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By R. V. Lundquist, H. Leitch

The solubility characteristics of mono calcium aluminate (CaO A₁₂ 0 ) in water and in NaOH , Na₂ CO₂ , and NaOH - Na₂ CO₂ solutions were measured by determining the changes in Al2O3 concentrations in solution over a period of time at a specified temperature . The monocalcium aluminate was synthesized by sintering its starting components for 72 hours at 1,375 ° C. Distilled water and aqueous solutions of technical grades of NaOH and Na₂ CO₂ were used as solvents . The extraction of alumina from the monocalcium aluminate was dependent on the composition of the solvent and partially dependent on temperature for leaching . About 98 percent extraction of alumina from the aluminate occurred in Na₂ CO3 solutions containing 10 to 12 percent NaOH . Other solution compositions produce lesser extractions .

Jan 1, 1963

By M. E. Volin

The Ladd manganese deposits are in San Joaquin County, Calif., about 13 miles southwest of Tracy. The deposits are confined in two main areas of development, roughly about 1,700 feet apart horizontally, and known as the Ladd mine and Fabian mine, respectively. The deposits occur as interbedded lenses in the white cherts of the Franciscan formation. The ore minerals are bementite, rhodochrosite and psilomelane. As a part of the Bureau of Mines program of investigation and development of domestic mineral deposits, a development program was started. August 24, 1940, and completed on June 24, 1941. The Federal Geological Survey cooperated by mapping the geology and logging the drill cores. The program included road building, trenching, rehabilitating the mine workings, trenching underground excavation, sampling, and core drilling. The following pages mention the location, give a brief history, and note the physical features of +1-.1, district. Mine workings are sketched, the deposit is described and the plan of the project is noted. The work performed by the Bureau of Mines is explained in the concluding pages with a summary of the drill hole logs.

Jan 1, 1949

By Richard L. Rains

During this study in 1983, the U.S. Bureau of Mines examined one mine and five prospects in the Greenwater Valley Wilderness Study Area (WSA). No mineral resources were identified within the WSA. Principal mineral commodities in the WSA are gold and silver with minor lead, and zinc. Two properties have significance; sample analyses indicate the Salsberry Prospect may have gold-silver-lead-zinc resources, and the Graham Jem Mine may have gold resources. The likelihood for development is greatest at the Salsberry Prospect, although the only recorded production from the study area was from the Graham Jem Mine; in 1908 less than 1 ton of gold-bearing ore valued at $25,000 per ton was produced. Gold, silver, lead, zinc, and copper minerals in the WSA are associated with rhyolite dikes and quartz veins in Precambrian gneissic rocks, commonly concentrated in sheared zones along the dikes and veins. Although known to contain silver-lead deposits elsewhere, Precambrian Noonday Dolomite sampled inside the WSA contained no significant mineral values. Much of the WSA is covered by relatively unmineralized Tertiary and Quaternary volcanic rocks. The Bureau collected 140 rock samples at four adits, nine shafts, four trenches, and 33 prospect pits in the WSA. In 1983, 14 lone claims and one millsite within the study area were current. No patented claims, placer claims, or coal, mineral, oil and gas, or geothermal leases were in the WSA.

Jan 1, 1985

By N. S. Dalal, X. Shi

"SUMMARYElectron spin resonance (ESR) measurements provide direct evidence for the involvement of the glutathionyl radical, as well as an isolable Cr(V)-glutathione intermediate in the Cr(VI) glutathione redox reactions. These results indicate a new mechanism for the reduction of Cr(VI) by glutathione in relationship to cellular environment and suggest that synergistic reactions of Cr(V) and GS· might be responsible for the (unexpected) increase in the Cr(VI)-induced DNA-strand breaks at high glutathione levels.INTRODUCTIONWhile the reduction of Cr(VI) by glutathione (GSH) is thought to be a critical' step in the pathogenesis of the Cr(VI)-exposure related carcinogenesis1- 4, the exact reduction mechanism is not yet understood. The following reaction steps have been suggested :(A) Initial step:Cr04 2- + GSH - GSCrOa - (1)(B) At high GSH levels:GSCroa- + GSH - Cr( IV) + GSSG (2)(C) At low GSH levels: GSC rO a - - Cr ( V ) + GS ·(3)Thus far, however, in these reactions, the GS· radical has eluded spectroscopic detection, while the evidence for the Cr(V) formation has been reported positives as well as negative2·. Her~ we present spin-trap ESR evidence for the formation of the GS· radical, and a definitive ESR detection of an isolable cr(V)-GSH intermediate in Cr(VI)-GSH reactions.MATERIALS. AND METHODSESR spectra were obtained at X-band (-9.7 GHz) using a Bruker ER200D ESR spectrometer. The magnetic field was calibrated with a self-tracking NMR Gaussmeter (Bruker, Model ER035M) and the microwave frequency was measured with a Hewlett-Packard (Model 5340A) frequency counter. The spin probes, a-(4-pyridyl-1-oxide) -N -tert-butylnitrone (4-POBN) and 5,5-dimethyl~1-pyrroline-1-ox1de (DMPO) were purchased from Aldrich, K2Cr201 from Fisher and used without further purification. All experiments were done at room temperature."

Jan 1, 1989

"MASSACHUSE'M'S INSTITUTE OF TECHNOLOGYBOLSAITIS, PETERMassachusetts Institute of TechnologyDepartment of Mineral Engineering77 Massachusetts AvenueCambr1dge,MA 02130(614) 253-5069ELLIOIT, JOHN F.Massachusetts Institute of TechnologyDepartment of Mineral Engineering77 Massachusetts AvenueCambridge, MA 02130(617) 253-3305RING, TERRYDepartment of Materials Science and EngineeringMassachu5etts Institute of TechnologyCambridge, MA 02130(6117) 253-4299"

Jan 1, 1988

By H. Kenworthy

Laboratory experiments were conducted on several materials to determine their suitability for the production of mineral wool. By blending raw charges in the proper proportions and in some instances by adding lime, acceptable wools were made from samples originating in Alaska, Florida, Texas, and Virginia. It was shown that satisfactory wools can be produced from many kinds of raw materials if the ratios of acidic and basic constituents are properly maintained. INTRODUCTION The Federal Bureau of Mines has facilities at the Mississippi Valley Experiment Station, Rolla, Mo., for examining and testing mineral-wool raw materials. Samples are evaluated through small-scale wool-blowing experiments, aided by petrographic, chemical, and physical analyses of the raw materials and finished wools. When enough experimental data have been accumulated they are made public through Government reports and periodicals. This report of investigations follows that published in 19513/ and presents test data on samples received and examined since 1951.

Jan 1, 1956

By Sidney Katell

This study estimates capital investment, operating costs, and selling prices for four underground bituminous mines producing coal with annual production ranging from 1.06 to 4.99 million tons. It is assumed that the mines have a 20-year life. Wages and union welfare payments are considered as of November 12, 1973, under the Bituminous Wage Agreement of 1971, and costs for material and equipment are based on 1973 indexes. Initial capital investment ranges from $12,540,700 for the 1.06-million-ton-per-year (MM tpy) mine to $44,720,500 for the 4.99 MM tpy mine. Total capital investment ranges from $21,850,700 to $75,693,500 for the same mines. Corresponding selling prices for the coal range from $8.76 to $7.53 per ton, assuming a 12-percent discounted cash flow rate of return after Federal income taxes.

Jan 1, 1974

By John H. Soulé

"INTRODUCTION The Mining Branch of the Bureau of Mines has used the wagon drill to sample mineral deposits in New Mexico. This method of sampling was successful and con¬stituted an important phase of the work on five exploratory projects undertaken in 1943, 1944, and 1945. The deposits varied in topographic features, geology, mineral content, and in the physical characteristics of the rocks drilled. The altitudes ranged from 630 to 7,800 feet. Three hundred and seventeen holes totaling 6,852 feet were drilled. The deepest hole was 66 feet; the average depth was a little less than 22 feet.The results of the above-mentioned work form the basis of this report. Special attention is given to the later and more improved techniques used. This report was written with the expectation that the procedures might prove advantageous to others in the exploration and sampling of near-surface mineral de¬posits, and that a more extended use of the technique might result.AcknowledgmentsAcknowledgment is due Charles H. Johnson, chief of the Rolla Division, Mining Branch, for helpful suggestions in starting this work, and to J. H. Hedges, chief of the Tucson Division, Mining Branch, W. R. Storms, engineer-in-charge of the Silver City, N. Mex., Field Office, and Donald H. Mullen, mining engineer attached to that office, for assistance in preparing and editing this report."

May 1, 1947

By Dougherty. E. Y., S. W. Zoldok, John W. Cole

"INTRODUCTION During its wartime program of exploration for minerals essential to the national economy, the Bureau of Mines was instructed to investigate sources of raw materials used in the manufacture of iron and steel. As a part of this investigation, some work was done on the iron deposits on the Neutral and Aztec claims on Buckhorn Mountain Canogan County, Washington, which was designed chiefly to indicate the nature and behavior of the ore deposits below the surface exposures. Diamond drilling was started in June and completed in July 1945. Preliminary laboratory tests on iron, ore from Buckhorn Mountain were completed during the fall and winter of 1945. This report presents the data obtained from the investigation.ACKNOWLEDGMENTSIn its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final re¬port. The Metallurgical Branch, R. G. Knickerbocker, chief, analyzes samples and performs beneficiation tests."

Apr 1, 1947

By C. P. Bowie

[Frequent accidents in the transportation and. handling off petroleum and its more volatile products, serve as a reminder that this is indeed a hazardous undertaking and should always be conducted with due caution. On October 4, 1920, vapors in the held of the British tanks steamer G. R, Crowe became ignited and, caused an explosion which, it is reported, killed 5 men, injured. 40 others and endangered the lives of some 300 more. On November 10, 1920 the Morgan, Line freighter El Mundo was almost totally sot destroyed in New York harbor by fire caused by an explosion of gases in a fuel-oil tank. These two disastrous explosions emu emphasize the ever- present danger attending the use of petroleum products. This is also shown by the frequent occurrence of minor fires and explosions, caused by careless handling of baseline, which result in loss of life or serious injury to railroad employees, to oil-tank drivers, and to individuals in various walls of life. Statistics indicate that the lighter cuts of petroleum products, because of fire hazards, are dangerous, and are so considered by the railroad and other transportation companies. According o the Bureau of Explosives (Bar-eau of Explosives Report No. 13 p. 7) during 1919 transportation of gasoline in the United States resulted in 172 accidents, causing 2 deaths and 31 injuries, and a property loss to the extent of $687,966. Among the causes of ignition, an open light in the vicinity of the container stands out most prominently.]

Jan 1, 1920

By James W. Miller

An investigation was begun by the Bureau of Mines in 1948 to determine the preparation characteristics of American coals. Results of the investigation were planned to be reported on a county basis and from the data developed, to determine: (a) Which coals either as mined or after beneficiation by conventional preparation are chemically suitable under present standards for producing metallurgical coke; (b) Which coals require special and more intensive treatment in preparation than is now practiced; and (c) Which coals cannot be considered potential sources of metallurgical coke, regardless of preparation. This report is one in this county series that describes the preparation characteristics of the coals of Perry County, Ky.

Jan 1, 1956

By E. W. Newman

The Bureau of Mines, in cooperation with the U. S. Geological Survey, developed the property of the Tungsten Metals Corp. by surface trenching and diamond drilling from November 1940 to June 1941 and from August 1943 to December 1943. The purpose of the work was to determine possible reserves of tungsten in the downward extension and lateral eastern extension of three major tungsten-bearing quartz veins. The property is 50 miles south of Ely, White Pine County, Nev., in the Minerva Mining District. Tungsten ore was discovered in the district in 1915, and mining started in 1916. The tungsten ore bodies occur as shoots in quartz veins that occur along faults in limestone. With the exception of a small-scale leasing operation in 1932, the property was idle from 1919 until 1936, when Tungsten Metals Corp. was organized to acquire the mines. Production ceased in May 1945, and the mines were idle until leased in 1947. Development by the Bureau of Mines during 1940 and 1941 consisted of surface trenching, sampling, and diamond drilling 37 holes for a total of 6,959 feet. Subsequent drilling of eight holes, totaling 3,067 feet, in 1943 disclosed additional reserves. This report sets forth in considerable detail the exploration work completed by the Bureau and briefly describes the mining and milling methods employed. Diamond-drill halo logs and sample analyses are shown graphically in the illustrations that accompany the report.

Jan 1, 1950

By Elaine T. Cullen, Albert H. Fein

Federal law mandates that all miners receive safety and health training when first entering the mining industry and at least 8 hours annually thereafter. Although the mining industry has historically relied on an experiential master-apprentice model for training new employees, the formal safety training provided to miners is generally done in a classroom, with mixed results. In a series of stakeholder meetings held by NIOSH across the West in 1997-2000, trainers identified significant gaps in materials that were available to teach new and experienced miners. They asked whether NIOSH could develop effective materials to fill these perceived gaps, as well as make training more effective for those who were required to attend, but who often refused to be attentive. Adult learning theories, social learning theories, mentoring, and storytelling were all employed in the development of a series of safety training videos that have become very popular in the mining industry. This Report of Investigations describes the theoretical frameworks that were used, the process that was developed to produce the videos, and the results of the evaluations as to whether or not they were effective in training new and experienced miners.

Jan 8, 2005

By D. B. Dow

The presence of sulphur compounds in petroleum and its products is, generally speaking, undesirable, and the problems involved in removing such compounds are of great importance to the petroleum refiner and to the manufacturer of gasoline. There are several types of these compounds which are dissimilar in physical and chemical characteristics, as evidenced by different objectionable features which they exhibit, and special treatments have been developed to meet conditions existing in various products. This paper deals with the treatment of natural-gas gasoline for the removal of certain sulphur compounds which, if not removed, impart on objectionable odor and in addition badly discolor the product. The presence of this particular type of sulphur compounds is detected by the "doctor" test.* In some instances natural-gas gasoline is purchased on "doctor" test specifications, and the ordinary purchaser, while not buying on "doctor" specifications, is insistent in his demand for a water white product. Gasoline which fails to meet the "doctor" test, if not received by the buyer within a few weeks after time Of manufacture, may be "off color" enough to warrant a deduction from the market price.

Jan 1, 1923

By A. L. Engel

This report describes results of laboratory-scale experimental treatment of nine ores containing gold and silver, including samples of products of previous plant treatment, from ore deposits in California and Nevada. The samples treated were taken by engineers of the Bureau of Mines during investigations of these ore deposits. The information reported is of interest for development of the mining districts represented or in future Investigations of similar ores from other sources. The treatment methods were as simple as possible. More complicated treatments were tried when required, The applicability of the methods and their limitations in treating the ores are shown by the data in this report. The following treatment methods were employed in the experiments described: Screen analyses were made to determine distribution of values in various screened-sized portions of crushed ore, or to determine optimum size to which a particular ore should be crushed or ground to liberate values, and some-times to determine residual values in various-sized portions of treated material.

Jan 1, 1961

By J. S. Browning

The purpose of this Bureau of Mines project was to develop a method for recovering kyanite and sillimanite from the present zircon-mill tailing of the Jacksonville and Starke, Fla., plants of Humphreys Gold Corp. The kyanite and sillimanite in the ore are not being exploited at present, but procedures for recovering the two minerals were worked out by the Bureau in the interest of conserving natural resources. The current zircon-mill tailing of the Starke plant contains up to 20 percent of a mixture of kyanite and sillimanite. A similar product of the Jacksonville plant contains up to 15 percent kyanite and sillimanite. The average annual production of the tailing now being stockpiled contains several thousand tons of the two minerals. Laboratory batch-flotation tests were made on the materials to determine the feasibility of flotation methods for recovering high-grade concentrates. Various reagents were employed under different conditions to determine the optimum conditions for flotation of kyanite and sillimanite and retardation of the gangue materials. The results of the preliminary flotation tests were encouraging enough to warrant more comprehensive testing of a larger sample of the ore in the laboratory pilot plant.

Jan 1, 1956

By A. W. Deurbrouck

This Bureau of Mines report describes the preparation characteristics of the significant coalbeds from which samples could be obtained in Upshur County, W. Va. One of the 14 samples collected was of metallurgical quality as received, 6 could be sufficiently upgraded to provide acceptable products, and 7 could not be upgraded to metallurgical quality because of their high sulfur contents.

Jan 1, 1967

By J. S. Hansen

In support of its objective to conserve mineral resources by minimizing premature failure of materials, the Bureau of Mines conducted a cooperative study with the U.S. Department of Energy on the erosion and abrasion resistance of hard materials for valves in coal conversion systems. This report describes a newly developed erosion-testing apparatus and presents data on the erosion resistance of over 200 materials. Erosion resistance of most metals was comparatively low. In contrast, ceramics and cermets such as B4C, WC, SiC, Si3N4, and TiB2, when fabricated to minimize porosity, displayed greater than five times the erosion resistance of metals. Coatings such as boron diffused into Mo and WC, chemical-vapor-deposited TiCN, and electrodeposited TiB2 were highly erosion resistant if applied in thicknesses ranging from 60 to 75 µm. Erosion resistance of cemented carbides was inversely related to metal binder content.

Jan 1, 1979

By Eugene T. Sheridan

The 23d annual survey of the peat industry by the Bureau of Mines, United States Department of the Interior, revealed that 75 producers in 17 States re-ported commercial production of peat in 1956. Forty-seven producers reported humus production, 19 reported reed-sedge peat, 17 reported moss peat, and 1 reported muck. This total exceeds the number of active operations, but several producers reported recovering more than one type of peat. Fifty-five percent of the total production was reported as peat humus, 30 percent as reed-sedge peat, and 15 percent as moss peat. A negligible amount was reported as other types. More than one-fourth of the total output was raw peat with no preparation, other than having been air-dried. The remainder consisted of processed peat prepared for use by cultivation, shredding, or kiln drying.

Jan 1, 1958

In the U.S. coal mining industry, a large cohort of miners is at or nearing retirement age. As these miners retire, there will be a need to hire and train thousands of new and most likely younger workers. Moreover, a large portion of safety trainers will also require replacement due to retirement. In a speech before the U.S. House of Representatives (2004), Bruce Watzman, Vice President for Safety, Health and Human Resources for the National Mining Association said, “[W]e will need to replace a major portion, approximately 50%, of the underground coal mining workforce within the next 5–7 years.” The large influx of new mine workers, along with the deficit in safety trainers, creates the challenge to provide consistent and effective safety training. Given the expected high turnover of the mining workforce, it is very likely that incoming workers will have much less experience than those leaving the workforce. Unfortunately, inexperienced miners have been shown to incur the highest rate of injuries. The piece of machinery most associated with these injuries is the roof bolting machine, which accounts for 56% of machinery-related injuries in underground coal mining. The National Institute for Occupational Safety and Health (NIOSH) has released a new report entitled “Roof Bolting Machine Operators Skills Training for a Walk-Thru Roof Bolter: Trainer’s Guide” (IC 9489). It is designed to help safety trainers develop struc-tured training for new operators of walk-thru bolting machines. This resource will help trainees learn, understand, and apply knowledge and skills. Included in the trainer’s guide are the following tools: [ ] a six-part DVD video series, a skills check survey, talking points, and a complete job training analysis. Also included is an exercise to help trainees learn more about their mine’s roof control plan, as well as a list of supplemental training and reading materials. On-site trainers can modify this guide to fit their particular mine conditions, machines and equipment, and work procedures. The goal of every coal mine safety professional is to increase safety awareness and make mines a safer place to work. The Walk-Thru Bolting Machine Trainer’s Guide will help teach new miners skills to create a safer working environment that will ultimately prevent or reduce on-the-job injuries. Safety trainers can also use the ideas and concepts from this guide to develop their own training skills for the safe operation of other pieces of underground coal mining equipment.

Jan 6, 2007