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By Helen W. Lang

The Bureau of Mines has developed a very rapid gas chromatographic method for routine determination of oxygen, nitrogen, methane, and carbon dioxide in mine atmosphere samples. Analysis is accomplished in 3 min; readout appears on a single strip chart. The gas sample is split between two columns contained in separate chromatographs. A 5 A molecular sieve column separates oxygen, nitrogen, and methane; a porous polymer column separates carbon dioxide from an air peak. Direct selective analysis of methane from this unresolved air peak is accomplished using a hydrogen flame ionization detector (FID). Carbon dioxide is catalytically converted to methane and detected by FID.

Jan 1, 1972

By Jerry L. Huiatt

An accurate and reproducible procedure was developed using the gas-liquid chromatograph to quantitatively measure oleic acid on flotation products and in flotation water phases. The method comprised extraction of the oleic acid from the mineral surfaces with alcoholic NaOH, esterification of the extracted oleate, and chromatography of the methyl ester with an internal standard. Quantitative analysis of oleic acid on flotation products from test tube and bench-scale flotation tests with pure minerals and with natural ores proved the applicability of the method on a variety of minerals. The accountability of oleic acid added was 100 percent, ±5 percent.

Jan 1, 1968

By Steven J. Page

Accurate measurement of workplace respirable dust concentration is an essential step in eliminating lung disease in any occupational setting. In the United States (U.S.) coal mining industry, this measurement process has relied upon a personal sampler that includes a 10 mm Dorr-Oliver (DO) nylon cyclone operated at a flow rate of 2.0 L min-1 to collect a respirable dust sample. Dust concentrations measured with this sampler are multiplied by 1.38, which was empirically derived, to convert them to measurements approximating the United Kingdom British Medical Research Council (BMRC) definition of respirable dust upon which the health effects of coal mine dust are based. The International Organization for Standardization (ISO) subsequently refined the respirable dust definition and the U.S. National Institute for Occupational Safety and Health (NIOSH) 1995 Criteria for a Recommended Standard presented a conversion multiplier of 0.857 to apply to the 2.0 L min-' DO (in addition to thel.38 multiplier) to obtain equivalent ISO concentrations, as approximated by the 1.7 L min-1 DO. However, the conversion multiplier 0.857 was derived indirectly from a limited size distribution data set rather than a direct comparison of the DO samplers. The present analysis focuses on providing a more accurate conversion multiplier derived from direct comparisons of the 2.0 L min-1 (with 1.38 BMRC equivalency multiplier) and 1.7 L min-1 DO cyclones. A weighted linear regression analysis of this database suggests that a more accurate estimate of the conversion multiplier is 0.815.

Jan 1, 2009

By Motohisa Kanda

The time and amplitude statistics necessary to adequately describe electromagnetic (EM) noise in mines are illustrated through computer software techniques. They are 1) Allan Variance Analyses (AVA), 2) Interpulse Spacing Distributions (ISD), 3) Pulse Duration Distributions (PDD), 4) Average Crossing Rates (ACR) , and 5) Amplitude Probability Distributions (APD) . These statistics are illustrated using data taken from a rather large store of raw analog data recorded in operational mines. The curves generated for the illustrations characterize the noise environment in the mines from which the corresponding data were taken, and should aid in the design of reliable communication systems for such mines.

By V. R. Miller

The Bureau of Mines has developed a technique to separate and recover the three major components, Pb, Zn, and Cd, from lead smelter flue dust. This research was conducted as part of the Bureau's effort to reduce environmental conflicts and occupational hazards associated with mineral-processing operations and to recover valuable constituents in emissions and effluents. The laboratory process utilizes sulfation roasting of the flue dust followed by water leaching to extract over 95 pct of the cadmium and zinc. Ninety-nine percent of the cadmium was recovered from solution by cementing with zinc dust, and zinc was electrowon from the resulting solution after purification. Zinc electrolysis was carried out in a 1-liter cell at 35° C with a cathode-current density of 8 A/dm2 in a solution containing 65 g/l Zn++ and 180 g/l H2S04, Current efficiencies of 80 pct were obtained. The leached residue consisted largely of PbS04, which was converted to PbC03 and leached with H2SiF6 to produce PbSiF6 electrolyte. Ninety-five percent of the lead contained in the residue was converted to electrolyte. Lead was electrowon from solutions containing 70 gil Pb++ and 90 g/l H2SiF6 using a lead cathode, Pb02-coated titanium anodes at 28° C, and a current density of 1.6 A/dm2. Current efficiencies approaching 92 pct were obtained. Accessory minerals such as cobalt and nickel were separated into purification residues and liquor.

Jan 1, 1982

Reduce the time, complexity and expense of dissolving metal and mineral samples in solution in preparation for chemical analysis. Approach In earlier research, the Bureau of Mines developed a rapid and inexpensive method for the dissolution of mineral and metal samples in plastic pressure bottles heated in a boiling water bath. Using this technique, samples could be prepared for chemical analysis in less than one hour compared with several hours by traditional dissolution methods (see Technology News No. 85, December 1980 for further details). By heating in a microwave oven, sample dissolution time can be reduced to approximately 5 minutes.

Jan 1, 1983

By C. W. JEFFERS

At its annual meeting on March 5, 1928, in Washington, D. C., the Joseph A. Holmes Safety Association gave to the Ford Collieries Co., Curtisville, Pa., a certificate of honor for "having worked 922,628 underground man-shifts from August 14, 1920, to December 31, 1926, producing 5,755,669 short tons of coal without a fatality." This remarkable record certainly deserved recognition. It developed that this company's freedom from fatalities continued until October 2, 1929, hence the full period during which no underground fatalities occurred was from August 14, 1920, to October 2, 1929, or 9 years, 1 month, and 18 days, the total tonnage being over 7,700,000. Table 1, shows the complete safety record of the Ford Collieries Co. since 1920 as given by the officials of the company. The first item in Table 1 shows a remarkable performance. This company since 1920 has mined 15 times more coal per fatal accident than the average pro- duction per fatal accident for the State of Pennsylvania in 1928 (255,257 tons). Excluding the two fatalities (one in 1922 and one in 1929) the severity rate for the same period has been 1.259 per thousand hours worked, a record of which the company may justly be proud. However, including the fatal accidents the rate is 2.407. This compares favorably with an average of 12.4 in 1928 for 66 mines in the National Safety Competition. The Ford Collieries Co. operates three mines located in the vicinity of Curtisville, Allegheny County, Pa. One of these mines, Benjamin No. 1, is idle at the present time. The officials are: A. R. Pollock, general manager, Curtisville, Pa., and C. W. Pollock, assistant general manager in charge of safety and operation.

Sep 1, 1930

By E. G. King

Low-temperature heat capacity determinations of the minerals goethite and pyrophyllite were made in the temperature range from 510 to 298° K. The entropies at 298.15° K were evaluated as 14.43 ±0.15 cal/deg mole for goethite and 56.6 ±0.5 cal/deg mole for pyrophyllite. The entropies of formation from the constituent oxides are -4.4 ±0.2 cal/deg mole for goethite and -12.3 ±0.6 cal/deg mole for pyrophyllite. The standard free energy of formation of goethite from its oxides is ?G°298.15 = 0.16 ±0.20 kcal/mole.

Jan 1, 1970

1. In 2001, a total of 785 nonmetal mining operations reported employment to the Mine Safety and Health Administration (MSHA). Examples of nonmetal mining operations include the mining of clay, trona, barite, phosphate rock, gypsum, talc, gemstones, and pumice. Nonmetal mines comprised 5.4% of all mining operations.1 • Nonmetal mining operations are located in all but seven states or territories (Alaska, Delaware, Maine, New Hampshire, Rhode Island, Puerto Rico, and the Virgin Islands). • The median number of operator employees per nonmetal mine was 6.1.2 • Mines producing common clay comprised 31.2% (n = 245) of all nonmetal mining operations.

Jul 1, 2003

By Launa Mallett, Charles Vaught, Kathleen M. Kowalski, Michael J. Brnich

This paper reviews research from the U.S. mining community to define issues relevant to an evolving national and international workforce and to relate them to the emergency response population. The authors further explore and relate the key problem of an aging workforce to the resultant changes and emerging physical and psychological needs of emergency workers. Finally, the authors cite examples from the mine emergency response community and mine rescue experiences to suggest practical recommendations that include both organizational and individual formats, with an emphasis on new approaches to training this changing workforce.

By Robert Blickensderfer

Equipment and procedure for the continuous roll bonding of metal strips are described. The reels, mill rolls, and furnace were located within a vacuum chamber capable of operation at a residual gas pressure of 1 x 10-4 to 1 x 10-5 torr. Several metals were successfully clad at rolling temperatures of 930° to 1,050° C in lengths up to 120 ft. The bimetals that were clad included stainless steel to carbon steel, molybdenum and nickel to stainless steel and carbon steel, and titanium to carbon steel. Bend tests of bond integrity are described, and microstructures of the interfaces are presented. The amounts of brittle intermetallic phases formed at the interface are minimized by this cladding method.

Jan 1, 1980

By E. J. Kloos

The Bureau of Mines evaluated all previously approved gas masks to determine their ability to provide respiratory protection against each of the following six selected amines: ethylenediamine, diethylamine, n-butylamine, ethylamine, methylamine, and hydrazine. Minimum requirements were a 24-minute service life at a flow rate of 64 liters per minute (32 liters per minute for hydrazine) and an amine concentration of 1.0 volume-percent (0.5 volume-percent for hydrazine). The three masks meeting these requirements were the LG4, Willson Products Division, The Electric Storage Battery Co.; the GMD-SS, Mine Safety Appliances Co.; and the 084-PHOV-R, Acme Protection Equipment Co.

Jan 1, 1966

By E. J. Kloos

The Bureau of Mines evaluated all previously approved gas masks to determine their ability to provide respiratory protection against each of the following six selected amines: ethylenediamine, diethylamine, n-butylamine, ethylamine, methylamine, and hydrazine. Minimum requirements were a 24-minute service life at a flow rate of 64 liters per minute (32 liters per minute for hydrazine) and an amine concentration of 1.0 volume-percent (0.5 volume- percent for hydrazine). The three masks meeting these requirements were the LG4, Willson Products Division, The Electric Storage Battery Co.; the GMD-SS, Mine Safety Appliances Co.; and the 084-PHOV-R, Acme Protection Equipment Co.

Jan 1, 1966

By J. S. Hansen

The U.S. Bureau of Mines developed a system for casting unique, slotted steel armor by modifying the conventional expendable pattern casting (EPC) process that is normally used for making aluminum castings. Three innovations were added to the EPC process to make the successful adaptation: (1) Vacuum was applied to sand molds, (2) continuous narrow-necked feeding systems were used to permit the casting of thin walls, and (3) fixtures were designed to prevent pattern damage and to hold critical casting tolerances, Potential problems and defects are described.

Jan 1, 2010

By John Nagy

This circular has been prepared for the guidance of safety engineers, shot firers, and coal-mine inspectors concerning multiple blasting with short-delay (millisecond-delay) detonators. These special precautions are suggested in addition to those normally followed in blasting, as outlined in the Federal Mine Safety Codes 5 6/ and in Miners' Circular 58.7/ INTRODUCTION The use of short-delay blasting has been proposed for promoting safety and increasing the rate of production in coal mining. Ideally, short-delay blasting, as compared with equivalent single-shot blasting, reduces exposure of the shot firer to dust, fumes, and weakened roof; as compared with equivalent simultaneous blasting, it reduces roof disturbance.

Jan 1, 1959

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

C 2 Complete Hoisting Systems A Above Ground Installations A total of seven companies were identified who supply complete emergency escape hoist units for above ground installations The units have been designed predominately to meet the needs of coal mine operators to satisfy the requirements of the Coal Mine Health and Safety Act of 1969. The seven companies are as follows 1 Dover Conveyor and Equipment Co. 2. Coeur d' Alenes Co. 3. Connellsville Corp. 4. Scott Midland 5. W W Williams Co. 6. Equipment Corporation of America 7. Timberland Ellicott Table VIII contains detailed specifications and price information on each of these units. The units have a number of similarities

Jan 1, 1976

The Sago Mine Disaster, on January 2, 2006, placed renewed focus on several different aspects of safety in the underground coal mining industry. One area which received increased attention since Sago and other underground coal mining events is the concept of Safety Culture. This report describes the results of a pilot Safety Culture Assessment implemented at a small Appalachian underground coal mine, hereafter referred to as the Mine. The purposes of this pilot assessment were to (a) evaluate the feasibility and usefulness of a methodology for assessing safety culture that had previously been developed for use within other industries, (b) to initiate an investigation into the understanding and defining of the existing safety culture of the underground coal mining industry, and (c) provide meaningful and useful recommendations for the participating mine for their consideration in their ongoing quest to enhance their existing safety culture. This pilot assessment was conducted in July 2007. The report provides information regarding the presence or absence of safety culture characteristics within the Mine. Observations regarding the characteristics of the Mine?s safety culture that should be sustained are presented. Areas in need of attention and management focus to improve the Mine?s safety culture are presented as well as recommendations for moving forward. Safety culture characteristics that are important for the existence of a positive safety culture have been identified to include: - Safety is a clearly recognized value in the organization. - Accountability for safety in the organization is clear. - Safety is integrated into all activities in the organization. - A safety leadership process exists in the organization. - Safety culture is learning driven in the organization. - A process for establishing a strong and effective Safety Conscious Work Environment (SCWE) is in place. Performance objectives are associated with each of the safety culture characteristics and particular behaviors and attitudes have been identified that can be measured to evaluate these objectives. Using a methodology originally developed with the support of the U.S. Nuclear Regulatory Commission, an assessment of selected organizational behaviors and attitudes was conducted to evaluate the Mine in terms of these safety culture characteristics and their associated performance objectives. The methodology involves obtaining a variety of quantitative and qualitative information, using multiple data-gathering methods. The information collected is largely based upon the perceptions of the individuals in the organization. The evaluation is a ?point in time? snapshot of the Mine, but cultural beliefs and assumptions do not change quickly. The feasibility and usefulness of the methodology was successfully demonstrated during this pilot assessment. All aspects of the methodology including functional analysis, structured interviews with accompanying behavioral scales, work observations, and the paper and pencil

Aug 1, 2007

Cement kiln dust (CKD) is a waste product generated at the rate of 4 to 12 million tons per year in the United States. The dust has considerable resource potential as a neutralizer for coal mine waste effluents and as a lime substitute in the agriculture and construction industries. However, little information has been published on the composition and characteristics of CKD, and a concern arose over the potential environmental effects of the waste when an analysis of a single sample from West Germany revealed lead and zinc concentrations of 5,620 µg/g and 16,200 µg/g, respectively. To assess the hazardous waste potential of CKD,

Jan 1, 1983

By RV. Ramanl, KV. K. Prasad, M. Swaminathan

The objective of the research in this project is to develop a knowledge based expert system for aiding the planning of mine ventilation systems. This system focuses on mine ventilation system design from a coal mine dust control standpoint. It is recognized that mine ventilation system design is an engineering problem involving not only rote numerical calculations to solve the pressure quantity problem but also substantial judgement and expertise to analyze a problem situation and Interpret the results of an algorithmic program. The thrust of this project is to i) extract this knowledge from public domain sources and recognized experts in industry, government and academia, 11) represent this knowledge in the form of IF ... TI-IEN rules in an expert system (ES) and 111) interface the developed expert system with a mine ventilation network analysis program vis. PSUMVS (Pensylvania State University Mine Ventilation Simulator). By providing the numerical computing and qualitative reasoning aspects of mine ventilation system design in a single Integrated system, better quality decision support will be made available to apprentice users.

Jan 1, 1988

By R. V. Ramani, A. S. C. Owili-eger

? THIS PROGRAM SIMULATES METHANE FLOWRATES THROUGH THE GOAL ? SEAM BY THE GAUSS-SEIDEL ITERATIVE TECHNIQUE. THE MODEL IS A TWO ? DIMENSIONAL SYSTEM. THE ITERATIVE FORM OF THE GAUSS-SEIDEL IS ? OBTAINED FROM A PARTIAL DIFFERENTIAL EQUATION OF FLOW BY CENTRAL ? FINITE-DIFFERENCING APPROXIMATION SCHEME ? NPRESS IS THE NUMBER OF SPECIFIED PRESSURES EXCLUDING ? RESERVOIR AND FACE PRESSURES ? NQUAN IS THE NUMBER OF SPECIFIED FLOW QUANTITY.... EXCEPT FLOW ? OUT OF THE FACE. THIS- QUANTITY CAN BE POSITIVE(INJECTION) OR ? NEGATIVE ( PRODUCTION) ? XPERM(I,J) I S THE DIRECTIONAL PERMEABILITY IN THE X-DIRECTION AT THE POINT (I,J) ? YPERM(I,J) IS THE DIRECTIONAL PERMEABILITY IN THE Y-DIRECTION ? AT THE POINT (I,J) ? RESEP' IS THE RESERVOIR PRESSURE ? FACEP IS THE FACE PRESSURE. THIS PRESSURE IS ASSUMED TO BE ? APPROXIMATELY ATMOSPHERIC ? LENGTH, WIDTH, AND THICK ARE THE ZONE OR MEDIUM DIMENSIONS * PUHL I S A DUMMY NAME FOR VISCOSITY ? DMAXI IS VARIABLE NAME FOR INITIAL MAXIMUM ERROR OF ITERATION ? DMAXF IS A VARIABLE NAME FOR FINAL MAXIMUM ERROR OF ITERATION ? NITER IS A VARIABLE NAME FOR STORAGE OF NUMBER OF ITERATIONS ? RAD IS A VARIABLE NAME FOR THE SPECTRAL RADIUS OF THE GAUSS¬ ? SEIDEL MATRI-X. THIS PARAMETER ALSO MEASURES THE RATE OF ? CONVERGENCE OF THE ITERATION ? KOUNT IS AN ITERATION COUNTER ? MAXIT IS THE MAXIMUM NUMBER OF ITERATION SPECIFIED BY THE USER # EPS IS THE MAXIMUM RESIDUAL ALLOWABLE ERROR-FOR CONVERGENCE

Jan 1, 1974