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By Henry E. Blake

The purpose of this Bureau of Mines investigation was twofold. The first phase of the work was to determine the technical and mechanical feasibility of defluorinating low-grade siliceous fluorspars on an intermediate scale by high-temperature pyrohydrolysis in a rotary kiln. The second phase was to react the liberated hydrogen fluoride (HF) offgas with alumina monohydrate to produce commercial-grade aluminum fluoride (85 percent AIF3). The two phases of the work were to be integrated into a single continuous process. Evaluation of the data shows that low-grade siliceous fluorspars can be successfully defluorinated, either in a solid or a molten state, in a gas-fired rotary kiln in the presence of water vapor at 1,250° to 1,350° C. The water produced by combustion of propane was sufficient to yield defluorinatians of 75 to 85 percent.

Jan 1, 1962

By R. K. Koch

In seeking substitutes for such critical metals as chromium, cobalt, and nickel, the Bureau of Mines investigated techniques for shape-casting titanium in rammed sand molds. Castings were made in olivine, garnet, chromite, and, for comparison, zircon. It was found that commercial-grade castings up to 31 lb (maximum capacity of furnace) could be made in zircon or olivine molds if a zirconia mold wash was used. Castings up to 4 lb could be made in chromite molds, but heavier castings suffered from some mold-metal reaction. Garnet molds were found to be unsatisfactory for castings of all sizes because of gas blows and rough surfaces. In other tests shell castings of acceptable quality were produced in water-glass-bonded zircon and olivine molds up to weights of 8 lb, but chromite molds were unsatisfactory because rough casting surfaces were caused by mold-metal reaction. Unlike the currently used commercial processes, neither the rammed-sand nor the shell-molding processes developed by the Bureau of Mines generate noxious fumes at any step.

Jan 1, 1980

By M. J. Reasor, J. M. Antonini, L. Wu, K. Van Dyke, Z. Ye

The inhalation of silica has been shown to produce a dramatic inflammatory and toxic response within the lungs of humans and· laboratory animals. Currently, no effective treatment exists for workers who may have been exposed to the inhalation of silica. The objective of this study was to develop an animal model in which we could evaluate the effect that anti-inflammatory steroids have on the acute silica-induced pulmonary inflammatory response. Male Fischer 344 rats were pretreated with either dexamethasone (2 mg/kg) or saline vehicle (i.p.) on days 1, 3, and 5. On day 6, the animals from the two groups were then intratracheally instilled with either silica (20 mg/0.5 ml saline vehicle) or saline vehicle (0.5 ml). Twenty-four hours after the instillations in the non-steroid group, significant increases occurred in total protein, total number of cells, neutrophils, and lymphocytes recovered from the lungs of animals treated with silica compared to saline controls. Silica also caused dramatic increases in the luminol-dependent chemiluminescence (LDCL) of lung tissue and bronchoalveolar lavage (BAL) cells. The LDCL reaction was markedly decreased by either superoxide dismutase (SOD) or N-nitro-L-arginine methyl ester hydrochloride (L-NAME). SOD is involved in the enzymatic breakdown of superoxide anion, while L-NAME, a nitric oxide (NO) synthase inhibitor, prevents the formation of NO. When the superoxide anion and NO react, they form the highly oxidizing substance peroxynitrite. This study then implicates peroxynitrite as an agent which may be involved in the silica-induced oxidant lung injury. When the animals were pretreated with the steroid dexamethasone, there was a complete protection against the biochemical, cellular, and chemiluminescent indices of damage caused by silica. The mechanism in which the steroid protects the lung from damage may be due to the ability of dexamethasone to block the induction of NO synthase. With further study in animals, the anti-inflammatory steroids may be useful in the treatment of silicainduced lung injury.

Dec 1, 1995

By W. W. Graff

This paper describing the mining practice at Mine No. 5 of the Marquette range, Michigan, is one of a series being prepared by the Bureau of Mines on mining practices, methods, tend costs in the various mining districts of the United States. The top-slicing system of mining, has been used ever since the present operating company took control of the property in 1903, the main level and sublevel layout being chanced only as local conditions required and the use of mechanical equipment increased.

Jan 1, 1930

By Charles L. Kimbell

Some comment on data availability must be an integral part of a study such as this. For many years, the centrally planned economy nations of the world regarded as state secrets much of their mineral commodity production information, as well as a considerable body of the foreign trade information on these commodities, and virtually all reporting on their consumption. Within the past 5 years, this pattern has undergone some evolution, and although these countries still fall short of market economy countries in their willingness to publish, there has been measurable improvement. Fit, China, and then subsequently the former CMEA member countries of Eastern Europe have released in print an increasing amount of information in organized, coherent formats, although in a number of cases it is not clear that the information provided is in perfect definitional accord with market economy country practices. Thus, these recently available statistics must be carefully studied to ensure that they are provided in terms of conventional market economy definitions. At the same time that heretofore unpublished information is becoming available for the centrally planned (or formally centrally planned) economy countries, there has been a slow but steady disquieting erosion of availability of production, trade, and consumption data for market economy countries. There are evident reasons for some of these losses in information. The foremost of these relates to corporate mergers. As the number of producing or consuming firms of a given commodity in a given political jurisdiction declines, it is increasingly difficult for government agencies to protect proprietary company data. In past years, this protection was afforded by aggregating data for the several companies operating in the area, but as the number of operators diminishes this is no longer always possible. Hopefully, given this situation, companies will at least authorize release of data after a period of time, when its publication will not provide competitors with unfair access, but will make possible longer term studies.

Jan 1, 1992

By W. S. Landers

Analysis of the size consist of broken coal has been extended in recent years beyond the mere representation of the relative quantities of the various sizes present in a given lot of the material. Fundamental characteristics of the coal related to the process of breakage fix the distribution of sizes, and it has been found by Rosin and Rammler4/ that a relatively simple law-governs this property. Benhett5/ has described a graphical method of expressing the relationship, and by its use considerable simplification in the expression of size distribution is possible.

Jan 1, 1946

By C. K. Man

Coal dust explosions are routinely conducted within the full-scale experimental mine at the National Institute for Occupational Safety and Health (NIOSH), Pittsburgh Research Laboratory?s (PRL) Lake Lynn Experimental Mine (LLEM) to meet the needs of numerous safety and health research programs. Many of these explosion tests over the years involved igniting different coal dust and limestone rock dust mixtures (up to 80% by volume rock dust). Following four more recent tests, floor dust samples have been collected and analyzed using the alcohol coking test and scanning electron microscopy (SEM) and the results compared to estimate the flame travel.

Jan 1, 2009

By Ludwig Schmidt

[The use of vapor-tight tanks has proved so effective in reducing the evaporation losses of petroleum that today practically all operators are using this typo of equipment. It has boon shown, however, that vapor-tight tanks should be supplemented with additional measures which will further reduce evaporation. Probably the most effective use of the supplemental measures are found on the small producing leases where the breathing losses from vapor-tight stock tanks materially affect the volume and gravity of the stored oil. The breathing loss from a vapor-tight stock tank that is filled and emptied daily is a negligible quantity. Also, the filling loss, which on the average varies between 0.1 and 0.2 per cent, usually is not of a sufficient quantity to affect materially the value of the crude. However, the combined breathing and filling losses from a vapor-tight tank requiring several days to fill are of sufficient importance to warrant the use of measures in addition to the vapor-tight tanks. The breathing losses are caused by atmospheric variations. Probably the greatest are the changes in atmospheric temperature which cause changes in temperature of the vapors in the tank. During the day, as the temperature increases, the gasoline-saturated vapors in the tank expand and are forced out into the atmosphere. At night the vapors are cooled and contract, drawing into the tank fresh air, which becomes saturated with gasoline vapor and is forced out of the tank during the following day. In Addition to the maximum and minimums temperature variations there are many smaller variations throughout a twenty-four period caused by showers, clouds, winds, and other atmospheric conditions which likewise cause the tank to breathe. The two mist common measures used by lease operators for reducing breathing losses in vapor-tight tanks are, first, operating; lease tanks under pressure, and second, the use of light colored paints anti tank houses. In this report these two methods are discussed together with their adaptability to lease operation. Results of experimental observations are given which show the reduction of evaporation looses where these supplemental measures have been used.]

Jan 1, 1927

By Louis A. Panek

The practice of roof bolting, now recognized as an effective method of support, is based largely on rule of thumb. Among the various applications of bolting, the support of stratified mine roof is by far the most common. The general principles relating to this type of reinforcement are presented in two companion reports; the first describes the function of the bolts, the bolting pattern, and the behavior of bolted roof (1), 2/ and the second describes the design of the models and the theory of the experimental method (2). This report presents a rational method for designing systems of vertical bolts to reinforce horizontally bedded mine roof, developed from model tests. The structure treated herein may be described as follows: The immediate roof, consisting of beds of like material and equal thickness with no bond between them, is reinforced by vertical bolts installed in straight lines across the opening; the case of suspension is excluded because the bolts are assumed not to extend above the immediate roof. The assumption is made that the behavior of the lowest bed approximates that of a rectangular plate clamped along two opposite sides (the ribs). These specifications represent approximately the roof conditions encountered in mining bedded deposits of all kinds - coal, potash, iron ore, etc. Thus, for the design of a roof-bolting system a quantitative solution to the following problem is required: For a roof composed of beds of given thickness and physical properties, how does the support depend upon the length, spacing, and tightness of the bolts?

Jan 1, 1956

By Richard Havens

Samples of low-grade oxide manganese ores were procured from two southern Utah properties by examining engineers of the Bureau of Mines during an investigation of manganese mineral deposits of continental United States. A 2-ton lot of ore was obtained from the Blackbird group of mining claims in Paiute County, 11 miles southeast of Marysvale, Utah. The deposit was described as an intrusive sheet or sill of altered brecciated rhyolite cemented together by manganese oxide minerals. A 2-ton sample from the Black John property, situated 32 miles northeast of Kanab, Kane County, Utah, was taken from open cuts on the vein. The blanket-type vein deposit consisted of nodules and streaks of manganese imbedded in compact gray clay.

Jan 1, 1949

By Leonard Obert

A triaxial procedure is described for measuring the modulus of elasticity and Possion's ratio of stress relief cores , that is , the concentric hole cores obtained by the overcoring technique . The elastic constant determinations can be made at stress levels comparable with those encountered in underground mining . The results from tests on an aluminum alloy calibration specimen and four rock specimens are included .

Jan 1, 1964

By W. E. Wallace

Volume-rate-of-flow measurements were made of the flow of mercury through porous samples under conditions of no field, magnetic field transverse to the direction of flow, and transverse magnetic field and electric current to determine if a magnetic method might be potentially useful in the study of pore-size distribution. No change was observed in the flow rate from the application of a magnetic field alone. The application of both field and current produced an electromagnetic pumping action with or against the direction of flow, depending upon the direction of the electric current. This pumping effect was observed to be greater in a rectangular porcelain sample than the calculated value for an equal-Sized open channel.

Jan 1, 1969

By David C. Oyler, Paul B. Stubbs

The Bureau of Mines and United States Steel Corp. are conducting a joint project to monitor formation pressures at a large (23-well) coal- bed gas drainage field near Oak Grove, AL. Three monitor holes were drilled in late 1981, and pressure monitoring began in December 1981. The Bureau of Mines direct method was used to obtain gas content data from cores taken in the monitor holes. Comparison of the 1981 gas con- tent data from the monitor holes with initial gas content values obtain- ed from the production wells in 1977 indicates a 50-pct reduction in ad- sorbed gas content inside the pattern and a 29-pct reduction at one point 500 ft outside the pattern. The combination of pressure and gas content data has also allowed an in situ isotherm curve, relating the formation pressure to adsorbed gas content, to be developed for the area of the production wells. From the current rate of pressure decline (1 lbf/inz per month), the observed changes in gas content, and the isotherm curve, it appears that most of the early gas production came from within the pattern, but since 1981 (and possibly earlier) most of the gas produced has been migrating to the wells from outside the pattern area.

Jan 1, 1985

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

1, Introduction This report is submitted in fulfillment of the requirements of USBM Contract No. J0255017, "Development of Emergency Escape Systems Guidelines for Underground Metal and Nonmetal Mines" Under this contract the history of past mine fires was studied. Representative metal and nonmetal mines were surveyed and escapeways, refuge chambers, life support, and emergency hoist requirements were studied to determine the problems in complying with the proposed regulatory standards and their enforcement by MESA Mine Inspectors. In addition, a computer program was written to evaluate mine evacuation performance. The completed program is included in the appendix. 1. 1 Historical Review of Metal and Nonmetal Mine Fires Early records of mine fires are poorly documented because there was no statutory provision for reporting fires to the Bureau of Mines. The survey of representative mines during the course of this contract indicated that many small fires still go unreported even though they are now required to report all fires A recent report survey approximately 80 disasters in metal and nonmetal mines, (6 ) Table I is a summary of some of these fires. Historically most metal and nonmetal mine fires have been caused by electrical problems. Spontaneous combustion and the use of welding equipment are the other major causes of mine fires(14) Although not documented, many mine personnel agree that 30 percent to 40 percent of underground metal and nonmetal mine fires have their origin from cigarettes and other smoking related materials. The number of fires related to spontaneous combustion is decreasing and equipment fires are on the increase. The reduction of spontaneous combustion fires can be attributed to the use of sandfill in more mines and the increase in equipment fires to the increased use of LHD equipment.

Jan 1, 1976

By John J. Mulligan

Lead-silver deposits in the Omilak area, on the western slopes of the Darby Mountains, Seward Peninsula, Alaska, were investigated by the Bureau of Mines, during the 1953 and 1954 field seasons, as a part of the U.S. Department of Interior's continuing program for the development of Alaska's resources. The Omilak area was the scene of early day prospecting and mining activity. The Omilak mine, which operated from 1881 to 1890, was the second producing lode mine in Alaska; the first was a small gold mine near Sitka. Several hundred tons of ore were produced at the Omilak mina; as an indication of grade, 41 tons shipped from Omilak in 1889 contained 75 percent lead and 142 ounces of silver per ton. A prominent, nearby occurrence of lead-silver minerals, found but not explored during this period, has since become known as the Foster prospect. Subsequent exploration of this prospect revealed an abundance of massive galena occurring on an outcrop and as float scattered through limestone talus. Evidence of lead deposition, together with the generally high silver content of lead ores previously shipped from the district, indicated that deposits might be found which would be commercially valuable even in this remote area. To investigate the possibility, the Bureau of Mines made a reconnaissance of the Omilak area and did bulldozer trenching, diamond core drilling, and sampling at the roster prospect. Data resulting from the investigation are presented in detail in this report and are summarized in the following paragraphs.

Jan 1, 1962

By D. T. Couillard

Video technology is becoming an important tool for many designers of industrial training programs. This report describes how trainers at the Minntac Mine, Mt. Iron, MN, have developed videocassettes of safe job procedures (SJP's) for training miners assigned to perform unfamiliar work tasks. All steps necessary for videocassette production, from idea to finished product, as well as the required equipment and prices, are listed and/or briefly explained. Minntac officials believe that the SJP videocassettes have contributed significantly to a reduction in mine accidents.

Jan 1, 1985

By W. T. Culler

"The ""rate-of-preduotion curve"" described in the revised Treasury Manual* was devised by the author in May, 1920, and since that time has been use by the oil and gas valuation section of the Treasury Department in determining the rate of production of wells for purposes of taxation. This curve is most useful for estimating the future production of a well, or group of wells, of known daily settled production, where future-production curves and tables based on yearly production records are available. It also provides a means for determining the past year's production of a well of known daily settled production, or conversely, the estimated production on any day for a well of known yearly production.The rate-of-production curve is auxiliary to the production decline curve and is derived from it in estimating the future production of a tract, a production decline curve formed from the records of the tract itself should be used. If such records are not available, and there is no information which leads to the belief that the average production decline of the wells in this tract differs from the average for the pool or district, an average curve for the pool or district may be used.The accompanying chart illustrates a typical rate-of-production curve, with the yearly production decline curve from which it is derived. The production decline curve shown is for an average well in the Augusta district, Butler County, Kansas, and has been constructed from the tables given on page 128 of the revised Treasury Manual.The ordinate (vertical scale on the chart) of any point on a yearly production decline curve represents the production of the well during the year previous to the date shown by the abscissa (horizontal scale). For example, the chart shows that an average well, which produced 100,000 barrels of oil in 1915. produced 92,000 barrels in the year previous to January 19, 1916, produced 53,300 barrels in the year previous to June 1, 1916; produced 49,000 barrels in the year previous to July 1, 1916, 27,000 barrels in 1916, and 10,000 barrels in 1917."

Oct 1, 1921

By J. B. Newson

This is one of a series of circulars dealing with mining methods, practices, and costs. It describes the method of sinking a shaft 60 inches in diameter with a shot drill, as employed at the Idaho Maryland mine, Grass Valley, Calif. The operation involved a great deal of experimentation in applying the shot-drill method to large bore drilling, overcoming mechanical and other difficulties which developed during sinking, and developing operating technique. Under such circumstances, costs are obviously higher than they would be after the pioneer work has been done, but even so, these actually obtained compare favorably with costs of sinking by more conventional methods. ACKNOWLEDGMENTS The authors are indebted to Mr. Errol McBoyle, president of the Idaho Maryland Mining Co., not only for his cooperation and advice during the sinking of this experimental shaft, but for permission to prepare this article for publication with the inclusion of cost data.

Jan 1, 1936

Lower workers' dust exposures during bag stacking while ergonomically improving the bag stacking process. Approach Install a new pallet loading dust control system which uses a push-pull ventilation technique along with a hydraulic lift table to control the pallet loading height throughout the entire loading cycle. How It Works A low-volume, high-velocity blower system operating at approximately at 120 cfm blows a stream of air over the top layer of bags on the pallet. The blower system is composed of two 3-inch air jets (approximately 1,200-ft/min velocity) directed toward an exhaust system on the opposite side of the pallet. As these air jets travel across the pallet, they en-train dust generated during bag stacking. The dust laden air is then captured by the exhaust ventilation system which draws approximately 2,500 cfm through an exhaust hood on the opposite side of the pallet.

Jan 1, 1989

By P. Comba

The U.S. Bureau of Mines investigated a hydrochloric (HC1)-calcium fluoride (CaF2) leaching procedure to treat domestic manganese (Mn)-bearing silicate resources. The proposed process is an alternative to high-temperature and energy-intensive extractive techniques. Single-stage leaching with a stoichiometric amount of HCl and a F-Mn mole ratio of 0.2 extracted 96 pct of the Mn when the leach conditions were 50° C, 3 h, and 35 pct solids. Ninety-eight percent of the Mn was extracted during countercurrent leaching at similar conditions. A process flowsheet was developed that incorporated HC1-Cab leaching, excess leach acid utilization, fluoride (F) recycle, and Mn recovery. When the domestic manganese silicate ore was processed, 98 pct of the Mn was extracted, 99 pct of the Cab was reclaimed, and a leach residue was produced that passed the Environmental Protection Agency (EPA) Extraction Procedure (EP) Test for nonhazardous waste.

Jan 1, 2010