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By C. W. Davis

Two general schemes have been used for the determination of gold and silver in material containing considerable quantities of copper ; one is known as the " all fire " method , and the other as the , " combination " , or " wet and dry" method . The all fire crucible method , using an excess charge of litharge , has been found satisfactory when the copper content of an ore is under 6 per cent , ( Loevy , J. , Zur Edelmetallbestimmung in hochprozentigen Kupfererzen : Chem. Ztg . Jarhrg . 35 , 1911 , p . 278 ) , or where the precious metal value is so great that a small sample can be used . In the latter case , silica is added until the copper ratio is sufficiently low . If there is more than 6 per cent of copper in an ore , the lead button obtained from a crucible fusion will require repeated scorification before . it can be cupelled successfully . Rescorification is not only tedious , but also causes a slag loss of precious metals . In combination methods , the copper is dissolved , and the gold and silver in the residue . is determined by fire assay Although some combination methods have given satisfactory results for gold and silver , they are not applicable when an estimation of the platinum metals is required . Since substances containing platinum are frequently high in copper , a study of methods which might be used for the estimation of small quantities of gold , silver , and the platinum metals in such material was considered worth while . The estimation of platinum in ores by fire assay methods has been described in Technical Paper 270 of the bureau; ( Davis , C.W. , The detection and estimation of platinum in ores : U. S. Bureau of Mines Tech . Paper 270 , 1921. ) the present paper , which is supplementary to that report , deals chiefly with the application of combination methods , taking them up to the point where the fire assay is to be applied .

Mar 1, 1921

By T. A. Sullivan

High-purity vanadium metal was prepared by electrorefining commercial vanadium in a molten sodium bromide, potassium bromide, and vanadium dibromide electrolyte. Variables investigated were operating temperature, current densities, electrolyte composition, and condition of the anode. The purity of the refined metal was in the range of 99.95 percent vana-dium. Iron and oxygen in the 50- to 250-ppm range were the only major impurities. Metal with hardness numbers of 50 to 60 in the Rockwell F scale was prepared from feed material with a Rockwell B hardness of 90. The arc-melted metal was highly ductile and could be cold-worked into sheet or foil.

Jan 1, 1965

By W. A. Dunkley

During the past year and a half the Western United Corporation of Aurora , Illinois , has been distributing carburetted water ges from its Lockport , Ill . , plant , to an extensive territory , under an initial pressure ranging up to 90 lb.. per sq. in . The most distant distributing point on the system is at Harvard , Ill . , about 35 miles from the plant.. The territory supplied is approximately 85 miles long and 35 miles wide , the total mileage of rains being 1223 , or approximately 24 per cent of all the gas trains in Illinois outside the city of Chicago .

Feb 1, 1923

By R. J. Gajan

As part of its research program on secondary metal refining, the Federal Bureau of Mines has developed a fast method for determining aluminum, iron, copper, cadmium, and lead in zinc-base alloys. The new method is intended for use by trained technicians in laboratories with inexpensive equipment. It can be used either in the analytical laboratories of the many small plants that are characteristic of the secondary metals industry or in laboratories engaged in basic research to improve refining processes. A complete analysis for the foregoing elements can be made in less than 3 hours from a single sample in solution. The method is especially helpful when a small amount of sample is available. Aluminum and iron are determined spectrophotometrically and the other elements polarographically. The new method is now being used for control analysis in metallurgical research, and the results compare favorably with previously used spectrographic methods. Luke and Braun4/ described a photometric method for the determination of aluminum in zinc diecasting alloys in which the aluminum was complexed with Aluminon reagent (ammonium salt of aurintricarboxylic acid), forming a red lake. An adaptation of this method was used for determining aluminum. Beers law is obeyed between 0.01 and 0.06 milligram of aluminum.

Jan 1, 1961

By F. P. Haver

The purpose of this investigation was to determine the effect of common impurities, that is, oxygen, nitrogen, carbon, and iron, on the Brinell hardness of electrolytic titanium. On a weight basis, nitrogen had the greatest hardening effect, followed by oxygen, carbon, and iron in order. The hardening effects of oxygen and carbon were almost identical up to a concentration of approximately 0.1 percent by weight. Above this concentration, the relative hardening effect of carbon decreased rapidly, possibly because of its limited solid solubility in a-titanium. Hardness vs. composition curves for both oxygen and nitrogen were essentially straight lines over the range of Brinell hardness numbers (B.h.n.) covered in the investigation. The hardness of titanium was also determined as a function of the percentage of impurity atoms. On this basis, iron in concentrations up to 0.17 atomic percent had a greater hardening effect than either oxygen or carbon. INTRODUCTION Determination of the as-cast hardness of arc-melted titanium is a method of quality control widely used in industry. Numerous studies4/ have been made of the effect of impurities on the hardness obtained by this method. However, most of them have been based on the use of either iodide titanium or commercially pure Kroll sponge (B.h.n. >90), as a starting material.

Jan 1, 1959

By R. Hogg

"The problems of sampling particulate materials, and of characterizing the distributions of particle size and composition are reviewed. Requirements for sampling from comminution systems are discussed and a simple formula is presented for estimating the minimum sample size needed. The limitations and errors associated with the techniques available for particle size analysis are evaluated and guidelines are suggested for the selection of appropriate methods. The use of microscopic and macroscopic approaches to the characterization of particle composition are discussed.INTRODUCTIONComminution is a process of particle size reduction in which the goal is to produce a material with a specified particle size distribution from a coarser feed. In mineral processing applications, the product size distribution is often qf secondary importance to the extent to which individual mineral grams can be liberated from one another. However, due to poor understanding of the nature of the liberation process and the lack of reliable procedures for characterizing it, the actual specification is normally in terms of particle size.Particle size distribution can be regarded as the fundamental characteristic of a particulate system. The distributions of particle shape and composition among the various particle sizes present are often sufficient to define the bulk properties and behavior of the system. Description of the distributions of size; shape and composition of the different phases which may exist within individual particles is necessary to complete the picture and is especially important for predicting liberation etc., in comminution processes. It is quite obvious that · the complete characterization of real particulate systems is a formidable, if not .impossible task. Practical characterization procedures should involve ·evaluation of those characteristics which are deemed to be important and which can be measured. In comminution systems, this should ideally include the particle size distribution, the size-by-size distributions of particle composition, and as much information as can be acquired on the internal composition and structure of individual particles. In most cases, of course, we fall far short of even this rather limited goal."

Jan 1, 1988

By Eugene T. Sheridan

The 25th annual survey of the peat industry by the Bureau of Mines, United States Department of the Interior, disclosed that 79 companies produced and sold peat from 81 operations in 21 States in 1958. Peat is a carbonaceous deposit, formed under water or in a water-saturated environment from plant material. It is the first stage in the development of coal and, when properly dried, can be used as fuel. Although 98 percent (estimated) of the total world production is used for energy purposes, the status of peat in the United States is somewhat unique in that none is used for fuel, and practically all is consumed as an agricultural product, chiefly for soil improvement purposes. The domestic peat industry has expanded rapidly since World War II, and production in 1958 was 327,813 net tons valued at $3,445,767. More than one-half million ton of peat was consumed in the United State in 1958, however, as 269,096 tons was imported.

Jan 1, 1959

By Paul M. Tyler

The colony of French Guiana ( or Cayenne ) is administered by a governor , assisted by a privy council of five members . A council - general of 16 members is elected by French citizens resident in Guiana, and the colony is represented 3 in the French parliament by one deputy . The area is about 34,740 square miles . French Guiana is the largest gold producer of the French colonies , producing nearly $ 1,000,000 worth annually . Considerable prospecting has been done on the bauxite deposits , which are extensive . Copper , iron , lead , and 4 mercury deposits are also reported . In 1931 , 10,000 prospectors for gold were reported as working . The French Government is taking an active interest and has sent a committee of mining experts to explore the region ; no permits are to be issued to individual prospectors while the committee is in the colony . Plans for development of mining industry include consideration of 4,500 convicts and 2,500 natives already in the colony and available for labor .

Apr 1, 1933

By E. C. Tarpley, H. M. Cooper, R. F. Abernethy

"INTRODUCTION The float-and-sink test 5/6/ is generally the first test used in determining the washing characteristics of coal. The simplest form of the test is that of using one solution of such specific gravity that the test sample is separated into ""float"" and ""sink"" fractions. In practice, however, a series of solutions is used, and the sample is separated into a number of fractions of a definite specific-gravity range. Analyses of a series of fractions of this type are often referred to as the ""specific-gravity analysis,"" and are of great value in the selection, construction, and operation of commercial washing equipment.The test is rather simple to use, provided a number of conditions are recognized and as many as possible held constant, such as:1. In laboratory testing, two types of solution are available -Aqueous solutions of calcium and zinc chlorides.Mixtures of organic liquids such as carbon tetrachloride, benzene, gasoline, bromoform, etc.2. Absorption of the solution by the coal,3. Solvent action of the solution toward the coal.4. Constancy of specific gravity during the test is affected by temperature changes, dilution, and evaporation.5. Personal technique of the test, such as the time the coal is in the liquid, rate of adding the sample to the liquid, stirring, time of draining, etc.6. Moisture content of the coal as tested."

Dec 1, 1947

By A. B. Hooker, P. G. Guest, E. J. Gleim

"From time to time the United States Bureau of Mines has received reports of gas explosions alleged to have been caused by correctly assembled flame safety lamps. In most of the mines where the explosions occurred the lamp was in use at a working face where the velocity of the ventilating current would be relatively low. The inference has been that the lamp was correctly assembled but that the gauze became sufficiently overheated to ignite the surrounding atmosphere.As part of its routine investigation of flame safety lamps the Bureau of Mines subjects each lamp to a test in still and moving atmospheres to determine its safety. Heretofore, as long as the lam, successfully passed this and other tests no determinations as to the margin between success and failure were made; hence, in attempting to answer inquiries concerning the reported explosions it was found desirable to be able to give actual gauze temperatures as a measure of the comparative safety of lamps under various conditions. The previous laboratory tests of flame lamps in still mixtures were made in a chamber or ""gallery"" of relatively small volume where the lamps might have been subject more or less to the smothering effect of the combustion products. It was therefore decided to make a special series of tests to obtain the gauze temperatures of both bonneted and unbonneted lamps in still and low velocity mixtures, using a larger gallery to offset any smothering effect.These tests are believed to represent the first attempt at measuring gauze temperatures by means of themocouples. The results will not only be of interest but will also be helpful to many in determining the status of flame safety lamps relative to gas ignitions in mines."

Feb 1, 1929

By B. I. Ferber

Sodium chloride aerosol was employed to determine respirator filter penetration in a manner suitable for use in Bureau of Mines approval and certification procedures. The aerosol was produced by an ultrasonic generator and treated to yield the proper conditions of relative humidity, particle size, and concentration. Respirator filters were exposed to the aerosol; filter penetration (down to 0.02 percent) was determined with a flame photometer. Results are comparable with those obtained in another laboratory using different equipment.

Jan 1, 1970

By Wilbur I. Duvall

A linear array of shot and gage holes 30 feet deep in a granite outcrop was used to compare the size and shape of radial strain pulses produced in the rock when short cylindrical charges of cast composition B were detonated axially or at one end. The axially detonated charges produced radial strain pulses that had shorter rise times and larger peak strain than the strain pulses produced by end detonated charges.

Jan 1, 1965

By A. L. Engel

In the period of 1942-1945, medium-grade, oxidized, lead-silver ore was mined and shipped from the Diamond district near Eureka, Nev. An encouraging tonnage of low-grade ore was developed during these operations and partly blocked-out for future mining. If the low-grade ore could be treated profitably, further development of the district would result, and production of an important strategic metal might be increased. A representative sample of Diamond district ore was obtained through the Reno office of the Mining Division for the studies described in this report. The sample consisted of lumps and fines of a highly altered siliceous rock containing much earthy red hematite and some granular black hematite. Examination with the binocular microscope showed the lead carbonate mineral, cerussite, in seams and disseminated in the hematite. No zinc or silver minerals were identified, and no sulfide minerals were present. Analyses of the ore showed:

Jan 1, 1951

[In selecting deposits of exploration projects, tabular deposits or large mineralized masses are favored because they may be explored systematically and because they afford the best opportunity for blocking out reserves in advance of mining, whereas irregular, small pipes and scattered]

Jan 1, 1941

By J. E. Berg

This paper3 describing the mining methods at the Page mine operated by the Federal Mining & Smelting Co., is one of a series being prepared by the United States Bureau of Mines on mining practices, methods, and costs in the various mining districts of the United States. The Page mine is the most westerly of the producing lead-silver-zinc mines in the Coeur d'Alene mining district of Idaho, being situated 5 miles west of the city of Kellogg and at an elevation of 2,677 feet above sea level. It may be classed as one of the new active producers, of the district and owes its present activity largely to the development of floatation.

Jan 1, 1930

By Tell Ertl, Ernest E. Burgh, John R. Wagner

The principal goal of the Oil-Shale Mining Division is to develop the most economical methods and practices for mining oil shale. Experimental work in the mine has not progressed far enough to conduct full-scale breaking tests; therefore, mining season - to October 31, 1945, has been confined largely to problems connected with drilling cost oil shale. Calculations have indicated that commercial production will result in breaking the oil shale; the largest individual turn will be for drilling. This paper is a report on the progress of phase two of drilling research to date; it outlines the development of a successful hard-surfaced rock bit for drilling oil shale.

Dec 1, 1948

By M. M. Tilman

The objectives of this research were to determine the practicability of using cobalt as a means of controlling the amount of ferrite in the micro-structures of semiaustenitic stainless steels, and to determine the effects of reduced ferrite content on mechanical properties of these steels. Cobalt additions of up to 3 weight-percent were made to type 17-7 PH2 (AISI 631) stainless steel. Ferrite contents were determined for alloys in the aged condition, and for alloys quenched from the hot working temperature. Ferrite can be completely eliminated from the microstructure of 17-7 PH stainless steel by additions of cobalt, but complete elimination of the ferrite phase results in lower tensile strength, yield strength, and hardness. Tensile properties, hardness, and impact strength were determined for aged material. A subzero temperature treatment before heattreating was necessary to obtain maximum strength in the alloys containing cobalt. Addition of 2 weight-percent cobalt enhances mechanical properties of 17-7 PH stainless steel.

Jan 1, 1968

[In selecting deposits for exploration projects, tabular deposits or large mineralized masses are favored because they may be explored systematically and because they afford the best opportunity for blocking out reserves in advance of mining whereas irregular, small pipes and scattered]

Jan 1, 1941

By M. J. Ferrante

Relative enthalpies of high-purity disodium hexatitanate (Na2Ti6013) were measured at the Bureau of Mines to provide new thermodynamic data needed to advance the technology of materials. Measurements from 298.15 to 1,478 K were made by drop calorimetry with a copper block. Tabulated values are listed for the standard relative enthalpy, heat capacity, en-tropy, and Gibbs energy function between 298.15 and 1,500 K. Enthalpy data are also given in equation form and are combined with thermodynamic data from the literature to derive values of standard enthalpies of formation, Gibbs energies of formation, and logarithms of the equilibrium constants of formation. Similar calculations were made for the reaction of Na20 with Ti02.

Jan 1, 1986

By R. V. Ramani, R. Bhaskar

"IntroductionThe behavior of dust clouds in mine atmospheres has been a subject of longstanding interest due to both health and safety reasons. Pioneering studies in Germany and SMRE focussed on ambient dust concentration, principally aimed at determining optimum velocities for effective dilution. A summary of studies related to this area is provided by Hall,(l) Efforts to understand dust deposition from the explosion hazard point of view led to experiments in return airways (2-4) followed by experiments in longwalls.(5) Concerted efforts, either experimental or theoretical, were not made until recently to relate ambient concentration with dust deposition in mines. In 1974 Hwang et a1 (6) developed a computer model to predict dust concentration which considered deposition-concentration relationships. Also, experimental studies involving concurrent dust deposition and ambient concentration were conducted in the U.S. by Courtney et al (7 ) in operating mines. Efforts to relate theory with experimental results have been made by Owen (8) and Hwang et al (6 ) for dust deposition. There has been limited work, however, to determine the application of the theories and assumptions from aerosol sciences for modeling dust flows in mine atmospheres. (9 ) This is the objective of the work currently underway in the Generic Technology Center on Respirable Dust since· 1983 under a project titled, ""Prediction of Ambient Dust Concentration in Mine Atmospheres."" The scope of the project activities include:1. Development of a mathematical model to predict dust deposition and concentration in mine atmospheres.2. Experimental studies on dust transport and deposition in mine airways.3. Comparison of the model results with the experimental data."

Mar 1, 1989