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By Alla D. Mah

The heat of combustion of TaC0.996 was determined by oxygen bomb calorimetry to be -302.8 ±0.4 kcal/mole. The corresponding heat of formation of TaC0.996 is -35.4 ±0.5 kcal/mole, and the calculated heat of formation of TaC1.00 is -35.5 ±0.5 kcal/mole.

Jan 1, 1965

By L. G. Marshall

The geology, mining, beneficiating, types of products, and costs in terms of percent of total costs and of labor, power, and supplies of two crushed- limestone operations in Madison County, Iowa, are described in this paper. The operations are basically similar, differing in refinements in mining, product types, and markets. The operations are comparable as to personnel and as to weighted costs in terms of percent of total costs and in terms of man-hours, power, and supplies. The waste-to-stone stripping ratio is 1 to 0.8 at both operations, the powder factor is 0.29 pound of explosives per ton of stone, and daily production is 95 tons per man-shift. Both companies use crawler-mounted diesel shovels for loading, truck transportation, wagon drills, and dry screening.

Jan 1, 1963

By L. J. E. Hofer

The Bureau of Mines determined rates of adsorption and desorption of methane as a function of particle size and temperature, using coals from the Pocahontas No.3 seam (lvb) from the Bishop mine of western Virginia, and the Pittsburgh seam (hvab) from the Pursglove No. 15 mine of northern West Virginia. For a given coal sample and temperature, the rate curves for adsorption and desorption are essentially the same when expressed on a fractional approach to equilibrium basis. The rates of adsorption and desorption increased eightfold as the particle size was decreased from 6-8 to 270-325 mesh per inch. The adsorption process appears to be diffusion controlled. Rate of sorption processes increased with increasing temperature; however, the amount adsorbed at equilibrium decreased.

Jan 1, 1966

By D. S. Kingery

Investigations over several years have disclosed that the principal manners of occurrence of shuttle-car injuries are in order: 1. Victims in contact with roof or crossbars. 2. Victims in contact with ribs or timber legs. 3. Victims falling from, or jerked from, shuttle cars. 4. Victims in contact with overhanging brows or protruding pine for pin timbers, or water lines. 5. Contact with persons or collisions with parked equipment. 6. Victims injured by roof falls or falling timbers caused by knocking out roof supports with shuttle cars. 7. Victims injured by runaway shuttle cars. 8. Victims injured while loading or unloading timbers or other materials from shuttle cars. These recurring types of shuttle-car accidents reflect the physical conditions of the working sections, certain safety deficiencies in shuttle-car maintenance and design, and unsafe practices by operators.

Jan 1, 1952

By Thomas E. Green

A combined solvent extract ion-spectrophotometric method for the determination of as little as 1 ppm of copper in tungsten metal or tungstic oxide has been developed and evaluated. Metallic samples are converted to tungstic oxide by treatment with hydrofluoric and nitric acids. The oxide is then dissolved in sodium hydroxide, and the copper is extracted as the colored neocuproine complex. Total elapsed time for the analysis is approximately 1-1/2 days; however, actual working time for a group of six or eight determinations is less than 4 hours. Precision at the 2-ppm level is better than 0.1 ppm.

Jan 1, 1963

By Curtis D. Edgerton

The Pittsburgh Mine Map Repository of the Bureau of Mines serves as a basic reference file for the archival preservation of mine map data of mines east of the Mississippi River. About 22,000 of an estimated 500,000 available mine maps have been microfilmed A computerized index serves as the mechanism for retrieval of any microfilmed mine map. The operation, equipment, and index are described in the report.

Jan 1, 1974

By Wilbert J. Huff

For the past 8 years the technical studies conducted by. the Explo- sives Division of this Bureau have been summarized in a series of annual reports.3 This report deals with activities from July 1, 1942, to June 30; 1943. Specific problems have been in immediate charge of section or unit leaders, to whom credit is given.

Feb 1, 1944

By Robert D. Thomson

Sheet mica is an important material in the manufacture of electronic and electrical equipment. Large quantities are consumed each year as an essential component in generators, transformers, radios, television sets, radar, electric lighting equipment, and electrical appliances. The nature, structural imperfections, and impurities determine to a great degree the usefulness of sheet mica. Proper processing and classification add greatly to its market value. This report is designed to assist producers in understanding the complexities of marketing muscovite sheet mica. ACKNOWLEDGMENTS Special acknowledgment is due S. A. Montague, of Spruce Pine Mica Co. and G. A. Purcell, mica consultant, General Services Administration, for their critical review and many helpful suggestions in the preparation of thin report. Assistance from other industry and Government representatives is acknowledged with thanks.

Jan 1, 1955

By L. G. Marshall

This report is one of a series published by the Federal Bureau of Mines describing mining methods and performance at individual operations throughout the United States. The objective of these papers is to promote development and conservation of our mineral resources by disseminating reliable technological information on mining methods, practices, and results that may be applied to the engineering analysis and solution of mining problems. SUMMARY Operation of a limestone quarry producing flux for the steel industry and crushed stone for production of concrete is described in this report. The deposit being mined is a flat-lying limestone formation under a thin overburden 2 to 25 feet thick. The height of the quarry face varies from 9 to 60 feet, averaging 40 feet. Production rate ranges from 4.5 to 5 million long tons per year.

Jan 1, 1959

By Lloyd A. Morley, Robert Stefanko

This report was prepared by The Pennsylvania State University, College of Earth and Mineral Sciences, ' Department of Mineral Engineering, University Park, Pennsylvania, under USBM Grant No. GO-133077. The grant was initiated under the Coal Mine Health and Safety Research Program. It was administered under the technical direction of the Pittsburgh Mining and Safety Research Center with Mr. G. J. Conroy acting as the technical project officer. Mr. J. A. Herickes was the grant administrator for the Bureau of Mines. This report is a summary of the work recently completed as part of this grant during the period 19 June, 1973 to 17 June, 1975. This report was submitted by the authors on 18 July, 1974. This technical report has been reviewed and approved.

Jan 1, 1974

By P. C. Good

Tungsten metal in fused form and of high purity was prepared by reducing tungstic oxide with redistilled calcium metal in a heavy-walled sealed reactor. Alloys of tungsten with vanadium, molybdenum) chromium, columbium, and tantalum were prepared by coreduction of mixed metal oxides in the same manner. This work was undertaken by the Bureau of Mines to investigate new approaches for preparing tungsten and its alloys in high-purity form. The standard method of producing tungsten metal has been the reduction of tungstic oxides by hydrogen. The resulting metal powder is compacted, sintered, and fabricated by powder metallurgy methods. Long experience in this field has resulted in the development of a technology that (by careful control of the variables such as metal composition, particle size, and sinterng technique) is well adapted to producing wire and the small shapes usually prepared from tungsten metal.

Jan 1, 1961

By H. W. Kilau

Thermodynamic calculations indicate that an electrochemical cell might serve as an analytical device for determining the composition of high-purity metals. An equation, readily derived, for the cell voltage, E, is as follows: [E I RT In F NFe unknown sample T of L NFe standard] The cell, however, must come to equilibrium, must be reversible, and must have no thermal effects or complicating side reactions whose magnitude is indeterminable. This Bureau of Mines investigation explores the feasibility of an electrochemical technique for the analysis of high-purity iron. Experiments were conducted using room-temperature aqueous cells and high-temperature molten salt cells. The room-temperature cells proved to be irreversible. The high-temperature cells utilizing FeCl2 and a eutectic mixture of KC1-LiCl were reversible, but did not attain a constant voltage necessary for analytical considerations.

Jan 1, 1963

By L. C. IlsLey

In the normal operation of mines, the aggregate effect of many seemingly minor op rations may be very important as respects economy and safety. Anion: these operations is the method employed in coupling and uncoupling mine cars. For economic reasons the equipment in mines has not been protected as well as railroad equipment. It is pertinent that haulage accidents rank second in severity among mine accidents, and that manual coupling of cars has been one of the most frequent causes of such accidents. One study4/ revealed that coupling was responsible for about 20 percent of haulage accidents underground. A review of early conditions on steam railroads, which were responsible for the introduction of safer methods of coupling cars, indicates how conditions in might be improved. THE STORY OF RAILROAD COUPLING As any considerable improvement in mine-car coupling probably will follow lines somewhat similar to those that brought order out of chaos for the railroads, it seems appropriate to review briefly the steps taken to improve railroad coupling from the days of link and pin couplings of various types to the adoption of the standard ?M.C.E? automatic coupler.

Jan 1, 1943

By Wing G. Agnew, Albert E. Long

"SUMMARY AND CONCLUSIONSTests conducted at Mount Weather indicate that clear water is the best bit coolant and cuttings-removal medium for diamond drilling. All of the mediums tested did show that drilling speed increased when drilling with the faster feed ratios (greatest pressure on the bits). In no case, how¬ever, did the increased drilling speed amount to over 16 percent, and even in a long hole the slight increase in drilling speed would be more than offset by the extra time consumed in setting up.Bit wear was excessive when lubricating agents were used, the most footage per bit was obtained when drilling with clear water in the normal manner, and the next best footage was obtained when drilling with circulated water containing no lubricating agent. The diamonds showed little or no wear in any of the bits, and all bits cut well throughout the tests. They were only taken out of service when erosion of the cast metal had progressed to the point where the diamonds were about to roll out. The lubricating agents evidently hold some of the cuttings in suspension, which in turn help to cut the rock but also wear the metal of the bit.No hard-matrix bits were tested, and it is possible that one or more of the lubricating agents might increase the efficiency of such a bit by keeping it sharp and doing away with the necessity of sharpening by sand blasting. Some tests are planned with hard-matrix-type bits and the same lubricating agents used in the tests under discussion, but it is realized that any drilling advantage gained by the bits sharpening themselves may but at least partly offset by excessive wear of the Pump parts."

Jan 1, 1945

By A. D. Garman

This paper presents one of a series of digests of foreign mining legislation and court decisions which is being prepared in advance of a general report relative to the right of American citizens to explore for minerals and to own and operate mines in various foreign countries. This interpretation of the laws of Colombia has been prepared from the best available information in Washington, but is released subject to correction and amplification; if necessary, by the proper American diplomatic and consular officers to whom it is being referred through the courtesy of the Department of State. SYNOPSIS OF LAW Minerals in Colombia belong to the owner of the soil unless otherwise provided in the law. The following lands and deposits, however, are described as fiscal property of the State: Class 1. The public lands, mines, and salines which belong to the individual States (now Departments) prier to the adoption of the present constitution (1886).

Jan 1, 1929

By John E. Pahlman

The Bureau of Mines investigated the feasibility of removing heavy metals from mineral-process waste streams by precipitation with lignochemicals and humic acids. Lignochemicals are by products from the paper industry, while humic acids are obtained by caustic treatment of peat, subbituminous coal, and lignite. These high-molecular-weight organic materials have many functional groups, which can coordinate and form innercomplex salts with heavy metals that are crystalline precipitates. Filtering of a humic-acid-or lignochemical-treated solution or waste stream containing these precipitates removes the heavy metal sequstrates. Tests were conducted with two lignochemical samples, three humic acid samples, lime (CaO), and sodium hydroxide (NaOH) in which increasing amounts of these additives were reacted with 50 mL of solution containing Fe3+ , Al3+, Cr3+, Pb2+, Cu2+, Cd2+, Zn2+, Co2+, Ni2+, Mn2+, and Hg1+. At the appropriate pH, greater than 90-and 99-pct removal was achieved for these 11 heavy metal ions from the 10-and lOO-ppm solutions, respectively, using lignochemicals and humic acids. Removal efficienC)' with these organic materials is better than that with CaO, especially for the more toxic ions, Hg1+, Cd2+, and Pb2+. Unlike the precipitates formed with NaOH or CaO, those with lignochemicals and humic acids are compact and noncolloidal. The volume of their sludge is sharply lower than that of the finely dispersed lime or soda precipitates; thus, their removal in settling tanks or by simple filtration is enhanced.

Jan 1, 1988

By M. G. Zabetakis

This publication presents a simplified graphic method for determining the explosibility of mine atmospheres under mine-fire conditions from mine- atmosphere composition data. Sometimes it is necessary to seal part of a mine during a fire to exclude air and thus extinguish the fire. Unfortunately, liberation of methane and formation of hydrogen and carbon monoxide in the sealed area may create an ex- plosive or flammable atmosphere if enough oxygen is present to support combustion. On the other hand, the oxygen concentration may be reduced through combustion processes and the concentration of inert gases (nitrogen and carbon dioxide) increased enough to render the atmosphere within the sealed area non-explosive. Before an area is unsealed, it is extremely important to know if the sealed atmosphere contains Flammable gases in proportions that might form explosive mixtures when air is introduced. If an explosive mixture forms and the fire is rekindled, a gas explosion will result. Various experimental methods may be used to determine the explosibility of a particular mine atmosphere; however, these methods usually are impracticable in the field.

Jan 1, 1959

By L. W. Kelly

The purpose of this circular is to show that, under the conditions prevailing in the Stony Point mine, wooden bolts were just as satisfactory as steel bolts or conventional timbering, with a reduction of approximately 80 percent in cost of material. This one fact alone is enough to justify an experiment with wood. This circular will show that production records have remained constant with both wooden and steel roof bolts. INTRODUCTION The successful use of steel roof bolts is now an accomplished fact in the coal industry, but the use of wooden bolts in place of steel is a rarity. The first experiment with wooden roof bolts was mane in 1949 in the Rio Verde mine, Norton Coal Corp., Nortonville, Ky.2/ This experiment was successful; the company obtained excellent results, but operations in the mine were suspended before enough time had elapsed to prove the value of wooden roof bolts conclusively. It is obvious that, if wooden roof bolts could be used in place of steel bolts or conventional timbering-methods, every mine operator would use word, as the cost is only a fraction of the other two methods. The Stony Point experience has proved conclusively that, under certain conditions and with a certain type of roof, wooden roof bolts can be used successfully.

Jan 1, 1952

By N. H. Coates

A small, special-purpose centrifugal compressor was developed to circulate 60 pounds per hour of helium at 1,000° F and 250 psig because standard, commercial units were not available. Performance characteristics of this compressor were determined at helium flows of 2,000 to 18,000 std cu ft per hour, pressures of 100 to 250 psig, and temperatures of 100° to 1,000° F. This range is 2 to 90 actual cu ft per minute. Several graphs show the adiabatic head developed by the compressor over this wide flow range at various combinations of temperature and pressure. A compressor performance map relates pressure ratio to mass flow, temperature, pressure, and speed. This map can be used to accurately predict compressor performance factors within the range of operating conditions covered by the experiments.

Jan 1, 1963

Provide reliable, early-warning fire detection instruments, telemetry, and control systems for noncoal underground mines. Approach Industrial-grade fire detection instruments and signal telemetry equipment were modified for long-term exposure to harsh underground mine conditions, then were installed in four mines to evaluate long-term performance and reliability. How It Works The elapsed time between the onset of a fire and its detection is critical because fires tend to grow in size and intensity with time. Early fire detection and warning permit the initiation of a mine's emergency plan (evacuation, fire fighting, etc.) while the fire is still small, or ideally, while it is still in the incipient stage. Fire detection and warning systems, utilizing sensitive heat, flame, smoke, and gas analyzers, provide the most rapid and reliable indication of a developing fire.

Jan 1, 1987