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By Stephanie L. Kaster, John G. Speer, Blake M. Whitley

Niobium-microalloying technology has been increasingly applied in a wide range of steel applications over the past half-century, to increase strength, control microstructure, enhance properties and enable a variety of applications. To achieve desired performance levels, thermomechanically processed microalloyed steels are widely supplied by the steel industry for high volume applications in hot-rolled plate, sheet and structural steels. However, in steel long products and forgings, the final properties are often generated by downstream users, after heat-treatment, surface hardening, forging or wire drawing. Two examples are presented highlighting advancements associated with Nb-microalloying, to enhance microstructures and properties developed during thermomechanical and/or downstream processing. In the first example, a 0.02 wt. pct. Nb addition was made to a medium-carbon bar steel intended for induction-hardening applications requiring fatigue and fracture resistance in bending and torsion. The Nb addition as well as thermomechanical bar processing led to beneficial refinement of both the pre-induction and post-induction microstructures. In the second example, a 0.01 wt. pct. Nb addition to a high-carbon wire rod was found to refine the pearlite colony size and interlamellar spacing, and increase the hardness.

Oct 1, 2019

By Edo Engel

Whereas only a handful of decades ago, typical blast furnace working volumes were below 1000 m³, such furnaces are currently designated compact or even mini blast furnaces. For certain business cases, however, small furnace sizes remain an attractive option. Decades ago, this size blast furnace would have produced a maximum of 0.3 Mtpa with its 600 m³ working volume over a campaign of up to four years. The current state of technology and operational know–how will allow a similarly sized furnace to produce over 0.7 Mtpa while achieving the multiple decade campaigns that have become familiar to steel producers in full sized operations. This level of productivity, but especially the reliability and supply security associated with mature technology, allows for integration into minimills or taking a first step towards a full scale BF–BOF integrated mill. Steel producers considering such scenarios, which are typically attractive for emerging economies, are confronted with fundamental decisions, one of which is for the technological basis for the compact or mini blast furnace to be included in the plant. This article addresses some of these decisions from an operations–based perspective. A small number of case studies is included.

Aug 16, 2017

By Fabiano Almir Barbosa, Eduardo Alves Machado, Felipe Ferreira Cajano, Bruno Rodrigues Henriques

Spring steels are usually classified as medium to high carbon low alloy steels with very high yield strength, enabling the part to return to its original shape regardless of significant bending or twisting. Despite the fact that plain carbon steels are suitable for small springs, larger and high performance springs usually requires alloy steels such as Cr-V or Si-Mn in order to achieve an even microstructure throughout the cross section. Clutch diaphragm spring is a high performance part that requires very good cleanliness and microstructure homogeneity, thus requiring an alloy steel. In this paper was studied, in an industrial scale, the process parameters and critical characteristics for the development of a Cr and V alloyed high carbon sheet steel for the production of clutch diaphragm spring. The steel was characterized throughout the entire process (casting, hot rolling, cold rolling + batch annealing and heat treated) using tensile test, hardness test, optical microscopy (OM) and scanning electron microscopy (SEM) to assess the mechanical and metallurgical properties of the studied steel. The results have shown the material’s microstructure evolution after each main stage of the process, from a ferrite-bainite/perlite based microstructure as hot band to fully spheroidized as cold-rolled/annealed and then fully martensitic as ready-to-use part.

Oct 1, 2019

By Jerin Russell

This paper presents a new instrument for real-time detection of excessively coarse material in the overflow pipes of individual hydrocyclones using a non-invasive acoustic measurement technique. The hydrocyclone is an important device used in mineral processing beneficiation circuits for classification of mineral slurries by particle size. It separates a single input stream into two output streams; an underflow of coarse particles that undergo additional grinding for further size reduction, and an overflow stream of finer particles that typically goes directly into a flotation circuit for recovery of the desired mineral. However the hydrocyclone is a major piece of equipment in the beneficiation process that has no instrumentation for directly measuring its performance. The parameters currently measured – inlet pressure, feed flow rate, feed flow density – are common to the entire hydrocyclone cluster which typically has three to twelve hydrocyclones. Thus no information is available to detect individual hydrocyclones that are operating poorly. The system described in this paper detects the presence of unwanted excessively coarse material in the overflow stream of a hydrocyclone using sensors mounted to the exterior pipe surface. It provides real-time monitoring, trending and alarming of the coarse material level. This enables operators to identify poorly performing hydrocyclones, and enables corrective action to reduce or eliminate the coarse material discharge. Improving the classification efficiency of individual hydrocyclones will improve the overall classification efficiency of a hydrocyclone cluster. This leads to less variation in the particle size distribution and slurry density in the flotation feed, which will in turn improve overall mineral recovery. The reduction of unwanted coarse material in the flotation feed reduces the accumulation of that material in flotation cells. This can lead to equipment damage, and unplanned shutdowns due to events such as blocked dart valves.

Aug 16, 2017

By Giulio Rodrigues Altoé

Environmentally correct composites, made from natural fibers, are among the most investigated and applied today. In this paper, we investigate the mechanical behavior of epoxy matrix composites reinforced with continuous fique fiber, through bending tensile tests. Specimens containing 0, 10, 20 and 30% in volume of fique fiber were aligned along the entire length of a mold to create plates of these composites, those plates were cut following the ASTM standard to obtained bending tests specimens. The test was conducted in a Instron Machine and the fractured specimens were analyzed by SEM, the results showed the increase in the materials tensile properties with the increase of fiber amount.

Aug 16, 2017

By Maycon de Almeida Gomes

Fiber reinforced polymeric composites have received widespread attention in the past four decades because of their high specific strength and modulus. In particular, research works have disclosed the potential advantages associated with the use of lignocellulosic fibers as the reinforcing phase in polymer composites (2-3). Among various natural fibers, pineapple leaf fibers exhibit excellent mechanical properties. The main chemical constituents of pineapple fibers are cellulose (70–82%), lignin (5- 12%) and ash (1.1%). The superior mechanical properties of pineapple leaf fibers are associated with their high cellulose content (6). This work aims to make the analysis of the Izod impact energy against volume fraction of palf fibers of epoxy composites reinforced with PALF. The fibers were incorporated into the epoxy matrix with volume fraction from 0 to 30%. After fracture the specimens were macro photograph analyzed.

Aug 16, 2017

By Kelen Juliane Mucelin

In order to better understand the tribological behavior of self-lubricating materials, Fe-Si-C matrix composites containing solid lubricants added during the mixing step were studied. The samples were produced by conventional powder metallurgy route, presenting total contents of 5%, 7.5% and 10% in volume of h-BN and graphite mixtures as solid lubricants. The composites were evaluated in terms of tribological properties, under reciprocating sliding conditions, and mechanical properties by using tensile tests. Additionally, the wear scars were characterized by Raman spectroscopy and scanning electronic microscopy. Higher total contents of solid lubricants greatly increased scuffing resistance however decreased mechanical properties. Furthermore, increasing h-BN contents reduces both properties. These results confirmed the applicability of such sintered composites as self-lubricating parts, reaching values up to 7000 N.m for scuffing resistance combined with ultimate tensile strength of 220 MPa.

Jul 31, 2018

By Gabriel Oliveira Glória

In the context of changing culture, the society is increasingly looking for environmentally friendly materials, the natural fibers appear as an option to substitute the synthetic. Among these natural fibers, the PALF fiber may be considered an option, but there is limited information about the flexural strength of epoxy composites incorporated with PALF fibers. Therefore, the objective of this work was to investigate the mechanical properties in bending tests of epoxy composites incorporated with up to 30% in volume of PALF fibers. The results showed that the PALF fiber increase the flexural strength of polymer composites.

Aug 16, 2017

By Rodrigo Fina Ferreira

This paper presents a mineral liberation study on two iron ore samples from the Quadrilátero Ferrífero, in Brazil: compact itabirite of low-grade metamorphism (CI) and friable itabirite of high-grade metamorphism (FI). The quartz liberation spectrum for both samples have been obtained through QEMSCAN analyses, carried out for several comminution degrees, to compare the liberation characteristics and to evaluate the evolution of the quartz’s liberation degree after fragmentation. The results have shown significant differences in liberation spectrum between the itabirite samples studied. The liberation process of FI was easier than of CI, due its high porosity and larger crystal size compared with CI, which has shown more complex mineral assemblages with low porosity and smaller crystals. The quartz liberation spectrum has shown that grinding at P95 of 0.210 mm for the FI sample, and of 0.045 mm for CI sample, should result in satisfactory liberation for subsequent concentration step.

Aug 1, 2018

By Xihuai Gong, Hongshuang Di, Jianping Li, Ning Yan

In this work, we investigated the effect of the rolling process (warm-rolled or cold-rolled) on microstructure evolution and mechanical properties of 9Mn steel. After intercritical annealing at 670°C for 10min, both cold-rolled and warm-rolled microstructures are composed of ultra-fined austenite and intercritical ferrite. The austenite in warm-rolled sample includes two types of morphology, namely equiaxed and lamellar, which exhibits a wide distribution of grain-size. The incomplete recrystallization or recovery behavior of ferrite in warm-rolled and annealed sample results in higher yield strength and shorter yield point elongation. Moreover, the warm-rolled and annealed sample extends the TRIP-related work hardening over a broad strain range, resulting in a better combination of ultimate tensile strength and total elongation.

Oct 1, 2019

By Osvaldo Guilherme Comineli

While the hot cracking of Cu-containing steels is a serious and widely known problem for the industry, the literature reports that copper only slightly impairs the hot-ductility measured in laboratory. A distinction is drawn between hot ductility and hot shortness and the respective cracking operating mechanism involved at the respective range of temperature. The representability of the laboratory assessment of hot cracking of Cu-containing steels by hot tensile tests compared with actual results in industrial practice is discussed. The effectiveness of the variable affecting in each cracking mechanism and respective temperature range, focused in improving the hot cracking assessment of Cu-steels and the relative importance of oxidation will also be discussed. It is concluded that the hot tensile test in argon might be a good simulation if properly interpreted and that the role of oxidation is secondary in causing hot shortness. A schematic diagram for the hot tensile test is proposed.

Oct 30, 2017

By Hongshuang Di, Tianyu Zhang, Huiqiang Huang

A CMnSiAl transformation induced plasticity (TRIP) steel was used to study the effect of retained austenite on room-temperature mechanical properties. The steel plates with retained austenite were obtained by hot rolling, cold rolling and subsequent continuous annealing. The starting and finishing temperature of hot rolling are between Ac1 and Ac3. Reduction ratio of cold rolling is 75%. The continuous annealing is carried out at different intercritical temperatures. The relationship between work hardening exponent and retained austenite was discussed. The results show that, the Ac1 and Ac3 were much high because of the alloy elements, and the temperature range between them was wide. Due to the high hot rolling temperature, the grains was hereditarily refined as a result of dynamic recrystallization. Annealing at intercritical temperature of 930 ºC, retained austenite with relatively high stability reached a maximum volume fraction of 25%, a maximum total elongation of 30.2% and a best ultimate tensile strength × total elongation of 20.1 GPa·%. Instantaneous work hardening exponent reflects strengthening mechanisms at different strain stages. The TRIP effect of retained austenite is the main mechanism during deformation. With retained austenite of sufficient amount and high stability, continuous work hardening was observed in the tensile specimen of 930 ºC.

Oct 1, 2019

By Javier Martinez Rubio

In this paper we will discuss the benefits of a very innovative way of introducing MgO in the blast furnace operation through the sinter, using mini lumps of dunite. By changing the traditional way of using an MgO bearing material in fines form (particle smaller than 5 mm), most of the MgO inserted material behaves as inert during the sintering process, with the effect of having the following parameters (among others) improved: productivity at the sintering bed, permeability inside the blast furnace, energy consumption, stability of the operation.

Aug 16, 2017

By Enrique Francisco Somolinos Garcia-Morales

In this paper we will discuss the benefits of a very innovative way of introducing MgO in the blast furnace operation through the sinter, using mini lumps of dunite. By changing the traditional way of using an MgO bearing material in fines form (particle smaller than 5 mm), most of the MgO inserted material behaves as inert during the sintering process, with the effect of having the following parameters (among others) improved: productivity at the sintering bed, permeability inside the blast furnace, energy consumption, stability of the operation.

Aug 1, 2018

By Antonio Adel dos Santos, Carmos Antonio Gandra, Fabricio Mazola da Silva Paiva, Vicente Tadeu Lopes Buono

Abstract Usiminas Steel Plant in Ipatinga installed an accelerated cooling device named CLC (Continuous On-Line Control) in 2010, enabling it to supply steels produced by TMCP (Thermo Mechanical Control Process) technology. This technology complements the TMCR (Thermo Mechanical Control Rolling), with the inclusion of the accelerated cooling process after controlled rolling. There are various gains in terms of quality and productivity associated to the application of such technology. However, the flatness control for API steel becomes crucial because large thermal stresses may be generated due to thermal heterogeneity during the fast cooling when the austenite phase decomposes mostly into ferrite and bainite. In literature, there is lack of knowledge regarding a full understanding of the relation among cooling conditions and plate flatness. Therefore, this work has focused on the effect of the cooling strategy for API steels, aiming at optimizing flatness and keeping the mechanical properties within the specified ranges. The starting point was dilatometer simulation, where cooling conditions such as start cooling temperature, SCT, finish rolling temperature, FRT, and cooling rate, CR, were changed in order to evaluate their effect on microstructure. Those laboratory conditions supposed to give the best results were transposed to industrial scale, so as to produce experimental lots of plates with five different cooling strategies. It was shown the possibility to find a cooling profile that guarantees the balance between mechanical properties and flatness requirements. The influence of cooling strategy on flatness was explained by the varied heat transfer regimes occurring from hot steel surface to the ambient

Oct 1, 2019

By Wenting Zhu, Liqing Chen, Junjun Cui, Zhenye Chen

In this presentation, a low carbon high strength steel microalloyed with Nb and Ti was processed by thermo-mechanical controlled process (TMCP) containing two stages of controlled rolling. The austenite with various grain sizes was obtained by austenitizing this hot-rolled steel at different temperatures. And the effect of austenite grain size on bainitic transformation was investigated in a dilatometer to reveal microstructural change. The results showed that the microstructure of the hot-rolled steel was mainly composed of granular bainite, lath-like bainite, and martenite/austenite constituents (M-A constituents). With increasing the austenitizing temperature, or increasing the austenite grain size, the microstructure was changed from granular bainite to lath bainite. When the steel was reheated to a lower temperature of 860 ºC, a relatively higher start temperature (Bs) was measured for bainitic transformation. This was mainly caused by the formation of solute-depleted region in the austenite and the promotion of the granular bainitic nucleation. The highest reaction rate occurred at austenitizing temperature of 1000 ºC with fine grain size, while the coarse austenite grain can lead to a sharp increase in the amount of bainite. An analysis was made on the kinetics of bainite transformation which was controlled by the volume diffusion of C atom.

Oct 1, 2019

By Tiago Seixas Bittencourt

Technological developments, associated with the constant worry about the environmental impacts arising from industrial activity, it has driven the development of technologies and practices for efficient fumes and particulates capture arising from the manufacturing processes of steel in steel plants in general. Currently, the electric steelshops in operation with Electric Arc Furnaces (EAF), seek parameterize/design dedusting systems able to retain most of the particulates generated during melting and refining of steel in FEA through configurations of equipment, technologies and parameters operation in order to equalize the antagonistic relationship between effective fumes capture and energy balance of the EAF. The present work gets as a fundamental premise to evaluate critically the possible different settings of the usual dust removal systems, as well as their respective classical parameterizations. The work main purpose is to establish a general rule evaluation technique for dedusting system considering the different modes of operation of an Electric Arc Furnace.

Jul 30, 2018

By Maycon Athayde

Samarco produces high quality iron ore pellets processed in straight grate furnaces. This process is essential in order to obtain adequate mechanical strength to the pellet transportation and operation in the reduction reactors. All mechanical properties of the agglomerates are obtained during the stage of firing where the slag and sintering bond happens, thus it is a decisive step to improve the pellet quality. Therefore, the velocity distribution of gas flow within this zone must have homogeneous and even velocity distribution. Hence, it was developed a mathematical CFD model to characterize the gas flow in the burning zone, applying the equations of conservation of momentum, mass and energy and an uneven flow distribution was identified and the gas velocity analyzed and validated through experimental data. On the other hand, on the present paper, an improved firing zone burner were developed and industrially implemented in a way to mitigate the uneven flow pattern detected aided by CFD. Different burner designs, based on CFD analysis, were experimented in order to succeed on the aggressive condition. The combustion was investigated and burner efficiency evaluated and compared with the simulation purposed.

Aug 2, 2018

By Luca Tommasi

Danieli complemented its wide range of production plants for the iron and steel industry with a further step upstream into iron ore pelletizing and beneficiation. Danieli has engineered and constructed a state of the art and fully automated pilot plant facility – pot grate and sinter box – at Altos Hornos de Mexico S.A. (AHMSA) Pelletizing Plant, Monclova, Mexico. Installation and commissioning were completed in October 2009. Key features of the pot grate include the avoidance of the need for operator intervention during the test, automatic system preheat, absence of dead time, heat recuperation system with an air/air heat exchanger, oxygen control in preheating and firing with zirconia oxygen analyzer, possibility to test deep beds up to 625 mm. A series of projects have been accomplished by AHMSA availing of the pot grate facility with the aim to enhance pellet plant productivity and to reduce operating costs. The results obtained by use of Danieli pot grate combined with the experience and skill of plant operators has shown significant technical and economical benefits thus fully justifying the initial investment made by AHMSA and confirming the importance of having an in-house testing facility in order to optimize industrial plant operations.

Aug 16, 2017

By Andrea Zanon

Slitting processes have been used for many years to increase the productivity of smaller diameter deformed bars, without making major investments in the rolling mill. This technology is used mainly for the production of reinforcing bars (7-20 mm diameter), but successful applications exist also for round bar production. The multi-slitting process enables to produce up to 5 bars starting from one billet, thus increasing the productivity of the smaller products. Danieli Morgårdshammar, world leader in the supply of rolling mills for long products, has been a front-runner in slitting technology since its first applications and has recently developed, first in the world, the technology to produce 5X8mm rebar. This process has been recently applied in BRSM steel, a company based in Bangladesh which is a worldwide benchmark for slitting technology performances. This paper presents the necessary modifications which need to be considered when developing a 5-strand slitting project (and multi-strand slitting projects in general), as well as the results obtained at BSRM Steel when the process was implemented in 2016, the first rolling mill in the world rolling 5X8 mm slit rebars.

Oct 30, 2017