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By Z. Ruetz

Portable X-ray fluorescence (pXRF) analysis has been widely adopted in the geochemical and environmental field as a cost-saving alternative to standard analyses. This paper outlines the efficacy of a method for indirectly quantifying organic copper content in solvent extraction circuits via stripping of the chelated metal with concentrated sulfuric acid in a single contact and subsequent pXRF aqueous analysis. pXRF analysis is common within the mining industry but presents unique challenges with liquid analysis, the most prevalent of which are briefly discussed. This method was developed specifically for mining operations with regional constraints and limited resources. Providing an in-field alternative to flame atomic absorption spectrophotometry and inductively coupled plasma optical emission spectroscopy, this entirely mobile XRF analysis method produces consistent and accurate results within minutes and at a fraction of the cost.

Jan 1, 2023

INTRODUCTION The SAIMM publishes technical information on various aspects of the minerals industry through several different media. (a) Monograph Series Books in the Monograph Series are high quality, detailed discussions on specialized topics. (b) Symposium Series This series consists of the proceedings of international conferences which are held in South Africa. (c) Special Publications Series This series covers titles which do not form part of the Monograph and Symposium Series. (d) The SAIMM Journal Papers published in the Journal cover al relevant areas of technical interest by striving for a balanced content and maintaining a consistently high technical standard. (e) School and Colloquia Notes The papers from al local schools and colloquia are published and handed out at registration. Should authors wish to have their papers considered for publication in the Journal, they should adhere to the guidelines outlined below.

Jan 1, 1991

Minutes of the Annual General Meeting Held at Harmony Country Club on Wednesday, 2nd August, 1978, at 7.30 p.m. Mr A. N. Shand (Chairman of the O.F.S. and Klerksdorp Branch) was in the Chair. Also present were:.... Induction of Chairman Mr A. N. Shand introduced Mr H. M. W. Eschenburg by briefly outlining his past career and achievements, and, in calling upon him to take the Chair, wished him a very successful year of office..... Address by the President of the S.A.I.M.M. The Chairman introduced Mr Von Wielligh by outlining his career and achievements. After completing his education, he joined J.C.I. in 1936 as a sampler, and from that time served the company in many capacities, culminating with his appointment to the Board in 1974.....

Jan 1, 1979

By M. J. U. T. Van Wijngaarden

SYNOPSIS The corrosion characteristics of a new steel, 14Cr, which is a modification of the well-known 3CR12, in aqueous sulphate solution were studied through polarization diagrams and a computer analysis based on the polarization¬resistance technique. It was found that the corrosion rate of 14Cr steel is independent of pH for pH values above 6, but, below a pH value of 4, the corrosion rate increases sharply with decreasing pH. In air-saturated solutions of neutral and mildly alkaline pH, the corrosion rate is approximately 60 µm per year. The 14Cr steel shows a twentyfold improvement in corrosion resistance over that of 3CR12 in sulphate solutions at pH 2,0. This is considered to be due to the beneficial effect of its higher chromium and nickel contents.

Jan 1, 1985

By Peter Smith

The construction of one of the world's largest goldrecovery plants to treat run-of-mine ore is progressing on schedule at the President Brand Gold Mine in the Orange Free State. Designed to treat 390 kt per month, the plant will recover 96 per cent of the gold from the ore at a capital cost of 160 million rands in terms of January 1983 money. It will replace the existing gold-treatment installation, as well as provide a 30 per cent increase in capacity. Mintek reports Report M161 Improved recoveries of gold from auriferous calcines and pyrites by fine milling. Report M171 The development of a versatile computer programme for the evaluation of batchflotation results. Report M178 The reduction of chromite in a transferred-arc plasma furnace. Report M179 Optimization of an inductively coupled plasma by the simplex method.

Jan 1, 1985

By J. le Grange, M. Tullmin, A. Strauss, F. P. A. Robinson, C. A. O. Henning

An experimental feritic stainless steel with a chromium content of 40 per cent was welded by laser and electron beam (EB) welding processes. These techniques were found to be particularly suited to the welding of this alloy in that the impact toughness of the weld metal and heat-affected zone (HAZ) of the laser welds compared favourably with those of the parent aloy. When the EB process was used, the impact toughness of the weld metal was over 180 J/cm2. Grain growth in the HAZ was minimal for welding with these two processes. Corosion tests, conducted in a solution consisting of 20 per cent sulphuric acid and 100 p.p.m. of potassium thiocyanate, and In a highly corrosive industrial solution, indicated that the laser and EB welds were free of sensitization effects, thus confirming the metalographic results.

Jan 1, 1989

By L. Cornish, P. A. Olubambi, J. H. Potgieter

Four 22%Cr series duplex stainless steels alloys containing varying nickel contents of approximately 5, 7, 9 and 13% were melted in a vacuum induction furnace, hot rolled, solution annealed and water quenched. Their corrosion behaviour was investigated in sulphuric acid and sodium chloride solutions using a potentiodynamic polarization technique. Increasing nickel contents have appreciable influence on their corrosion behaviour. Polarization curves show similarities in the uniform corrosion behaviour of the alloys in the solutions and a significant difference in their pitting behaviour in chloride environments. Alloy 2209 generally exhibited highest resistance to uniform corrosion while 2213 displayed distinct and best pitting corrosion resistance. Their corrosion behaviour were attributed to the influence of nickel on phase modification, microstructural refinement, and the probably types of films formed in different environments. Keywords: Duplex stainless steel; Nickel; Microstructure; Phase modification; Corrosion

Jan 1, 2006

The case for national research in mineral processing PRESIDENTIAL ADDRESS given by R. E. Robinson*, Ph.D., B.Sc. (Eng.) (Wits.) Some of you have only raised your eyebrows, some have made tactful comments, and a few of you have been fairly outspoken, but all of you in industry are concerned at the high level of State expenditure by bodies such as the National Institute for Metallurgy. The case for a national research organization in mineral processing is not clear-cut and in fairness I must present both cases - for and against. Competition for student members Each year the South African Institute of Mining and Metallurgy offers a prize (or prizes should the entries warrant it) of up to Rl00 for the best paper or dissertation on a topic appropriate to the interests of the Institute.

Jan 10, 1975

By B. Z. Weiss, N. R. Comins, F. Blum

Some aspects of the mechanical behaviour of chromium-containing dual-phase 3CR12 steel were investigated as a function of the temperature and strain rate. The yield stress was found to depend on both the temperature and the strain rate, with no substantial differences between the longitudinal and the transverse directions. The strain-rate sensitivity decreased with increasing temperature. The yield stress could be presented as a function of a temperature-strain-rate parameter. Impact test results showed substantial differences between the energy absorption of the transverse and longitudinal specimens above the ductile-brittle transition temperature. Changes in energy absorption with temperature were gradual for specimens in both orientations, and the transition from ductile to brittle behaviour occurred between 373 and 173 K. Strain rates ahead of the tip of notches with different geometries were calculated and measured experimentally.

Jan 1, 1990

By K. I. Afewu, L. C. Woollacott

The design of in-pulp adsorption vessels in the gold industry has, for the most part, been seen as a problem involving the suspension of fine particles o ore in a slurry. The need for the vessel to be designed as a mass-transfer contactor has received insufficient attention. The current series of papers addresses this need The previous paper considered the question of the scale dependence of the film transfer coefficient. This paper examines the mixing considerations that are relevant. A review of the literature and an examination of a limited set of data provide some insight into the mixing conditions needed for the dispersion of the particles of adsorbent. The mixing requirements for the suspension of the ore particles are also considered, and conclusions are drawn in regard to the design of mechanically agitated vessels for gold in-pulp adsorption circuits.

Jan 1, 1995

By P. G. Van Der Walt

This paper deals with the reticulation of deslimed tailings from surface to the stope face underground. Reference is made to the experience gained at the pilot plants operating on four of the gold mines administered by Gold Fields of South Africa, as well as at the full-scale system at East Driefontein which was commissioned recently. Mine-wide backfill systems are currently being installed on five other mines administered by Gold Fields. These six full-scale systems are capable of handling more than 270 000 tons of backfill solids per month. The type of reticulation system chosen, the selection of flowrates and the composition of the slurry, as well as the selection of the appropriate pipes and ancillary equipment are discussed. Both theoretical and practical aspects are taken into consideration. Other aspects covered include the design of underground storage dams and communication systems.

Jan 1, 1988

By P. J. F. Fourie

The purpose and frequency of comprehensive performance testing and the types of tests to be included are discussed. The results obtained from a series of such tests are reviewed.

Jan 1, 1980

By J. Levin, I. J. Corrans

Wet high-intensity magnetic separation (WHIMS) for the concentration of gold and uranium was tested on many Witwatersrand cyanidation residues, and on some ores and flotation tailings. The results varied, but many indicated recoveries of over 60 per cent of the gold and uranium. The main source of loss is the inefficiency of WHIMS for material of smaller particle size than 20fLm. The recoveries in the continuous tests were lower than those in the batch tests. The continuous tests indicated an operational difficulty that could be experienced in practice, namely the tendency for wood chips and ferromagnetic particles to block the matrix of the separator. It was decided that a solution to the problem lies in the modification of the separator to allow continuous removal of the matrix for cleaning. A system has been developed for this purpose and is being demonstrated on a pilot-plant scale. Promising results were obtained in tests on a process that combines a coarse grind, gravity concentration, and WHIMS. In the gravity-concentration step, considerable recoveries, generally over SO per cent, of high-grade pyrite. were obtained, together with high recoveries of gold and moderate, but possibly important, recoveries of uranium. A simple model describing the operation of the WHIMS machine in terms of the operating parameters is described. This should reduce the amount of empirical test work required for the optimization of operating conditions and should provide a basis for scale-up calculations. The economics of the WHIMS process is discussed.

Jan 1, 1979

By H. F. Fuls

Skorpion Zinc, an integrated zinc mine and refinery located in the south of Namibia, has a production capacity of 150 000 t/a of special high grade (SHG) zinc. The Skorpion zinc oxide resource will be depleted by 2017. Extensive exploration drilling for additional zinc oxides was conducted without success. With the abundant availability of zinc sulphide concentrates regionally (Black Mountain and Gamsberg in the Northern Cape or Rosh Pinah Zinc and new deposits in the Rosh Pinah region) the life of the operation can be extended by processing of zinc sulphide concentrates. The leach kinetics of zinc sulphides is vastly slower than for oxides, preventing the processing of zinc sulphides in the existing process under current conditions, and Skorpion Zinc faces the challenge to identify a suitable zinc sulphide treatment process that can be integrated with the existing plant. Various zinc sulphide processing options were identified through an extensive literature search and non-viable options were eliminated. Mass and energy balances were established for potential options and an economic evaluation (including capital and operating cost estimation) was conducted to identify a suitable process. It is concluded that ferric leaching of sphalerite in a sulphate medium under atmospheric or pressure leach conditions are suitable processes for Skorpion Zinc. These processes present advantages over all other zinc processing options when elemental sulphur is preferred as the final deportment for sulphide sulphur. Both these processes can be integrated into the existing refinery and will be able to process concentrates with a wide composition range.

Jan 1, 2013

The established shared laboratory facilities between the Departments of Metallurgy and Chemical Engineering of the Vaal Triangle Technikon and the University of Potchefstroom are already proving to be a great success.

Jan 1, 1992

By J. Keyser

The realization of an Integrated Technical Resource Asset Management System (ITRAMS) has so far evaded all software developers in the mining industry. The major factors that have prevented the development of such a system are limitations on software, hardware and network systems. Several factors have come together at Venetia Mine, which has made the undertaking of such a project both possible and desirable. This has led to the formation of a strategic partnership between Venetia Mine and Gemcom Software International Inc. This partnership is dedicated to develop and provide an Integrated Technical Resource Asset Management System based on Microsoft Back Office architecture, Gemcom for Windows™ and the MinRas system. This paper will elaborate on the phased approach of the integration of systems into the core repository, mechanisms of integration, the functionality of the system, final results, techno-economic benefits and general project management issues.

Sep 1, 2001

The proceedings of the Centenary Banquet that was held on Friday, 25 March 1994 at The Bal Room of The Carlton at 19:30 follow. Dr H. Scot-Russell The Chemical and Metallurgical Society of South Africa-a forerunner of this Institute-was founded at a meeting held in Johannesburg on the 24th of March, 1894. One of the traditions established early in the life of the Society was the Annual Dinner, which became a major event in Johannesburg's social calendar. It was always attended by people of stature in the industry and in the community, and was usually addressed by a high-ranking Government figure. We are delighted that, on this one hundredth birthday of the Institute, we have been able to continue the tradition. I welcome you, Mr State President, and your charming wife, and we look forward to hearing your address later this evening.

Jan 1, 1994

The South African Institute of Mining and Metallurgy mourns the passing of one of its most distinguished sons. Professor J. de V. Lambrechts died at Franschoek on 30th January, 1988, at the age of 76 years after a long illness. Mintek Application Reports A new series of Mintek reports made its appearance in 1987. These are Application Reports, which present an overall perspective of each of Mintek's technical thrusts to ensure that the existing expertise can continue to be readily accessed. The successful development of an industrial process for the recovery of platinum-group metals from the UG-2 Reef. Application Report no. 1. 1987. 16 pp. The development and implementation of a computer control strategy for conventional milling circuits. Application Report no. 2, 1987. 15 pp. The development of an integrated carbon-in-pulp process for South African conditions. Application Report no. 3. 1987. 17 pp.

Jan 1, 1988

1. Book reviews ? Second International Conference on Hydrocyclones. Cranfield (Bedford, MK43 OAT, England), BHRA Fluid Engineering Centre, 1984. £33. Reviewer: R.P. King This volume contains the 28 papers presented at the Second International Conference on Hydrocyclones, which was held in Bath (England) in September 1984. The format and presentation of the papers are similar to those of the first volume in the series, and this volume con¬tinues the series as an authoritative account of much of the research work associated with hydrocyclones that is being undertaken throughout the world. The volume was produced from camera-ready copy supplied by the authors, but the quality of reproduction is very high and both text and figures are legible throughout the volume. Although most of the work reported deals with the hydrocyclone as a classification device, important sections are devoted to liquid-liquid separations and heavy¬medium separations.

Jan 1, 1985

By P. A. J. Cabassi, B. K. Loveday, M. J. Wilkinson, P. H. Radcliffe

The recovery of gold, uranium, and pyrite from accumulated residues at mines in the Orange Free State is adversely affected by the presence of pyrophyllite, which is naturally floatable and must be prevented from floating with the desired constituents by the use of a mica depressant, and of thucholite (uraniferous kerogen), which contains significant quantities of uranium and gold but does not float readily in the presence of a mica depressant. In laboratory tests on these residues, the use of a mixture of MIBC (methyl isobutyl carbinol) and paraffin in addition to the suite of reagents normally used was found to increase the gold recovery substantially, but the sulphur grade was lower. The recovery of thucholite also increased considerably, but the proportion of uranium associated with this mineral was small. Plant trials, which are continuing, have been encouraging, indicating an increase in the gold recovery of 4,6 per cent.

Jan 1, 1983