schists and limestones. Cenozoic volcanic rocks, principally of semi-basic composition, have been intruded into this complex and sometimes cover it as lava flows.

Jan 10, 1918

By P. B. Baxendell, R. Thomas

Work on the calculation of vertical two-phase flow gradients by Cia. Shell de Venezuela has been based mainly on the "energy-loss" method proposed by Poett-mann and Carpenter in 1952. The "energy-loss-factor" correlation proposed by Poettmann and Carpenter was based on relatively low-rate flow data. This correlation proved inapplicable to high-rate flow conditions. In an attempt to establish a satisfactory correlation for high rates, a series of experiments was carried out at rates up to 5,000 BID in Cia. Shell de Venezuela's La Paz field in Venezuela, using tubing strings fitted with electronic surface-recording pressure elements. As a result of these experiments a correlation between energy-loss factor and mass flow rate was established which is believed to be applicable to a wide range of conduit sizes and crude types at high flow rates (e.g., above 900 BID for 27/8-in. OD tubing). It is anticipated that the resulting gradient calculations will have an accuracy of the order of % 5 per cent. At lower flow rates the energy-loss factor cannot be considered as constant for any mass rate of flow, but varies with the free gas in place and the mixture velocity. No satisfactory correlating parameter was obtained. As a practical compromise for low flow rates, a modification of the curve proposed by Poettmann and Carpenter was used. In practice this was found to give gradient accuracies of approxirnately ± 10 per cent clown to flow rates as low as 300 B/D in 27/8-in. tubing. INTRODUCTION Production operations in Cia. Shell de Venezuela's light- and medium-crude fields are principally concerned with high-rate flowing or gas-lift wells. Under these conditions the analysis of well performance, the selection of production strings and the design of gas-lift installations are vitally dependent on an accurate knowledge of the pressure gradients involved in vertical two-phase flow. Initially, attempts were made to establish the gradients empirically as done by Gilbert,' but the results were not reliable due to scarcity of data over a full range of rates and gas-oil ratios. Several methods of calculation based on energy-balance considerations were attempted, but the computations were cumbersome and the results cliscouraging. In 1952 a paper was published by Poettmann and Carpenter' which proposed a new approach. Their method was also based on an energy-balance equation. but it was original in that no attempt was made to evaluate the various components making up the total energy losses. Instead, they proposed a form of analysis which assumed that all the significant energy losses for mutiphase flow could be correlated in a form similar to that of the Fanning equation for frictional 1osses in single-phase flow. They then derived an empirical relationship linking measurable field data with a factor which, when applied to the standard form of the Fanning equation, would enable the energy losses to be determined. The basic method was applied in Venezuela to the problem of annular flow gradients in the La Paz and Mara fields" This involved establishing a new energy-loss-factor correlation to cover high flow rates and, also, some adaptation of the method to permit mechanized calculation using punch-card machines. The final result was 1 set of gradient curves for La Paz and Mara conditions which proved to be surprisingly accurate. With the encouraging results of the annular flow calculations, several attempts were made to obtain a corresponding set of curves for tubing flow. Here, unfortunately, little progress could be made. The original correlation of Poettmann and Carpenter was based on rather 1imited data derived from low-rate observations in 23/8- and 27/8-in. OD tubing. It did not cover the higher range of production rates, and extrapolation proved unsuccessful. A new correlation covering high flow rates was required, but this proved to be extremely difficult to establish since tubing flow pressure measurements at high rates did not exist—due to the difficulty of running pressure bombs against high-velocity flow. The necessity for reliable tubing flow data increased with the development of the new concessions in Lake Maracaibo, where high-rate tubing flow from depths of 10,500 ft became routine. Thus. it was decided to set up a full-scale test to establish a reliable energy-loss factor for tubing flow conditions. A La. Paz field light-oil producer with a potential of approximately 12,000 B/D on annular flow was chosen. To obtain full pressure gradients, a special tubing string was installed which was equipped with electronic surface-recording pressure measuring devices,

By R. G. Hite, R. G. Rowe

The Crandon deposit, located in northern Wisconsin, is a 65.8 million ton Precambrian volcanogenic massive sulfide deposit which averages 1.4% copper and 5.8% zinc. The deposit is classic in origin, mineralogy and shape. Comprehensive understanding of the geology of both the deposit and the project site has been fundamental to the credibility and success of project feasibility studies and regulatory permit preparation. Mine development in the current investment and regulatory climate requires thorough and timely application of geologic tools. From 1977-1980 geologic activities were focused on the typical objectives of orebody delineation, reserve estimation, depositional geology, and general site investigation. Results from these programs formed the basis for the project's preliminary feasibility studies. Since 1981 further geologic investigations have provided criteria for project design, site management, and operational permitting. Activities have included mine entry position definition drilling, developing geostatistical reserve modeling, large diameter (150 mm) core drilling for mill pilot samples, rock mechanics testing, and evaluation of the glacial overburden/deposit geohydrology for computer simulation.

Jan 1, 1984

By Welton Crook

UNLESS present in considerable proportion, metals of the precious-metal group-other than gold and silver-are not readily detected by the methods of fire assaying usually applied to ores and metallurgical products. Platinum, when present in small quantity, will ordinarily be reported as silver unless special methods of parting are used. Other elements occurring in the gold itself are all fluxed and slagged in the assay operation and if analyses are made on bullions the melting and slagging operations to which the bullion has been subjected may eliminate most of the associated elements. On the other hand, the analysis of precipi-tate from the cyanide treatment of gold ores may reveal the presence of many unexpected elements, such as tungsten and molybdenum. It is uncertain, however, whether many of the elements present in the pre-cipitate are derived from the ore gangue or from the gold itself. No very general survey of the distribution of metallic elements in gold seems to have been made. Rose and Newman,1 in connection with the composition of native gold, say in part as follows: Gold is occasionally found alloyed with copper and sometimes also with iron, bis-muth, lead, mercury, tin, antimony, palladium or rhodium. Rhodium gold from Mexico was found to be of the specific gravity 15.5 to 16.8 and contained 34 to 43 per cent of rhodium. The native alloy of palladium, gold, and silver from Porpez con-tains 85.98 per cent of gold, 9.85 per cent palladium and 4.17 per cent silver. Mal-donite, from Victoria, contains gold 64.5 per cent, bismuth 35.5 per cent (Louis). Dana' says that native gold is usually alloyed with silver in varying amounts, and that sometimes it also contains traces of copper and iron. Rare varieties contain palladium, rhodium and bismuth. Other authors, for instance Zeigler3 and Clark,4 give similar information. Most refer-ences on the subject agree that ordinary native golds contain, in common, the elements silver, copper and iron. After completion of the work of which this paper is a record, the conclusion is reached that all ordinary native gold probably does contain these elements and, although in certain cases other elements may be found to be present, that it is difficult to

Jan 1, 1939

By F. N. Rhines

Sintering may be defined as the process by which powders bond themselves into coherent bodies, usually, although not necessarily, under the influence of pressure and elevated temperature. For the sake of clarity and simplicity, the present survey will exclude from consideration the sintering of mixed or alloyed powders, with attendant complications, but at the risk of overlooking information of general applicability. Sintering in the presence of a liquid phase is thus automatically eliminated. The sintering of alloys involves much additional subject matter and deserves separate consideration. Since the literature of the subject is extensive and widely scattered, it will not be feasible to consider the contributions individually. Instead, the subject matter will be classified according to experimental observations and theory, and will be presented in summary form. It should be noted that the appended list of references does not constitute a complete bibliography; it includes only those works quoted below. More extensive bibliographies are included in several of the references; see particularly references 7, 9, 28, 34, 38, 50, 52, 54, a "Bibliography on Powder Metallurgy" published by the Library of Congress and a pamphlet published by the Metals Disintegrating Co. entitled "The Field of Powder Metallurgy and Bibliography." 11. Summary of Experimental Observations The following classified list is composed of general statements of established fact derived from the experimental results reported in the published literature. A few contested observations are included, because of their potential importance; these are labeled as such. Any satisfactory and complete theory must be capable of explaining all of the uncontested facts. Obviously, some important facts may be missing from this list and these may hold the key to the correct explanation of the sintering process, but the possible lack of such material should not deter attempts to understand the subject on the basis of what is available here. A, The Initial Bond at Room Temperature a. To a limited extent uncompressed powders and massive metals adhere at room temperature. Clean tin powder forms a weak "cake" on standing at room temperature, the strength increasing with time. Clean gold surfaces adhere on light con-tact, as do those of many other substances, including nickel.27 b. Upon compression the strength of the bond- is increased progres-ivelv. There is a limit of pressure

Jan 1, 1946

By F. N. Rhines

Sintering may be defined as the process by which powders bond themselves into coherent bodies, usually, although not necessarily, under the influence of pressure and elevated temperature. For the sake of clarity and simplicity, the present survey will exclude from consideration the sintering of mixed or alloyed powders, with attendant complications, but at the risk of overlooking information of general applicability. Sintering in the presence of a liquid phase is thus automatically eliminated. The sintering of alloys involves much additional subject matter and deserves separate consideration. Since the literature of the subject is extensive and widely scattered, it will not be feasible to consider the contributions individually. Instead, the subject matter will be classified according to experimental observations and theory, and will be presented in summary form. It should be noted that the appended list of references does not constitute a complete bibliography; it includes only those works quoted below. More extensive bibliographies are included in several of the references; see particularly references 7, 9, 28, 34, 38, 50, 52, 54, a "Bibliography on Powder Metallurgy" published by the Library of Congress and a pamphlet published by the Metals Disintegrating Co. entitled "The Field of Powder Metallurgy and Bibliography." 11. Summary of Experimental Observations The following classified list is composed of general statements of established fact derived from the experimental results reported in the published literature. A few contested observations are included, because of their potential importance; these are labeled as such. Any satisfactory and complete theory must be capable of explaining all of the uncontested facts. Obviously, some important facts may be missing from this list and these may hold the key to the correct explanation of the sintering process, but the possible lack of such material should not deter attempts to understand the subject on the basis of what is available here. A, The Initial Bond at Room Temperature a. To a limited extent uncompressed powders and massive metals adhere at room temperature. Clean tin powder forms a weak "cake" on standing at room temperature, the strength increasing with time. Clean gold surfaces adhere on light con-tact, as do those of many other substances, including nickel.27 b. Upon compression the strength of the bond- is increased progres-ivelv. There is a limit of pressure

Jan 1, 1946

By W. A. Backofen

THE preferred orientations, or textures, resulting from many of the various methods for testing and forming metals have been the subject of numerous investigations.1,2* Despite this large amount of work, however, only a few limited studies have been made of the texture that is developed by torsional deformation. Ono3 found that in severely twisted wires of copper and aluminum a [Ill] direction lies parallel and a [1101 direction perpendicular to the longitudinal axis of the wire. Sachs and Schiebold4 have reported that a double-fiber texture exists in a twisted aluminum wire with both the [Ill] and [loo] directions parallel to the axis of the wire. Twisted iron wires have also been examined by Ono.8 Both the [1101 and [1121 directions were reported as parallel to the axis of the wire. Goss5 concluded from a study of twisted rods of a low-carbon steel that the preferred orientation existing at fracture is quite complex, but that many grains have a [1101 direction parallel to the axis of the wire. In addition to the earlier experimental work, some suggestions have been made about the possible nature of the torsion texture. These suggestions are based on the results of many experiments which indicate that the cold-working texture of a particular metal is largely determined by the geometrical change in shape that the metal undergoes during plastic deformation.1,6 Hibbard and Yen7 have considered the problem of deformation textures and have presented an analysis which is able to explain why equivalent changes in shape should yield similar textures. Therefore, a knowledge of the principal strains associated with torsional deformation would seem helpful in the interpretation of the torsion texture. The necessary analysis has been made of the state of strain in an element of metal lying in the surface of a cylindrical rod or tube that has been subjected to pure torsion.8,9 This analysis shows that the directions of the principal normal strains rotate continuously within a torsion specimen while it is being twisted. After the first infinitesimal amount of twisting, these directions make angles of 45" with the longitudinal axis of the bar. They rotate from this position as twisting proceeds, and after an infinite amount of twisting, the direction of the principal tensile strain is perpendicular, and the direction

Jan 1, 1951

By William L. Fink, Kent R. Van Horn

Zinc is one of the effective elements introduced to enhance the strength of aluminum. This strengthening is principally attributable to the high solid solubility of zinc in aluminum and the pronounced variation of solubility with temperature. Consequently an accurate determination of the solid solubility curve is desirable. The solid solubility relations have been studied by numerous investigators. Shepherd1 first established the existence of a solid solution region at the aluminum end of the diagram (-v phase) by specific volume and microscopic determinations. Bauer and Voge12 published a constitutional diagram which showed the limits of solid solubility as determined by thermal and microscopic methods. Hanson and Gayler3 presented the aluminum-zinc diagram which is now most generally accepted (Fig. 1). Chill-cast samples were given thermal treatments designed to obtain equilibrium conditions, quenched, and microscopically examined. The solubility was placed between 15 to 20 per cent at 60" C., 20 to 22 per cent at 140" C. and 36 to 38 per cent at 270" C. Sander and Meissner decidedly modified the limits of the -y phase field of Hanson and Gayler's diagram by using similar methods on chill-cast specimens annealed for a shorter period of time. Tanabe,s utilizing dynamic hard-ness, electrical conductivity and dilatometric measurements of specimens at temperature, obtained values comparable to Hanson and Gayler's at room temperature, but appreciably lower at higher temperatures. Nishimura6 concluded from age-hardening results of aluminum-zinc alloy chill castings, which had been quenched from 400" to 500" C., that the solubility of zinc in aluminum at room temperature is less than 5 * Metallurgical Division, Aluminum Research Laboratories. 1 E. S. Shepherd: Aluminum-Zinc Alloys, Jnl, phys. Chem. (1905) 9, 504. 2 0. Bauer and 0. Vogel: Aluminum-Zinc Alloys, Int. Jn1. Melallog. (1916) 8, 101. 3 D. Hanson and M. V. L. Gayler: A Further Study of the Alloys of Aluminum and Zinc. Jnl. Inst. Met. (1922) 27, 267. 4 W. Sander and K. L. Meissner: ZII~ Kenntnis der Konstitution der Aluminium-Zinklegierungen. Ztsch. f. Metallkunde (1922) 14, 385. 4 T. Tanabe: Studies in the Aluminum-Zinc System, Jnl. Inst. Met. (1924) 32, 415 6 H. Nishimura: On the Age-Hardening of Aluminum-Rich Al-Zn Alloys. Mem. Kyoto Imp. Univ. (1924) 3, 133.

Jan 1, 1932

By Henry M. Howe

THIS paper gives the composition of the iron and slag at different stages in the "air-furnace" process of preparing "hard metal," or white cast-iron, for conversion into malleable cast-iron by annealing. The details of the process are given in an appendix. One of us had been trying for years to work some chemist of some of our malleable-iron works up to a degree of enthusiasm which would lead him to make such au investigation. It would have had the advantage of the greater familiarity with the conditions which one habitually on the spot must have. Failing in this, he made use of an opportunity which presented itself of taking samples here represented, with such fairness as the conditions permitted, holding firmly that a rough approximation to the truth is better than the complete lack of data, or that a bird in the hand is worth two in the bush. We hope that this attempt may stimulate others effectively to duplicate this work, and thus correct or confirm it. Our results are shown in Table I. and graphically in Figs. 1 and 2. Discussion.-At the time when the first two samples were taken, the metal and slag were still too sluggish to permit fair sampling, and not until sample 6 were the conditions really favorable, because at the time of the fourth sample the metal was not fully melted, and even at the time of sample 5 it was still sluggish. Indeed, the slag was probably very heterogeneous throughout, because it took up silica and alumina rapidly from the bottom, and because it was so siliceous as to be sluggish at this relatively low temperature. This hetero-geneousness is exaggerated in the two samples of slag 8, apparently by the great viscosity due to its extraordinary acidity. Note that the manganous oxide of one sample is about two and

Mar 1, 1909

By A. Sutulov

The segregation process, an alternative to benefi-ciation of oxidized and mixed sulfide-oxide copper ores, is studied here with particular emphasis placed on time, temperature, and coke and salt percentage factors. The results show that in a segregated charge, the copper assay of the coarsest fractions normally is of the same order as the copper assay of the tails obtained from grinding and flotation of the same charge. This observation suggests the possibility of limiting or even eliminating the grinding step from the flowsheet of a segregation plant. The segregation process, which offers an alternative to beneficiation of oxidized and mixed sulfide-oxide copper ores, was discovered in 1923 by Moulden and Taplin1,2 who were attempting to apply the Perkins process3'4 to a Chilean ore from the Sagasca mine. After a number of investigations and pilot plant tests,'-' the segregation process became a successful industrial operation.'r9 The process aroused considerable interest in Chile because of the existance of large reserves of oxidized copper minerals which could not be treated by conventional hydrometallurgical methods because of the high consumption and prohibitive cost of sulfuric acid. During the last two years, the Mineral Dressing Dept. of the Institute de Investigaciones Tecnology cas of University of concepci6n (Chile) has carried out a test program on 23 different ore samples representative of the national territory. These tests were carried out on a semi-continuous and batch scale with a rotary, automatically controlled and gas-fired furnace (supplied by Bartlett and Snow, Fig. 1). The results of these tests indicate that out of the 23 samples 20 can be successfully treated by this process with recoveries of copper ranging from 85 to 95%.10,11 The purpose of this paper is to treat some specific problems related to the segregation process. TIME AND TEMPERATURE FACTORS Time and temperature of calcination play an important role in the segregation process. When moderate salt and coke conditions were maintained (each of reagents was added in the quantity of 1 — % wt), systematic testing easily demonstrated the influence of these two factors on segregation and flotation recovery. The pertinent results are summarized in Fig. 2. To determine what specific changes the segregation process made on the ore, the samples, segregated at 700°C for different periods of time and under standard conditions, were granulometrically analysed and

Jan 1, 1963

Page Foreword. By Edmund M. Wise..................... 3 A.I.M.E. Officers and Dircctors...................... 4 Institute of Metals Division Officers and Committees............ 7 Institute of Metals Division Annual Award Certificate............ 8 Institute of Metals Division Lectures and Lecturers............. 9 Photograph of E. H. Dix, Jr., Institute of Metals Division Lecturer...... 10 PAPERS Acceleration of the Rate of Corrosion by High Constant Stresses. By E. H. Dm, JR. (Institute of Metals Division Lecture, T. P. 1204).......... 11 Variation of Internal Friction with Grain Size. By Clarence Zener and R. H. Randall. (T.P. 1146, with discussion) .............41 Changes in Damping Capacity during Annealing of Alpha Brass. By John T. NoRton. (T.P. 1168, with discussion)................49 An Electron Diffraction Study of Anodic Films. By R. A. HarrinQton and H. R. Nelson. (T.P. 1158).....................62 Determination of Orientations by Etch Pits. By Charles S. Barrett .and L. H. Levenson. (T.P. 1171, with discussion).............76 Process of Precipitation from Solid Solution, I—A Crystallographic Mechanism for the Aluminum-copper Alloys. By Carl H. Samans. (T.P. 1186). . . 85 Age-hardening of Aluminum Alloys, IV — Discussion of the Theory. By WilTJam L. Fink and Dana W. Smith. (T.P. 1083, with discussion). . . 95 Structure of Aluminum after Compression. By Charles S. BaRREtt and L. H. evensonON. (T.P. 1104, with discussion)................112 Recrystallization Texture of Aluminum after Compression. By ChaRlEs S. BarRett. (T.P. 1141, with discussion)................128 Plastic Deformation and Recrystallization of Aluminum Single Crystals. By J. A. Collins and C. H. Mathewson. (T.P. 1145, with discussion) . . . 150 Recovery and Recrystailization in Long-time Annealing of 70-30 Brass. By S. E. Maddigan and A. I. Blank. . (T.P, 1166, with disonssion).....170 Correlation of Deformation and Recrystallization Textures of Rolled 70-30 Brass. By R. M. Brick. (T.P. 1144, with discussion).........193 Tensile Deformation of Critically Oriented Brass Crystals. By H. L. Burghoff. (T.P. 1149).............................214 Recrystallization of Lead. By Paul A. Beck. (T.P. 1101, with discussion). . 222 Simple Method of Thermal Analysis Permitting Quantitative Measurements of Specific and Latent Heats. By Cyril Stanley Smith. (T.P. 1100, with discussion).............................236 Metallographic Study of Internal Oxidation in the Alpha Solid Solutions of Copper. By Frederick N. Rhines. (T.P. 1162, with discussion). . . . 246

Jan 1, 1940

Page Foreword. By Edmund M. Wise..................... 3 A.I.M.E. Officers and Dircctors...................... 4 Institute of Metals Division Officers and Committees............ 7 Institute of Metals Division Annual Award Certificate............ 8 Institute of Metals Division Lectures and Lecturers............. 9 Photograph of E. H. Dix, Jr., Institute of Metals Division Lecturer...... 10 PAPERS Acceleration of the Rate of Corrosion by High Constant Stresses. By E. H. Dm, JR. (Institute of Metals Division Lecture, T. P. 1204).......... 11 Variation of Internal Friction with Grain Size. By Clarence Zener and R. H. Randall. (T.P. 1146, with discussion) .............41 Changes in Damping Capacity during Annealing of Alpha Brass. By John T. NoRton. (T.P. 1168, with discussion)................49 An Electron Diffraction Study of Anodic Films. By R. A. HarrinQton and H. R. Nelson. (T.P. 1158).....................62 Determination of Orientations by Etch Pits. By Charles S. Barrett .and L. H. Levenson. (T.P. 1171, with discussion).............76 Process of Precipitation from Solid Solution, I—A Crystallographic Mechanism for the Aluminum-copper Alloys. By Carl H. Samans. (T.P. 1186). . . 85 Age-hardening of Aluminum Alloys, IV — Discussion of the Theory. By WilTJam L. Fink and Dana W. Smith. (T.P. 1083, with discussion). . . 95 Structure of Aluminum after Compression. By Charles S. BaRREtt and L. H. evensonON. (T.P. 1104, with discussion)................112 Recrystallization Texture of Aluminum after Compression. By ChaRlEs S. BarRett. (T.P. 1141, with discussion)................128 Plastic Deformation and Recrystallization of Aluminum Single Crystals. By J. A. Collins and C. H. Mathewson. (T.P. 1145, with discussion) . . . 150 Recovery and Recrystailization in Long-time Annealing of 70-30 Brass. By S. E. Maddigan and A. I. Blank. . (T.P, 1166, with disonssion).....170 Correlation of Deformation and Recrystallization Textures of Rolled 70-30 Brass. By R. M. Brick. (T.P. 1144, with discussion).........193 Tensile Deformation of Critically Oriented Brass Crystals. By H. L. Burghoff. (T.P. 1149).............................214 Recrystallization of Lead. By Paul A. Beck. (T.P. 1101, with discussion). . 222 Simple Method of Thermal Analysis Permitting Quantitative Measurements of Specific and Latent Heats. By Cyril Stanley Smith. (T.P. 1100, with discussion).............................236 Metallographic Study of Internal Oxidation in the Alpha Solid Solutions of Copper. By Frederick N. Rhines. (T.P. 1162, with discussion). . . . 246

Jan 1, 1940

I. PRESIDING OFFICER. At all business meetings of the Institute the President, or, in his absence, the First Vice-President, or, in the absence of both of them, any other Vice-President or Director, chosen by the meeting, shall preside. At all other meetings of the Institute the President, or, in his absence, one of the Vice-Presidents, shall preside. If none of these be present the meeting shall elect a Chairman. II. ORDER OF BUSINESS. At each business meeting of the Institute the order of business shall be as - follows : 1. Reading of minutes-of preceding meeting. 2. Report of the President. 3. Report of the Treasurer. 4. Report of the. Secretary. 5. Election of Directors. 6. Reports of Standing Committees. 7. Reports of Special Committees. 8. Special Orders. 9. Miscellaneous business. This order of business may be changed at any meeting, by a vote of a majority of the Members and Associates present. At all sessions of the Institute, other than business meetings, the order of pro¬ceedings and the time of adjournment shall rest in the discretion of the presiding officer. III. SECRETARY OF THE INSTITUTE. The Secretary shall keep a record of the proceedings of all meetings of the Institute. He shall be custodian of the corporate seal, of the minute books, and of all legal documents belonging to the Institute. He shall have charge, on behalf of the Institute, of all correspondence except such as pertains directly to the office of the Treasurer. He shall notify all Officers and Directors and all members of committees of their election and appointment; shall issue notices of all meetings of the Board, and of the annual and other business meetings of the Institute; and shall; in calling, special meetings of the Directors, specify the objects of such meetings. He shall act as clerk at all the meetings of the Board of Directors and at all meetings of the Institute. The Secretary shall be custodian of all technical or scientific papers submitted to the Institute for its consideration, shall have general charge and supervision of the editing and proof-reading of all material published by the Institute, and of the distribution thereof, and be ex officer Chairman of the Committee on Publications. On the first day of May following the year in which each volume of Transac-

Jan 1, 1925

By R. R. Wilson, Robert Henderson

The Cassidy Colliery operated by the Granby Consolidated Mining Smelting & Power Co., Ltd., is situated about 9 miles in a southerly direc tion from the city of Nanaimo on Vancouver Island. The coal seam worked, which is called the Douglas bed, outcrops in the western part of the property, dipping easterly, and is opened by a slope 7 by 14 ft. in the clear, and is timbered by 12 to 14-in. framed sets of timber, 4 ft. center to center. A separate manway provides for a traveling road and at the same time forms an intake airway. The general average of the dip of the seam at Cassidy is 18º, and varies in thickness from 1 to 25 ft., averaging about 8 ft. The main slopes follow straight down the dip a distance of 4845 ft. At the bottom of the main slope two rock tunnels were driven a distance of 1500 ft. to the south, cutting through a fault, and opening up an area in the same seam which is known as No. 7 South Section. The coal is found in this section at a vertical depth of 1560 ft., and is very soft and friable. The immediate roof is a strong, sandy. shale overlain by massive sandstone while the floor is a light-colored shale, hard when freshly exposed. It does not soften materially on exposure. In the folding of the coal measures a great thrust caused a movement along the coal seam as indicated by the slickensided nature of the coal. The floor has buckled and this has rolled and squeezed the coal so that with rare exceptions it shows no normal bedding but curved slip planes, which frequently start at right angles to the floor, curving upward and then in the direction of the dip. As such planes are slickensided it is probable that there is a coating of clay which is more or less impervious to gas. Outbursts of Gas and Coal Outbursts of gas and coal have occurred in this mine previous to 1921, but not until June 14 of that year was a complete record kept of them. No outbursts occurred above the fourth levels, or, in other words, until a vertical depth of about 900 ft. was reached. Since that time quite a

Jan 1, 1927

By O. N. Carlson, A. L. Eustice

The tensile properties of iodide vanadium were determined as a function of hydrogen concentration. It was shown that the presence of 10 ppm H is sufficient to cause embrittlement of vanadzum over a limited temperature range. The temperature of the observed ductility mininlum is approximately -l00°C, this being a function of strain rate and hydrogen concentration. The yield stress of hydrogenated vanadium is raised sharply in the brittle temperature range. THE present investigation was initiated to determine the effect of hydrogen on the tensile properties of high-purity vanadium as a function of temperature and the role of hydrogen in the brittle-ductile transition. Loomis and Carlson&apos; reported a change from ductile to brittle behavior in iodide vanadium at -110°C with a return of ductility at temperatures below -140°C. Vanadium wire containing 270 pprn of hydrogen was brittle at room temperature while wire containing 100 ppm was ductile under the same conditions. Roberts and Rogers&apos; reported a ductile-brittle-ductile fracture sequence in vanadium containing 400 to 600 ppm of hydrogen. Their data show that hydrogenated vanadium is ductile at 150"C, brittle at room temperature and ductile again at -196°C. Magnusson and Baldwin found a minimum in ductility in vanadium containing 80 ppm hydrogen from tensile tests performed at several strain rates. Information available on the vanadium-hydrogen equilibrium system4 is somewhat incomplete. The absorption of hydrogen is exothermic in accordance with the decline in solubility with rising temperature. The limit of solid solubility at temperatures below 400°C has not been determined due to the difficulties in obtaining equilibrium at these temperatures. Data on the hydrides of vanadium are rather limited. Roberts6 studied the structure of VD,., by neutron diffraction, and observed the ordering of the deuterium atoms below -65°C into a primitive cubic cell with a lattice constant about twice that of the disordered bcc vanadium solid solution. EXPERIMENTAL PROCEDURE Vanadium of 99.9 pct purity was prepared by the iodide refining process6 for use in this investigation. This vanadium contained the following analyzed impurities; <20 pprn calcium, 150 ppm carbon, 200 ppm chromium, 30 ppm copper, 10 ppm hydrogen, 200 ppm iron, <20 ppm magnesium, <20 ppm nickel, <5 ppm nitrogen, 150 ppm oxygen, <50 ppm silicon, and <20 ppm titanium. specimen Preparation—Tensile specimens were machined from swaged rods of iodide vanadium. The

Jan 1, 1962

By W. P. Blake

THIS furnace is designed especially for the oxidation of sulphur or arsenic in pyritic ores, but may be used for all oxidizing or desulphurizing operations, and for calcining, roasting and chloridizing ores, or for drying ores in large quantities preparatory to treatment by magnetic separators or otherwise. It is of the tabular, revolving type, with automatic feed and delivery, and is a modification of the Cornish calcining furnace, designed by Brunton, from which it differs, however, not only in construction, but in two or more radical features, for which novelty is claimed and patents have been applied for. The principal of these novelties are: 1. A series of concentric terraced floors, one above another. 2. The introduction of superheated air upon the charge without contact with the fuel. In the furnace which I have had in operation for more than a

Jan 1, 1893

By B. S. Blakeney, E. P. Abrahamson II

The effect of the transition elements in binary solid-solution additions upon the recrystallization temperature of iron has been investigated. All these elements immediately raised the temperature, the majority having their greatest effect in less than 0.10 at. pct. A correlation is noted between the rate of change of recrystallization temperature with atomic percent solute and the electron configuration of the solute element. THE work of Abrahamson and rant&apos; on binary chromium-base alloys indicated that a correspondence existed between the effect of each solute element on the brittle-to-ductile transition temperature of chromium and the ground-state electron configuration of the element added. This was felt to be a bonding phenomenon and would be expected to be observed in measurements of other properties involving the breaking or exchange of atomic bonds. From this work it was postulated that a like correspondence should be found for other properties of binary alloys, such as recrystallization. This study is an effort to check this postulation using binary solid-solution iron-base alloys. Previously, the majority of recrystallization studies were carried out on steels. However, Tammann2 investigated the recrystallization of iron as effected by Co, Ni, Si, Mn, Mo, and Cr and stated that elements with the same crystal structure at room temperature as iron appeared to be more effective in raising the recrystallization temperature. Austin, Luini, and Lindsay3 studied the effects of Ni, Cr, Mn, Co, Si, and Mo on cold rolling and annealing, but noted no trend. Abrahamson and rant,&apos; in their work on the effect of both substitutional and interstitial elements upon the brittle-to-ductile transition of chromium, have shown that the outer electron configuration in the ground state of the solute element appears to be the prime determinant of the transition temperature. PROCEDURE All alloys were made using 99.95 + pct Fe with 0.02 wt pct 0, 0.004 pct C, and 0.001 pct N. All alloying elements were 99.9 + percent pure. Metal-lographically the alloys, out to at least 0.1 at. pct, appeared to be in solid solution. Though several published phase diagrams tend to dispute this.4 All alloys were arc melted six times and cast into square 400-g ingots under an argon atmosphere.

Jan 1, 1961