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By R Lastra, J. A. Finch

An artificial standard material has been developed and used to examine the robustness of some of the procedures for correcting stereological bias. Different mineral liberation distributions were constructed from the standard material. The particles were mounted, sectioned and the sectioning data measured with an electron microscope interfaced to an image analyser. Four correction procedures were used and the corrected and true liberation distributions compared. It was found that the large-sections correction provided a simple, uncorrupted correction. Hill's fast approximation performed well except in cases of narrow liberation distributions; the sectioning data appeared to support the assumption that the locked section and locked particle distributions are identical. Barbery's correction performed well in most cases, having difficulty only with the very irregular liberation distribution. The PARGEN correction was able to provide a good estimate of the true amount of free material, but had difficulty in predicting the locked particle distribution

Jun 21, 1905

By C. L. Schneider, C. O. Gomes, R. P. King, J. A. Finch, D. Lin

Discussion is presented by Prof. King and Dr. Schneider of the paper by Lin, Gomez and Finch published in Trans.IMM C, vol.104, 1995, p.C155-C161. They conclude that the correction procedures used for simulated observations of simulated capped spheres are not reliable when applied to mineralogical data and that their relative ranking should not be extrapolated to other situations. Properly regularised solutions obtained with the use of appropriate kernels can be safely used for routine mineral liberation work and can be calibrated accurately against real mineralogical samples in the laboratory

Jun 19, 1905

By C. T. Aimone-Martin, V. L. Rosenhaim

The response of two structures to blast-induced ground vibrations were evaluated and compared in order to quantify the impact of different blasting operations, hard rock and soft rock blasting, upon the structures movements. The first instrumented structure was a residential type, located in the operational area of a coal mine, were blasting is conducted in soft rocks, such as siltstone and coal, with compressive strength ranging from 20 to 50 MPa. Blasting is characterized by low benches, with hole lengths averaging 5.5 m (18 ft) and low powder factors, 140 to 210 g/m3 (0.236 to 0.354 lb/yd3), resulting in very little horizontal movement of the rock during the blast. The second structure was a commercial building, located in a basalt quarry (compressive strength between 109 and 180 MPa), where blasting is conducted in 12 m (39.4 ft) benches with powder factors ranging from 200 to 350 g/m3 (0.337 to 0.590 lb/yd3). Velocity sensors were placed on the structure walls to measure wall displacements and calculate blast-induced strains in the walls, and these results were compared with the driving ground excitations. The calculated strains were compared with the limits of rupture of the cement grout used as mortar between bricks and as wall coating, considered to be the weakest material in the structure composition. The blast-induced response of existing cracks in the structures were also measured using displacement gages and compared to the daily influence of weather fluctuations, such as changes in temperature and humidity, on crack movement. The results show that for the same levels of ground motions the structures present different movement, resulting in distinct levels of induced strains on the walls depending on the geology. The influence of long-term temperature and humidity variations on crack movements on both structures is very similar, during the same seasons of the year. Crack response to long-term weather changes is 2.5 to 3.5 times greater than blast influences.

Jan 1, 2015

The Gympie Province is a unique tectono-stratigraphic unit which does not fit into the overall palaeogeographic pattern of the New England Fold Belt (NEFB), and part of it has been proposed as an exotic terrane more closely linked to New Zealand. From E to W the Gympie Province comprises 6 distinct units which can be evaluated as suspect or exotic terranes.

Jan 1, 1990

By Peter Fajfa, Heinz Palkowski, Jakob Kraner, Matjaž Godec

The study of asymmetric rolling on the AA 5454 aluminium alloy plates was carried out. The plates were taken directly from the industrial hot rolled sheet. They were cold rolled on the laboratory mill with different rotation speed of the upper and the lower work roller with the strains around 33 % and 44 %. To get closer to the industrial conditions the maximal dimensions of the rolled plates for laboratory rolling mill and the special industrial lubricant were used. After deformation the plates were annealed to the soft condition. This research was focused on all possible effects of asymmetric rolling: The reduction of rolling force, the increase of strain at same set roll gap, bending of workpiece, finer microstructure, more heterogeneous textures and as a consequence of that better mechanical properties. The asymmetric rolling with favourable mechanisms in the deformation zone has created the material with the homogeneous hardness in the cross section and with lower anisotropy, which is crucial for improvement of formability properties of aluminium work hardened alloys and to get closer to properties of steels. In the presented paper the general impact and different effects of speed difference of rollers was investigated on cold rolled aluminium alloy. Obtained and analysed results explain the function of asymmetry in rolling process and the options to implement the asymmetric rolling in industrial plant.

Oct 1, 2019

By Serdar Aktaş, Özgün Küçükoğlu, Burcu Nilgün Çetiner, Mehmet Hakan Morcalı

This study compares the cementation performance of metallic iron, metallic aluminum, and metallic tin in terms of the reaction conditions and parameters in synthetic antimony chloride solutions. The effects on the antimony recovery (%) caused by the cementators’ types, stirring speed, reaction time, and temperatures were explored thoroughly. The cementation kinetics of antimony were also explored for each cementator. The activation energies were determined to be 10.99, 9.09, and 13.58 kJ mol– 1 for Al, Fe, and Sn, respectively. The results reveal that the reaction is diffusion controlled, and comparable results were obtained for each cementator. At 25 °C, 40 mg of iron powder was found to reduce all antimony ions (i.e., approx. 99% recovery), but even when 100 mg of Al and Sn cementators were used, the antimony recovery did not reach 100%. This result shows that iron is the best candidate to cement antimony out of the solution.

Jan 28, 2022

By Hiroaki Sakurai

Using batch reactors equipped with CO and CO2 gas sensor, CO oxidation over Au catalysts in room air has been investigated and compared with Pt catalysts. For both Au and Pt catalysts, the logarithm plot of CO concentration data during initial 10 min are well fitted by straight line, which mean the first order dependence on the CO concentration between 10 and 10,000ppm. The rate constant value (k) over Au and Pt catalyst generally decrease with increasing initial CO concentration above 100ppm. The value decrease especially rapidly between 100ppm and 1,000ppm over Pt catalysts, which should be due to the strong adsorption of CO on Pt. The k value over Au catalyst has become ten times or more as large as the Pt catalysts at 1,000ppm. Already for the initial concentration of 100ppm CO, the strongly adsorbed CO on Pt metal has been clearly observed by FT-IR during the reaction over Pt/Al2O3. A part of the strongly adsorbed CO has been remained on Pt after the disappearance of gas phase CO, and has gradually changed to gas phase CO2. Such strongly adsorbed species on Au has never been observed on Au/TiO2 under the same reaction conditions. These features of Au catalysts are favorable for indoor air purification.

Oct 1, 2003

By Priscila Tavares de Paula, Márcia Mika Saito, Henrique Gonçalves Teixeira, Felicio de Freitas Simoões

In this paper a sample of the apatite flotation from Cajati-SP was studied. Four alternatives of depressants were analyzed: corn starch, cassava starch, sodium hexametaphosphate with corn starch and sodium silicate with corn starch. The cassava starch had a gain of 7.5% in the metallurgical recovery and a collector consumption 13.8% greater than corn starch. Alternatives with hexametaphosphate and silicate sodium had a loss of 6.7% and 7.8% in recovery respectively in comparison with corn starch.

Oct 3, 2019

By C. Liu, G. Zhu, Y. Liao

"The effect of particle size on the flotation kinetics of a low-rank coal was compared using air bubbles and oily bubbles. Five kinetic models were applied to the data from the tests to derive the relationships between the flotation rate constant, the ultimate recovery, and the particle size fraction. The results show that oily bubble flotation (OBF) resulted in a lower ash content and higher combustible recovery than air bubble flotation (ABF), especially for the -125 ??m size fraction. It was found that the flotation of a low-rank coal in individual size fractions using air bubbles and oily bubbles can be best described by a first-order model with rectangular distribution of tendency to float and the classical first-order model respectively. OBF yielded higher ultimate combustible and ultimate ash recoveries. The flotation rate constants for OBF were higher in all the models except for the fully mixed reactor model. The ultimate recovery values and modified rate constants first increased and then decreased as the size fraction decreased. The trend of the flotation rate constants as a function of the size fraction was similar in all the models except for the fully mixed reactor model. IntroductionFroth flotation is a physical-chemical separation method that is widely used in coal beneficiation for the separation of fine coal particles from associated minerals in water slurries. Since the cumulative recovery of a component in the concentrate is proportional to flotation time, the flotation process can be considered as a time-rate recovery process (Emad, Mohammad, and Bahram, 2010). Therefore, the general mathematical flotation models that incorporate both a recovery and a rate function can describe flotation time recovery profiles.The kinetics of coal flotation, as a measure of coal recovery as a function of time, have been studied in detail by many researchers. Different kinetic models have been proposed and published in the literature. The order and the rate constant are strongly dependent on the flotation conditions, such as the particle size and size distribution, the bubble concentration, the reagent concentrations, and the operating parameters (Zhang et al., 2013). The particle size has been reported to affect the flotation kinetics to a great extent (Yoon, Luttrell, and Asmatulu, 2002; Ntengwe and Witika, 2011). Numerous researchers have studied the aspects of flotation kinetics while paying special attention to particle size (Meftuni and Ibrahim, 1997; Rubinstein and Samygin, 1998; Graeme, 2012). However, the effect of particle size on the flotation kinetics of a low-rank coal has been relatively little discussed."

Jan 1, 2017

By Tchingis Lekhatinov, Lev Filippov, Vyacheslav Severov, Alexandre Matinin, Victor Samyguin, Inna Filippova

"Comparison of flotation efficiency of the new multi-zone flotation cell (MZFC) and different conventional cells was carried out at lab and pilot scales on the various samples: high contrast pyrite tailings and old copper containing tailings. MZFC is a cell of intensive flotation, which provides optimal hydrodynamic conditions for all flotation sub processes. Enhancing of particle attachment, creation of conditions for coalescent flotation, selection of spatially separated zones according to optimal hydrodynamic conditions for flotation sub-processes are proposed as main principles to design an MZFC. The bubbles/pulp stratification was pointed out as a limiting step in the existing intensive flotation machines. Two strategies to improve bubbles/pulp stratification in the MZFC were studied: (a) impact of pulp-bubble jet to the surface of a prismatic insert inside of cell, which provides the detachment of low hydrophobic particles from bubbles, and (b) profiling the pulp/bubbles jet from the reactors due to a specific geometry of cell walls. The new continuous MZFC devices were demonstrated similar or higher efficiency in comparison with laboratory batch flotation cells for pyrite flotation. Higher flotation efficiency (82%) with pure pyrite concentrate (51.2% of sulfur) and a recovery level of 92% was obtained in MZFC when the cell with stratification by impact was used. Similar results were obtained with old Cu-containing tailings. Although MZFC had 1.5 times greater yields of concentrate than a batch flotation cell, it provided the increase of chalcopyrite recovery by 29.4% and concentrate grade by 4.8%. An original organization of pulp/bubbles stratification in the separator part of the new intensive flotation machine using variable geometry inserts allowed the best flotation selectivity with a bubble mineral loading coefficient 1.5 fold higher than the laboratory mechanical or pilot cells."

Jan 1, 2014

By H. Cevizci

"Numerical simulation of the plaster stemming method (PSM) was performed and compared with the conventional drill cuttings stemming method (DCSM). Many earlier in situ tests have proved that PSM can use the blast energy more efficiently than DCSM. Despite PSM generating more blast vibrations, it has advantages over DCSM such as better fragmentation and lower cost per unit volume of rock blasted. In this study, numerical simulation with Autodyn software using a 2D tool was employed to prove the efficiency of plaster stemming by comparing parameters such as pressure, Y-velocity, Y-force, internal energy, acceleration-Y, and compression. For example, the maximum pressure attained at the top of explosive column was 7 395 MPa for DCSM whereas it was as high as 11 945 MPa for PSM. Most of the computed parameters were significantly higher in PSM than those obtained for DCSM. This paper is the first study elucidating the efficiency of PSM by numerical simulation. It is concluded that PSM can save substantial amounts of money and effort. IntroductionThe stemming of blast-hole collars in surface mines with an inert material redirects blasting energy to the rock more efficiently, thus the blast-induced energy is utilized more effectively in breaking rock. With proper stemming, the gases should not escape due to loose stemming material. More efficient stemming with better confinement therefore increases the blast fragmentation. In addition, the distance of scatter is increased, giving rise to a looser rock pile that can be more easily loaded and transported. In order to improve the performance of a blast, stemming is used to help maintain the gas pressure over time (Konya and Konya, 2018). Proper stemming has been shown to increase the explosive efficiency by over 41% (Snelling and Hall, 1912).The most common stemming material in open pits and quarries is drill cuttings because of their ready availability at blast sites and the drill cuttings stemming method (DCSM) is a low-cost method. However, it has a major disadvantage in that dry drill cuttings eject very easily from blast-holes during an explosion, thus a great percentage of the blast energy is wasted and lost to the atmosphere. Cevizci (2012, 2014, 2013, 2017) studied blasting parameters in open pits and obtained better results with the plaster stemming method (PSM) in many limestone, basalt, and clay quarries. Moulding plaster is preferred for stemming because of the fast hardening time of 25–30 minutes."

May 1, 2019

By F. M. Lyon, F. J. Chernosky

Research efforts have not developed techniques for the complete desulfurization of coal that is needed to reduce air pollution caused by burning coal and to reduce the sulfur in metallurgical coke. Sulfur in coal occurs in three forms and of these, the pyritic sulfur occurs as discrete mineral particles and, at least theoretically, should be subject to physical rejection. Pyrite occurring in hard rock mining is concentrated by froth flotation; therefore, the possibility of removal of pyrite from coal by flotation does exist. With this possibility in mind, the flotation and adsorption characteristics of ore and coal-pyrite were compared while using potassium ethyl xanthate as the collector.

Jan 1, 1973

By L. Gutierrez, R. Yepsen, F. Alarcón

Chile is the world's largest copper producer which is mostly in the form of sulfides for which froth flotation is the most efficient concentration process. As a result a concentrate that contains high concentrations of copper sulfides such as chalcopyrite, chalcocite and enargite is obtained. In the last decades processing of ores containing high concentrations of enargite (Cu3AsS4) has continuously increased in Chile, which is related to the fact that ore deposits nawadays are more heterogeneous and complex. Enargite is a mineral that contains arsenic and its presence in the copper concentrates implies severe penalties. In addition, the shortage of fresh water has driven the search for new alternative sources of water, among which seawater has proved to be one of the most attractive. The objective of this research is to study the behavior of the enargite in the process of flotation using seawater, and at the same time to compare its behavior with the results obtained using conventional water. The study was carried thorugh micro-flotation tests using pure samples of enargite, at pH values ranging from 4 to 11, both in fresh and seawater. PAX and MIBC were used as collector and frother respectively. Micro-flotation tests were also done at different redox potential conditions so that the effect of the surface oxidation of enargite was evaluated in seawater. The results indicate that the recovery of copper from enargite is reduced in seawater compared to fresh water, in particular at the pH values close to those of the formation of the first hydroxy complexes of Mg and Ca. In general, the experimental data indicate that the floatability of enargite is strongly affected when seawater is used, in particular at oxidizing conditions. These results suggest that Mg2+ and Ca2+ ions contained in seawater interact with the surface of enargite forming hydrophilic species.

Jan 1, 2018

By J. Killian, S. Cox

Many questions exist within the geotechnical industry as to the applicability of Strength Reduction Factor (SRF) values to the design acceptance criteria (DAC) of mining operations. There are many factors that contribute to changes in the SRF estimate, some of which are numerical (e.g. dilation angle) and some of which are geometric (e.g. model grid size)[1]. Numerous studies have confirmed equivalent values of SRF and FOS are found for soil slopes of limited height as presented in, [2] and [3]. However, significant deviation of the SRF value was observed for highly cohesive materials (rock slopes) of heights typically encountered in mining, [4]. This paper builds on the work presented in [4], providing a more rigorous examination of the modeling parameters that control the SRF estimate. The failure mechanism assumed for this study was a simple circular shear surface in a uniform material. Both LEM and numerical methods are suited well for analysis of this failure mechanism. A parametric study was completed to evaluate and test the relationships of key numerical variables that affect the estimated value of the SRF using Itasca’s Fast Lagrangian Analysis of Continua (FLACTM) software. The effect of groundwater has been tested and may be significant but is not presented as part of this body of work for brevity and simplicity of presentation.

Mar 2, 2022

By W. U. Reimold, R. Armstrong, R. G. Charlesworth

For many years rockbursts have plagued the mining industry. Although much research has gone into studying this phenomenon only a small proportion of it has been on the actual source mechanism. A study was recently carried out to compliment the previous work done on the micro-structure of these features and to compare it to the micro-structures seen on shatter cones, from meteorite impacts. Both optical and electron-microscopy were used during the study. Samples were collected from rockburst sites by the CSIR Miningtek Rockburst Investigation Unit, and from the collar of the Vredefort Impact Crater. In the optical-microscopy study, the pinnate fractures observed in previous studies were seen in the shatter cones, through all the material. In the rockburst samples, the fractures were observed only in the quartz grains. Quartz micro-crystals were present in the rockburst samples and appeared to be the product of comminution rather than crystallisation. Cataclasite was present on rockburst and shatter cone fracture surfaces. The observations of the shatter cone surfaces with the scanning electron microscope are in agreement with previous work, including the observed presence of melt features, spherules and spheroidal material. The deformation in the rockburst samples is concentrated in the quartz grains, highly complicated with brittle features like sub-conchoidal structures and step structures present. A quartz spherule was identified on one rockburst sample and rhombic-dodecahedra type micro-crystals were present and seen fracturing off quartz grains. It is clear that the rockburst and shatter cone fracture surfaces are quite different; the shatter cone deformation is equally distributed across the sample and involves plastic-deformation, while the deformation in the rockburst material is concentrated in the quartz grains and, with the exception of spherule formation, is brittle. This study agreed with the current explanation for the formation of the rhombic-dodecahedra, and disproved the possibility of it being coesite or fine-grained meta-chert. Although there is no definite evidence of the mechanism of formation of the spherule, it is believed to be the product of vaporization and condensation, and the presence of this material indicates the extreme conditions under which this event occurred.

Jan 1, 2003

By M Chen, Q D. Gao, Y G. Hu, P Yan, W B. Lu

The safety and stability of construction structures are often affected by blast-induced waves. Investigating the generation mechanism of shear wave (S-wave) during blasting is important, because it has a strong effect in blasting damage. In this paper the generation mechanism and verification of S-wave was studied analytically and numerically. Under the finite velocity of detonation (VOD) of cylindrical charge or the compression wave (P-wave) communicating with the interface of different media during the propagation, the generation mechanism of S-wave was analysed. Propagation of blasting wave in cylindrical charge was simulated with the elastic model, and the generation of S-wave induced by finite VOD was proved. To compare with different numerical methods in simulating the generation of S-wave, the blasting process of instantaneous detonation was simulated by using the elastic model, elastic-plastic model and smoothed particle hydrodynamics and finite element method (SPH-FEM) coupled model. Results demonstrate that the S-wave could not be found in middle section of the charge if the elastic model is employed. But when using elastic-plastic model and SPH-FEM coupled model, the generation of S-wave could be verified. Under the SPH-FEM condition, the amplitude of S-wave is larger and the arrival time difference between P-wave and S-wave is closer to theoretical results.CITATION:Gao, Q D, Lu, W B, Hu, Y G, Chen, M and Yan, P, 2015. Comparison of the generation of shear wave with different simulation approaches, in Proceedings 11th International Symposium on Rock Fragmentation by Blasting, pp 79–88 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 24, 2015

By A. Rahmati

Geological and geo-statistical modeling of the ore deposits play a prominent role in resource and reserve estimation for geo-statistical evaluations. Sheytoor iron deposit is located in the Bafq iron ore district (Central Iran) and in the south-east of the Esfordi 1:100000 sheet. According to the geological data, limestones and dolomitic limestones are situated in the north and central parts of the area, on the other hand, iron ore outcrops are observable in the center, south-west and south-east of the studied area. Meanwhile this ore deposit represents a sulfide one. Based on the boreholes data, geological and geostatistical models of the high and low grade iron mineralization zones were generated by Rockworks v.15 software. The IDW method was selected and employed for processing the collected data and a good adaptation between the results was revealed. The distribution model of Fe concentration displayed a relatively high grade Fe in the center, south and south-east parts of the area. Furthermore, this model illustrated a relatively high grade S and P in some parts of the center, north and south-east of the area. The Fe concentration, in the high grade mineralization zone, was between 45 and 61.5%. In addition, in the low grade mineralization zone, it was between 3.64 and 57.64%. Moreover, in the intrusive granites, the Fe concentration was between 30 and 48.73%. Due to the significant amount of the sulfur in the deposit model, most of Fe-bearing minerals are pyrite, so it is recommended an evaluation on Cu-bearing minerals and their related elements in the area to get done. Additionally, there are too much Fe values in granitic zones which could be caused by possible measurement errors and the geological classification of the area. Therefore, it should be done more carefully.

Aug 1, 2013

By Vincent Scovazzo

This paper compares the two most common pillar design equations used worldwide by John T. Boyd Company; the Mark-Bieniawski Equation, an empirical approach, and the Wilson Equation, an analytical approach. The equations are compared in two ways; by their stress profiles and by the Mark-Bieniawski Equation stability factor. Contrasting the two equations based on the visual comparison of their stress profiles is straight forward but evaluating their resulting pillar designs is problematic. Complications arise due to the differences between the use and development of stability factors for empirical equations and safety factors for analytical equations. To work around these differences, comparisons are made between the two equations by first calculating pillar sizes using the Wilson Equation and then determining the Mark-Bieniawski Equation stability factor for these pillars. Pillars designed using the Wilson Equation were based on site-specific data from 23 mines located in the Americas and Australia. Comparing sizes of pillars designed by the Wilson Equation to the Mark-Bieniawski Equation; the Wilson Equation pillar sizes were smaller in 77% of the cases, similar in 3%, and larger in 20% of the cases.

Jan 1, 2008

By Kim Le Roux

Cemented paste backfill (CPB) is a relatively new material that is increasingly being used in open stope mining across the world. The advantages offered by this high density tailings backfill include: a lower total cost associated with backfill placement, reduction of excess water underground; and the elimination of the need to process the tailings prior to placement. However, almost all backfill design is based on the performance of laboratory prepared samples since it is difficult to obtain undisturbed samples and conduct in situ testing due to the lack of access to backfilled stopes and the safety concerns in accessible areas. The logistical problems associated with conducting in situ testing and obtaining undisturbed samples of cemented paste backfill (CPB) has lead to the reliance in the mining industry on performance data obtained from laboratory prepared CPB samples. The degree to which these laboratory prepared samples represent the actual in situ condition is not well defined, partly because the influence of the mixing, transport and placement process on the material properties it is not well understood. Therefore, there is a need in the industry to understand how the material properties and hence the performance of the laboratory prepared CPB compares with in situ material. This paper reports the findings of an investigation into the in situ properties of CPB at a gold mine in Northern Ontario. A combination of in situ and laboratory testing, conducted on undisturbed samples, was used to quantify the in situ properties and performance of the CPB. These results were then compared to those of a laboratory based investigation of the same CPB. It is evident from this investigation that the bulk properties of the in situ CPB are different from those of the laboratory prepared CPB. The most significant observed differences are that the in situ CPB has a higher void ratio and a lower degree of saturation than the laboratory prepared material. The implication of these differences on the stability and performance of the CPB will also be explored in this paper. 1

May 1, 2002

By H. Möller, L. Mashigo, C. Gassmann

Wire-arc additive manufacturing (WAAM) is a directed-energy deposition technology that uses arc welding procedures to produce computer-aided designed parts, such as three-dimensional printed metal components. A challenge of additive manufacturing is the anisotropy. Interstitial elements play a significant role in the mechanical properties of Ti6Al4V of different grades. In this research, the mechanical properties of Grade 5 and Grade 23 Ti6Al4V were compared for this application. Samples were extracted from WAAM-produced Ti6Al4V walls in different directions (horizontal and vertical) and at different positions (top and bottom). The samples were subjected to optical microscopy and tensile and hardness tests. Grade 5 Ti6Al4V samples were found to have greater strength, greater hardness, and lower ductility, owing to the higher content of interstitial elements compared with Grade 23. The bottom samples had higher strength than the top samples, which is attributed to thermal cycling during manufacturing, resulting in different microstructures.

Jul 1, 2021