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By Chang Chia -Fu

The generic structure of our bimesogens is shown in and for a typical blue-phase mixture of the type we describe here. We use mixtures of the ratio 33.4% (n =2.6), 34.1% (n =6.57), 36.6% (n= 11.15) with of the high twisted power (HTP) agent BD H1381(available from Merck Chemicals and described in ref. We then studied the electric-field dependency of the selective reflection in BP I* at 20.7 °C by applying increasing and the decreasing pulsed alternating current (a.c.) electric fields (100 Hz).

Jan 1, 2006

By Ko-ichiro Ohno

It is recently recognized that the iron reduction and melting as well as the slag separation of a composite of granular iron ore and coal are completed in a very short period of about 10 minutes when the composite is rapidly heated up to approximately 1673K. These phenomena are expected to be applied to a new iron-making process. The mechanism of iron ore reduction and iron-slag separation during rapid heating has not yet been revealed and the fundamental research has just started. Carburization of the reduced iron is regarded as one of the most important steps in this process. In the present work, the composite was prepared from four kinds of coal or graphite as a carbon source and electrolytic iron powder as a completely reduced iron ore. The temperature at which the liquid formation and iron carburization occurred was monitored. Direct observation of smelting reduction behavior was made by a confocal laser-scanning microscope combined with the infrared image-heating furnace to clarify the effect of molten ash on iron carburization. It was found that the meltdown temperature of composite became lower as the melting temperature of coal ash decreased. From the observed result, it was presumed that the liquid slag would act as an important media for the carbon transfer from coal to iron. The carburization mechanism during the smelting reduction was estimated as follows. When slag containing iron oxide melted down and contacted carbon, iron oxide in the slag was reduced and the formation of the metallic iron particle as well as the its carburization occurred simultaneously at the slag-carbon interface. Carburized iron particle was carried from slag-carbon to slag-iron interfaces due to the slag convection flow caused by the difference of the interfacial tension between the carbon-slag and iron-slag interfaces. Carburization of reduced iron could proceed with a repeat of the above-mentioned process.

Jan 1, 2003

By H. B. Pulsifier

THE following report on the structure of copper is the result of work done in the laboratory of the Rome Wire Co. early in 1925. Previous work had indicated to the author that excellent results might be expected if a suitable technique in surfacing and etching could be developed. The resources of the Rome Wire Co. enabled this metal to be studied more intensively than previously, although none of the materials were investigated exhaustively. The material presented is hardly more than a preliminary summary of the most obvious character of the metal; a much longer research would have been necessary to solve many of the pressing problems connected with the casting and working of copper. The Rome Wire Co. has generously released the paper; to Dr. E. H. Darby, technical supervisor of the company, are due particular thanks for his appreciation of the importance of metallographic study of copper and for his effective support in the prosecution of the work and in making its publication possible.

Jan 1, 1926

By R. Karl Zipf, Z. T. Bieniawski

"A set of fracture profile photomicrographs is presented for fractures generated under mixed mode loading of the Pittsburgh coal. The fractal dimension is used· to characterize the irregularity of these profiles and a tentative relationship is presented between the fractal dimension and the fracture toughness. Surface roughness appears to depend solely on the stress intensity and no other dependence was observed with fracture loading mode, loading rate· or specimen orientation. Observations of crack bifurcations.in fracture profiles can indicate crack growth direction whereas direct surface observations generally cannot in materials such as rock and coal.1 INTRODUCTIONThe production of fine fragments of material as a result of some loading event occurs in many industrial processes. In crushing and grinding, the efficient production of fine fragments is the desired end result; .however, in coal cutting, the production of fine fragments may lead to high levels of respirable dust in the immediate atmosphere with the danger of human lung diseases. Two of the most important sources of fragments in the 1 to 10 micron size range during a cutting process are 1) severe crushing in a zone near the loading tool and 2) subsequent shearing along major crack surfaces that form the larger fragments during material reduction. These and other sources of fine fragments generation are discussed by Roepke (1984) and Zipf and Bieniawski (1986). The physical character of the nearly created major crack surfaces is believed to have a strong influence on the amount of fine fragment generation that occurs during subsequent shearing movement. When the major large fragments initially form, they are ""locked"" in place by the irregular character of the new fracture surface. Only after some relative motion has occurred between fragments are they actually liberated, and the net result is the formation of additional fine fragments. The fine fragmentation is not necessarily limited to the shearing of high points from the macrocrack surf ace since material remaining in the wake of the crack tip is damaged to a substantial depth below the actual crack surface."

Aug 31, 1989

By C. G. Fink

A PART of the material incorporated in this paper was derived from the studies of ancient metal objects examined by the authors from time to time for museums and art collectors, in order to verify the age of the metal. The data thus accumulated during several years was systemati-cally surveyed and supplemented by new material obtained in examina-tion of a set of specimens that had been generously donated by museums for this study. Altogether over 50 pieces were investigated, of which 39 are described in this paper. Every specimen is at least 1500 years old; the majority are considerably older. Exact conditions to which these bronze and copper objects were exposed in the ground are unknown, unfortunately. It is safe to say that exposure conditions did not remain constant during the long period of burial. Although the collection of specimens studied represents a wide variation in location and age of the objects, as well as in the nature and composition of the metals, it was found that fundamental changes in the metal structure were limited to a few typical cases which, therefore, may be considered as more or less general. The authors' chief aim was to study the effect of extremely long periods of corrosion on the structure of bronze and copper.

Jan 1, 1936

By William C. Grady

Microscopic pyrites are present in all West Virginia coals. Sizes of these pyrites range from 0.1 µ 500 µ (1/2 mm) , and four types are noted: massive, patches, framboids, and isolated crystals. The relative and absolute abundances of the four types vary from seam to seam, and these distributions have a marked effect on the ease with which a seam may be cleaned of pyritic sulfur.

Jan 1, 1978

By Homer Turner

COALS, other than anthracite, have been so thoroughly studied under the microscope during recent years, that we now know what kinds of plants and what parts of plants form the bulk of lower rank coals from peat to bituminous coal. The microscope has also shown the state of preservation of such vegetation as well as the nature and distribution of products of plant decay. These and further details have been ascertained mainly through the employment of two methods of attack, section cutting and maceration. Anthracite has failed to respond to these methods, so well adapted to the study of lower rank coals and, therefore, has been neglected by investigators to such an extent that there is much doubt as to its microscopical characteristics. The object of this paper is to lift anthracite from its realm of obscurity by demonstrating the wealth of microscopical detail that is revealed when reflected light is used on a properly polished and etched surface and, further, to show the relationship between anthracite and bituminous coal.

Jan 2, 1925

By Satu Strömberg

Four different nickel concentrates were oxidized in a laboratory scale laminar flow furnace in simulated flash smelting conditions. The major nickel- and iron-bearing minerals in the con- centrates were pentlandite, violarite, gersdorffite, and pyrite and pyrrhotite, respectively. Thermal decomposition, ignition and oxidation behavior of nickel and iron sulfides were examined by using optical and scanning electron microscopy. General reactivity of the concentrates was monitored with sulfur removal which was most effective in violarite-based concentrate. Pentlandite-concentrates needed higher experimental temperatures for complete desulfurization and gersdorffite-based concentrate contained 5 - 10 % of the original sulfur even in the most oxidizing conditions studied (1 100°C, 50 vol-% 02). The reactivity of the iron minerals was found to depend on the other minerals present in the concentrate. In this paper, the observed re- action products and mineralogical changes are presented and preliminary conclusions of possible reaction mechanisms of nickel-bearing minerals are discussed.

Jan 1, 1997

By Roger Cabos

El presente texto señala la necesidad de estudios microscópicos determinativos y cuantitativos como complemento de los análisis químicos, de forma que se explore la posiblidad de beneficiar el mineral oxidado por métodos convencionales.

Jan 1, 1987

By A. J. Sideris

It is known that Mg can act as a catalyst/solvent in the high pressure high temperature diamond synthesis. However, above pressure levels of the order of 7 GPa, and temperatures from 1700 ? 1800oC, it was not possible yet to use Mg for the industrial production of diamond. A possible alternative is the use of MgNi based alloys. However, owing to the great Mg reactivity, it was consider, so far, a difficult task to deal with such alloys. The present work presents successful results regarding the production of MgNi alloys, with different composition, at high pressure conditions. The behavior of the alloys and their microstructural characterization is analyzed.

Jan 1, 2006

By Gregory B. Poole

Data collected with 16K sampling at a variety of blasting sites (construction, quarry, trench, mine) and monitoring locations was analyzed to effectively show the 16 different 1K readings all based on the microsecond that the unit went into monitoring.

Feb 1, 2020

By J. L. Ellenberger, P. W. Jeran

A deep longwall coal mine was instrumented with a three-dimensional microseismic system in order to help determine the exact strata mechanics associated with the rock failure, redistribution of stress and the associated gob formation from the longwall. Overall, 5,000 well calibrated seismic events were recorded during the mining of the panel. Analysis of these events showed a close correlation between the seismic activity and advance rate, and that the majority of the recorded seismic activity occurs in the immediate area of the advancing longwall face.

By J. L. Ellenberger, P. W. Jeran

A deep longwall coal mine was instrumented with a three-dimensional microseismic system in order to help determine the exact strata mechanics associated with the rock failure, redistribution of stress and the associated gob formation from the longwall. Overall, 5,000 well calibrated seismic events were recorded during the mining of the panel. Analysis of these events showed a close correlation between the seismic activity and advance rate, and that the majority of the recorded seismic activity occurs in the immediate area of the advancing longwall face.

Jan 1, 2002

By Gary L. Mowrey

Visible and sometimes audible indications of excessive underground rock pressure such as pillar fracturing, squeezes on chocks, and "roof talk" are familiar to mining engineers. Such signs often precede rock failure on a larger scale and therefore may be used as a warning. Nevertheless, these subjective observations do not provide an adequate means of evaluating the existing rock pressure conditions in a mine. One method which appears to be extremely promising in determining the stability of geologic structures in general is that of monitoring their associated micro seismic activity. Mining engineers generally agree that during the process of rock deformation and failure small-scale seismic ("microseismic") vibrations are produced in the rock itself. These transient vibrations propagate through the rock structure and may be detected at a considerable distance from the failed rock by employing suitable electronic monitoring equipment. Hardy (1) has presented a detailed review of microseismic research in the mining, petroleum, and geoscience areas, and it is apparent that relatively little application of micro seismic techniques have been made in coal mines. This is especially true in North America since here most coal mines are fairly shallow and consequently are not generally subjected to excessive stresses. Furthermore, strict Federal and State mining laws limit the use of electrical equipment in coal mines complicating the use of the necessary monitoring facilities. In terms of both mine safety and economics, monitoring microseismic activity appears to be invaluable in the detection and location of over-stressed pillars and unstable roof conditions caused by development and production work. In 1970 The Pennsylvania State University Rock Mechanics Laboratory became involved in a research project, sponsored by the U.S. Bureau of Mines, to investigate the feasibility of using microseismic techniques to detect and to locate potential regions of instability around a longwall coal-mine operation [Hardy and t10wrey (2); Mowrey (3)]. In this study geophones (velocity gages) located in an array of shallow boreholes drilled from the surface above the active area of the longwall were employed to detect microseismic activity, and a mobile micro-seismic monitoring facility was used to condition and record this data for later analysis. This project is unique in that measurements were made from near-surface geophones rather than geophones installed on the mine itself. Two advantages are apparent, namely that (1) there are no electrical limitations on the monitoring system and that (2) mining operations can continue normally because there is no monitoring equipment or cables in the mine.

Jan 1, 1978

By Will S. Pettitt

Fracture Network Engineering (FNE) is the engineering design of rock mass disturbance through the use of advanced techniques to model fractured rock masses numerically, and then correlate field observations with simulated fractures generated within the models. Microseismic (MS) monitoring is a standard tool for evaluating the geometry and evolution of the fracture network induced during a hydraulic treatment, principally by source locating MS hypocenters and visualizing these with respect to the treatment volume and infrastructure (Figure 1). The integrated use of Synthetic Rock Mass (SRM) modeling of the hydrofracturing with Enhanced Microseismic Analysis (EMA) provides a feedback loop in which the SRM is constrained by the information provided by the MS data and the in-situ behavior of the fracture network is better understood, leading to informed decisions on future field operations. This paper discusses the technologies used in FNE and some of the developmental challenges we face in order to provide a more efficient and robust application of the approach. One particular challenge is the accurate representation of MS source data within the models (locations, magnitudes and mechanisms), and the ability to correlate these data effectively with field results. This challenge is being overcome by the development of more efficient numerical modeling algorithms, providing simulations in three dimensions at reservoir scale, combined with validation of these algorithms using laboratory and field case studies.

Jun 1, 2012

By Ahmed M, Leung L

A program of microseismic noise monitor ing for gas outbursts, in conjunction with other mining engineering measurements and observations, is being undertaken at Leichhardt colliery in Queensland. Headings are developed at present by shotfiring. The equipment being used in this study includes piezoelectric accelerometer assemblies to detect microseismic noise which is then transmitted to a surface base station by cable. Data are recorded on an analogue magnetic tape recorder and are also analysed on-line using a commercially-available acoustic emission pulse analyser. It is proposed to re-interpret recorded data using various modes of analysis and to interface a desktop computer to the existing system to permit continuous monitoring on the mine site. No outbursts have been recorded or analysed and only a limited number of develop- ment shots, and the resultant microseismic activity, have been recorded to date.

Jan 1, 1980

By G. R. Corbett

Between 1977 and 1984, No. 26 Colliery, at Glace Bay in the Sydney Coalfield, suffered from a series of 37 rock/gas outbursts. These events were characterized by the complete pulverization of a sandstone which was propelled into the mine roadway and an associated release of methane gas. The events began to appear at a depth of 700 m and increased in intensity and damage to the excavation as the mining depth increased. At the time of the closure of No. 26 Colliery (as a result of an unrelated fire), these outbursts were the subject of intensive investigation. Although No. 26 is now closed, there is concern that similar events could appear at Phalen Colliery where current development work is proceeding at a depth close to the 700 m threshold. Past investigations into rock/gas outbursts included studies of in situ stresses, the simulation of outburst events in the laboratory, investigations into the potential for destressing an& degassing of problem sandstone and the development of numerical models to assist in the design of openings in outburst prone ground. However, despite this work, methods of predicting outburst conditions are presently limited to examination of probe hole cores for core discing, and methods of working under such conditions are limited to boring and firing and using volley firing techniques to initiate any outbursts while workers are safely out of the heading. During this investigation of worldwide occurrences of this phenomena, literature obtained suggested that outbursts might generate microseismic precursors. An intrinsically safe (IS) microseismic monitoring system was designed and developed based on CANMET's rockburst monitoring system currently in use in hardrock mines, and installed in a development roadway at the deepest extent of the Phalen Colliery. The system will record microseismic activity associated with development work to try to identify characteristic precursors of outburst-prone conditions. This paper describes the steps taken to identify a microseismic system suitable for use at Phalen colliery, of which part of the requirement was that it be IS and approved for use in the Sydney Coalfield. The modifications to the selected system are described, along with its capabilities and the preliminary results of its performance over the first few months of use.

Jan 1, 1994

By J. L. Condon

The Bureau of Mines, through in-house and contract research, monitored mountain bump-prone areas of the Olga #2 Mine, near Welch, WV, using microseismic techniques for 15 months during 1985 and 1986. During this period, two ground failures occurred that were considered "mountain bumps" owing to excessive stress buildups. One failure damaged the roof and 4 pillars around an intersection; the second failure, which released much greater energy, resulted in significant damage to over 100 coal pillars. Analysis of the microseismic data collected provided significant insights into the magnitude and location of each failure. The actual failure zone was clearly delineated prior to the mountain bump occurrences through analysis of source locations of each microseismicevent. Trends in cumulative rate plots indicated the onset of structural instability. Although the data could not be analyzed automatically, the significance of the data interpretation cannot be overemphasized. Microseismic monitoring of bump-prone areas can be successful in providing a means to actually observe the structural stability occurring in underground coal mines. This paper discusses data collection techniques, analysis methods, and implications of the monitoring technique, with special emphasis on actual data from two large mountain bumps in West Virginia.

Jan 1, 1987

By G C. Reed, J M. Murray

During more than 100 years continuous mining of the lead-zinc orebody at Broken Hill, an immense amount of geological data has been collected about shear zones related to the orebody. The challenge to current mine geologists is to synthesise and interpret these data sets in a way that is applicable to production demands. Precise knowledge of the locations of major shear zones is important not only for the determination of ground conditions but also to develop an understanding of ore remobilisation along these structures. Traditionally, geological information has been collected from drill core and back and wall mapping underground, and interpreted on sections that are approximately 20 m apart. The recent introduction of MaptekÆs Vulcan software has enabled the shear zones to be modelled in three dimensions. The new three-dimensional shear models have been combined with seismic data from the Southern Cross area. The seismic data is collected from a microseismic monitoring system installed in the Pasminco Southern Operations in August 1996 (Rauert and Tully, 1998). The addition of seismic information to the shear zone models has led to a greater degree of certainty about the shear zone locations and has provided information about shear zones in areas yet to be drilled.

Jan 1, 2000

By Peiwei Xiao, Xiang Li, Biao Li, Haoyu Mao, Nuwen Xu

As an advanced method of rock engineering construction safety monitoring, microseismic monitoring technology can monitor the micro-fracture of rock masses within an effective range, and then perform forecast analysis of rockburst, cracking, falling blocks and other disasters. Although the application of microseismic monitoring technology has become more mature, how to improve its application efficiency remains to be further studied. At present, artificial intelligence has been extensively developed, and the use of intelligent algorithms to improve the efficiency of rockburst forecast can provide a valuable reference for the safe construction of underground engineering. To this end, this paper proposes a microseismic multi-parameter rockburst early warning model based on dynamic Bayesian networks. First, the sensitivity of microseismic source parameters to rockburst forecast is analyzed based on microseismic monitoring data and actual rockburst information of a hydropower station. Second, the main seismic source parameters and their data are selected and imported into a dynamic Bayesian network for learning to obtain the rockburst forecast model. The model is confirmed in its self-validation and K times cross-validation, and the receiver operating characteristic curve of the model is also analyzed, it is found that the area under the curve is close to 1, indicating that the model has good accuracy. Finally, the analysis of the influence strength of the parent and child nodes in the model reveals that the moment magnitude and source scale are the most sensitive parameters, which can be used as an important reference for rockburst forecast.

Apr 26, 2022