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By L. B. Pankratz

High-temperature heat contents were measured for two praseodymium oxides and three terbium oxides. There were: Pr2O3 (298° to 1,600° K), PrO1.833 (298° to 1,050° K), Tb2O3 (298° to 1,600° K), TbO1.719 (298° to 880° K), and TbO1.812 (298° to 850° K). With the exception of PrOl.833, all results were regular. PrO1.833 had a small thermal anomaly at 760° K with an extra absorption of 380 cal/mole. The measured heat content values, tabulated smooth heat contents, and entropy increments are reported. Heat content equations were derived.

Jan 1, 1966

By J. G. Eisele

Solvent-extraction characteristics of dodecyl phosphoric acid (DDPA) were investigated to determine its potential as a fractional or selective extract-ant for individual elements in a rare-earth-yttrium mixture. The DDPA is an effective extractant for splitting rare-earth mixtures into light and heavy subgroups. Yttrium normally extracts with the heavy rare-earth elements but may be shifted toward an extraction sequence with the light rare-earth elements by increasing the pH. Elements in the light and heavy ends of the rare-earth series can be separated from middle-group rare-earth elements by using diethylenetriaminepentaacetic acid (DTPA) as an aqueous phase counter-extractant. Hydrogen-ion dependency of the distribution coefficients differs from that reported for similar systems at tracer-level concentration.

Jan 1, 1965

By O. E. Traubert, E. G. Meiter

"The daily sulphur dioxide content of the air at the Pittsburgh Experiment Station of the Bureau of Mines was determined by the bureau at the request of Committee D-14 on Screen Wire Cloth of the American Society for Testing Materials. The purpose of the investigation was to obtain data for use in interpreting screen-corrosion tests, which were conducted simultaneously and jointly by the committee4 and the Bureau of Mines.The plan of this investigation was to vale a single daily determination, except on Sundays and holidays, of the SO2 content of the atmosphere at the exposed test screens, for a period of one year. No attempt was made to determine the variation during the day, except on the morning of October 15, 1927, when the atmosphere was unusually foggy and smoky. Several successive determinations were made on that date to ascertain changes in the SO2 as the morning haze disappeared. The SO2 determinations were begun on August 11, 1927, and continued until August 11, 1923.The Pittsburgh Experiment Station of the Bureau of Mines is in a residential section about 3 miles east of the central or main business district of Pittsburgh. The air samples were taken on the roof above the auditorium, or the center rear of the building. This was also the place where the pieces of screen were placed for corrosion tests. The height was about 40 feet above ground level. Several sources of considerable smoke and SO2 are in the immediate vicinity. On the west side of the building is a double-track railroad. At this point the line runs through a cat below the level of the building. The horizontal distance between the air-sampling position and the railroad tracks is about 400 feet, and the vertical distance about 70 feet. The power plant for the Bureau of Mines building is about 250 feet south of the sampling position. About 1000 feet farther to the south are the engineering building and power plant of Carnegie Institute of Technology, and 1/4 mile to the southwest is the power and heating plant for the Carnegie Library and Museum. About 1 to 2 miles farther south and also southwest"

Jun 1, 1930

By W. E. Wallace

Volume-rate-of-flow measurements were made of the flow of mercury through porous samples under conditions of no field, magnetic field transverse to the direction of flow, and transverse magnetic field and electric current to determine if a magnetic method might be potentially useful in the study of pore-size distribution. No change was observed in the flow rate from the application of a magnetic field alone. The application of both field and current produced an electromagnetic pumping action with or against the direction of flow, depending upon the direction of the electric current. This pumping effect was observed to be greater in a rectangular porcelain sample than the calculated value for an equal-Sized open channel.

Jan 1, 1969

By Joseph J. Wallace

1. From the standpoint of known recoverable reserves, the following is the order of importance of the beds: Upper Kittaoning, Lower Kittanning, Upper Freeport, Lower Freeport, Middle Kittaning, Clarion, Pittsburgh, and Redstone. 2. mown measured and indicated reserves in all beds, based on a minimum thickness of 14 inches and on 1,800 tons per acre-foot of coal in place, me estimated at 1,859 million short tons as of January 1, 1952. Of this, 1,351 million short tons me in beds 28 inches and more thick. Areas in each bed were omitted from the estimates because available data relative to the bed characteristics are too meager to make an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these areas, such reserves should be added to the total estimated reserves.

Jan 1, 1953

By John A. Organiscak

[Fugitive Just is generated alone unpaved mire reads from intermittent equipment traffic. Typically, the majority of such traffic consists of trucks hauling either mine product or waste [rum the surface mime pit and/or the processing plant. Fugitive dust generated along these unpaved mine roads includes particles of all sizes which become airborne. The potential hazards include the deleterious effects to human health of inhaled dust, traffic visibility hazards and environmental impacts on the localized area by the larger-sized visible airborne dust. Two held surveys were recently conducted to quantify fugitive dust generation and dispersion from truck traffic on unpaved and untreated mine haulage roads For these surveys., airborne glow sampling was conducted at multiple sampling fixations away from an unpaved haulage road at a limestone quarry/plant and at a coal mine preparation plant lo measure the size characteristics, concentrations. and dispersive behavior of the dust cloud generated from truck traffic- Results show that at least 80% of the airborne Just generated by haul trucks was larger than 10 µm- Airborne respirable, thoracic, and total dust concentrations all decreased and approached background concentrations 30.5 in (100 feet) from the road This report describes the average and instantaneous peak dust levels that were measured tip to 30.5m (100 feet) Iron the haulage road. Keywords: Unpaved mine road, fugitive dust, silica.]

Jan 1, 2008

By Terry S. Cory

This report covers antenna design, analysis, and development work suited for use with a wireless radio communication system operating at medium frequency. The work includes the test and evaluation of prototype vehicular antennas developed during the program.

Jan 12, 1978

By David C. Oyler

The U.S. Bureau of Mines and the United States Steel Corporation evaluated the progress of methane drainage at the Oak Grove, AL, degasification pattern. Coalbed pressures were monitored between December 1981 and November 1985. Formation pressures, in the lower bench of the Mary Lee Coalbed, were reduced from 400 lbf/in2(ga) in 1977 to 50 lbf/in2(ga) in November 1985. Gas contents of coal cores obtained from monitor wells were compared with coalbed gas contents measured in 1976. Data indicated a 48- to 56-pct reduction within the pattern and a 29-pct reduction at a point 500 ft outside the pattern. The effect of the advance of a section of the Oak Grove Mine on changes in gas and water production rates in the pattern was evaluated. Gas production increases were noted in 12 wells; water production decreases were noted in 6. The times of initial influence indicate the presence of a zone of high permeability within the pattern. This zone correlates well in orientation and location with a fracture zone mined through at the mine. The existence of such fracture zones could have a significant effect on productivity of individual coalbed methane wells.

Jan 1, 1989

By W. G. Hopkins

The development of systems for location of miners who have become entrapped following a mine disaster has been one of the major research goals in the Bureau of Mines. This study details the preliminary development of such a system. Current technologies for locating trapped miners from the surface are either simple direction finders or time difference pulse systems that have accuracy limitations. Developing technologies using full vector field measurements at several receiving points are currently being studied. The necessity of measuring field strength with great accuracy can be a drawback in these systems. A system that operates with continuous wave radio signals, whose phase differences can be measured accurately even in weak signal conditions, greatly improves the location accuracy. A microcomputer would be used in conjunction with the system, to gather and manipulate the data to automatically pinpoint the location of the trapped miner. Comparison of this system with existing technology indicates a favorable accuracy/complexity ratio for the phase difference of arrival technique.

Jan 1, 2011

By A. L. Engel

This report is a compilation of preliminary and, in some cases, more extensive concentration experiments by the Federal Bureau of Mines on low-and medium-grade fluorspar ores from three localities in Nevada and one in California. The work was done on samples obtained from Shoshone mine, Nye County, Valery mine, Pershing County, and the Broken Hills mine, Mineral County, all in Nevada, and Dirty Weather mine, Inyo County, Calif. These investigations were made to aid in the development of domestic fluorspar resources, in line with the Bureau's long-established program of conservation of mineral resources. The treatment methods employed in the experimental work described included simulated or "heavy-liquid" gravity concentration of coarse minerals and comparatively fine-grained minerals, and flotation concentration of finely-ground minerals. These methods were attempted in order to beneficiate the ores and produce concentrates which could be marketed readily, with as high a recovery rate as possible, while using simple treatment methods suitable for small-scale operation.

Jan 1, 1961

By V. A. Marple, K. L. Rubow, Y. Tao

"A personal diesel exhaust aerosol sampler has been designed and evaluated in both laboratory and field settings. The sampler uses size selective sampling for the determination of the respirable mass concentrations of mineral dust and diesel exhaust particulate matter found in underground coal mines. This design is based on the premise that diesel exhaust particulate matter is predominantly less than 0.8 um while mineral dust is greater than 0.8 gm. Operating at a flow rate of 2 L/min, the sampler consists of a 10 mm Dorr-Oliver respirable dust cyclone followed by an 0.8 gm cutpoint impactor and an afterfilter. Field evaluations consisted of sampling at 6 different locations in these underground coal mines. Measured aerosol concentration less than and greater than 0.8 um have been compared with a well characterized cascade impactor.Techniques must be developed for measuring the mass concentration of diesel exhaust particulate matter found in underground coal mines due to the health concerns associated with worker exposure to diesel exhaust particulate matter. Diesel exhaust particles are in the respirable size range and have been regarded as a potential occupational carcinogen by NIOSH (1988). Furthermore, a 1988 MSHA advisory committee directed MSHA to develop a sampling protocol for assessing worker exposure to diesel exhaust particles.The University of Minnesota and the Bureau of Mines, over the past 4 years have measured the size distribution of diesel exhaust particles and mineral dust, both in the laboratory and underground mines (Cantrell, 1987; Cantrell et al., 1987; Cantrell and Rubow. 1988; Marple et al, 1986; Rubow et al., 1988: and Watts et al., 1989). To date, measurements have been made in nine coal mines. Seven mines utilized diesel-powered equipment at the mine face while two used electric-powered equipment. The results of these field tests indicate that mineral dust and diesel exhaust particles can be differentiated on the basis of particle size. The measured particle size distributions have been found to be bimodal with a saddle point at 0.8 um. This has led to the hypothesis that one method for measuring worker exposure to diesel exhaust particles would be to collect size fractionated particle samples separated at 0.8 um with the diesel particles being less than 0.8 um and the mineral dust particles greater than 0.8 um.Aerosol size distribution measurements, using a micro-orifice uniform deposit impactor (MOUDI), have been conducted in the mine intake air portal, intake entry to the working section, haulageway, and section return entry. The MOUDI is a ten stage cascade impactor with particle cutpoints ranging from 0.1 to 15 um aerodynamic diameter (Marple and Rubow. 1984b; Marple et al., 1989). The sampling flow rate is 30 L/min."

Mar 1, 1992

Develop a more efficient method of testing the integrity of in-situ leach mining operations. The Problems For economic and environ-mental reasons, in-situ leaching operations must be sure that wells do not leak. Loss of solution in large quantities can be expensive in itself, and if such losses result in pollution the costs can be even higher. Wells are usually tested for leaks by sealing them with packers, pressurizing them and monitoring the pressure drop. However, many commercially-available packers are designed to be used in steel-cased wells rather than the fiberglass-or plastic-cased wells used for in-situ mining. These packers are heavy, cumbersome, expensive, and often leak. In addition, commonly used well-integrity-test systems require lengthy test periods and drill rigs or hoist trucks with rigid pipes must be used to run the packers in and out of the well. The Bureau of Mines has developed a mobile, self-contained leak-testing system that is faster, uses trailer-mounted equipment that can be operated by one person, and features a new inflatable packer.

Jan 1, 1985

By W. A. Grosh

In 1951 the Federal Bureau of Mines became interested in the reports of copper-nickel mineralization in northern Minnesota. Several outcrops on the north side of the Duluth gabbro in the Kawishiwi River area were sampled by the Federal Bureau of Mines and George M. Schwartz of the Minnesota Geological Survey. Because these samples showed appreciable amounts of copper and nickel, a 100-pound sample of an un-altered outcrop was obtained for metallurgical testing. Results from this preliminary work were all favorable; therefore, in the fall of 1953 the Bureau of Mines diamond-drilled three holes near the outcrop of the con-tact between the Duluth gabbro and the Algoma granite. A total of 686 feet of NX size hole was drilled, and 100 percent of the core was recovered. Each hole intersected the contact, and the strike and dip for that locality were established. The core was split, and half was used for analyses and further metallurgical tests; the remainder was retained for permanent record in the Bureau of Mines core-storage warehouse.

Jan 1, 1955

By W. H. Oppelt

To provide a relatively structurally stable form of dried lump lignite, two North Dakota lignites from Mercer County were dried by the Fleissner process in an atmosphere of saturated steam at 200, 300, and 370 p.s.i.a. pressure, corresponding to steam temperatures of 382°, 417°, and 437° F., respectively. Two series of experiments were made at each test pressure with the individual lignites. In one series, the autoclave was preheated to the processing temperature before charging the lignite; in the other the lignite was charged into the autoclave at room temperature. In each case, heat losses were determined by blank tests of steam consumption over a similar operating cycle with the empty autoclave. The degree of moisture removal and net steam consumption were calculated from material balances. The amount of water removed as a liquid from the two North Dakota lignites during the heating and steaming periods was compared with results calculated from previously published data on drying Austrian lignite and Australian brown coal. These lignites, covering a wide geographical area, had original moisture contents ranging from 35 to 49 percent. The Austrian lignite and Australian brown coal are considered to be of Miocene Age, and the Dakota lignites belong to the Paleocene.

Jan 1, 1955

By Miles B. Royer

The experimental blast furnace has attracted increasing interest during the past decade as a practical means for investigating a broad range of blast-furnace smelting problems. Under experimental-furnace conditions, information can be obtained with less expenditure of time and raw materials and, therefore, at lower cost than comparable information could be obtained under industrial operating conditions. Furthermore, the experimental furnace may be operated beyond the range of smooth operation, even to failure, to delineate the limits of operability. Such deviation from normal operating practice would be economically intolerable in industrial operations where production and operating stability might be disrupted. The Federal Bureau of Mines experimental blast furnace at Bruceton, Pa., near Pittsburgh, has been operated and under development since 1951. However, the usefulness of this experimental data to industrial practice was somewhat nebulous in early experiments, and the correlation of the experimental blast furnace with the industrial blast furnace was not known.

Jan 1, 1961

By C. J. Chindgren

A refractory-lined, garage-type automobile incinerator with a natural gas afterburner for air pollution control was cooperatively constructed and tested by the Bureau of Mines and the Wasatch Metal & Salvage Co. in Salt Lake City, Utah. The incinerator is capable of relatively smokeless burning of 32 to 60 cars per day, dependent on the degree to which the cars are stripped prior to incineration. Preliminary burning campaigns indicate the cost of incineration to be approximately $2.75 per car.

Jan 1, 1970

By K. Kar, A. Sreeoath, M. Gautam

"This paper presents results of an experimental investigation of the sampling efficiency of a blunt cylindrical sampler oriented with respect to the oncoming flow. The number of particles sampled by the cylindrical blunt sampler and an isokinetic sampler is measured using the TSI Aerodynamic Particle Sizer. A technique is described to conven the ratio of the particles sampled into the sampling efficiency. The experimental data thus obtained is then compared with the impaction model of Vincent and Mark (1982) with the empirical constant determined from our experiment.. The comparison shows excellent agreement for 0° and 90° orientation.1.0 IntroductionCylindrical dust samplers are widely used in practice to determine the concentration of the airborne particulate matter. The sampler is simply a means to collect particles from the ambient, whose concentration is subsequently measured by some size selective techniques. Gravimetric and optical techniques are the two most commonly used methods to measure the particle sizes. While impactors are used in gravimetric analysis, Aerodynamic Particle Sizer, Aerosizer. Electron microscope, Coulter Counter etc. use the optical method to measure the particle sizes. The Aerodynamic Particle Sizer (APS) and the Aerosizer are the new generation devices which employ the time of flight of particles within intersecting laser beams to determine the particle size.The introduction of the sampler in the free stream disturbs the flow pattern due to two distinct actions of the sampler on the fluid stream: one of them results due to the conformity of the flow to the geometry of the circular cylinder and the second one is caused by the flow into the suction orifice. If the sampler performance is determined by the number of particles entering into the sampler inlet relative to the number of particles present in the free stream, then the particle trajectory outside the sampler and into the inlet is the deterministic factor for the sampling efficiency. The particle trajectory inside the sampler is not important in this case."

Nov 1, 1995

By F. P. Haver

The Federal Bureau of Mines investigated aqueous electrolysis as a means for reducing lead chloride prepared by ferric chloride leaching of galena concentrate: NaC1 PbS + 2FeC13 ? PbC12 + 2FeC12 + S°. During electrolysis, metal was produced from solid lead chloride in contact with the cathode rather than from lead in solution. Relatively high current densities--up to 300 amp/ft2--were possible when operating in this way. A very simple cell, having a horizontal lead cathode at the bottom and a vertical graphite anode at the top, was employed. Lead chloride crystals, covering the cathode, were converted to metal powder during electrolysis, and chlorine gas or FeCls was produced at the anode, depending on the electrolyte composition. Electrolytes tried included aqueous solutions of HCI, NaCl, NH4Cl, and FeC12-NaC1. Optimum results (96-pct current efficiency, 0.23 kwhr/lb Pb) were obtained with 20 pct HC1 at 25° C, using a current density of 15 amp/ft2 and an electrode spacing of 1 inch. When the current density was increased, the energy requirement increased also but only to 0.41 kwhr/lb at 150 amp/fr3 and 0.58 kwhr/lb at 300 amp/ft2.

Jan 1, 1978

By D. Harrington

"In order to stimulate general interest in mine safety among their employees the mining companies of Butte, Mont., instituted in 1918 a Miners' Field Day, and this field day has since been held annually about the end of July, the last one being on July 25, 1921. The mining companies of the Butte district finance this meet in proportion to the number of men employed at the time of the meet, the contributing companies with number of working force, end proportional contributions for the opening field day in 1918 being given below:COMPANY NUMBER EMPLOYED AMOUNT CONTRIBUTEDAnaconda Copper Mining Co.,12,500,$ 1,078.53Butte & Superior Mining Co.,1,800,155.32North Butte Mining Co.,,1,294,111.67East Butte Copper Co.,,850,73.36W. A. Clark Interests,,600,51.78Davis-Daly Mining Co.,,340,29.35,,,,17,384,$ 1,500.00*Note: In many mining districts it is now the custom to hold an annual Miners' Field Day. The field day, as a rule, is financed principally by the mine operators, and was instituted primarily to promote interest among miners in the ""Safety First"" movement. Usually demonstrations or contests in first aid and mine rescue are the leading feature of the day's events, which include games, races, dancing, and all the other amusements usual to a gala holiday. Thus the field (ley serves the double purpose of stimulating interest in mine safety and promoting cordial relations and community fellowship. This paper is an interesting account of the way in which the Miners' Field Day in the Butte district is organized, with data on costs, plan of organization, method of conducting, and the practical benefits derived from it. - Ed"

Oct 1, 1921

By Robert L. Jones, Clifford Dunham

"INTRODUCTION The Wah Wah mine was examined 3/ by the Bureau of Mines in September, and a project was started in November 1942. Assistance was given by the Federal Geological Survey in formulating proposals and plans, and two geoloists were assigned to map the surface and underground workings in October 1942.HISTORYThe Pine Grove mining district was organized in 1S73, but no work was done there until it was reorganized in 1879, after which it is reported that a little ore was shipped. The Wah Wah Mining Co. was incorporated September 2, 1937. Prior to that time, predecessor organizations had spent approximately $122,000 on the property now held by this company. The board of directors of the Wah Wah Mining Co. approved expenditure of $47,652.14 from September 1937 to June 1942 for development. This work was confined to the Tasso shaft and connecting levels. Shipments in 1939 amounted to 925.789 dry tons with a gross value of $12,477.83. This ore contained 20,130 pounds lead, 1,390 pounds copper, 7,434 ounces silver, and 65.09 ounces gold. The mine was idle from July 1941 to November 1942, when, the Bureau initiated a project to unwater the Tasso shaft and proceed with the exploratory work as outlined in the War Minerals Report."

Apr 1, 1946