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By Gustavo Borges Tiboni

The erosive wear caused by the impact of solid particles against a surface is a tribological phenomenon present in many segments of the industry, such as transportation, aerospace, mining, power generation, among others. The most usual method to set the wear rate is by measuring the mass loss of the material. In order to apply one technique with potential to determine the rate of erosion wear, this study developed a dedicated equipment and conducted preliminary erosion tests monitored by non-destructive testing known as acoustic emission technique (AE). This can be defined as a technique able to detect mechanical waves generated by the release of elastic energy accumulated in the material. Erosion tests were performed in order to evaluate the ability of equipment to collect data from AE and to correlate these data with the wear of the samples. Samples of low carbon steel eroded by the impact of angular aluminum oxide particles suspended in air at three different velocities: 45, 57 and 67 m/s. The impact angle between the particles and the sample was set at 30 degrees and the test temperature at approximately 20°C. The wear rate has changed with the velocity in accordance with the kinetic energy of the particles and the AE parameter RMS showed sensitivity to the variation of particle impact velocity and to the wear of the sample eroded. The rate of AE signals collected over time correlated with the flow of particles striking the sample, and with the parameters of energy, rise time and duration of the signal.

Jul 31, 2018

By Edo Engel

Whereas only a handful of decades ago, typical blast furnace working volumes were below 1000 m³, such furnaces are currently designated compact or even mini blast furnaces. For certain business cases, however, small furnace sizes remain an attractive option. Decades ago, this size blast furnace would have produced a maximum of 0.3 Mtpa with its 600 m³ working volume over a campaign of up to four years. The current state of technology and operational know–how will allow a similarly sized furnace to produce over 0.7 Mtpa while achieving the multiple decade campaigns that have become familiar to steel producers in full sized operations. This level of productivity, but especially the reliability and supply security associated with mature technology, allows for integration into minimills or taking a first step towards a full scale BF–BOF integrated mill. Steel producers considering such scenarios, which are typically attractive for emerging economies, are confronted with fundamental decisions, one of which is for the technological basis for the compact or mini blast furnace to be included in the plant. This article addresses some of these decisions from an operations–based perspective. A small number of case studies is included.

Aug 16, 2017

By Cristina Escudero Martinez

The purpose of the Basic Oxygen Steelmaking (BOS) is to refine the hot metal produced in the blast furnace into raw liquid steel, which may be subsequently refined in the secondary steelmaking shop. Appropriated fluxes for the BOF could require low melting point to reduce the energy consumption, to reduce the energy to fluidity the slag at lower temperature and to melt at lower temperature than steel. It is necessary a good Tumble test result and the fluxes do not generate fines which could obstruct the blowing plugs, so we would have a homogeneous flux. A homogeneous chemistry that allows to control the basicity (Si and MgO levels) and a high absorption characteristics to combine the flux with P, S, Si, etc. are necessary. PASEK Dunite is an ultramaphic rock exploited in the north of Spain with a basic chemical classification being olivine and serpentine its principal minerals. It is formed by orthopyroxene, clinopyroxene and olivine in variable proportion. Dunite is a very homogeneous and hard stone. The main characteristics are: High hot and cold resistance to mechanical stress (shatter / crushing / abrasion), softening and melting points of a flux, not a refractory material, large porosity which is increased more than 20% when dunite is heated at BOF process temperature, and high absorption level, and stable components with low melting points. PASEK Dunite is a good flux in BOF process and its use is recommended if the BOF process produces pig iron with low Si content, generates high levels of slag and it is necessary maintaining the basicity index and the MgO amount and with high value of hot metal ratio (high amount of phosphorus to remove).

Aug 16, 2017

By George Schipper, Peter Gelten, Pepijn Adriaen, Hugo Uijtdebroeks

Tata Steel IJmuiden Hot Strip Mill 2 (HSM2, 5.5 Mtonnes/yr) is currently being upgraded, resulting in an increased rolling force and motor power capacity. With the current conventional work roll spray cooling, a deterioration in work roll & strip surface quality performance is expected as a result of the increased mill capacities. In order to improve strip surface quality, HSM2 decided to do a full-scale production trial with High Turbulence Roll Cooling (HTRC) at stand FM2. HTRC is a novel way of roll cooling using a high turbulent flow regime. HTRC is positioned very close to the roll surface and gap exit, which is beneficial for the roll surface quality. It is operated at a high flow rate but at a low pressure. HTRC not only significantly improves the roll surface quality, in addition, it makes high pressure pumps, needed for the conventional spray cooling, redundant, leading to substantial savings on electricity costs and thus CO2 emissions. HTRC is in trial operation since 7 August 2018. Results show no operational issues, an excellent roll surface quality and an increased cooling efficiency. In summer 2020 stands FM1-FM2-FM3-FM4 of HSM2 will be equipped with HTRC.

Oct 1, 2019

By Ian James McDonald

Each year, approximately 400 million tons of blast furnace slag is produced worldwide with a tapping temperature of around 1,500°C. It is normally used as a substitute for cement clinker or as an aggregate material in road construction. Currently, the slag is granulated in wet-granulation plants using large volumes of water and to date, it has not been possible to utilise the remnant heat energy of the molten slag, which amounts to approximately 1.8 GJ of energy per ton. However, in an R&D project currently underway led by Primetals Technolgies and industrial partners, a new dry atomising technology is being investigated to use air to cool molten slag and recover the lost heat energy. The resultant pelletised slag fulfils the same criteria as wet-granulated slag for use in the cement industry. Phase 1 of the project has now been completed where a technical plant was set up at the University of Leoben in 2012. A series of dry-slag granulation campaigns were carried out using remelted blast furnace slag. The elevated offgas temperatures and the quality of the slag product as verified by the FEhS Building Material Institute have shown the process suitability as an industrial application and the decision was taken to escalate the project from large laboratory scale to a full size pilot plant. The phase 2 development of this plant is now underway and is scheduled for installation at the site of an industrial partner in early 2016 where full slag flow will be fed directly to the plant from Blast Furnace ‘slag runners. This paper will show the development path taken to date and the planned route to our goal in 2016 of being the first to industrialise the ‘game changing’ process of dry Slag Granulation with Heat Recovery from the slag.

Aug 16, 2017

By Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Antônio Cezar Faria Vilela

A minor change in the chemical composition and temperature affects the slag viscosity, which has a great extent of the physical properties in regarding refining slags. Optimizing those parameters may affect the steel cleanliness. The viscosity measurement process is considered expensive, so the cost-effectiveness does not favor the measures at high-temperatures. Alternatively, it is possible to apply mathematical models or thermodynamic softwares to obtain viscosities for a given range of chemical composition and temperature of slags. The present work contemplates a validation of the experimental data, collected in the literature, with a calculated data and proposes an accurate representation of iso-viscosity curves applied for secondary steelmaking slags, covering the composition ranges: 0–100 wt.% CaO, 0–80 wt.% SiO2, 0–77 wt.% Al2O3 and 0–15 wt.% MgO (CSAM) system at 1500ºC. The viscosity representation fields include fully liquid and a partially liquid slags in the CSAM system and the viscosities were calculated using the FactSage 7.2 (for Liquid Phase) and the Roscoe-Einstein equation (for Phase mixture) for a total of 5976 slags. The preliminary results indicated that there is a great convergence between the calculated and experimental viscosities data, promoting an efficient approximation of the iso-viscosity curves for the CSAM slag system in the high-temperatures.

Nov 1, 2019

By Francisco Morganti

Weight reduction is the main target of all carmakers, which results in a continuous development of new steel grades. Latest 3rdgeneration advanced high-strength steel grades (AHSS) are complex materials with special chemical compositions and multiphase microstructures. The pickling, annealing and galvanizing processes of these grades aresomewhatdifferent due to the changed chemical compositions and microstructures. Therefore, these innovative steel grades place new demands on the plant technology of pickling, annealing and galvanizing lines. The most significant challenges for the pickling process are sludge occurrence during pickling, varying pickling times, weld ability of the materials, changed visual appearance and required high surface qualities. The most important topic concerning annealing line is a precisely controlled and very flexible heating and cooling process in the furnace.One of the new requirements in galvanizing linesis the prevention of surface faults caused by bare spots, which can occur since these materials feature a higher content of alloying elements like silicon or manganese. Prevention is possible with the special pre-oxidation technologies.Due to the higher strength of the material also the mechanical equipment has to be designed differently in these lines. This paper describes the influences of the changed chemical composition and material characteristics of modern steel grades on the pickling, annealing and galvanizing process and gives an overview about the technical solutions.

Oct 30, 2017

By Rodrigo Sanchotene Silva

Currently the industries of paint have directed their efforts on cleaner production of products that provide effective performance in corrosion protection of metallic materials. This work search introduce a new alternative of organic coating, without the presence of hazardous metals and replace equipments commercials used method of anodic protection for protection of oxidized metals. From this it, was produced Smart Paint (SP), consisting of Paint Acrylic Commercial (PAC) mixed the 1 % of binder, compound by the conducting polymer, Polyaniline Emeraldine Base (PAni EB) and plasticizer 4-chloro-3-methylphenol. The SP and PAC were applied to plates of carbon steel AISI 1010, with the aid of dip coat technique and then were subjected to drying for 48 h. The SP was characterized by thermals and physicochemical analyzes in order to verify possible changes in chemical properties of the ink produced, beyond perform electrochemical tests of Open Circuit Potential and Electrochemical Impedance Spectroscopy, employing equipment Potentiostat/Galvanostat Autolab PGSTAT302 Ecochemie, and aqueous 2 mol.L-1 of H2SO4. The results obtained allow us to state that the plasticizer does not alter the electrochemical properties of PAni and application of binder PAni EB to PAC does not alter the physicochemical properties of commercial coating. The binder PAni EB adds to PAC the capacity to induce the formation or maintenance of protective oxides in oxidizable metals submitted to harsh environments, method known as anodic corrosion protection.

Aug 8, 2018

By Eric Yoshimitsu Sako

One of the main difficulties in the operation of trough and runners at Arcelor Mittal Tubarão (AMT) Blast-furnace no.02 is the reduced amount of time available for repair procedures. The consequence is that the castable installation must often be performed during hot conditions and the installed castable could easily detach from the base material during the early stage of operation, exposing the previously oxidized base material to molten iron and corrosive slag attack. When events like this happen, emergency repairs must be executed, resulting in increased refractory unit consumption and an unplanned shutdown of unit operation. Considering these targets, Nippon Crucible Co. and Saint-Gobain HPR Brazil have developed a high-performance Al2O3-SiC-C composition based on an entirely novel anti-oxidation technology. Oxidizing reactions could be attenuated by adding an oxidant inhibitor and a water reducing agent. As a result, the open porosity was significantly reduced, resulting in an improvement of campaign life in terms of pig iron throughput when compared with the regular castable. An analysis of this life improvement showed successful results for the material after 250 days of campaign. The main reason for such successful results was that the deterioration caused by the oxidation was significantly less and that this change made on the high cohesive structure of the base material was maintained for a long time. The attained results allowed Arcelor Mittal Tubarão to achieve longer trough campaigns, and avoid any unplanned stoppages with zero breakdown risks.

Oct 30, 2017

By Manfred Hackl, Sergey Bragin, Alois Seilinger

The demand for hot rolled strip is growing in multiple ways. To remain competitive, new and existing mills must meet arisen challenges in the best possible way. The production of hot strip is a key element of steel production. Since close to half of all steel produced is hot-rolled to strip, mills require maximum throughput and availability combined with geometrical precision and the ability to create optimum material properties. Today there is a clear trend in developing new steel grades with high-strength and improved formability, like 3rd generation AHSS (Advanced High Strength Steels), as well as a trend to produce thinner and wider gauges. This trend challenges hot strip mills because it requires new technologies which provide more flexibility in metallurgical treatment during the rolling process. In order to meet and promote these trends Primetals Technologies is currently working on different concepts and solutions. One example is the development of a new mill stand technology Flex-HI HOT which allows to adapt the last finishing mill stands by efficiently switching from 4-high to a 6-high mode with small work roll diameter based on production needs. Another solution is to apply a permanent 6-high rolling stand at the end of the finishing train. A smaller work roll diameter allows to achieve higher specific thickness reductions and deformation rates resulting in significant thinner hot-strip gauges with valuable metallurgical benefits. The developed solution concepts with technological and metallurgical benefits will be presented in this paper.

Oct 1, 2019

By Jens Kempken

A competitive landscape pressurizes the steel producers business, zero defect requirements from customers forces the operators for additional efforts in process control and quality management. The so called quality related cost, which include also rework, cost for downgrading or even scabbing of material is already a remarkable lever in a plants profitability breakdown. The introduction of advanced state of the art grades in the product portfolio requires already a budgeting for the expenses for R&D and quality management. PQA has been developed as a process and quality management software solution next to existing level 2 or level 3 automation systems. It is focusing on the analysis of process data, equipment information, in line quality measurement devices and trend analysis to obtain an answer whether the process is according to definition and expectation and whether the intermediate or final product can be shipped for further processing as prime material. Advanced analytics which are linked to an expert know how based configuration identifies deficiencies in the production and processing process. An intelligent, state of the art quality rating system evaluates tolerable deviations. PQA comprises the software platform including the database, data configurator and collector from the different sources in the production process and units. The core element of the platform is the knowledge based expert know how package defining process and quality determining fundamentals. The paper describes the structure of the software package, it gives insights on the expert know how package, process and quality evaluation and points out the customer benefits, cost reduction, improvement yield, customer satisfaction increase. The link to recent operational references is given.

Oct 30, 2017

By Andrelio Marcos Ribeiro, Lucio Ribeiro Camisao, Antonio Carlos Ataíde, Alan de Sousa Pereira, Renato Siqueira Campos

The annealing and pickling line n. 1, responsible for the production of stainless steel 3xx, 4xx and 430a in thicknesses from 4 to 0.4 mm, has two vertical strip accumulators. These are intended not to let the material exceed the determined time in the furnace and in the pickling, and consequently do not cause defects like burning and excessive pickling. Strip accumulator n. 1 avoids the line from stopping during welding execution of the coils in the welding machine. In sequence, the strip accumulator n. 2 avoids the line from stopping at the end cutting of the tips, and in the coils removal from the pickling. The strip accumulators have a roller table that during the strip accumulation moves vertically downwards while its counterweight moves vertically upwards, and do the inverse movement when the material is released. On December 12th 2018, the failure occurred in the strip accumulator n. 1, where it was verified that the shaft of one of the pulleys had been fractured by high-cycle mechanical fatigue, which was characterized by alternating bending. With the fracture of the shaft, occurred the unevenness of the counterweight that damaged the guides. Failure analysis of this occurrence was based on the PDCA methodology, when was verified a weld between the shaft and the pulley. The analysis of the microstructure transformation in the molten zone, in the heat affected zone and in the base metal was carried out in an optical microscope, and no abnormality was observed. It was also carried out the end test by penetrating liquid, finding an inadequate weld in its geometry, as well as longitudinal trunks along the center of the weld bead. However, after a huge investigation of the causes, it was found that the failure was triggered by an inadequate design of the pulley shaft. It was also verified that the shaft had an open measure, inadequate for the operational context. After the analysis, action plans were drawn up based on the FMEA methodology to inhibit the failure recurrence.

Oct 7, 2019

By José Adilson de Castro

In the integrated steel industries the sintering process plays an important role furnishing raw material to the blast furnace. In this work, a computational simulation of the sinter process is developed that is able to predict the most important phenomena within the sintering bed. The model is based on the multi phase concept with multiple components described by conservation equations of each component coupled with the momentum, chemical reactions and heat transfer. The model validation was carried out comparing the model predictions with averaged industrial data and local temperature measurements within the sinter strand. The model predictions presented good agreement with the averaged values measured on the industrial sinter process.

Aug 2, 2018

By Marco Antonio Meggiolaro

Notches are preferential sites for fatigue and for environmentally assisted cracking (EAC) initiation. Semi-empirical notch sensitivity factors have been used for a long time to quantify notch effects on fatigue design. Recently, this concept has been mechanically modeled using techniques which properly consider the notch tip stress gradient influence on the fatigue behavior of mechanically short cracks. This model properly calculates such values from the basic fatigue resistances of the material, its fatigue limit and crack growth threshold, considering the characteristics of the notch geometry and of the loading, without the need for any adjustable parameter. Such criteria to estimate notch sensitivity and tolerable short cracks on fatigue have been extended to EAC conditions and verified by proper tests. In its simplest version, the criterion for the maximum tolerable stress under EAC conditions uses the resistances to crack initiation and to large crack propagation and the characteristic short crack size under EAC, considering the crack size and stress intensity factor. Moreover, the tolerance to short cracks under fatigue and under EAC conditions can be unified in an extended Kitagawa-Takahashi diagram, a new and potentially very useful tool for material selection tasks.

Aug 8, 2018

By Sara Hornby

After almost half a century of experience in using DRI/HBI in electric arc furnaces (EAFs), and taking into account the decrease of natural gas cost in the USA, it is interesting to revisit some trends and controversial issues around this alternative iron source. This paper reviews aspects like the evolution of iron ore quality and its influence on EAF operation; DRI stockpiling and transport, regarding the risk for selfcombustion; optimum charge design; cold DRI/HBI charging (fifth hole, bucket, transporter); hot charging (ways and results); carbon content, metallization and silica in DRI/HBI, and its influence on EAF operation and performance; oxygen / carbon balance; chemical energy and DRI/HBI charge.

Aug 16, 2017

By Edgar Ivan Castro Cedeño

En la producción de aceros limpios el control inclusionario es crítico para la obtención de un producto que cumpla con los requerimientos de calidad. El análisis de la distribución de tamaño de inclusión mediante modelos estadísticos permite estimar la incidencia de inclusiones en el producto solidificado a partir de mediciones tomadas en muestras relativamente pequeñas. En seis coladas de acero bajo carbono desoxidado con aluminio se tomaron muestras de acero a lo largo del procesamiento en horno olla y colada continua. Las muestras se prepararon para estimar mediante análisis metalográfico los tamaños de inclusión. Los datos de tamaño de inclusión se analizaron mediante modelos estadísticos de valores extremos, se hace una comparativa entre la distribución Gumbel (que forma parte de la norma ASTM E-2283) y la distribución Generalizada de Valores Extremos (GEV). Mediante una prueba de hipótesis con el estadístico Anderson-Darling, análisis de cuantiles y con la función de supervivencia se demuestra que la población inclusionaria se describe de una mejor manera con la distribución GEV. Finalmente se da un estimado de la incidencia probable de inclusiones en el producto solidificado.

Aug 16, 2017

By Hiroshi Ichikawa

In 2013, Nippon Steel & Sumikin Engineering Co., Ltd. (hereafter referred to as NSENGI), Tenova HYL and Danieli have entered into an agreement to combine ENERGION DR technology into blast furnace technology and/or with syngas technologies. This new alliance will allow the three companies to combine research and development activities with their respective expertise in ENERGIRON DR technology, Blast Furnace technology and Syngas (by-pro gas and coal gasification) technology, with the ultimate objective to develop breakthrough iron making technologies and create such EPC projects. This paper introduces the concepts and the features of our breakthrough technologies of combining of ENERGIRON DR technology, Blast Furnace technology and Syngas technology.

Aug 16, 2017

By Florian Markus Penz

The increase in Basic Oxygen Furnace (BOF) plants in steelmaking has given rise to renewed interest in a dynamic simulation of the BOF process. Material and process costs can be saved with optimized process times and targeted charging of scrap and slag formers. Beside hot metal, scrap is the main source of iron in the BOF process. Furthermore, scrap is used as a coolant during the process due to exothermal chemical reactions occurring in the BOF. In this paper, the melting and dissolution behaviour of scrap in the BOF process is discussed. A new dynamic thermodynamic and kinetic Matlab® model used to simulate scrap melting behaviour as a function of various scrap surface parameters and particle size is presented, as well as the influence of scrap properties on liquid bath temperature and final crude steel composition after a defined blowing period.

Oct 30, 2017

By Marco A. Ramírez-Argáez

A 2D mathematical model was developed for the plasma arc welding process. Computational simulations based on mass and momentum conservation equations as well as Maxwell equations were performed by using the commercial software PHOENICS. The model predicts the electric characteristics of the arc column, flow patterns, temperature contours and electrical potential, by varying the composition of the cover gas, in this case, argon and nitrogen. It was found that an arc of nitrogen with respect to one of argon generates more intense jets, greater voltages, and lower temperatures in the arc column for welding arcs current of 150 A and 10 mm arc length.

Oct 30, 2017

By Giulio Rodrigues Altoé

Environmentally correct composites, made from natural fibers, are among the most investigated and applied today. In this paper, we investigate the mechanical behavior of epoxy matrix composites reinforced with continuous fique fiber, through bending tensile tests. Specimens containing 0, 10, 20 and 30% in volume of fique fiber were aligned along the entire length of a mold to create plates of these composites, those plates were cut following the ASTM standard to obtained bending tests specimens. The test was conducted in a Instron Machine and the fractured specimens were analyzed by SEM, the results showed the increase in the materials tensile properties with the increase of fiber amount.

Aug 16, 2017