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By Mery-Cecilia Gómez-Marroquín

O presente trabalho trata da formação da ferrita de zinco a partir da mistura e posterior reação solido-solido entre o óxido de zinco e óxido de ferro - Fe2O3 puros em proporções equimolares. A faixa de temperatura onde teve lugar a formação foi entre 1073 e 1373 K. Testes de redução da ferrita de zinco sintética-ZF e pós de aciaria elétrica–EAFD foram realizadas usando misturas de CO e CO2 que variaram entre 50 e 100% CO. Ambos os testes (formação e redução de ZF e EAFD) foram suportados usando técnicas de caracterização física, química, estrutural e microscópica. No caso da redução, foi observado que tanto a temperatura como a percentagem de CO, foram os fatores que, mais afetaram a redução de ferrita de zinco contida no EAFD. A máxima percentagem de redução foi 85%, para 100% CO, 1373 K e 105 min, e 52%, para 50% CO, 1373 K e 105 min. Por outro lado, atingiu o 100% para 100% CO, 1273K, em 80.75 min, 60%, para 50% CO a 1373 K durante 105 min.

Aug 16, 2017

By Mery-Cecilia Gómez-Marroquín

O presente trabalho trata da formação da ferrita de zinco a partir da mistura e posterior reação solido-solido entre o óxido de zinco e óxido de ferro - Fe2O3 puros em proporções equimolares. A faixa de temperatura onde teve lugar a formação foi entre 1073 e 1373 K. Testes de redução da ferrita da zinco sintética-ZF e pós de aciaria elétrica–EAFD foram realizadas usando misturas de CO e CO2 que variaram entre 50 e 100% CO. Ambos os testes (formação e redução de ZF e EAFD) foram suportados usando técnicas de caracterização física, química, estrutural e microscópica. No caso da redução, foi observado que tanto a temperatura como a percentagem de CO, foram os fatores que, mais afetarem a redução de ferrita de zinco contida no EAFD. A máxima percentagem de redução da ZF foi 85%, para 100% CO, 1373K e 105 min, e 52%, para 50% CO, 1373K e 105 min. Por outro lado, atingiu o 100% para 100% CO, 1273K, em 80.75 min, 60%, para 50% CO a 1373K durante 105 min. no caso da redução do EAFD

Aug 17, 2017

By André Carlos Silva

Dewatering stage is among the most important industrial unit operations, and is wide adopted in many different industries, due the fact that a large portion of industrial products is produced using suspensions of solids in liquids. Nowadays the mineral processing tailings disposal is a big problem due the environmental degradation produced. The phosphate rock processing in Anglo American Phosphate Brazil, situated in Catalão/Go/Brazil, generates around 180 t/h of tailings for a plant feed of 480 t/h (approximately 37,5% of the processing plant feed), with 5 to 10% of solids and approximately 14% of P2O5. Nowadays the tailings are sent direct to the tailings dam. The present work proposes the paste production using with the tailings from phosphate rock processing plant divide in two different stages. The first one composed by the free settling of the material in presence of industrial flocculants in a graduated cylinder with 2.0 L of internal volume for one hour, in the same way it must occur in conventional thickeners. After that time, the clarified liquid was drained and the remaining pulp was sent to the second stage consisting in the tailings vacuum filtration. Ten different flocculants and nine different filter media were tested. The found results were satisfactory for paste tailings production with solids percentage around 65%.

Aug 8, 2018

By Marco A. Ramírez-Argáez

A 2D mathematical model was developed for the plasma arc welding process. Computational simulations based on mass and momentum conservation equations as well as Maxwell equations were performed by using the commercial software PHOENICS. The model predicts the electric characteristics of the arc column, flow patterns, temperature contours and electrical potential, by varying the composition of the cover gas, in this case, argon and nitrogen. It was found that an arc of nitrogen with respect to one of argon generates more intense jets, greater voltages, and lower temperatures in the arc column for welding arcs current of 150 A and 10 mm arc length.

Oct 30, 2017

By Adriane Lopes Mougo

Super duplex stainless steel presents a biphasic structure composed by ferrite and austenite with different characteristics and properties. In the micromilling process the cutting edge radius has similar dimensions to the grain size. The biphasic structure found in this material could influence on the cutting tool life and the surface integrity of the workpiece. Due to its low machinability, caused by high hardening level and low thermal conductivity, the process can produce built-up edge and high surface roughness (Ra). In this work it is performed an experimental study of the micromilling of super duplex UNS 32750 and the influence of the cutting speed (Vc) and feed per tooth (fz) on the surface integrity and tool wear. The design of experiments considered two levels and three replicates. Results indicate the increase of roughness for bigger feed per tooth, small influence of the cutting parameters on the burr formation. The tool presented flank wear after the experiments.

Aug 8, 2018

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019

By Márcio Corrêa de Carvalho

Welded deposited chromium carbide overlay’s has been widely used in various branches of welding overlay’s industry related to wear. Characterization techniques are an important tool in the development of chromium carbide overlays resistant to wear, enabling the identification of phases, constituents and defects. In this work one used optical microscopy, scanning electron microscopy and energy dispersive spectroscopy on chromium carbide overlay’s deposited by submerged arc welding process. The characterization techniques identified precisely the elements of the overlay’s enabling point of the main cause of the observed defects such as cracks, porosity and clusters of particles known in the industry as " rice crispy" .

Aug 16, 2017

By Clebson Joel Mendes de Oliveira

Sulfur control in steel have been challenging process experts since the discovering of it deleterious effect on most of steel product properties. To separate this slag from hot metal is mandatory to complete desulfurization process. The preferred method is to skim hot metal surface physically removing the contaminated slag, attributing to the operator the evaluation of skimming efficiency. Thus, we present a new lower cost system using image processing methods foreseeing a future full automation skimming process.

Aug 16, 2017

By Adriana Amaro Diacenco

This work presents the finite element modeling of Euler-Bernoulli beams constituted of a metallic material, discussing theoretical and numerical aspects. The numerical analysis uses Hermitian interpolation functions and finite elements with two degrees of freedom per node. A numerical simulation will be done for uniform loading considering two kinds beams (steel and aluminum). The paper is organized as follows: introductory comments and numerical simulations to evaluate the static and dynamical behavior of the metallic beams.

Aug 7, 2018

By Jan Lampke

Increasingly pelletizing discs are used for the recycling of dust and sludge. The applied pellet feed is highly variable, for example in terms of chemical composition, grain size distribution and raw density. These raw materials related factors lead to a destabilized pelletizing process, which initially must be homogenized through special mixtures, as well as the use of binders or additives. There are many possibilities to reach stringent restriction of material related target factors. On the one hand it is helpful to be flexible by changing the process parameters of the pelletizing disc. On the other hand, it is necessary to use a material-binder-formulation, which leads to a highly stable pelletizing process. The paper deals with an example of the use of agglomerating device, pelletizing disc, to prepare different dusts and sludges for material recycling. These dusts und sludges are mostly generated in metallurgical processes, e.g. sinterplant, blast furnace and steelworks.

Aug 16, 2017

By Michael Breuer, Christian Mengel, Luis Acainas Caballero, Olaf Jepsen

Stability of the hot strip mill rolling process remains a main topic when it comes to processing thin and hard materials. Strip steering especially at the end of rolling and tail out rips are a main source of unscheduled down times in a hot strip mill. Main focus of this paper is the new X-Roll® Guide system to improve mill stability and quality. An overview of SMS group developments in the recent years regarding equipment and control strategies is given. The new side guiding system in the entry area of the finishing mill is introduced and explained with operational examples. The system provides reproducible conditions for the threading process and during rolling. Steering control has a direct benefit on the availability of the mill. New developments of the roll alignment control strategies based on roll force and mill stand entry guide force measurement will be presented. Additionally a camera based measuring system is introduced that generates a direct process feedback of the strip position. It provides together with the roll alignment control the necessary control parameters for adjusting the roll gap and guiding the strip correct centered through the mill. As a summary the SMS group system is explained combining all features.

Oct 1, 2019

By Luciana Lezira Pereira de Almeida

With the increasing use of ornamental rocks, mainly in civil construction, sundry problems were identified in relation to rocks cutting, such as efficiency in the cutting process and rock quality lumber. In recent years several composites have been developed to solve these problems. In this context, the study of the binomial matrix metal-diamond interaction is of paramount importance for the development of new composite materials to improve the efficiency of the cutting tool. The diamond impregnated matrix metal often reveals a reaction between the diamond surface and the matrix. Besides the mechanical connection, chemical reactions can sometimes occur. Therefore, this study aims to assess the achievement of diamond composites in the system Fe / Cu / Ni / Sn via powder metallurgy, with added CRB2. Analyzes have been performed to characterize chemical / physical and mechanical. The results have showed that addition of CRB2 promote significant changes in the properties of composites, especially in wear resistance and fracture toughness. Furthermore, the presence of the composite CRB2 causes a significant improvement in thermal stability.

Aug 16, 2017

By Andreas Jungbauer

The Chinese steel producer Rizhao Steel is now focusing on the highly attractive local and export markets for high-quality, thin-gauge strip products. The first line of five Arvedi ESP plants began operations in the spring of 2015. The new casting-rolling complex is designed for a total annual production capacity of 11 million tons of highquality, ultra-thin, hot-rolled strip products with widths of up to 1,600 mm and thicknesses down to 0.8 mm. The energy consumption and related costs are reduced by up to 45% compared with conventional casting and rolling processes. This also means a major reduction in CO2 emissions. During the project phase, the plant personnel from China received extensive training at the licensor’s plant – Acciaieria Arvedi S.p.A. in Italy – to prepare them to deliver the best operational performance with the new state-of-the-art endless casting-rolling facility. The plant setup, the training and support program, as well as the latest results from the start-up are presented in this paper.

Aug 16, 2017

By Günther Staudinger

Aperam is a global player in producing of stainless, electrical and special steel qualities. The steelmaking plant in Timoteo Brasil is equipped with one AODconverter for stainless steel and one MRPL-converter for special steel production. The MRP-L converter is almost in operation for 20 years. In order to improve production Aperam decided to install a new converter with increased reaction volume equipped with DANIELI state of art technology. This paper describes the major changes and improvements of the new converter installation.

Aug 16, 2017

By Christiano Gianesi Bastos Andrade

Clays with high content of smectite are denominated bentonites, and are widely used in industry as, for example, agents for bleaching of vegetable oils, animals and minerals. For this use, the smectite clays are treated with inorganic acid of high concentration at temperatures under boiling point, which provide the bentonite´s bleaching power. In the present study, a sample of smectite from Cubati, Paraiba, Brazil, was submitted to treatment under moderate conditions (90°C, reaction times of 1, 6, 12, 18 and 24hours in close reactor, concentration of the aqueous solution of hydrochloric acid 1.5 M, acid solution/clay ratio of 1g/10mL), aiming to reduce impurities, responsible for the color of the clay, without causing significant changes in their structure. Thus, clay can be used in the cosmetics industry and other products with high added value. The treated clay was characterized by scanning electron microscopy (SEM), stereomicroscopy, energy dispersive X-ray detector (EDS) and X-ray diffraction (XRD). It was observed a bleaching in samples with time of 12h to 18h. With the DRX was possible to monitor the peak intensity of the clay structure and the sample with 12 hours of treatment was not significantly altered its crystalline structure, maintaining the peak clay at d001. The most pronounced changes in the bleaching occurred within the first 12 hours of acid treatment.

Aug 8, 2018

By Breno Totti Maia

Due to operational conditions and locations, BOF suffers variations in important parameters whose effects on the liquid bath are usually neglected. The present paper investigated two aspects: inner BOF pressure and oxygen temperature in the stagnant reservoir. The results have shown that oxygen temperature changes properties like density and velocity but has small influence on jet penetration. The BOF inner pressure has significant influence on jet penetration and creates a new challenge regarding nozzles dimensions considering overexpanding and underexpading jets.

Oct 30, 2017

By Armando Vazquez

When water enters the EAF, some chemically dissociates to H2 while some remains as H2O vapor. Depending on operating conditions the levels of combustible gases (CO and H2) and H2O are continually changing throughout the course of any individual heat and on a heat-toheat basis. The EFSOP® system has been implemented in more than 80 installations as a powerful tool to reduce furnace operation costs but with water detection technology the off gas technology is a valuable solution to improve safety. This paper describes the latest results when using Tenova Goodfellow’s new standalone water detection technology that for the first time provides real-time analysis of both H2O vapor and H2 from start-to-end of a heat. It involves a newly designed water cooled probe and heated line that eliminates condensation during off-gas sampling and an analyzer equipped with a proprietary system for analyzing both H2O vapor and H2.

Jul 30, 2018

By Armando Vazquez

This paper will provide an overall technology update on Tenova’s modular i BOF® technology package for improved endpoint detection (Carbon and Temperature), slop detection and auto-tapping control, with a primary focus will be on Tenova's Slop Detection System (SDS). Accurate Slopping prediction is a critical tool in the operation of a BOF. It provides the steelmaker with an additional protective system to increase yield & productivity while reducing operating costs. Tenova Goodfellow's i BOF® slop-detection technology uses lance vibration analysis with real-time alerts to give steel makers advance warning of the onset of a slop and a measurement of the slop severity. The system is designed to provide direct feedback control of lance position and oxygen flow rate, for rapid mitigation of potential slopping events. This paper will provide a summary on how the i BOF® technology package has been implemented, including trials and general results.

Jul 30, 2018

By Beatriz Pereda, Ana Clara Fonseca da Silva, Tiago Seixas Bittencourt

Reinforcing steel bars are usually specified based on mechanical properties with flexibility in chemical composition and processing. Most developments, in these steels, are normally focused on alloy and process design to reach minimum cost and conformity to specification. Processing routes using quenching and self-tempering (QST) and accelerated cooling are the most common. Microalloying with V and Nb have been used in rebar. When acicular constituents must be avoided, a combination of Nb microalloying with judicious control of cooling is one of the preferred options. Niobium can contribute to improvement in tensile properties through austenitic grain size control during hot working, precipitation hardening due to carbonitrides or clusters, and hardenability increase. In the present work the alloy design and development processes of a Nb microalloyed steel for rebars are presented. The designed steel has fulfilled the required specification and is under regular production. Austenitic grain size refining – when comparing with the “basic composition” normally used was observed, even without any change in the thermomechanical processing cycle. There are indications that precipitation hardening may also occur. Results indicate that Nb is a good alternative as a microalloying element in rebars.

Oct 1, 2019

By Frank Schrama

The Steel Plant Model (SPM) is an advanced logistic simulation model for steel plants. With the SPM, bottlenecks can be solved and logistics can be optimized. Both existing plants and greenfield designs can be simulated. All movements and actions simulated, from hot metal to cast products. Not only all major equipment and their relevant components (like a sublance) are simulated, but also ladles, scrap boxes, transfer cars and cranes. The whole plant is simulated in 3D and actual distances and speeds determine transport times. The SPM includes process time deviations and equipment downtimes for maintenance or unexpected breakdowns. This ensures more realistic and reliable results. Logistic optimization is based on comparison of different scenarios. For a new scenario, equipment and practices, etc. can easily be modified, added or removed. At the same time the SPM produces all relevant data for every new scenario, which can be presented conveniently. This makes the SPM the ultimate tool to find bottlenecks or optimize plant logistics. The SPM is validated for several plants world-wide, with different characteristics and layouts. The SPM not only realistically simulates existing plants with all utilizations, crane movements and waiting times, but also to accurately predicts the influence of plant modifications or unexpected events like breakdowns. Given the flexibility of the SPM, any (new) steel plant can be simulated quickly when a layout and the requested data are provided.

Aug 16, 2017