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By Verônica Scarpini Candido

O conhecimento das características microestruturais de materiais utilizados como constituintes mássicos de cerâmica vermelha é de grande importância para a compreensão das propriedades das peças queimadas. Assim, este estudo tem por objetivo caracterizar microestruturalmente a escória granulada de aciaria proveniente de uma siderúrgica do estado do Pará visando a sua incorporação em argilas para produção de peças de cerâmica vermelha. O resíduo passou pela etapa de beneficiamento e, depois, foi realizada a difração de raios-X (DRX) e fluorescência de raios-X (FRX). Além disso, realizou-se também a análise morfológica por microscopia eletrônica de varredura (MEV). Os resultados mostraram que hematita, magnetita e wustita são as fases predominantes associadas aos óxidos de ferro. A análise química por FRX mostrou que o resíduo apresenta baixos teores de sílica (SiO2) e alumina (Al2O3), associados a elevados teores de óxidos de ferro e óxido de magnésio. Dessa forma, a caracterização da escória granulada de aciaria mostrou que esse resíduo apresenta-se como um potencial constituinte mássico cerâmico podendo contribuir para a formação de fase liquida durante o que acarretaria em melhoria das propriedades tecnológicas como absorção de água e resistência mecânica.

Oct 30, 2017

By Ruy José Feijó Alves

O policarbonato é um polímero quimicamente neutro, 100% reciclável, resistente a altas temperaturas, impermeável, durável que oferece uma combinação fantástica das suas propriedades físicas, químicas, mecânicas, térmicas e eléctricas (isolante eléctrico). O policarbonato é um dos plásticos de maior venda e que mostra a maior taxa de crescimento anual no mundo, devido às suas excepcionais propriedades e versatilidade de aplicação e uso. Devido à grande utilização de polímeros nas mais diversas aplicações ao ar livre, surgiu a necessidade de estudar sua resistência às intempéries, não somente por aspectos estéticos, como descoloração ou perda de brilho, mas também por mudanças nas suas propriedades. Os polímeros quando expostos a luz solar na presença de oxigênio são degradados, no entanto as taxas de degradação foto-oxidativa dependem fortemente da natureza química do polímero. Durante o processo de degradação ocorrem mudanças físicas e químicas no polímero que levam à descoloração, fissuramento, perda de brilho e queda de resistência mecânica. Tais fenômenos estão quase sempre associados a processos de cisão de cadeia e, em alguns casos, ocorrem também reticulações. Para se avaliar a estabilidade, ou mesmo avaliar a eficiência de um polímero, é necessário submetê-los a ensaios que simulem as condições às quais ele estaria exposto durante a sua vida útil. Nesse contexto será apresentada uma avaliação sobre a degradação do polipropileno exposto a radiação ultravioleta.

Aug 8, 2018

By Carlos Alberto Mourão, Robson Martins, Letícia Madureira Moreira, Hélio Braz Loss, Joilson Moreira Ferreira da Silva, Edilson Simões Cavalieri, Mauricio Ferreira Coelho

O conversor AOD-L é de uso exclusivo para a produção de aços inoxidáveis na Aperam South America. Entre janeiro a julho de 2018, o consumo de FeSi estava acima do orçado, acarretando em perda de gestão para a Aciaria. O aço inoxidável AISI 304 representa 50% da produção da Aciaria na rota duplex (sem uso do VOD), portanto, esse projeto teve como objetivo a redução do consumo da liga de FeSi no AOD-L para o aço AISI 304. Essa redução foi possível através da utilização da metodologia Lean Six Sigma na qual a causa raiz foi identificada e as ações implementadas o que permitiu uma maior estabilidade operacional, além de aumentar a competitividade da Aperam South America frente aos demais produtores mundiais.

Oct 1, 2019

By Lucas Silva Fontes

Este estudo trata da metodologia de projeto de tratamento térmico para pinos J. O pino J funciona como fusível mecânico do obturador de produção de petróleo e deve romper numa determinada faixa de carga de cisalhamento, a fim de que não haja excesso de tração no obturador. Foram feitas análise química, análise da intensidade de tensões devida à forma do pino, ensaios de dureza e ensaios de cisalhamento. O estudo foi eficiente para determinar o adequado tratamento térmico a fim de garantir a tensão de cisalhamento estipulada no projeto do pino.

Aug 16, 2017

By Lucas Breder Teixeira

O uso de ferramentas de simulação numérica para análise estrutural vem se expandindo nos últimos anos, sobretudo utilizando o método dos elementos finitos. Nesse trabalho são apresentados dois exemplos de otimização de projetos envolvendo componentes de mecanismos de válvula gaveta, realizados pela Magnesita Refratários S.A. Partindo da geometria inicial até o produto final, é analisado como o campo de tensões é adequado a valores admissíveis, conforme modificações de projeto são realizadas. Por fim, é demonstrada a importância desse tipo de estudo para alcançar maior confiabilidade e segurança em projetos mecânicos.

Aug 16, 2017

By Ivan César Lopes Diniz

Stretcher Reducing Mill (SRM) is a mill used in production of tubes. It is composed with a set 24 of stands responsible to define the final outside diameter (OD) of tubes. External appearance is critical in this process even though this requirement has no effect on mechanical properties. For this reason, an investigation of external longitudinal marks mechanism is in progress using 6 Sigma methodology. This paper is a part of the investigation with focus on the rolls and its mechanical properties. Destructive tests were performed in the rolls and compared with the project. After a detailed investigation, it was concluded that rolls were out of hardness specification and the project was poor of information. A new supplier was developed (internal market) based on the new project and all requirements were achieved as demonstrated in this paper. A monopolistic market for this product in VSB (Vallourec Soluções Tubulares do Brasil) was eliminated. Concerning the effect on the external longitudinal marks, the new rolls developed within hardness range minimized the mechanism of wear on rolls surface and consequently on tubes surface. A collateral effect has been faced, but still better than external longitudinal marks on tubes surface. The quenched and tempered rolls are more sensitive for process variation, mainly linked with cooling system and temperature of tubes (mechanical resistance for deformation). Nevertheless, a new material has been aimed focusing on reduction of rolls breakage with good tenacity and affordable cost.

Oct 4, 2019

By Luciana Lezira Pereira de Almeida

With the increasing use of ornamental rocks, mainly in civil construction, sundry problems were identified in relation to rocks cutting, such as efficiency in the cutting process and rock quality lumber. In recent years several composites have been developed to solve these problems. In this context, the study of the binomial matrix metal-diamond interaction is of paramount importance for the development of new composite materials to improve the efficiency of the cutting tool. The diamond impregnated matrix metal often reveals a reaction between the diamond surface and the matrix. Besides the mechanical connection, chemical reactions can sometimes occur. Therefore, this study aims to assess the achievement of diamond composites in the system Fe / Cu / Ni / Sn via powder metallurgy, with added CRB2. Analyzes have been performed to characterize chemical / physical and mechanical. The results have showed that addition of CRB2 promote significant changes in the properties of composites, especially in wear resistance and fracture toughness. Furthermore, the presence of the composite CRB2 causes a significant improvement in thermal stability.

Aug 16, 2017

By Adriana Amaro Diacenco

This work presents the finite element modeling of Euler-Bernoulli beams constituted of a metallic material, discussing theoretical and numerical aspects. The numerical analysis uses Hermitian interpolation functions and finite elements with two degrees of freedom per node. A numerical simulation will be done for uniform loading considering two kinds beams (steel and aluminum). The paper is organized as follows: introductory comments and numerical simulations to evaluate the static and dynamical behavior of the metallic beams.

Aug 7, 2018

By Valdicleide Silva Mello

Nowadays the biodiesel use is obligate in Brazil, in order to reduce the emissions of fuel burn. However, it is important to analyze which percentage of biodiesel is necessary to keep or improve the lubricant action of fuel for diesel engine, as well which kind of biodiesel give better performance. Therefore, this work aims to analyze the parameters that keep the lubricant action of biofuels, by using the Box-Behnken design type to optimize them. In this design was evaluated the input parameters: the type of the biodiesel (soybean, sunflower and palm), the concentration (5%, 20% and 100%) and the temperature of contact (25°C, 40°C and 60°C). The analyzed output parameters were the percentage of film formation, coefficient of friction, wear scar diameter (WSD) of ball, these output parameters were obtained by HFRR tribometer and they were analyzed applying response surface methodology. With this methodology was possible to determine the simultaneous influence and the interactions between two or more independent variables investigated. The response surfaces generated for the coefficients of friction, WSD, film formation showed a higher lubricant action for higher levels of concentration of biodiesel. An increase in lubricant action was found to high and intermediate temperature.

Jul 31, 2018

By Michael Breuer, Christian Mengel, Luis Acainas Caballero, Olaf Jepsen

Stability of the hot strip mill rolling process remains a main topic when it comes to processing thin and hard materials. Strip steering especially at the end of rolling and tail out rips are a main source of unscheduled down times in a hot strip mill. Main focus of this paper is the new X-Roll® Guide system to improve mill stability and quality. An overview of SMS group developments in the recent years regarding equipment and control strategies is given. The new side guiding system in the entry area of the finishing mill is introduced and explained with operational examples. The system provides reproducible conditions for the threading process and during rolling. Steering control has a direct benefit on the availability of the mill. New developments of the roll alignment control strategies based on roll force and mill stand entry guide force measurement will be presented. Additionally a camera based measuring system is introduced that generates a direct process feedback of the strip position. It provides together with the roll alignment control the necessary control parameters for adjusting the roll gap and guiding the strip correct centered through the mill. As a summary the SMS group system is explained combining all features.

Oct 1, 2019

By Antonio Augusto Gorni, Kenji Camey, José Herbert Dolabela da Silveira

Recently several studies have been developed on the use of microalloyed steels with low Mn content (below 1%) in the controlled rolling of heavy plates for the manufacture of pipes. However, this novel concept of alloy has peculiarities in its thermomechanical processing. Lower Mn contents should lead to the acceleration of NbCN precipitation kinetics during rolling, leading to a reduction in the soluble Nb content in austenite that delays its recrystallization by drag effect. This fact, plus the heavy and fast passes applied under virtually isothermal conditions in a heavy plate rolling mill with high power, increases the risk of partial recrystallization during the finishing stage of the controlled rolling, since strain hardening of austenite becomes significant and the interaction between precipitation and recrystallization is increasingly delayed. The objective of this study was to analyze the evolution of mean flow stress during the finishing stage of controlled rolling in these low Mn, high Nb microalloyed steels, in order to better understand the metallurgical mechanisms acting during this process and identify conditions that allow full compliance with the requirements of this product class.

Oct 1, 2019

By Daniel Antonio Kapper Fabricio

A avaliação das propriedades de mecânica da fratura dos materiais é uma necessidade crescente, sobretudo no setor de óleo e gás. Esse cenário exige a garantia da qualidade na execução de ensaios de tenacidade à fratura. Esse trabalho tem como objetivo realizar uma comparação intralaboratorial para o ensaio de tenacidade à fratura KIC variando o executante do ensaio, visando atender ao requisito de garantia da qualidade da norma NBR ISO/IEC 17025. Os resultados foram comparados através de análise de variância. As diferenças entre os operadores não foram significativas frente ao erro residual a um nível de confiança de 95%, sendo tal resultado considerado satisfatório.

Aug 16, 2017

By Henrique Silva Furtado

Concerning production of low phosphorus steel critical grades at ArcelorMittal Tubarão site, bottom blowing system plays a very important role. For those systems with independently controlled tuyeres, some non-uniform bottom blowing patterns seem to be promising in improving metal-slag mixing; however, based on computational fluid dynamics (CFD) results of ArcelorMittal Tubarão’s post oxygen bottom blowing, this may not be generalized. Also, from industrial trials it became clear that higher the bottom blowing flow rate, the closer were the end point P to the equilibrium. Despite this result an analysis of the apparent mass transfer coefficient has shown a week correlation with the classical power stir correlation suggesting a more complex kinetic limiting step for phosphorus removal.

Jul 30, 2018

By Waleska Campos Guaglianoni

With the growth of nanoscience and nanotechnology, the synthesis of nanostructured oxides has received a special attention. Metal oxides are widely used in the manufacture of microelectronic circuits, piezoelectric devices, fuel cells, catalysts, filters and bactericides systems. These metal oxides represent a large class of semiconductor materials suitable for photocatalytic processes. In recent years, new materials of this class such as TiO2 and ZnO have been developed due to their photo-catalytic abilities to degrade various environmental pollutants. This work aimed to evaluate the photocatalytic activity of zinc oxide previously synthesized by combustion synthesis in solution using citric acid as fuel and different reasons fuel/oxidant. After synthesis, the powders were subjected to heat treatments at different temperatures and photo-catalysis. The photocatalytic activity was evaluated by the degradation of a solution of methyl orange in a photochemical reactor of UV illumination, after which the transmittance of the samples measured with the assistance of a spectrophotometer. To analyze the results, a commercial zinc oxide was used as standard. The products of combustion synthesis in solution showed that photocatalytic activity varied according to the ratio fuel/oxidant and as a function of heat treatment. The results showed a higher photocatalytic activity for the products obtained with disabilities fuel in the reaction and heat treated.

Aug 8, 2018

By Frenk van den Berg

In the manufacturing of steel strip for the automotive sector, the mechanical properties are largely defined by the process conditions in the hot strip mill. In particular the phase transformation, from austenite to ferrite, which takes place during the forced cooling stages on the run out table (ROT) after the finishing mill, governs the microstructure and hence the mechanical properties.In current practice, metallurgical models are used to predict the phase state at each position in the strip. These model predictions are supported by pyrometer measurements along the ROT. Although reliable in the majority of the situations, both measurements and models sometimes have difficulties in providing robust output. In this paper, we present a new type of inline measurement, which directly measures the amount of phase transformed. The instrument is based on a technique known as impedance spectroscopy. As result of a collaboration of different institutes and companies, the equipment is robustly running during several years exclusively in the Hot Strip Mill of Tata Steel in IJmuiden.

Aug 16, 2017

By Salete Martins Alves

The future lubricants must be more environmentally adapted, with a higher level of performance lower total life cycle, cost than currently used lubricants. Environmental friendly, the biodegradable alternatives are available for a large variety of mineral oil based lubricants. Vegetable oils are the major source of these base fluids, although they have lower thermal and oxidation stability and even worse low-temperature behavior than mineral oil. These physical and chemical properties can be improved by chemical modification. The aim of this study was to evaluate physicochemical properties and film formation from modified vegetable oils. The vegetable oil was chemically modified by epoxidation reaction with acetic and formic acid using sunflower oils. Viscosity, iodine value, density, acidity value and thermal stability were determined for epoxidized oils. The film formation was analyzed using a HFRR tribometer. The results showed that epoxidized vegetable oils had excellent properties to be used as lubricant, and their tribological performance is higher than mineral oil.

Jul 31, 2018

By Mark Gilliam

Control of true steel level in the tundish during casting is desired in order to maintain the correct pressure head and thus provide a stable flow to the mold. Also the control of tundish draining prevents slag carryover and can increase yield at each end of cast sequence. At Steel of West Virginia (part of the SDI Group), it was understood that to be able to measure the true steel running level and control the drain level at the end of casting would be a great benefit during production at their three strand billet caster. This paper sets out to show how an evaluation process was started to find the best method to determine steel level in the tundish and to prevent the steel level dropping low enough to allow slag to enter the mold. Also how the decision was taken and a real time molten steel measurement system was installed and by utilizing the resulting data in the process, how slag in the mold was removed as an issue, how lost production was reduced and how consistent steel level has provided constant casting speeds and improved stream integrity, all leading to realized quality improvements. Other areas discussed within the paper will be the training of operational staff, the difficulties to be overcome when first installing new equipment and how these teething problems were cured by close co-operation between the steel plant and the equipment suppliers. In conclusion the paper will discuss the production improvements achieved, production cost savings at the plant and how the generated data was integrated into the plants process control system.

Aug 16, 2017

By Nelson SOUTO, Nicolas LEGRAND, Sami ABDELKHALEK, Zafer KOONT

A work roll thermal crown model has been developed for a wide range of hot and cold rolling mill applications. The model is extremely fast, robust and accurate to determine the evolution of thermal crown all along the rolling campaigns. It has also ability to consider work roll shifting, multiple segmented cooling zones along the length and circumference of the roll as well as composite rolls properties (e.g. different thermal properties between mandrel and core of the roll). Moreover, the model includes simultaneously fast and slow temperature evolution calculations, respectively near roll surface (skin area) and at a certain distance below the roll surface (bulk area). This gives to thermal crown predictions a higher accuracy than conventional thermal crown models from literature that consider only the slow temperature evolution regime. An optimization procedure together with roll surface temperature and roll thermal profile measurements have been used to tune the model. The tuned model applied to hot rolling conditions has shown a significant influence of roll shifting and composite rolls properties on the prediction of roll temperature distribution and thermal crown during rolling. The tuned model applied to cold rolling conditions highlights the importance of mill operators practices to modify cooling distribution across roll barrel length with the segmented cooling zones to adjust the thermal crown and to get better strip shape control.

Oct 1, 2019

By Martin Chabicovsky, Milan Hnizdil

Emulsions are frequently used for the cooling and lubrication of working rolls during the cold rolling. The fact that the lubrication and cooling are not separable makes the optimization of both functionalities difficult. The higher emulsion temperature decreases the cooling efficiency compared to cold water. Heat transfer and fluid flow laboratory (Czech Republic), CRM (Belgium), Tata steel (Netherlands) and Henkel (Germany) cooperated on the increasing of a cooling efficiency during cold rolling. Part of this research was focused on an influence of the emulsion composition on a cooling intensity. The cooling efficiency was laboratory investigated. The stainless steel sample with thermocouple was heated and then it was cooled by a nozzle. Tests were performed with various emulsions and pure water. The heat transfer coefficient was computed from measured temperatures. The cooling intensity (heat transfer coefficient) of all tested emulsions was similar but an increase of the cooling intensity was found with water. Further various emulsions concentrations were tested. Results showed decreasing cooling intensity with increasing oil concentration. Adding additives therefore is thought to cause a noticeable decrease of the cooling intensity.

Oct 1, 2019

By Masahiro Shimura, Yoshiki Takahama, Toshiyuki Shiraishi, Daisuke Kasai

When advanced high strength steel (AHSS) is rolled at a high reduction ratio, the forward slip ratio in cold rolling tends to be lower than that of the other softer strips such as low-carbon steels, and the work roll sometimes skids the strip. To identify why forward slip ratio of AHSS at a high reduction ratio becomes smaller than that of low-carbon steel, the relationship between the reduction ratio and forward slip ratio was investigated by a rolling experiment. For this trial, a 4Hi laboratory cold mill was used. AHSS and low-carbon steel coils were rolled by two different rolls that were set to 0.3 and 0.6 μmRa to create two types of friction conditions. Furthermore, the rolling conditions were numerically analyzed to determine the influence of friction coefficient and flow stress on the relationship between forward slip ratio and reduction ratio. The experimental investigation and numerical analysis revealed that the forward slip ratio reduced with increasing rolling reduction ratio in a low friction state; contrarily, it increased with increasing rolling reduction ratio in a high friction state. This feature was clearly visible when harder materials were rolled.

Oct 1, 2019