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By Jerry L. Huiatt

An accurate and reproducible procedure was developed using the gas-liquid chromatograph to quantitatively measure oleic acid on flotation products and in flotation water phases. The method comprised extraction of the oleic acid from the mineral surfaces with alcoholic NaOH, esterification of the extracted oleate, and chromatography of the methyl ester with an internal standard. Quantitative analysis of oleic acid on flotation products from test tube and bench-scale flotation tests with pure minerals and with natural ores proved the applicability of the method on a variety of minerals. The accountability of oleic acid added was 100 percent, ±5 percent.

Jan 1, 1968

Reduce the time, complexity and expense of dissolving metal and mineral samples in solution in preparation for chemical analysis. Approach In earlier research, the Bureau of Mines developed a rapid and inexpensive method for the dissolution of mineral and metal samples in plastic pressure bottles heated in a boiling water bath. Using this technique, samples could be prepared for chemical analysis in less than one hour compared with several hours by traditional dissolution methods (see Technology News No. 85, December 1980 for further details). By heating in a microwave oven, sample dissolution time can be reduced to approximately 5 minutes.

Jan 1, 1983

By J. Douglas Causey

In 1984, at the request of the Bureau of Land Management, the Bureau of Mines studied 29,020 acres of the 43,165-acre Terry Badlands Wilderness Study Area (MT-024-684) in order to evaluate its mineral resources. Within this report, these 29,020 acres are referred to as the study area. Located in Custer and Prairie Counties, MT, the study area is about 2 miles northwest of Terry. The study area is underlain by essentially flat-lying units of the Fort Union Formation of Paleocene age with some Quaternary alluvial deposits in stream valleys. No mines or prospects were found in the study area. Bentonitic clays and lignite coal units were examined and sampled; however, no clay resources or coal reserves were identified. Estimates of coal resources will be reported by the U.S. Geological Survey in a joint U.S. Geological Survey-U.S. Bureau of Mines publication. Gravel along the Yellowstone River, a source of agate for private collectors, could also be used as sand and gravel aggregate although material on the south bank of the river is closer to population centers and road systems. Clinker found in the study area could be a source of road metal, but is not well situated in relationship to areas of use. No geothermal resources have been identified although water suitable for direct heat applications may underlie the study area. All the area is leased for oil and gas exploration.

Jan 1, 1985

By L. A. Panek, A. J. Barry, John A. McCormick

"INTRODUCTION During recent years, roof bolting has become widely accepted as a systematic method of supporting both coal- and metal-mine roofs. Today, over 2 million roof bolts are installed monthly. Most of the information on bolt installation procedure reported to date (1,2,3,4,5,6) 3/ has been obtained by trial and error by individual groups or operators. To insure good roof control, experience and field tests have indicated that roof bolts should be installed immediately after the exposure of new roof, and they should be preloaded enough to minimize sag of the roof over the opening. The question of the proper initial preload for roof bolts is under study, although it is a general practice to impose an initial load on a bolt of approximately 10,000 pounds. This created a problem of measuring bolt loads at installations in underground mines, which was partly solved by using a commercial-type torque wrench; a device that permits a direct reading of the torque applied to the nut on a roof-bolt assembly from which the corresponding load can be determined by referring to specifications furnished by the manufacturers. However, considerable apprehension was expressed regarding the accuracy of this measuring procedure because of variations in the manufacture of roof-bolting materials and the degree of care exercised in making bolt installations. In the process of loading a bolt, only a small part of the effort is expended in producing strain in the bolt - the larger part of the effort is used in overcoming frictional effects in the nut-bolt-washer assembly. These frictional effects are subject to many factors, such as condition of threads, type of lubrication, if any, the finish on the nut and bearing plate, and the alinement of the bearing plate on the bolt. The object of this investigation was to determine the accuracy with which the load developed in a slotted-type roof bolt installed in a conventional manner in shale or sandstone roof rock can be determined from the torque applied to the nut.This report is the first of a series relating to basic research in roof bolting in underground mines. A future report will cover results obtained using expansion-type bolts under similar conditions. Other reports will consider the efficiency of bolt anchorages, the long period stability of bolts, and the design of safe and efficient roof-bolting systems."

May 1, 1953

By J. R. Long

The investigations described herein are concerned with a portion of a systematic research, by the Federal Bureau of Mines on ductile titanium. The Bureau's work on the metal has resulted in development of a semi commercial process for the preparation of titanium and has also made available significant information on the fabrication and physical properties of this new strong, light, corrosion-resistant metal. Considerable interest has been aroused by this work, and a number of other laboratories have begun similar investigations. However, the necessity for Consolidating titanium by normal powder metallurgy methods presents difficulties in producing commercial forms and shapes on a large scale. This investigation was therefore undertaken for the purpose of improving the technique for consolidation of titanium powder into solid nonporous metal.

Jan 1, 1949

By R. Blickensderfer

An impact wear testing machine was devised by the Bureau of Mines that simulates the repeated impact conditions encountered in large milling and grinding operations where breakage and spalling are problems. The apparatus provides data on materials that may help in the design of alloys with improved resistance to deformation, spalling, and breakage. The test blocks are 2 in thick by 6 in by 8 in. Impacts are produced by dropping 3-in-diam balls weighing 4 lb from a height of 10 ft. Tests were run until breakage occurred or to a total of 100,000 impacts. Four types of failures of the test block were observed: (1) cold flow of the bulk material by plastic deformation, (2) flaking of the surface in the impact region, (3) spalling of the block to form a crater in the region of impact, and (4) breakage of the test block into two or more major pieces. The effects of composition, heat treatment, microstructure, and hardness on types of failure are discussed.

Jan 1, 1983

By R. V. Ramani, R. Bhaskar

"IntroductionThe behavior of dust clouds in mine atmospheres has been a subject of longstanding interest due to both health and safety reasons. Pioneering studies in Germany and SMRE focussed on ambient dust concentration, principally aimed at determining optimum velocities for effective dilution. A summary of studies related to this area is provided by Hall,(l) Efforts to understand dust deposition from the explosion hazard point of view led to experiments in return airways (2-4) followed by experiments in longwalls.(5) Concerted efforts, either experimental or theoretical, were not made until recently to relate ambient concentration with dust deposition in mines. In 1974 Hwang et a1 (6) developed a computer model to predict dust concentration which considered deposition-concentration relationships. Also, experimental studies involving concurrent dust deposition and ambient concentration were conducted in the U.S. by Courtney et al (7 ) in operating mines. Efforts to relate theory with experimental results have been made by Owen (8) and Hwang et al (6 ) for dust deposition. There has been limited work, however, to determine the application of the theories and assumptions from aerosol sciences for modeling dust flows in mine atmospheres. (9 ) This is the objective of the work currently underway in the Generic Technology Center on Respirable Dust since· 1983 under a project titled, ""Prediction of Ambient Dust Concentration in Mine Atmospheres."" The scope of the project activities include:1. Development of a mathematical model to predict dust deposition and concentration in mine atmospheres.2. Experimental studies on dust transport and deposition in mine airways.3. Comparison of the model results with the experimental data."

Mar 1, 1989

By J. Tomlinson

Shuttle car trailing cable splices were tested for resistance to failure upon being subjected to repeated bending, abrasion, and tensile shocks using a new testing method that closely simulates shuttle car induced stress. The results show that under normal stresses, splices can be made to withstand the equivalent of three months of operational use. Restoring the tensile strength to the conductors is found to be as critical as restoring flexibility. Splices in which the conductors are of slightly unequal length did not present as serious a workmanship problem as previously thought since test results show that the conductors tend to equalize when longer cables, in contrast to short cables employed in previous testing methods, were used. Dynamic recordings of cable tensile stresses are presented for a shuttle car and the new simulated testing method. Two simple but effective methods for removing insulation using a knife and a pair of pliers are described. None of the designs tested for a sacrificial splice covering were satisfactory.

Jan 1, 1979

By S. P. Kinney

[The blast-furnace operator is often confronted with the problem of determining the size of the materials which are used in the furnace burden. The statement is heard that the coke is larger or smaller or that certain ore is finer than that previously used. A screen analysis of the materials used gives a measure of the different sizes of materials in an aggregate. When one is fine and the other is coarse, the difference is obvious; but when the materials are of similar sire, it is more difficult to estimate the degree of finances or coarseness. In considering raw materials it would be desirable to be able to judge the size of the radio ideal materials entering the furnace and the burden as a whole, by one representative value, such as the average size of particle. Previous work by Perrott and Kinney3 developed a method for measuring the average size of particle in a mass of finely ground materials, and an attempt will be made to apply this method to the materials included in the blast-furnace charge and to the entire burden.]

Jan 1, 1930

By Irving Hartmann, F. P. Christofel, John Nagy, E. B. McGibbeny

"INTRODUCTION When permissible explosives are used in c procedure recommended by the Bureau of Mines 5/ they are relatively safe, and, no mine explosions are known to have resulted from this type of blasting. However, unsafe blasting practices - the use of nonpermissible explosives or the improper use of permissible explosives - have caused many serious disasters. In fact, such unsafe practices constitute the third most important cause (exceeded only by electricity and the use of open lights and smoking) of coal-mine explosions in the United States. During 1929-1947, inclusive, 81 explosions, resulting in 475 fatalities, were ascribed to unsafe blasting. 6/The hazards of black powder, dynamite, and other nonpermissible explosives in coal mines have been recognized for many years, and attention has been called to this in numerous Bureau of Mines publications. Not only can these explosives ignite flammable gas-air mixtures readily, but they can also ignite coal dust, as has been illustrated repeatedly in tests and at educational public demonstrations at Bruceton and elsewhere. 7/Research in the Experimental coal mine 8/ of the Bureau of Mines at Bruceton, Pa., and unfortunate experience in commercial mines have proved beyond doubt that improper use of explosives that have passed the official permissibility tests can cause as explosions. In limited tests with a fey American permissibles at Bruceton, and in more, extensive tests with permitted explosives at the Polish experiment station, 9/ explosive charges were fired from steel cannon and freely suspended in coal-dust clouds. In these experiments coal dust was ignited under some conditions. However, it has never been definitely established whether permissible explosives can initiate coal-dust explosions when fired in a coal seam. It is true that a few mine explosions were strongly suspected to have resulted from ignition of coal dust by misuse of permissibles, but in each case other complicating factors introduced some doubt in the minds of the investigators. Full knowledge of the problem is important, because coal dust is present in most blasting operations in coal."

Apr 1, 1952

By Dennis A. Long

"The size of off-highway trucks has increased substantially over the last decade, bringing about a radical change in truck maintenance practices and procedures. As a result, surface mine maintenance mechanics today are faced with the increased hazards of working with larger and heavier tools and components and doing repairs at greater heights, thereby exposing them to a high potential for serious injury or death. Not surprisingly, the number of accidents involving truck maintenance mechanics is significantly increasing.The Bureau of Mines has assessed the haulage truck maintenance safety problem, analyzing maintenance-accident data over the 7-yr period, 1978- 84, in terms of personnel, job activities, truck components and systems, tools involved, and truck design. This assessment, based on the review and interpretation of 1,225 haulage truck maintenance accident reports, identified major factors contributing to these accidents. Overall, young, inexperienced workers are involved in most accidents. A typical maintenance accident involves a male mechanic under 33 yr old, with less than 5 yr job experience. INTRODUCTIONOver the past decade, surface mine maintenance and repair operations have changed radically. The number of maintenance personnel has grown along with the hazards of working with larger and heavier components at greater heights and with larger and heavier tools. Furthermore, transfer of skills from over-the-road vehicle mechanics is not as feasible as it once was, because of the ever increasing size of mining equipment and the complexity of its design. In short, surf ace mine equipment maintenance and repair has become increasingly sophisticated as well as labor intensive, necessitating further research and evaluation in terms of both safety and efficiency (1, 7-8) 2"

Jan 1, 1986

By W. Miola, R. V. Ramaoi

"The MSHA prescribed method for the determination of quartz in airborne respirable-dust samples from underground coal mines is the P-7 method, a combination of /ow-temperature, radio-frequency ashing (LTA) and infra7 red analysis (IR). There is no prescribed procedure for quartz analysis in bulk samples of coal and host rock. Dispersive infrared (IR), Fourier-transform infrared (FTIR) and X-ray diffraction (XRD) methods are most commonly used for the analysis of quartz in powders. Several aspects of the experimental procedures, such as the preparation of the analysis sample from bulk samples, ashing techniques, scanning procedures, peak measurement location, calibration techniques, sample amounts, size consist and data interpretation, affect the results from each of the methods differently. Significant differences in analytical results obtained from X-ray diffraction (XRD) and infrared spectroscopy (IR) on the same samples are reported. All studies point to the need for reliable quartz analysis methods.In a recent research program, a procedure for preparing bulk-coal and host-rock samples for quantitative quartz analysis was developed. Further, the results from X-ray diffractometry and infrared spectroscopy for quartz content on identical samples were compared. Calibrations with pure and mixed standards were used to assess the influence of particle-size distribution, matrix and calibration on the analytical results. In this paper, several issues concerning the measurement of quartz in the samples of coal, host-rock and airborne respirable dust from mines are outlined and quantified. IntroductionThe literature on coal-mine airborne-dust control has identified a need for a better understanding of the sources, mechanisms and amounts of quartz in mine airborne respirable dust (Althouse, 1984; Jankowski, Nesbit and Kissel, 1985; Ramani 1988; Qin, 1988; Bhaskar and Xu, 1990; Bhaskar and Li, 1992; Ramani, Qin and Miola, 1991 ). To understand the quartz content in the source materials, bulk samples of coal and host rock must be analyzed. Establishing an analysis procedure for determining the quartz content in bulk-coal and host-rock samples is necessary for identifying the sources of quartz in mines; for establishing the relationships between the quartz contained in the source and in the airborne dust; and for controlling the content of quartz in the mined product and in the airborne respirable dust."

Dec 1, 1996

By William C. Larson

This Bureau of Mines report discusses uranium in situ leach mining in the United States to acquaint the public with an overview of this emerging mining technology. This report is not intended to be a technical discussion of the subject matter, but rather should be used as a reference source for information on in situ leaching. A list of in situ leaching publications is included as well as engineering data tables for almost all of the active pilot-scale and commercial uranium in situ leaching operators. These tables represent a first attempt at consolidating operational data in one source, on a regional basis. Additional information is given that discusses the current Bureau of Mines uranium in situ leaching research program. Also included is a listing of various State and Federal permitting agencies, and a summary of the current uranium in situ leaching operators. Finally, a glossary of terms has been added, listing some of the more common terms used in uranium in situ leach mining.

Jan 1, 1978

By E. H. Denny

"IntroductionOn May 27, 1927, a coal-dust explosion occurred at the Palagua No. 5 mine of the Victor American Fuel Company, Delagua, Colorado, resulting in the loss of even lives and in and in considerable damage to the main slope and to several overcasts the explosion did not extend into the mine working where 125 additional men were employed but escaped uninjured. It is believed that the saving of these 125 men and the evidence of large property loss were due in a large measure to coal-dusting and of other sanity measures taken by the coal company management. A number of features connected with the explosion and mine safety practice seem worth the attention of the mining public and grateful acknowledgment is made to the Victor American Fuel Company for its aid in assembling the data herein contained."

Nov 1, 1927

By F. L. Wideman

Materials handled at metal and non-metal mines in the United States increased 10 percent compared with those of 1965 as a result of expansions in output at existing mines and development of others to meet increasing demands for mineral products. The tonnage of commercial materials mined or quarried increased as did the quantity of waste handled. Crude material from which metal or nonmetal products were derived comprised 71 percent (75 percent in 1964) of the total materials handled. Great strides were made in mining technology and there were indications that, in the future, earth moving by the mining industry will involve materials-handling systems of increasing size and complexity. Materials Handled.-Output of ore and waste at metal and nonmetal mines and quarries in the United States in 1966 totaled 3,518 million tons (3.213 million tons in 1965). The quantity of materials handled has increased at an average annual rate of 5 percent since 1962. Ore production increased 4 percent over that of 1965, also comparable to the average annual rate of increase in the last 5 years. Waste removal in 1966 increased 25 percent over that of the previous year.

Jan 1, 1967

Develop a simple and practical technique to measure in situ rock mass properties for realistic design and stability evaluation of underground structures. Background The Bureau of Mines has developed basic principles and techniques to determine in situ rock mass properties including Poisson's ratio, deformation modulus, and yield and failure strengths. An instrumentation package consisting of three pressure cells is installed in a single drill hole. Cell pressure response data are acquired and used to calculate and determine the rock mass properties. How It Works A test hole of BX size (approximately 5.7 cm) or larger is drilled to the approximate depth of the measuring point. The last portion of the test hole is drilled with precision bits to EX size (approximately 3.8 cm). The instrumentation package, which consists of one 3.8-cm-diameter cylindrical pressure cell (CPC) and two 5.7-cm-diameter cement-capsulated, flat borehole pressure cells (BPC's), is then installed. A complete history of cell response to changing strata loads is acquired on a continuous basis with a chart-type hydraulic pressure recorder. From these cell pressure data, Poisson's ratios, deformation moduli, and yield and failure strengths are calculated and determined.

Jan 1, 1990

By L. E. Geyer, W. W. Adams, M. G. Parry

"More than 73 million pounds of rock dust were used by the bituminous-coal-mining companies in the United States during 1930 to present or limit loss of life and destruction of property from explosions of gas and coal dust in underground mining operations, according to statistics compiled by the United States Bureau of Mines from reports furnished by mine operators. The mines using rock dust produced 65. 691, 753 tons of coal during the year, more than 30 percent of the total production of bituminous coal from underground mines in the United States that year. Although only 382 out of a total of 5,629 active underground bituminous mines applied rock dust to underground working as a precaution against explosions, they were chiefly the larger producing mines, employing 25.4 percent of all of the underground bitumious mine workers in the United States and accounting for 27.4 percent of the total number of man-hours worked underground at bituminous mines.a summary of the reports for the 382 mines using rock dust showed a total production of 96,691,755 tons of bituminous coal, 89,503 men employed underground, and 129,718,965 man-hours worked by the underground employees. (See tables 1 and 2.) These mines averaged 8.76 pounds of rock dust per ton of coal shown by reports from 385 mines using rock dust in 1932 (See table 3.)"

Nov 1, 1935

By James V. Kelly

During the spring and summer of 1947, the Bureau of Mines conducted an investigation and core-drilling program in the vicinity of the Rodham mine, approximately 4 miles north of Shullsburg, Wis. This work was undertaken as a part of a general study of the zinc and lead-producing area of southwestern Wisconsin. Work in the Rodham-mine area was done to investigate further a mineralized area frilled in part by the Puritan Exploration Co., a Delaware corporation, with offices in Galena, Ill. Some significant lead-bearing samples were obtained, but no continuous ore body was disclosed as a result of the Bureau of Mines work.

Jan 1, 1949

By M. A. Schellhardt

"INTRODUCTION The augmented demands for natural gas in many parts of the United States as a result of war have increased the need for information regarding the producing characteristics of natural-gas and gas-condensate-type wells capable of delivering large volumes of gas, as such information is important to the formulation of conservative and efficient operative and recovery practices.,For many years, the capacity of natural-gas wells to produce gas has received studied consideration by Bureau of Mines' engineers, and three reports 3/ on gaging gas-well capacities have been published. In Report of Investigations 2929, Pierce and Rawlins point out that for accurate gaging, the actual pressures at the face of the sand in the well and the relationship between such pressures and the rates of flow of gas through the sand must be determined. Their report describes a method of attacking the problem of determining the actual pressures at the sand by means of observations of pressures and volumes at the wellhead.In Report of Investigations 2930, Pierce and Rawlins explain how the fundamental relation"

Aug 1, 1944

By B. W. Jong

The U.S. Bureau of Mines investigated anhydrous chlorination and caustic-acid leaching processes to recover Ni, Co, Mo, and W from waste hydroprocessing catalysts. In batch laboratory-scale equipment, the chlorination process extracted 61 to 99 pet of the metals. Final recovery was 65 to 99 pct. The caustic-acid leaching process extracted 81 to 98 pct of the metals. Final recovery was 36 to 99 pct. Chlorination processing included roasting, chlorination, hydrolysis of metal chlorides for recovering Mo or W, water leaching of Ni or Co from the spent charge, purification, and solvent extraction or precipitation of Ni or Co from the purified solutions. Caustic-acid leach processing included NaOH leaching, solvent extraction of Mo or W from the NaOH leach liquor, H2S04 leaching of the NaOH leach residue, purification, and solvent extraction or precipitation of Ni or Co from the purified solution. The estimated fixed capital cost for a commercial-scale plant processing 39,000 Ibid of waste Ni-Mo-AI catalyst was $8 million for the chlorination process and $9.6 million for the caustic-acid leaching process. The estimated operating cost was about $0.20 and $0.40 per pound of the waste catalyst, respectively, for the two processes.

Jan 1, 1989