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By G. E. Rennick, F. E. Armstrong, J. Pasini, J. R. Abrams

An oil well penetrating the Pittsburgh bituminous coalbed in northern West Virginia was plugged and safely mined through 3 months later. A sensitive chemical tracer, introduced into the oil reservoir before the test, was not detected in the mine air following the plugging and during mining of the pillar and penetration of the well. Effectiveness of the plugging in preventing reservoir gas from entering the mine through the well hole was verified by continuous monitoring of the mine air for indications of sulfur hexafluoride, an inert gas detectable in amounts as minute as 112 part per billion. Expand- able cement and fly ash-gel-water slurry were utilized to seal the well above and below the coal seam. Three other wells were also plugged using various techniques.

Jul 1, 1972

By Joan T. May

Anhydrous methods were tested for the extraction of beryllium from low-grade source materials. The purpose of the investigations was to find new extraction processes that are applicable to domestic ores. Beryl, helvite, and phenacite materials containing from 0.1 to 2.8 percent BeO were used as starting materials for direct halogenation tests and pretreatment followed by halogenation. The results of the investigations showed that direct fluorination and carbide-chlorination are two practicable methods that can be applied to low-grade concentrates. Treatment of concentrate-carbon mixtures with anhydrous hydrogen fluoride extracted 99 percent of the beryllium in the concentrate; the soluble fluoride product, converted to an oxide, contained 70 percent BeO. Chlorination of beryllium-silicon carbide, prepared from low-grade concentrates, extracted beryllium into the volatile chloride product.

Jan 1, 1962

By George J. Conroy

This Bureau of Mines publication describes several fault locators and methods, including time domain reflectometers, a frequency domain reflectometer, tone generators, an infrared method, the Murray loop method, and high-voltage "click" methods. The Bureau of Mines has been conducting research into these methods for several years, to improve mine safety and facilitate production through rapid, safe location of trailing-cable faults. The problems encountered in practical applications are discussed, and schematic diagrams of several instruments fabricated by the Bureau are presented. Since no present single method of locating trailing-cable faults is universally applicable, a kit composed of several of the more promising fault locators is advisable.

Jan 1, 1978

By James P. Ulery, Stephen J. Kravits, William P. Diamond

This report presents results of a cooperative research project between the U.S. Bureau of Mines and Beth Energy Mines, Inc. Four coreholes (two before mining and two after mining) were drilled at a longwall mine operating in the Lower Kittanning Coalbed to obtain coal and rock samples from overlying strata to determine their gas content at various times in the mining cycle. The results of those tests indicate that 91 pct of the gas removed from the overlying strata came from coalbeds. Material balance calculations were made to compare the volume of gas produced both from gob gas vent holes drilled on the panel and gas removed by the mine's ventilation system with the volume of gas removed from strata directly overlying the panel to a height of 275 ft. This analysis indicates that only 40 pct of the total gas produced from the panel actually came from the strata directly overlying the panel. The remaining volume of gas production probably migrated to the Iongwall gob from overlying, and perhaps underlying, strata immediately adjacent to the panel and perhaps from greater distances downdip because of the establishment of a long-term pressure gradient in the study area.

Jan 1, 1992

Provide respiratory protection for escape in a toxic or oxygen-deficient atmosphere with a device small and light enough to be belt-worn. Approach Combine a 10-minute, belt-worn respirator with a stored, larger, long-duration (60-minute) attachment that can be plugged into the 10-minute unit without removing the mouthpiece. How It Works The 10-minute device will be carried by the miner at all times, and the 60-minute canister or attachment will be stored near the miner. In the event of a disaster, the 10-minute device would be donned immediately. The miner would then proceed to the stored 60-minute unit and plug it into the 10-minute unit. For the 10-minute unit, a breathing circuit was developed in which air is passed through the KO2 bed twice per respiration. The 60-minute canister differs from the 10-minute unit in that air is drawn only once through the chemical bed per respira-

Jan 1, 1981

By C. W. Smith

Research was conducted by the Bureau of Mines to determine the effectiveness of various types of crushers for use with the Bureau-developed pneumatic concentration technique for mica. Three types of crushers were investigated in this study, a roll crusher, a jaw crusher, and a hammer mill. All the mica concentrates produced contained over 82 percent mica, but recoveries varied considerably. The roll crusher gave the lowest recovery of 46 percent of the mica followed by the jaw crusher with a recovery of 50 percent of the mica. The hammer mill proved the most effective, producing four concentrates with recoveries of at least 70 percent.

Jan 1, 1981

By George R. Schottler

The Bureau of Mines investigated the distribution of uranium and various methods of ore sampling in a uranium deposit typical of those in the Morrison Formation sandstone of the Ambrosia Lake area, Grants mining district, north-western New Mexico. Chemical and radiometric assays of diamond-drill core samples are compared in detail by statistical techniques, and the assay data are correlated with the stratigraphy of the deposit. Conclusions applicable to ore-reserve estimation in geologically similar uranium deposits are drawn.

Jan 1, 1971

By John H. Perry

The Bureau of Mines has developed several techniques for draining methane from coalbeds in advance of mining. Drilling long horizontal holes from an underground location is one such technique, which was successfully demonstrated in the Pittsburgh and Sunnyside Coalbeds. The same technique has now been applied in the Mary Lee Coal bed at Jim Walter Resources, Inc.'s No. 4 Mine, Brookwood, Ala., where two holes were drilled horizontally--one to a depth of 1,010 feet (308 m) and the other to 540 feet (165 m). The 1,010-foot (308-m) hole proved successful in degasifying a portion of the Mary Lee Coalbed. The hole drained methane for 1 year, during which time the initial gas flow of 200,000 ft3/d (5,663 m3/d) declined to 65,000 ft3/d (1,840 m3/d). Total gas production was 40 x 106 ft3 (1.1 x 106 m3). The gas was of commercial quality, with 98 pct methane and a heat rating of 990 Btu/ft3 (36.89 Mj/m3). The methane emissions from the faces of the mine section advancing into the degasified zone were reduced by 60 pet. The 540-foot (165-m) hole was terminated prematurely when it became impossible to maintain an open hole. Because of caving, very little gas was drained through this hole.

Jan 1, 1982

By John J. Sammarco

Computer-related accidents have caused injuries and fatalities in numerous applications. Normal Accident Theory (NAT) explains that these accidents are inevitable because of system complexity. Complex systems, such as computer-based systems, are highly interconnected, highly interactive, and tightly coupled. We do not have a scientific methodology to identify and quantify these complexities; specifically, NAT has not been operationalized for computer-based systems. Our research addressed this by operationalizing NAT for the system requirements of safety-related computer systems. It was theorized that there are two types of system complexity: external and internal. External complexity was characterized by three variables: system predictability, observability, and usability -the dependent variables; internal complexity was characterized by modeling system requirements with Software Cost Reduction dependency graphs, then quantifying model attributes using 15 graphtheoretical metrics the independent variables. Dependent variable data were obtained by having 32 subjects run simulations of our research test vehicle: the light control system (LCS). The LCS simulation tests used a cross-over design. Subject perceptions of these simulations were obtained by using a questionnaire. Canonical correlation analysis and structure correlations were used to test hypotheses 1 to 3 - the dependent variables predictability, observability, and usability do not correlate with the NAT complexity metrics. Five of 15 metrics proposed for NAT complexity correlated with the dependent data. These 5 metrics had structure correlations exceeding 0.25, standard errors < 0.10, and a 95% confidence interval. Therefore, the null hypotheses were rejected. A Wilcoxon signed ranks test was used to test hypotheses 4 to 6 - increasing NAT complexity increases system predictability, observability, and usability. The results showed that the dependent variables decreased as complexity increased. Therefore, null hypotheses 4 to 6 were rejected. Lastly, this work is a step forward to operationalize NAT for safety-related computer systems; however, limitations exist. Opportunities addressing these limitations and advancing NAT were identified. Lastly, the major contribution of this work is fundamental to scientific research - to gain knowledge through the discovery of relationship between the variables of interest. Specifically, NAT has been advanced by defining and quantifying complexity measures, and showing their inverse relationship to system predictability, observability, and usability.

By M. L. Odenbaugh

The viscosity reduction effect of varied concentrations of leonardite (a naturally oxidized form of lignite) and leonardite-caustic on the rheological properties of a standard bentonite drilling fluid was studied and evaluated. The minimum plastic viscosity was found to occur at application rates of 4 lb of leonardite and 1.33 lb of caustic per barrel of drilling fluid. Leonardite-caustic treatment was not beneficial in treatment of salt-contaminated drilling fluids. Although filter loss rate was reduced; both yield values and gel strength were increased. Compared with other viscosity control agents) including quebracho) ligno-sulfonate) humic acids extracted from leonardite) as well as other reaction products of lignite) leonardite is less effective at low application rates but is an effective treating agent at rates of 2 Ib/bbl or more. Considering the comparable merits of the substance tested) the major factor in determining which agent to use should be based on cost consideration.

Jan 1, 1967

By S. R. B. Cooke, J. Bruce Clemmer, Will H. Cognill, F. D. DeVaney

"INTRODUCTION The domestic production of potash has made rapid strides in the past 4 years. In 1929 the United States produced 109,820 tons of potash-bearing material, equivalent to 61,590 tons of pure potash (K20). In 1933 to this had increased to 331,110 tons, containing 143,378 tons of potash, due chiefly to the development of the potash deposits near Carlsbad, N. Mex. The potash ores of that district occur at a depth of about 1,000 feet and as mined consist of a mixture known as sylvinite containing about 40 parts of sylvite (KC1) and 60 parts of halite (NaCl). By careful mining the extraneous material does not amount to more than 2 or 3 per cent. Such ore was used in the experimental work here reported.The usual chemical method for the recovery of potash from sylvinite, while efficient in the production of pure potassium chloride, requires,expensive equipment and is costly to operate. It occurred to the Bureau of Mines that ore-dressing methods, which have been applied to other nonmetallic minerals, might be adapted for the production of a grade of potash suitable for the fertilizer industry. After preliminary study by the Bureau of Mines showed that ore-dressing treatment was possible the investigation was extended under a cooperative agreement between the U.S. Bureau of Mines, the Potash Company of America, and the Missouri School of Mines and Metallurgy, Rolla, Mo.ACKNOWLEDGMENTSAcknowledgment is here given for valuable assistance in the laboratory of R. G. O'Meara, assistant metallurgist. U.S. Bureau of Mines, Tuscaloosa, Ala. who was on detail at the Rolla station during the early work; by E. W. Gieseke and Albert Ollar, temporarily employed by the Potash Company of America; and to N. H. Lenz, an engineer temporarily assigned to the station."

Feb 1, 1935

By John Henderson

If you missed this year?s Texas State Holmes Safety Association meeting, you missed a great one. On January 23 & 24, 2009, we held the meeting that was rescheduled when Hurricane Ike threatened Corpus Christi in September 2008. Sixty-five persons from across the state attended the meeting held at the Holiday Inn Emerald Beach. The weather was 82 degrees, and the sky was clear and perfect for a safety meeting. Evaluations submitted by the attendees gave the presentations, the networking, and even the food top marks. There were eight councils represented; Big Country, Central Texas, Costal Bend, Heart of Texas, Hill Country, North Texas and North Central. Presentations included Workplace Examinations, Emergency Preparedness, Screen Safety, Contractor Responsibilities, Powered Haulage, Supervising for Safety, and Basic Inspections of Slings and Rigging. Mr. Edward Lopez, SC MSHA District Manager, gave the State of the District Address.

Jan 1, 2009

By D. E. Wolfson

The Bureau of Mines carbonized 21 coal samples from Fayette, Greene, and Washington Counties, Pa., at 900° C, using the Bureau of Mines-American Gas Association (BM-AGA) method, and determined yields of products and physical properties of the coke. These samples represented high-volatile A Pittsburgh, Sewickley, Waynesburg, and Upper Freeport and medium-volatile Upper Freeport and Lower Kittanning coals. About 20 percent of all coals presently carbonized in commercial coke ovens in the United States are mined in Greene and Washington Counties, principally from the Pittsburgh seam. Sulfur content of the Pittsburgh coals in these counties is moderately high (1.0 to 3.2 percent) but, because of extremely large reserves, accessibility to eastern United States markets and excellent blending characteristics to yield strong coke, these counties will continue to be an important source of metallurgical coals in the future. Most coals from the other seams contained more than 2 percent sulfur, which would limit their use as metallurgical coals.

Jan 1, 1968

By Yael Miron

Ammonium nitrate-fuel oil (AN-FO) mixtures are used as blasting agents in mining pyrite-bearing ores. The temperature of these ores can increase by the continuous, though at times slow, oxidation weathering of the pyrites. At elevated temperatures, AN-FO reacts exothermally with pyrite, and the reaction becomes self-sustained at 120° C ± 10° C. The Bureau of Mines has conducted an investigation to determine the reactivity of mixtures of AN-FO with pyrite containing ferrous sulfate. The results of tests in a heated vessel simulating a hot borehole demonstrate that small amounts of ferrous sulfate, a major product of pyrite weathering, initiate a self-sustained exothermic reaction with AN-FO at 80° C. Five pct by weight of urea was found sufficient to prevent a reaction among the three ingredients, at least within the limits of the test, which reached 180° C. Smaller amounts of urea and of potassium oxalate slowed down the reaction and delayed its onset to higher temperatures, but did not prevent it.

Jan 1, 1979

By James A. West

THE South Asian countries of India, Ceylon, Pakistan, Afghanistan, Nepal, Bhutan, and Sikkim have a large variety of mineral resources; however, in spite of mineral industry growth during 1964, development of resources remained far short of possible development, and, in terms of value of trade in minerals, the area remained a sizeable net importer. India&apos;s mineral industry is by far the most significant; its minerals production in 1964 accounted for more than 90 per cent of the total value of all minerals produced in the area. The total value of all minerals produced in South Asia in 1964 was only about 1 percent of the area&apos;s estimated gross national product of $55,125 million. Despite the rather small current contribution of minerals to the economy, development of mineral resources figures prominently in plans for the industrial development of the nations of this area.

Jan 1, 1966

By P. G. Barnard

The Nation&apos;s steel industry is largely dependent on shipments of manganese from foreign sources for steel production. An adequate substitute for the manganese requirements of our present steel technology would improve our national self-sufficiency and also contribute substantially to the conservation of our manganese resources. As each of these objectives is a major interest of the Bureau of Mines, possible substitutes for manganese in steel were investigated. Titanium was selected as the most promising substitute because the published results of several investigations indicate that titanium would perform the most obvious function of the manganese in steel: The elimination of iron sulfide and its deleterious effects. The investigation involved extending the published data on titanium additions in steel to provide enough information for an accurate evaluation of the practical value of the substitute. Therefore, quantitative data were obtained on the partition of sulfur and carbon between iron and relatively small titanium additions.

Jan 1, 1962

By Robert F. Holub

The Bureau of Mines has evaluated four working-level radiation-measurement methods and optimized them from the inherent and statistical error standpoint. Optimization with respect to various sampling and measurement times yielded no marked improvement over the existing methods. However, when appropriate approximations are made and evaluated, these two-measurement methods can be reduced to simple formulas, eliminating a need to use nomograms. These modified methods also have improved inherent error characteristics. A new method--a combination of two existing methods--with improved inherent and statistical errors has been suggested. All the pertinent equations are given, together with the computer program, so that any two-measurement method can be readily evaluated.

Jan 1, 1980

By Kathleen J. D?Amico

This summary appears in Minerals Year- book volumes I-II, and III, which cover mineral production in the United States, its island possessions, the Canal Zone, and the Commonwealth of Puerto Rico, as well as the principal minerals imported into and exported from the United States. The sections of this chapter and the area chapters in volume III contain further details on production. A summary table comparing world and U.S. mineral production also is included. Mineral production may be measured at any of several stages of extraction and processing. The stage of measurement used in the chapter is normally what is termed "mine output." It usually refers to minerals in the form in which they are first extracted from the ground, but customarily includes for some minerals the product of auxiliary processing operations at or near mines.

Jan 1, 1970

By Martin Hertzberg

In this Bureau of Mines report, the optical detection of fires and explosions is considered fundamentally. The measured spectral radiances from methane-air ignitions are compared with the background irradiances from stray and ambient sources, and with the spectral sensitivites of various sensors. The comparison naturally suggests the optimum spectral ranges and signal processing logic that can uniquely characterize the ignition event. Both ultraviolet (UV) and infrared (IR) are considered. Several alternate sensing methods are proposed and discussed. The development and testing of an IR system designed for use in ignition suppression devices in mines is described.

Jan 1, 1975

By Annie G. Smelley

The Bureau of Mines, U.S. Department of the Interior, as part of its mission to effect pollution abatement, conducted research to devise means for disposing of phosphatic clay wastes and reclaiming mined land. Part of the investigation was performed in a cooperative research project with 10 phosphate companies in Florida. The colloidal properties of the phosphatic clay suspensions, called slimes, make them difficult to dewater and dispose of without impoundment storage aboveground. Various reagents to flocculate and dewater these plant wastes were evaluated, and a polyethylene oxide polymer was found to function in a specialized flocculation dewatering technique. The flocculation dewatering method was investigated in bench-scale batch tests and applied in continuous dewatering tests using standard mineral-processing equipment. In continuous tests at feed rates of up to 58 liters per minute, wastes at 4 percent solids were dewatered to about 20 percent solids. About 0.8 kilogram of polymer was used for each metric ton of dry waste clay solids; processing time was about 4 minutes. Requirements for the treatment system are (1) proper mixing of the clay-waste feed and flocculant, (2) rapid removal of water as it is released, and (3) physical manipulation to promote cohesion of solids.

Jan 1, 1979