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By V. Shumila, T. Butler

Microseismic monitoring systems listen to a rockmass and record ground vibrations associated with brittle rock fracture. Modern systems record continuously and can identify as many as one thousand small and possibly larger magnitude events occurring each day from induced stress change and redistribution. This paper presents examples of the real time use of microseismic information in mining applications. It shows how alerts can quickly identify large magnitude events or unexpected clusters of seismicity and how seismic re-entry protocol can help to improve safety decisions. Additionally, newly developed advanced analysis techniques applied to mine seismic data sets are shown including the use of clustering methods to see into a cloud of seismic data to identify significant activity and quantify possible planar features. The use of source parameter trend analysis is shown to be a beneficial method for interpreting changes in relative stress levels. Seismic moment magnitude distributions are analyzed using the TGR (Truncated Gutenberg Richter) and TMD (Tapered Moment Distribution) methods to estimate bvalue and expected maximum magnitude. Seismic hazard analysis is shown as a useful way to simplify a dataset and highlight seismic hot spots. The rockmass response to excavation is a complicated spatial and temporal process and microseismic monitoring is a method that can be used to help understand the location and mechanics of failure occurring in the rock ultimately helping to improve safety and productivity at a mine site.

Jan 1, 2015

By Pavel Vasak

Microseismic monitoring is becoming standard practice in the Canadian mining industry, particularly as mines get deeper. Full-waveform microseismic systems allow the operator to distinguish the event source mechanism, e.g., blast, shear slip or stress-induced fracture. At mine sites that heave a microseismic system operator blasts are manually identified by comparing the event waveform traces to the morning blast logs. However, this procedure is not routinely done at sites where a system operator is not present and this can lead to misinterpretation of the data at a later stage, particularly where the interpretation is outsourced, often many years later. It is critical to improve the microseismic data quality and consistency for processing and interpretation with a reliable technique to filter out blasts and blast related seismicity. This paper presents the development and implementation of a simple blast identification and filtering routine. The routine was developed specifically for Vale?s Creighton Mine about a decade ago, but is made sufficiently general so that it can be used at any mine site with an ESG (Engineering Seismology Group Canada) based full-waveform microseismic systems. The routine is strictly a post-processing procedure developed for use with the Access database data structure used by ESG. The algorithm was tested at Creighton Mine and a success rate of 80 to 90% was achieved, when compared to manual blast picks.

Oct 1, 2010

By Wilson Blake

This report presents the results of a 7-year Bureau of Mines program to review, revise, and make an effective engineering tool of the microseismic method of determining the stability of rock structures. The program consisted of developing new microseismic equipment and data analysis techniques and extensive field investigations to demonstrate the effectiveness and potential of the broad-band microseismic method. The guidelines for choosing the components of a microseismic system are presented along with approximate cost figures. Different microseismic systems are discussed, including completely automated systems. Procedures for conducting microseismic investigations and analyzing microseismic data are discussed in detail. Field situations which show the full value of the microseismic technique as an engineering tool are described.

Jan 1, 1974

By N. Economou

Temporary local seismic networks were installed in western Crete, in central Crete, and on Gavdos, an island south of western Crete, in order to image shallow seismically active zones of the Hellenic subduction zone. Data acquisition was divided in four campaigns through the years 1996 to 2001. More than 4000 events in the magnitude range between 0.5 and 4.8 were detected and localized. The resulting hypocenter distribution allows the localization of seismically active zones in the area of central Crete from the Mediterranean Ridge to the Cretan Sea. The comparison of the hypocenter distribution and the structure has allowed intraplate and interplate seismicity to be distinguished. A southwards dipping zone of high seismicity within the Aegean lithosphere is found south of central Crete in the region of the Ptolemy trench. Between 20 and 40 km depth beneath central Crete, the Aegean lithosphere appears to be seismically inactive. Especially for the year 2001, 1560 events were localized, by the seismic network installed on Messara, central Crete. Most of the seismic events were located, as expected, in the South region of central Crete. National Observatory of Athens (NOA) maintains a permanent seismic network in Greece. In this work a comparison of the earthquake epicenters obtained from both the NOA network and the BOCHUM-TUC network is presented.

Jan 1, 2006

By K Thorpe

Amorphous silica deposits have been identified at Tikitere and Taheke near Rotorua. Two areas at Tikitere have been surface sampled and drilled to establish a resource of amorphous silica in excess of one million tonnes. A pilot plant was established to develop a process to manufacture a high quality super pozzolanic material. This development process took two years before a commercial product was introduced to the construction industry in 1996. The amorphous silica product, marketed as Microsilica 600, is used as a pozzolanic material to produce high quality strong and durable concrete, sprayed tunnel linings, mortars and grouts. Microsilica 600 has been used locally and exported to 11 countries.

Jan 1, 1999

By O. A. Ojo, E. Anisimov, A. K. Khan

Electro-spark deposition (ESD) has recently generated a great deal of interest in processing aerospace materials. This is due to its potential for joining and repairing difficult-to-weld precipitation strengthened nickel-based superalloys without having problems of welding cracking that often plaque these materials. The short duration of current pulses involved in the process combined with the intermittent contact results in extremely rapid thermal cycle that produces nearly no heat affected zone in the substrate material. The microstructure of electro-spark deposited superalloy was meticulously studied in this work by scanning electron microscopy (SEM) and analytical transmission electron microscopy (TEM). The results show that in contrast to general assumption, the extreme rapid cooling rates involved in the ESD process did not produce partition-less solidification that is devoid of second phase microconstituents in the material. The secondary microconstituents were found formed along the intercellular regions of the solidification microstructure. The nature of these particles and the possible implication of their formation on mechanical properties of ESD processed material are reported and discussed.

Jan 1, 2015

By Jorge A. S. Tenorio, Chuanwei Zhuo, Joner O. Alves, Yiannis A. Levendis

"The ever increasing number of automobiles and the consequential increase in consumption of tires have generated a pressing environmental issue, concerning the disposal of unserviceable tires. The worldwide disposed of waste tires is approximately 1 billion units per year and this amount is expected to increase by 2% each year. This work presents a microstructural characterization of nanomaterials synthesized in a catalyst system from the effluent of burning waste tire chips in a horizontal two-stage laminar-flow furnace. Controlled combustion of waste tire chips took place at temperatures of 900 or 1000 °C, and stainless steel meshes were used to synthesize the nanomaterials at 1000°C. Produced materials were analyzed by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The catalyst meshes were covered by materials with diameters of 20 to 200 nm and lengths of about 40 µm. They possessed structures similar to those of carbon nanotubes.IntroductionThe motor vehicles on the road have been increasing annually. World motor vehicle production in 2009 approached 62 million units. Consequently, the consumption of tires has also been on the rise; about 1.4 billion units were produced around the world in 2007 [l]. The disposal of scrap tires is a serious environmental problem. The worldwide disposed of waste tires is almost 1 billion units per year with an expected increase of around 2% each year. However, less than 7% of produced waste tires are recycled (excluding reuse, retreading or incineration). The waste rubber tires are a thermoset polymer, which cannot be reprocessed like thermoplastics polymers, therefore the recycling of this material requires special techniques that demand big investments [2, 3].A solution to the disposal of waste tires is the sequential pyrolysis/combustion process. Past research showed that waste tires are an attractive potential fuel due the high heating value (29-3 7 MJ/kg), which is comparable, or even higher to those of typical bituminous coals [ 4, 5]. Pyrolysis is a process wherein the material is thermally decomposed at elevated temperatures at the absence of an oxidizing gas. Combustion is characterized by the addition of the oxidizing gases during the process. Several studies indicate that the pyrolysis and combustion processes for the tires treatment have a great energy conversion potential [4, 5, 6]."

Jan 1, 2011

By Dae Jin Ha

Sticking phenomenon occurring during hot rolling of two STS 430JlL ferritic stainless steels was analyzed by hot-rolling simulation tests. The sticking started from the initial nucleation stage in which the rolled materials were stuck onto the roll specimen surface, proceeded to the growth stage in which stuck fragments grew further, and reached the saturation stage. The modified 430JlL steel had a smaller number of sticking nucleation sites and slower growth rate than the conventional 430JlL steel because of higher high temperature hardness, thereby leading to less serious sticking. When the simulation test was conducted at 1070 °c, Cr oxides were formed on the surface of the rolled materials, and thus the sticking was drastically reduced because of the increased surface hardness of the rolled materials. In order to prevent the sticking, high-temperature properties of the rolled materials should be enhanced when rolled at 900°C or 1000 °C, and rolling conditions and alloying compositions, under which the oxide formation was promoted, were more important than high-temperature properties when rolled at higher temperatures than 1000 oC.

Jan 1, 2008

By Vera Lúcia Othéro de Brito

Literature has shown that spinel Co-Mn ferrite have potential application in magneto-mechanical sensors, due to its relatively high magnetoelastic sensitivity. In this work, Co-Mn ferrite was processed by means of the ceramic method, using Fe2O3, MnO and Co3O4 as raw materials. Samples were liquid-phase sintered, using Bi2O3 additive as liquid-phase former. X-ray fluorescence analysis was carried out in the raw materials in order to evaluate their impurity content. Atomic absorption spectrometry analysis was used for quantifying the Co/Mn/Fe proportion in the ferrite. The microstructure of the sintered sample was analyzed by means of Scanning Electron Microscopy. The magnetization and magnetostrictive behavior of the ferrite were evaluated, obtaining curves for magnetic hysteresis, magnetostriction and magnetoelastic sensitivity. The impurity inclusions and the Bi-rich particles formed from the liquid phase were characterized. The sintered ferrite had a total magnetostriction of -126ppm, which is lower than the values reported in literature for a Co-Mn ferrite of similar composition. It was verified that sintering was carried out within a critical temperature range, in which the decomposition of Mn ferrites may occur when sintering in air. This decomposition affects the magnetic properties of the material, and it may be avoided by using controlled sintering atmospheres.

Aug 8, 2018

By D. A. Akinlade, N. L. Richards, D. C. Murray, W. F. Caley

To investigate the effect of adding Ti to a Ni-Cr-Fe powder metallurgy alloy, a thermodynamic software package was used to predict the phase transformations that occurred during thermal processing. Specifically, the effect of adding 3w/o Ti to a 6w/o Al modified ternary Ni-Cr-Fe alloy (the quaternary) was simulated and the phase transformations that might occur in the material on sintering were obtained using the thermodynamic modeling tool. These predictions were subsequently compared with experimental results obtained by X-ray diffraction and metallography. For comparison, selected compacts were prepared containing only the ternary + 3w/o Ti (no Al). Based upon compressibility curves, the optimum pressure for producing the new Ti compacts was 500 MPa vs 600 MPa for the quaternary composition with Ti. In each case, hardness of the base alloy was enhanced by the Ti addition whereas the residual porosity remained relatively constant at about 19%. Finally, although SEM/EDS failed to confirm the presence of Ti in the gamma prime intermetallic, XRD spectra showed a shift in lattice parameter on addition of Ti, suggesting that the intermetallic was of the form Ni3(Al,Ti).

Jan 1, 2010

By Matthew SP, Hayes PC

The product morphologies formed on the reduction of dense wustite crystals are classified into three types,A) porous iron, B) porous wustite covered with dense iron and C) dense wustite covered with dense iron. The mechanisms of formation of these structures and the effects of impurity elements on the product morphologies are discussed

Jan 1, 1984

By Ananda Moreira Vaz Ourique de Avila

Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells (SOFC) interconnects, replacing the ceramic materials. However, at high temperatures, on the order of 700-850 0C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the SOFC. Thus, the knowledge on kinetics of oxidation/corrosion of these steels and their relationship with the microstructural transformations are of great importance. In this study, samples of ferritic stainless steels AISI 430, AISI 441 and Crofer22APU® were tested for oxidation at high temperature (800 0C) for long periods of time (up to 3,600 hours) and mass gains were monitored allowing the determination of the oxidation behaviors of these steels. Additionally, the microstructural characteristics of the samples before aging (corrosion-oxidation test) and after various oxidation times were evaluated by optical (OM) and scanning electron microscopy (SEM), as well as by micro chemical elemental analysis (EDS) and X-ray diffraction (XRD) phase analysis. Electrical characterization allowed determination of electrical area-specific resistances (ASR) characteristics of the systems studied, thus relating the electrical and oxidative behaviors of steels evaluated.

Aug 7, 2018

By Dumitru Mitrica, Vasile Soare, Elvira Alexandrescu, Mihai Ghita, Marian Burada, Petru Moldovan, Raluca Maria Florea

"Aluminum metal matrix composite Al-Si /SiCp was prepared by reactive gas injection and subsequent remelting. The influence of the remelting process on the microstructure and physicalmechanical properties of the resulted material was investigated. Samples resulted from the synthesis process contained silicon carbide agglomerations in the vicinity of primary silicon and large pore concentrations. In-situ formed silicon carbide presented mostly a polymorphic structure with particle sizes varying from 1 to lOµm. Physical and mechanical properties were largely influenced by the porosity distribution. The remelting process provided a decrease in the composite material porosity and pore size, with significant improvements in the particle distribution and physical-mechanical properties of the composite material. Additions of up to lwt.%Mg in the starting alloy improved the in-situ carbide formation and particles distribution in the solidified material. However, stable and large particle agglomerations were detected in the material in absence of conventional stirring or controlled solidification techniques.IntroductionThe remarkable properties of composite materials (yield strength, stiffuess, hardness and resilience at a reduced specific weight) make them attractive for applications in automotive, aerospace and military industries. Particle reinforced aluminum metal matrix composites (PAMMC) are known for their high strength to weight ratio. The recent development of P AMMC created the possibility to obtain large particles concentrations, exceeding 10% by volume ofreinforcement (SiC, AIN, Al203, etc.). The improvement ofhigh temperature strength and wear resistance made them appropriate for the use in automotive applications, such as the pistons, rotors, disc brakes, and propeller shafts [ 1]. The present main disadvantage of the P AMMCs is their high costs for obtaining and processing related to the final product performance. In order to benefit from the advantages that offer composite materials properties a reasonable production cost - performance ratio must be obtained [2]. Recent innovations in the manufacturing of aluminum-based metal matrix composites provided notable performance improvements but no feasible solutions were found for lowering their present high prices."

Jan 1, 2014

By Varadarajan Seshadri

Geometallurgical characterization of iron ore which is a raw material for Iron making as in the case of charcoal blast furnaces operating in Brazil or for production of agglomerates such as iron ore sinter which serves as burden material for blast furnces of high productivity or pellets extensively used in the direct reduction processes all over the world in the iron and steel industry. Selection of proper raw material after due characterization should lead to an improvement of the productivity of the respective processes The usual classification of quality of iron ore is uniquely based on chemical analysis, granulometric and physical parameters. However not much emphasis has been given to the structural characteristics which also are important in the processes. Different typological categories of Brazilian iron ores have been used in the characterization . For instance, several kinds of hematite crystals like specularite, martite and microgranular hematite, etc with variable crystal sizes are found in the different ore types. They are also composed of different of fabrics and types of accessorial mineralogical constituents and have different porosities, pore diameters, etc which influence the cold and the hot agglomeration stages of the ore fines, and also chracteristics such as reducibility, decrepitation etc, important for assessment of quality of iron ores. . The first step for attaining a good characterization of ores is to know in detail about the structure of the deposit, shape of the body, types of iron ores and their distribution. This requires a geological-structural study and the mapping of the bodies using mineralogical criteria for typological classification of ores. followed by structural characterization of materials in stages of mining, comminution, screening and concentration processes. In this contribution a geometallurgical approach for quality control of Brazilian iron ores for sintering and pelletizing processes is highligted.

Jan 1, 2006

By Sergio N. Monteiro

Polymeric matrix composites with dispersed hard particles are being as wear resistant tools in industrial polishing operations. In the present work, the microstructure of epoxy composites with different amounts of embedded diamond particles, up to 30 wt.%, was investigated for the effect on fracture characteristics. It was found that the introduction of diamond particles promoted an increase the porosity of the epoxy matrix. Moreover, the particle morphology associated with a non-uniform distribution within the matrix was responsible for the nucleation of cracks that caused rupture of the composites.

Jan 1, 2006

By Jorge A. S. Tenorio, Chuanwei Zhuo, Joner O. Alves, Yiannis A. Levendis

"Reduction of combustion-emitted greenhouse gases, which are associated with global warming, may be achieved by use of CO2-neutral alternative fuels, such as bio-ethanol. Distillers Dried Grains with Solubles (DDGS) are the main co-products of the com-grain-based ethanol industries. In 2009, the North American production of ethanol from com was about 38 billion liters, which generated approximately 31.5 million tons of DDGS. Samples of DDGS were pyrolysed at temperatures of 600-1000 °C in a two-stage laminar-flow horizontal furnace, and a catalyst system was used to synthesize nanomaterials. This work presents a microstructural characterization of these nanomaterials by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Results showed that the nanomaterials produced from pyrolysis of DDGS were in the form of long, entangled, rope-like structures with rugged walls, lengths in the tens of microns, and axially non-uniform diameters in the range of 100-300 nm.IntroductionThe interest in ethanol has increased considerably worldwide due to the necessity of finding renewable and cleaner energy resources [1, 2]. According to the Renewable Fuels Association (RF A), the world ethanol production in 2008 was approximately 65.7 billion liters (17.3 billion gallons), which figure represented a 24% increase in the production over that in the previous year [3]. The major producers of ethanol are the USA and Brazil, which together account for 90% of world production. The main feedstock for ethanol in USA is com grain, whereas sugarcane predominates in Brazil [2-4]."

Jan 1, 2011

By Toshiro Kuji, Masakazu Fujita, Tetsuji Saito

"The magnetic properties of the magnetic materials were deeply dependent on the microstructures. In this study, the novel technique to produce the desired microstructures in a controlled manner was proposed. The technique consisted of the production of the amorphous alloys and the control of the crystallization process. The technique was applied to improve the magnetic properties of Nd-Fe-B permanent magnets. The microstructural control of the magnets exhibited the excellently high energy-products of higher than 430 kJm-1. The relationship between the magnetic properties and the microstructures of the Nd-Fe-B permanent magnets was discussed.IntroductionThe intrinsic properties of the materials are basically determined by the properties of the constituent elements or the compounds. However, it is often noticed the difference between the observed properties and the theoretical values expected from the intrinsic properties of the materials. This indicates that the observed properties of the materials are determined not only by the properties of the constituent elements. In other words, the observed properties of the materials are also strongly dependent on the morphology of materials. This means that the microstructural control may creates a great improvement of the properties of materials.In Nd-Fe-B permanent magnets, the superiority arises from the uniaxial intermetallic Nd2Fe14B compound which has a large saturation magnetization and a high anisotropy field [1,2]. The magnetic properties of the Nd-Fe-B permanent magnets are dependent on the microstructure, that is, the size, shape and degree of the crystallographic alignment of the Nd2Fe14B phase. Currently, the Nd-Fe-B permanent magnets have been produced by either sintering or melt-spinning [3,4]. In the sintered magnets, alignment of the Nd2Fe14B phase is achieved by the prior green compaction of the crushed ingot powders in an applied magnetic field [3]. In the melt-spinning approach, alignment of the Nd2Fe14B phase is achieved by hot deformation [5]. Amorphous melt-spun ribbons are comminuted and then are consolidated into bulk form by hot pressing before hot deformation. As-hot-pressed magnets have randomly oriented Nd2Fe1~ grains [6]. Subsequent die upsetting of as-hot-pressed magnets gives rise to the crystallographic alignment of the Nd2Fe14B phase."

Jan 1, 1998

By Ian H. Clark

A series of numerical experiments were performed in order to elucidate the stress distribution, fracture strength and mineral liberation potential in single specimens of rock during crushing. Fracture strength was shown to reduce under eccentric loading conditions. Similarly, the presence of inclusions, both hard and soft, reduced the fracture strength. The predicted crack paths indicate that mineral liberation is unlikely to be preferential.

Jan 1, 1992

By Keizo Uematsu, Satoshi Tanaka, Nozomu Uchida, Ronne Hendrajaya

"The influence of microstructural defects on strength in Si3N4 is reviewed. The presence of cracks, pores and inclusions greatly affects the strength of Si3N4. The micron order crack size and distribution were quantified by micrographic technique. The observed defect size was range from 4 µm to 28 µm.The density of defect increases as the defect size decreases. The correlation between defects size and density was better represented on the logarithmic graph. The correlation was linier. IntroductionFracture in ceramics materials occurs from. In order to understand the relationship between strength and defects, it is necessary to examine the fracture process quantitatively.1In this study, the micrographic technique is used to determine the defects size and distribution in Si3N4. The observed data will be used to predict the material strength by using fracture mechanics rnodel.2Experimental ProcedureThe sintered Si3N4 specimens ( SNl, Japan Fine Ceramics Center) were sliced into 1mm thick . The both sides of specimen surface were polished into by using diamond slurries with particle size down to 2µm. The final thickness was 0.045 mm. The optical microscope (NIKON OPTIPHOT02-POL) was used to observed the internal defects with transmission mode. The reflection mode was used to determine the surface defects, so that the internal defect could be distinguished from surface defect. The measurement and counting was taken on the micrograph and the longest part of the defect was measured as the defect size. The size density distribution of internal defect is taken."

Jan 1, 2000

By J. D. Ecuyer, L&apos

he microstructure of galvanneal coatings formed on extra low carbon and interstitial free steel substrates has been characterized using electron microscopy (TEM and SEM) and x-ray diffraction. The coatings are found to consist of a mixture of gamma, delta and zeta phases, of which delta is the main constituent. The amounts of each phase influences the powdering resistance of the coating which was evaluated using reverse Olsen testing and 60" bending. For the three heat input conditions considered, IF coatings were always found to contain a significant amount of gamma and only those which retained zeta phase on the surface exhibited a satisfactory powdering resistance. In much the same way, ELC coatings with relatively thick gamma layers performed satisfactorily only when some zeta was retained. It was also found, however, that coatings with minimal zeta and gamma had an excellent powdering resistance. The latter coatings were produced under galvannealing conditions of lower relative heat input. These results indicate that in addition to the zinc bath composition, coating weight and galvanneal thermal cycle, the base steel chemistry also has an effect on the coating microstructure. Knowledge and control of all aspects of galvannealing is therefore essential to consistently produce acceptable coatings.

Jan 1, 1992