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By H. R. Beard

The citrate process for sulfur dioxide emission control was developed in pursuit of the Bureau of Mines goal of minimizing the adverse environmental impact of mineral-processing operations. This publication describes the gas analysis procedures used during development of the process. The research required the capability to analyze SO2, H2S, CO, CO2, COS, volatile hydrocarbons, NO, NO2, O2, N2, and H2. The methods described include gas chromatography, electrochemical detection, infrared spectroscopy, and the use of a computer program to predict the product composition in complex reactions. Laboratory and pilot plant applications are discussed.

Jan 1, 1979

By A. P. Grossman

'This report was prepared by Shell Oil Company, Mining Ventures Department in accordance with Cooperative Agreement No. 14-09-0070-b53 dated September 10, 1976, between the United States of America, Department of the Interior, Bureau of Mines and C(b) Shale Oil I Project, Ashland Oil Inc., Shell Oil Company, Operator. After completion of this report the Shell Oil Company withdrew from participation In the C(b) Shale Oil Project and advised the Bureau of Minus that plans for publication of this report had also been withdrawn. The Bureau of Mines acting under terms of the Cooperative Agreement hereby releases this report for general information.

Jan 1, 1976

By G. E. McElroy

This paper3/ is one of a limited series being prepared by the Bureau of Mines to supplement a more extensive series on mining and preparation methods in the various mining districts of the United States. It describes ventilation methods and practices at the anthracite collieries in the Northern field of the anthracite measures of Pennsylvania as obtained by personal inspections in twenty of the larger collieries during 1933 and 1934 and from supplementary information furnished then and later by operating officials. This field is one of the four major divisions - Northern, Eastern Middle, Western Middle, and Southern - into which the anthracite deposits of Pennsylvania are naturally divided, and constitutes, in plan, a slightly bowed lens, about 60 miles long, and that extends from Forest City on the north through Scranton, Pittston, Wilkes-Barre, and Nanticoke to Shickshinny on the south with a. maximum width of 6 miles. It is the oldest and largest producing field of the four, and has produced continuously from 1S09. The total anthracite production for the State reached a peak of about 100,000,000 tons a year in 1917, but in recent years production has averaged about 50,000,000 tons, of which somewhat over half comes from this Northern field. The operations of three of the largest producing organizations in the State are almost wholly included in this field, as well as about half of the operations of two others of the six largest producers, It comprises the first 14 of the 25 numerically designated anthracite State inspection districts.

Jan 1, 1937

By R. V. Ramani, R. Bhaskar

"An airborne dust cloud is an ensemble of particles of varied size, density, shape and states of aggregation. An understanding and quantifying of the dispersion and deposition of the du.st generated in mines is essential to the development of measures for reducing worker exposure to dust.In coal mining, the major portion of the dust is generated during the cutting of coal using a shearer or a continuous miner. The major phenomenon affecting ambient concentration is the deposition of dust. Panicle deposition may take place due to the effect of gravitational, inertial, electrostatic, and thermal forces, and mechanisms such as Brownian and eddy diffusion and inenial impaction. The three major mechanisms of deposition in turbulent flow in mines are diffusion (Brownian and eddy), sedimentation and inertial impaction. The mechanisms determining panicle deposition are size dependent.From a review of the literature, there appears to be a knowledge gap in the understanding of the deposition phenomena in mine airways. In order to obtain a better understanding of the deposition of dust for various particle sizes, and to develop a set of data for evaluating predictive mathematical models/or dust flow in mines, a series of dust-flow experiments was performed under controlled conditions in mine airways. It appears that the deposition data generally follow the theoretical behavior of dust based on the combined effect of diffusional and gravitational deposition. Jn this paper, the findings of the study on the deposition of dust in mine airways and its dependence on size, velocity and concentration are discussed. A set of deposition equations that could be used to determine the approximate deposition at various points in a mine airway are presented.IntroductionThe major factor affecting ambient dust concentration in mine airways is the deposition of dust. Particle deposition may take place due to the effect of gravitational, inenial, electrostatic, and thermal forces, and mechanisms such as Brownian diffusion, eddy diffusion and inertial impaction. The major mechanisms of deposition in turbulent flow in mines are diffusion (Brownian and eddy), sedimentation and inertial impaction. Inertial impaction is significant only during changes in direction, but the change in direction of flow with resultant powerful eddies may cause increased re-entrainment of the particles, thus having a compensating effect. While the literature in aerosol sciences contain several references on deposition, most studies were done in small diameter tubes for diffusional deposition (Liu and Agarwal, 1974). The deposition data from small diameter, short tube experiments may not be applicable to studying deposition in mine airways that have large areas and extend several hundred meters. Further, the change in concentration along the length of a mine airway may significantly affect the deposition an aspect that may not be easily determined in short tubes in laboratory experiments."

Mar 1, 1992

By Fred Kissell

The Bureau of Mines has developed the shearer-clearer--a new type of dust control system for longwall shearers. The system partitions the airflow around the shearer into a clean split and a contaminated split. The dust cloud is confined to the vicinity of the coal face, while the shearer operators remain in the clean split on the gob side of the machine. The shearer-clearer operates on the principle that each water spray moves air like a small fan and can be positioned to direct the dusty air towards the face. The hardware is inexpensive and can be installed in a single shift. It consists of several strategically mounted water sprays and one or more passive barriers. Laboratory testing indicates reductions 1n shearer operator dust exposure as high as 97 pct. Preliminary results from an underground demonstration in one mine also indicate that considerable dust reductions at the shearer may be obtained. In conjunction with the development of the shearer-clearer, dust surveys were conducted in three other mines to determine if some shearer spray systems currently in use partition the flow in a manner similar to the shearer-clearer, and if so, whether this partially accounts for markedly cleaner conditions on some longwalls. Results from these surveys indicate this to be the case. A feature of the cleaner longwalls was a downwind orientation of their water sprays, which is a key element of the shearer-clearer system. The shearer-clearer system described in this report was designed for an Eickhoff EDW 300 shearer working a 7-foot coal seam. The testing to date has concentrated on cutting directions counter to the primary airflow. The development effort continues for different mining equipment and conditions. It is expected that different systems will be required to accommodate the range of conditions occurring underground. Application of the system presented here to conditions different than those described is not likely to produce the same results.

Jan 1, 1981

By Mackenzie Burnett

A high efficiency ejector has been developed which solves the abrasion problem associated with remote pneumatic stowing. The system can also produce cemented fills. The ejector is capable of moving the fill material over 70 ft from the injection point and filling the mine opening to the roof level for a distance of about 30 ft in all directions from the borehole. This system operates by the transfer of momentum from a supersonic air stream to the fill material. The momentum transfer results in a horizontal stream of fill material and air at a velocity of about 100 fps. The ejector fits on the bottom end of a 3 in diameter vertical pipe. Fill material is fed into the ejector at a controlled rate through a hopper mounted over the borehole. High pressure air used to operate the ejector is fed through a second 3 in diameter pipe. This system has the additional feature of mixing water in the air stream which increases the potential momentum of the air stream. Where necessary, cement can be added to the gravel to create a cemented fill. The design parameters and test results for four versions of the ejector are presented in this report.

Jan 1, 1991

By M. L. Whisman

The Bureau of Mines developed a radiotracer method for detecting the contribution of selected components and additives to thermally induce deposits of turbine aircraft fuels. Fuels were examined before and after 52 weeks of storage at 130° F. Of particular concern was the influence of aromatic hydrocarbon fuel constituents on thermal-stability quality of jet fuels during storage. A microfuel coker test apparatus was used to thermally stress the test fuels and blends, and the resultant contribution to deposits of selected fuel components, labeled with carbon-14, was determined by radioactive-counting techniques. Ninety-one blends of five test fuels with carbon-14-labeled fuel additives or components were prepared, tested, stored for 52 weeks at 130° F, and reanalyzed for deposit-forming tendency. These additives included two anti-oxidants, a metal deactivator, and a corrosion inhibitor. Of the labeled hydrocarbon fuel systems studied, the greatest reaction was observed in blends containing methyl-and ethyl-substituted indenes. Other aromatic types also showed some contribution to the deposits. Three of the additives showed a marked tendency to degrade and react during storage and thermal stress. A cresol antioxidant, however, barely contributed to deposit formation. Oleic acid interacted with cadmium present in aircraft fuel systems and produced deleterious effects upon the thermal-stability quality of the fuel.

Jan 1, 1971

By James P. McGee

Preliminary calculations show an economic advantage in using nuclear energy to supply the endothermic heat required for gasifying coal. It should be noted that the various assumptions used in preparing these calculations must undergo further evaluation through additional engineering design and research. The proposed system for gasification is the indirect process cycle with helium heated in a nuclear reactor and passed through an exchanger-type gasifier for the reaction of coal and steam to form CO (carbon monoxide) and H2 (hydrogen gas).

Jan 1, 1960

By W. O. Vanderburg

This paper describing the methods of concentrating tungsten pros at the mills of the Atolia Mining Co. is one of a series of similar papers being prepared by the United States Bureau of Mines. The writer acknowledges the assistance and cooperation of A. V. Udell, president, Louis Warnken, bookkeeper, and C. K. Dennis, superintendent, of the Atolia Mining Co. in the preparation of this paper.

Jan 1, 1931

By G. A. Howes

This is one of a series of circulars dealing with the cost of equipping and developing mining properties in the United States and Canada, prepared and published by the Bureau of Mines in cooperation with various mining and exploration companies. This group of circulars is designed to supplement an earlier series which covered the methods and costs of mining and milling at a large number of producing properties. ACKNOWLEDGMENTS The authors desire to thank Robert A. Bryce, president of Macassa Mines (Ltd.), for permission to use the data presented in this paper, and to acknowledge the cooperation of A. J. Keast, under whose direction as manager the plant was installed and equipped and the shaft was sunk to a depth of approximately 2,000 feet.

Jan 1, 1932

By Raymond W. Hiteshue, Henry H. Ginsberg, Paul S. Lewis

Coal was gasified in the presence of up to 3.57 million roentgens of gamma rays by the Bureau of Mines to determine whether the irradiation increased the gasification rate or yields of methane and hydrogen . High volatile A bituminous coal was gasified with steam at 500 and 1,500 psig and temperatures of 1,400 ° and 1,800 ° F ; five other coals ranging in rank from lignite to anthracite were gasified at 500 psig and 1,800 ° F. The average results of replicate experiments with and without radiation were compared for possible effects of radiation from 40,000 curies of radioactive cobalt . The irradiation had no gross effect on the gasification rate or on the yield and distribution of methane and hydrogen . It was concluded that gammaray irradiation produced no improvement in the technology or economics of coal gasification .

Jan 1, 1964

By L. C. IlsLey

The cool drills that have received the approved of the Bureau of Mines may be divided into three general classes: (1) Hand drills, small drills that are held in the hands or supported against the body while in use; (2) post drills, drills that are too heavy or powerful for hand operation and therefore require some mechanical mounting when in use; and (3) drilling machines. Besides these three classes, drilling equipment has been incorporated in the design n of a number of permissible coal-cutting machines, but such drills are considered an integral part of the cutting machine and are not given separate approval. The hand drills have been described in Report of Investigations 3363, which is cite of several papers that have been published dealing with miscellaneous types of permissible motor-driven mind equipment not covered in bulletins. The present paper describes post drills and drilling machines approved by the Bureau of Mines up to July 1, 1937.

Jan 1, 1938

By L. C. IlsLey

[The cool drills that have received the approval of the Bureau of Mines may be divided into three general classes: (1) Hand drills, small drills that are held in the hands or supported against the body while in use; (2) post drills, drills that are too heavy or powerful for hand operation and therefore require some mechanical mounting when in use; and. (3) drilling machines. Besides these three classes, drilling equipment has been incorporated in the design n of a number of permissible coal-cutting machines, but such drills are considered an integral part of the cutting machine and are not given separate approval. The hand drills have been described in Report of Investigations 3303, which is cite of several papers that have been published dealing with miscellaneous types of permissible motor-driven mind equipment not covered in bulletins. The present paper describes post drills and drilling machines approved by the Bureau of Mines up to July 1, 1937.]

Jan 1, 1938

By A. W. Deurbrouck

This Bureau of Mines report describes the washability characteristics of 14 coalbed samples collected in Wyoming. Such data is needed to evaluate the quality of the coals of the West where most of our low-sulfur-content coal reserves are found. Of the 14 samples included in this report 13 had a total sulfur content of 1.1 percent or less. All of the samples contained low per¬centages of ash or could be readily washed to a desirable ash level with minimal loss of yield. The coals ranged in rank from high-volatile B bituminous to subbituminous C, although 10 of the samples were high-volatile C bituminous. The coalbeds varied in thickness from 4.5 to an unknown thickness greater than 67.5 feet.

Jan 1, 1971

By Fred R. Biggs

This report was prepared by the U.S. Bureau of Mines to present a brief history of the listing of Iron Mountain Mine as a Superfund site on the National Priorities List (NPL) and subsequent remedial actions. The mine area is located on 4,400 acres near Redding, CA, and includes underground workings, an open-pit area, waste rock dumps, and tailings piles. This property involves multiple sources of acid mine drainage (AMD) that are high in copper, zinc, and cadmium. The selected remedial actions, based on the Record of Decision of 1986, would partially cap the Richmond mineralized zone to reduce infiltration of clean water, divert clean surface waters away from contaminated areas, fill surface subsidence areas, and enlarge the Spring Creek debris dam to provide increased surge capacity. Site remediation efforts at Iron Mountain are well into the remedial design-remedial action phase. Costs to date for remedial action are $7.5 million. Details of activities and designs of remedial elements are presented and future activities discussed.

Jan 1, 1991

By L. G. Austin

"This paper is based on the development of the Maza-Austin technique for characterizing thousands of coal particles by approximate analysis of the major inorganic constituents Ca, Al, Si, K, Na, Fe and S in each particle. The technique has sufficient sensitivity to work on small volumes, is fast enough to handle large number of particles within a reasonable period of time, and consists of scanning electron microscopy combined with energy dispersive x-ray spectrometry (SEK-EDS). A computerized SEK-EDS system that allows the automated analysis of hundreds of coal particles per hour' is described. The analysis is based on the location and tracing of coal particles embedded in a polished specimen, the selection of sampling points on the traced particles, the collection of an x-ray spectrum from each sampled point for a defined period of time, and the processing of the x-ray intensity to calculate point composition using ZAF corrections. Procedures for correcting for dead time, background, detector efficiency and spectrum overlap are described. These corrections are essential if reasonably accurate analyses are to be obtained from unknown complex mixtures of the elements in a coal or fly ash particle. Examples are given. INTRODUCTION Coal is a complex mixture of organic and inorganic materials. The inorganic fraction is referred to as mineral matter (Gluskoter, 1978) but can occur in three modes: (i) an observable mineral species; (ii) as cations held by ion exchange to carboxylic groups; and (iii) in chelate complexes. The mineral matter content normally represents a significant proportion of a coal, with an average value of about 15% for US coals (Gluskoter, 1975). The standard methods of analysis of the mineral matter in coals are performed on a sample selected to represent the whole coal as closely as possible, and give the overall inorganic composition in the coal. Such analyses are of limited use for solving problems originating from the behavior of individual coal particles, whose compositions vary widely from the average value. This is particularly true in pulverized coal combustion, where the current methods of predicting the slagging and ·fouling potential of a coal are based on the bulk ash composition, but the fly ash particles which create the deposits originate from coal particles with large differences in mineral compo1ition. Some examples can be found where, in a comparison between two coals, the one with the smaller slagging potential according to the mean ash composition was the one that behaved worst in the furnace (Moza et al., 1980; Koza and Austin, 1983). The u1e of gravity fractionation to assess the slagging potential of pulverized coals has shown that conventional ASTM analysis is not sensitive to differences in the distribution of mineral matter when comparing coals (Borio and Narciso, 1979). Bryer (1979) concluded that coals should be examined for fouling and slagging potential by analyzing gravimetric and size-fractionated coal, preferably pulverized· and ground to the size expected at the mill outlet."

Jan 1, 1989

By D. Harrington

The placing of much, sometimes practically all, of the burden of the expense of mine accidents on the shoulders of the mine operator by compensation laws, and the fact that the problem of protecting the life end limb of workers is now by public opinion largely if not wholly passed to each industry to solve (and present-day thought strongly supports the justice of both of these propositions), are forcing industrial organizations into accident-prevention. Work. This policy is being adopted not alone to protect the companies; in addition, executives alert to their opportunities and obligations are taking part in this work personally to protect themselves. The functions of industrial executives in accident-prevention work are becoming numerous and complex. Executives who are logical in their reasoning, quickly see that before a company can constantly ask or expect the workers to heed safety suggestions, the company and its officials must "put their house in order" by laying down a concrete, definite safety program. For mines this includes primarily adoption of a to a logical mining method, the installation of safe miming equipment and practice the netting forth in definite form (preferably do a printed pamphlet) of the company's minimum safety requirements, and the organization of its operating officials into an accident-prevention body. After the company has its own affairs so arranged that it can go to its workers with "clear, hands" in promoting a safety program, the real work begins; and this is especially applicable in mining.

Jan 1, 1939

By H. C. Miller

The removal of the mud sheaths that are deposited against the faces of productive oil sands during rotary drilling is one of the important problems confronting operators, especially in semidepleted fields where formation pressures are low. Unless the mud sheaths behind the perforated oil strings and liners are removed and the sands exposed, oil cannot enter the wells. Consequently much oil that otherwise might be produced from low-pressure sands is trapped and never recovered. Various types of perforation washers, down swabs, and agitators are used at present for breaking down the mud sheaths and removing the disintegrated clay particles from wells after the perforated Wipes have been inserted. Mechanical methods for removing mud sheaths are :quite satisfactory, but prompted by the request of certain .operators in the California oil fields Bureau of Mines engineers have conducted a series of laboratory tests with the view of developing a chemical method for removing mud sheaths in oil wells that will be applicable to field conditions. This report describes the laboratory work and deals generally with a chemical method for removing the mud sheath, cake, or plaster deposited against the face of oil sands in drilling wells end in wells that, on being shut in temporarily during periods of overproduction of oil, are conditioned for the shutdown .period by filling the well opposite the producing formations with mud fluid. The method described in this report was devised in the San Francisco laboratory of the Bureau of Mines and, as far as the writers have been able to determine, differs from any chemical method ever used in actual wells. The method proposes to add a small amount of calcium carbonate (preferably pulverized limestone) to the mud fluids before they are introduced into the wells so that the resultant mud sheaths will be susceptible to disintegration by acid solutions when it is desired to expose the faces of the oil sands in the wells.

Jan 1, 1934

By H. C. Miller

The removal of the mud sheaths that are deposited against the faces of productive oil sands during rotary drilling is one of the important problems confronting operators, especially in semidepleted fields where formation pressures are low. Unless the mud sheaths behind the perforated oil strings and, liners are removed and the sands exposed, oil cannot enter the wells. Consequently much oil that otherwise eight be produced from low-pressure sands is trapped and never recovered. Various types of perforation washers, down swabs, and agitators are used at present for breaking down the mud sheaths and. removing the disintegrated clay particles from wells after the perforated pipes have been inserted. Mechanical methods for removing mud sheaths are quite satisfactory, but prompted by tie request of certain operators in the California oil fields Bureau of Mines engineers have conducted a series of laboratory tests with the view of developing a chemical method for removing mud sheaths in oil wells that will be applicable to field conditions.

Jan 1, 1934

By Richard F. Hewlett

Use of digital computers makes possible a more efficient and complete analysis of data from a mineral deposit . This computer program was written and used during an investigation into the efficiency of methods of computing grade and tonnage of ore , wherein it was necessary to make repeated computations involving different combinations of data . This investigation was part of a continuing program of sampling methods research at the Bureau's Denver Mining Research Center.2-4 This program is designed to compute tonnage and average grade for 40 cutoff grades using either the statistical or polygonal methods . tational rate is from 200 ( input bound ) to 1,400 assays per minute , depending on the use of either individual ( one assay per card ) assay- interval length or

Jan 1, 1963