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By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

D. 1 Most Effective Salts A. Ammonium Phosphates Monammomium phosphate and diammonium phosphate (salts of ortho phosphoric acid) are superior to the triammonium salt in fire-resisting properties. Of these two, the monammomium salt is chemically the more stable. It is also held very retentively by a number of woods, thus reducing leaching out of the salt if exposed to water. Saturated aqueous solutions of mon- or di-ammonium phosphates have vapor preservatives corresponding to an atmospheric relative humidity of 9Z to 93 percent, the wood, will, therefore, not attract any moisture at humidities below this figure. Low concentrations (1 lb dry fire-retardant per cubic foot of the dry, treated timber) will stop flame and high concentration (5 lbs. per cubic foot) will prevent smoldering. B. Ammonium Sulphate In low concentrations ammonium sulphate has only a small effect on flame propagation, but its effect is marked when concentrations of the order of 20 percent are employed. It has no appreciable effect on smoldering. It is more corrosive to metals than are the phosphates, but is less corrosive than ammonium chloride or magnesium chloride. It is possible to leach it out of wood by prolonged and continuous action of water The vapor pressure of the saturated solution corresponds to 81 percent atmospheric humidity.

Jan 1, 1976

By Kathleen M. Kowalski-Trakofler

This paper discusses human judgment and decision making under stress. The authors review selected recent literature across various disciplines and suggest a definition of stress within the context of decision making during the management of emergencies. They also discuss fieldwork by the Pittsburgh Research Laboratory, NIOSH, which explores traumatic incident stress, the relationship between previous training and performance under stressful conditions, and human behaviour in underground mine fires. The authors assert that stress is one of the factors that decision makers must contend with in most life-or-death situations. They suggest that a better understanding of individual judgment and decision making activities whilst under stress would yield a better understanding of how people reach the choices they make in emergencies. This enhanced understanding would be of enormous value to emergency managers, researchers and policymakers.

Jan 1, 2003

By L. O. Bacon

This Bureau of Mines report summarizes the results of laboratory work in the design of instrumentation for obtaining the dynamic tensile strength of rock at minimum loading. Minimum loading is defined as the lowest tensile loading by pulse reflection to cause fracturing. The instrumentation for obtaining dynamic tensile strengths of rock cores evolved into the use of a compressed-air pellet gun to impact one end of a rock core, suspended by wires, at increasing increments of air pressure. Maximum strain was measured on most or all of the impacts, and the strain at fracture of the core was obtained by extrapolating the pellet velocity-strain curve to the pellet velocity at fracture. Stress at tensile fracture was obtained from the maximum s train, and the dynamic Young's modulus was calculated from the rod velocity by using simple rod theory.

Jan 1, 1962

By Nabil A. Bibawy

The U.S. Bureau of Mines has established a method for the calibration of class 2 and class 4 standards of mass using a procedure from designs developed by the National Institute of Standards and Technology (NIST). This method produces a weight calibration that is within 1.0 pct of the balance sensitivity. A set of four 1-kg weights yielded a standard deviation of 3.25 mg compared to ±2.91 mg balance sensitivity. The method employs the use of a high-accuracy balance to measure the difference between a set of weights calibrated by NIST and the set to be calibrated. The error of the balance is included in the error for each weight calibrated.

Jan 1, 1989

By Clarence Hall, Charles E. Munroe

In accidents resulting from the use of explosives in metal mines and quarries in the United States more than 130 men were killed and 250 seriously injured during the calendar year 1913. More- over, an unknown number of miners suffered from the effects of breathing the harmful fumes and gases given off by the burning or the incomplete explosion of some explosive. Consequently, the Fed- eral Bureau of Mines, which is endeavoring to increase safety in mines and to abolish conditions that tend to impair the health of miners, is studying the kinds of explosives used in mining and the conditions under which these explosives can be used with least danger to the miner. Information about the different explosives used in coal mining and the precautions to be taken in using those explosives has been printed in Bulletin 17 and other bureau reports, the names of which may be found at the end of this bulletin. The bureau has not been able to give much attention to explosives used in metal mines and quarries, but has published some information about these explosives in Bulletin 48, "The Selection of Explosives Used in Engineering and Mining Operations"; Technical Paper 17, "The Effect of Stemming on the Efficiency of Explosives"; and Miners' Circular 19, "The Prevention of Accidents from Explosives in Metal Mining." This bulletin aims to give the metal miner and the quarryman information similar to that given the coal miner in Bulletin 17. In- flammable gas or dust is seldom, if ever, found in quarries or metal mines, and the danger from using explosives there is less than in coal mines; but, as the figures show, the number of men killed and injured yearly in accidents caused by explosives proves the need of both miners and mine officials striving to see that none but proper explosives are used and that these are used properly.

Jan 1, 1915

By L. D. Tracy

"This paper represents work conducted by the Bureau of Mines in cooperation with the Illinois Geological Survey and the Engineering Experiment Station of the University of Illinois.IntroductionThe present report covers conditions and mining royalties in District VIII of the coal fields of Illinois, as designated by the Illinois Geological Survey. The various districts have been described in the reports on the Illinois coal-mining investigations, carried on cooperatively by the Illinois Geological Survey, the engineering experiment station of the University of Illinois, and the U. S. Bureau of Mines. This district includes Vermilion and Edgar Counties, but as the coal-mining operations in Edgar County amounted to only 827 tons in 1923, the data here given have been confined to Vermilion County.A similar report on District VI (Williamson and Franklin Counties) has been issued as Serial 2722 of the Bureau of Minos.A description of geological and mining conditions, and a discussion of market and transportation facilities, have been included because these have an important bearing on the royalties specified and the general conditions of the lease.Mining ConditionsDistrict VIII is better known as the Danville district and in 1923 produced 4,177,000 tons of coal, or approximately L per cent of the total output for the entire State for that year, which was 79,300,000 tons."

Apr 1, 1926

By Elizabeth A. Johnson

Minor-element behavior and interaction in the copper matte-iron silicate slag system have been studied by the Bureau of Mines. In the present work, the possibility of interactions among the minor elements As, Sb, Bi, Se, and Te was investigated. Equilibrations of matte, slag, and one of each of the five minor elements were performed at 1,250° C under typical matte smelting atmospheres of CO, CO2, and S02 for mattes containing 40, 50, and 60 pct Cu. Results are compared with those of a previous Bureau of Mines study in which all five minor elements were present simultaneously.

Jan 1, 1984

Publicize the valuable information resources covering research conducted by the U.S. Bureau of Mines (USBM) and other federal laboratories that may be of interest to USBM customers. Access to this information is important for promoting further research and in transferring the technology to the end user. USBM Information Resources The USBM serves as the Nation's premier agency for mining- and minerals-related research. In sharing the benefits of this research with American industry and the American people, the USBM supports information systems outlining this vast array of technical knowledge. The USBM is dedicated to making its technology readily available and will continue to expand its electronic communications capabilities. The following resources provide instant access to USBM information. U.S. Bureau of Mines Bulletin Board. The Bulletin Board is a free service accessed by computer modem. All that you need are a computer, a modem, and communications software. The telephone number for the Bulletin Board is 202-501-0373; for information on using the system call 202-501-0406. Use X-modem protocol set to 1200, 2400, or 9600 baud, 8 data bits, and 1 stop bit (8,N,1). The information on the system can be viewed or downloaded. This service includes the following: announcements on Bulletin Board and other USBM activities; mineral news, features, and press releases from the Bureau's Office of Public Information; a list of recent publications and articles by USBM authors; mineral commodity data and Mineral Industry Survey reports; USBM Technology News, concise factsheets announcing milestones in USBM research and technology; a current list of computer products available from the USBM and the National Technical Information Service (NTIS); and a listing of cooperative research opportunities with the USBM.

Jan 1, 1995

By Thomas M. Barczak

The safety of mine workers depends on the proper installation of roof supports to prevent the ground from collapsing into the working areas of an underground mine. As new support systems are developed, they need to be properly evaluated to make sure that they are capable of providing adequate roof support before they are first used in a mine. In addition to making certain that the supports meet basic safety criteria, the limitations of the support need to be fully defined in order to avoid improper application of a particular support design. The National Institute for Occupational Safety and Health (NIOSH) operates a world-class facility called the Safety Structures Testing Laboratory. This laboratory contains a unique load frame, the Mine Roof Simulator, which is capable of simulating the ground behavior in underground mines for conducting full-scale evaluations of roof support systems. Safety performance testing protocols using the unique Mine Roof Simulator have been developed for both standing roof support systems and longwall shield supports. The purpose of this paper is to describe these test procedures. The protocol for standing roof supports incorporates seven test series:( 1) uniform loading baseline tests, (2) height evaluations, (3) asymmetric loading, (4) biaxial loading, (5) load rate studies, (6) active loading determination, and (7) static loading evaluations. For longwall shields, a four-series test program that accurately simulates in-service conditions on a longwall face is proposed. This test program consists of (1) transfer of horizontal load to the caving shield-lemniscate assembly (zero-friction test),(2) point loading of shield joints due to lateral movement or rotation of the canopy, (3) evaluation of leg socketand leg cylinder integrity, and (4) face-to-waste racking of the shield. In addition, an evaluation of the shield’s hydraulic components will be conducted prior to the performance testing. These protocols will provide state-of-the-art safety performance evaluations of emerging support technologies, as well as a means to assess the safety of both new and aging longwall shields. Hence, this effort will enhance the safety of mine workers by ensuring that critical support elements are properly designed and that aging supports are retired before their support capability is jeopardized.

Jan 10, 2000

By H. M. Lawrence

"In the land-pebble district of Florida a lively interest in the possibilities of obtaining increased recoveries of phosphate rock is evident. Research in several directions is being carried on by companies operating in the district to increase the yields obtained by the washing plants. The Bureau of Mines is cooperating with this research program to promote more efficient plant practice and to avoid unnecessary depletion of mineral resources.Washing practice, as carried on in the district at present for the recover of phosphate rock from the crude ores or matrix, is not a complicated process. Flow sheets of the several companies are similar, although the equipment varies with the preferences of the individual operators. For disintegrating the matrix log washers are favored, although revolving drums equipped with flights to break up lumps of clay are also used. Fine sand is removed by screening. Vibrating screens have become well established in the district, although stationary flat screens and trammels are also employed.The writer acknowledges with appreciation the cooperation of the phosphate companies in the land-pebble district; suggestions and criticism by Will. H. Coghill, supervising engineer, Ore Dressing Section of the Bureau of Mines; and the laboratory assistance of J. O. Davie, J. W. Pamplin, and E. Roca, cooperative fellows of the University of Alabama.Losses in the Finer SizesOf the phosphate that is not recovered by present washing methods the greater portion is in the finer sizes. In these sizes the phosphate grains are accompanied by grains of sand - largely quartz - of the same size, and recovery of these phosphate grains as a commercial product is not possible by simple washing methods. Phosphate recoveries approaching complete extraction can only be effecte by applying metallurgical processes, either mechanical or chemical. As yet, most of these processes have not advanced much beyond the laboratory or perhaps the pilot-plant stage. Such processes may have some application to the beneficiation of phosphatic ores or washer rejects, but a discussion of them is not within the scope of this paper."

Apr 1, 1929

By F. Garcia, J. Cervik

Recent advances in the commercial separation of gases using membranes have renewed interest in the possibility of applying this technology to the recovery of methane ( CH4 ) from mining operations . This Bureau of Mines report briefly reviews the history of the development of membranes for gas separation , the theory of how they work , and their application to the separation of methane from air and associated problems . However , methane -air mixtures are difficult to separate with membranes because the pertinent gas couples , 02 - N2 , 02 - CH4 , and N2 -CH4 , have poor separation characteristics , as indicated by their separation factors of about 3 or less . Even if these separation factors were substantially higher , there is doubt that methane could be recovered economically from the low concentrations in mine ventilation exhaust ( 2 vol pct or less ) . The exhaust pressures are not sufficient for adequate separation . The power cost of compressing the methane recovered . these mixtures would far exceed the value of New discoveries could make separation of gob hole methane - air mixtures practical . These mixtures have much higher concentrations of methane (from 30 to 100 vol pct ) ; however , for safety reasons , be limited to gob gas with 60 vol pct CH4 or more .

Jan 1, 1988

By W. J. Fene

It is often desired to obtain samples of air in places where collection by ordinary methods is not feasible, as in shafts amore means of descent or ascent are not provided, in sewer manholes, in gas or water wells, in empty oil tanks, and in sealed areas in mines. Heretofore, when such sampling was required, it was necessary to utilize the aspirating method, which was not always satisfactory; and to obtain samples of air in deep shafts, it was necessary to use long sections of rubber tubing, which was not always available. DESCRIPTION OF NEW DEVICE A new method or "device" employs a common snap-type mousetrap to break the neck of a vacuum tube at the place where it is desired to collect the sample (see fig. 1). A mousetrap is mounted on one end of a block of wood 11-3/4 by 3 by 3/4 inches in such camper that a lead weight attached to the trigger hall spring the trap when the device is given a sharp jerk. A vacuum tube is placed on the other end of the block and held in place by a strong rubber band. A strip of corrugated rubber is placed on each side of the grooved block to prevent the tube from clipping when the sample is taken. An adjustable shoulder, provided with a rubber cap, is pieced se that the neck of the vacuum tube will rest on it. The shoulder is made adjustable to accommodate various sizes of tubas and to keep the neck of the tube from breaking tee far back from the point. A metal handle is fastened to one end of the block, with a hole in the end through which the brass wire used for lowering the device is tied. The device is enclosed by a strong wire-gauge covering, hinged on one side and so arranged that it can be locked shut on the other side. This covering prevent: breaking of the tube while it is being lowered or raised in a shaft or other place. Brass wire of not less than 22 gage should be used for lowering the device. A detailed drawing of the device is shown in figure 2.

Jan 1, 1940

By Lars Osen

This investigation was undertaken to contribute to the understanding of underground pull tests by conducting laboratory tests under closely controlled conditions. Steel bolts, instrumented with electrical resistance strain gages, were anchored in an aluminum block, a granite block, and a steel sleeve, and were subjected to pull tests. The bearing plates used were either flat7 dished, or embossed. In pull testing a bolt that is prestressed, there is a range of loading during which bolt load is greater than the jack-applied load, This study showed that preload, the size, shape, and type of bearing plate; and the geometry of the system determine the point at which bolt load and applied load become equal. The effects on bolt load of both a theoretical solution and actual pull tests were analogous and led to similar results.

Jan 1, 1965

To cost-effectively reduce noise and vibration in newly manufactured mantrip vehicles. Approach Previous Bureau of Mines research demonstrated that noise controls could be in-stalled on existing mantrip vehicles, thereby substantially lowering noise levels inside the mantrip. Under Bureau sponsorship, a manufacturer of mantrip vehicles agreed to incorporate similar noise controls into a new vehicle during manufacture. Throughout this project, durability, maintainability, and cost were considered to be as important as noise reduction. How It Works The following noise-control features were included in the new mantrip: (a) Suspension Isolation- The suspension components were isolated by inserting elastomeric materials between them and the vehicle frame.

Jan 1, 1982

By C. E. Reistle

[In producing crude oils of paraffin base and of mixed base the producer is often confronted with the problem of preventing and removing paraffin that settles out of oil and accumulates in the well. This paraffin consists of heavy waxes with some sand and asphalt, and varies in. consistency from a soft semifluid wax to hard gummy wax. This problem is by no means a new one as troubles have been encountered with it since the earliest days of the industry. However, with the discovery of the panhandle, Texas, field and other large fields in which extensive troubles have been encountered, the problem has assumed added importance. In new fields the most serious trouble with paraffin is in the flowing wells the paraffin accumulates in the casing and tubing of such wells and unless removed will completely plug the well. This condition also develops in wells which are produced by gas lift, and often presents a serious problem when, this method of producing the oil is used. In older fields paraffin is also deposited on the face of the producing sand that on the walls of the hale or within the interstices of the sand near the hole, and this materially affects the amount of oil that can enter the well.]

Jan 1, 1927

Develop technology for preparing thick corrosion-resistant coatings and electroforms of iron-chromium-nickel alloys. Approach To reduce the United States' dependence upon foreign sources for supplies of strategic and critical metals such as chromium, cobalt, and nickel, new technology must be devised to conserve these valuable commodities. One approach being investigated by the Bureau of Mines is the use of a modified-aqueous-electrodeposition method to prepare thick (-25 µm), complex alloy coatings (e.g., stainless steel composition) with properties similar to the commercial alloys. An alloy coating on a low-alloy steel or carbon steel substrate would require significantly less strategic and critical metals than those contained in an equivalent mass of the commercial alloy. Coatings applied to appropriate mandrel materials make possible the preparation of intricately-shaped alloy electroforms (near-net-shape parts). As a result, the loss of valuable metals associated with machining finished products would be minimized.

Jan 1, 1986

Provide guidance on the selection of millisecond initiator delays between blastholes in surface mine blasting to provide a desired degree of rock fragmentation consistent with safety and vibration considerations. The Problem Blasting remains the primary means of fragmenting, rock for all kinds of mining, quarrying, construction, and excavation activities, and it is the only practical and economic method of breaking up and moving large amounts of material such as coal overburden and stone aggregate. Because of the large amount of blasting done, typically using 4 billion pounds of explosive to break about 8 billion tons of rock annually in the United States, a small improvement in blasting performance will have a significant productivity impact. Standard blasting practices involve the selection of time delays in a blast for at [cast three purposes: (1) to control energy flow to minimize adverse vibrations, (2) to provide sufficient time relief for good rock displacement, appropriate muck pile shape for digging, and the prevention of collar violence, misfires, and flyrock, and (3) to provide an appropriate amount of interhole stress wave and gas pressure action for a desired fragmentation size distribution. Timing guidelines that exist are based on subjective observations rather than measurements, even for the relatively new casting methods. Until this Bureau study, no definitive analysis had been done to quantify the fragmentation and productivity of full-scale blast rounds as functions of precision delay timing.

Jan 1, 1989

By Joseph A. Sutton

The prospect of utilizing bacteria in mining and metallurgical processes introduces a new and challenging area of investigation. Elements of bacteriology and metallurgy are discussed in connection with possible areas where biological science might be applied in extractive metallurgy. Bacteria may prove important in the selective separation of metals from ores and metallurgical solutions, the production of sulfur from gypsum or pyrites, and the production of sulfuric acid from elemental sulfur. A series of reports concerning the experimental applications of bacteria on minerals and metallic ores will follow this paper. For several years the Bureau of Mines has been investigating the action of bacteria in the oxidation of sulfide minerals and their potential uses in metallurgical processes. Primary attention has been given to the possible utilization of certain strains of autotrophic bacteria that live in industrial leaching solutions or fractures of mineral outcrops. The purpose of this paper is to acquaint the mining and metallurgical engineer with micro-organisms and some of their possible applications in the field of extractive metallurgy.

Jan 1, 1961

Improve the performance of waterjet nozzles used for water-jet-assisted cutting to optimize rock cutting efficiency. Approach The performance of a longwall shearer equipped for water-jet-assisted cutting was evaluated during an earlier study (Tech News No. 277). Waterjet nozzles were used to direct the solid streams of water that impacted the rock near the tip bits. The maximum water pressure that could be delivered to the nozzles was about 6,000 psi. Due to the "break up" of the solid stream of water, some of this pressure was lost before the water reached the rock. The pressure could have been increased by moving the nozzle closer to the bit tip but) moving the nozzle too close increases the possibility of damage to the nozzle. Study Results A test apparatus was built to measure water pressure at the location of water jet impact (see illustration). The target, a tungsten carbide plate with a 0.013 inch diameter orifice, was placed at the location of water jet impact. A pressure transducer, used to monitor impact water pressure, was positioned under the plate. Water pressure at the nozzle was maintained at 6,000 psi. The distance between the nozzle and target was varied from 2 to 5 inches.

Jan 1, 1988

Develop new technolgies and techniques which enable recovery of strategic and critical minerals such as cobalt from domestic resources, thereby easing the U.S. dependence upon foreign producers for these valuable commodities. Approach The Bureau of Mines, through research, developed a process which uses mineral beneficiation techniques to recover cobalt-rich products from Missouri lead ores. Before development of this process, cobalt was lost as an impurity in the copper, lead, and zinc concentrates and in the mill tailings because the technology to recover it with minimum impact on present production did not exist.

Jan 1, 1989