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By Steven George Jansto

The hot ductility behavior of different microalloyed steel chemical compositions was examined simulating the thermal and strain conditions through the straightening or unbending section of the continuous casting machine. All samples were obtained from industrial slab casters ranging from 200 to 300 mm in slab thickness from steel mills throughout the world including China, Brazil, North America and Europe. The slabs were crack-free and hot rolled into prime quality products. No laboratory heats were tested. Although these microalloyed steels exhibit inherently lower hot ductility behavior, as measured by percent reduction in area at elevated temperature, these steels still exhibit sufficient ductility to satisfactorily meet the unbending stress and strain gradients existing in the straightening section of most casters. The majority of the published hot ductility data, as measured by % reduction in area (%RA), were based on laboratory heats and hence, are inaccurate in accessing the propensity for slab cracking on an industrial caster. This situation then results in invalid conclusions for different chemistries. This research has determined the minimum required %RA for crack-free casting is significantly lower than results based upon previously published laboratory generated data. For example, the literature quotes 40% RA minimum for Nb-bearing steels when in fact as low as 10% minimum RA is more than sufficient to assure crack-free casting based upon the extensive testing and analysis performed in this study. Instead of %RA, the measurement of strain energy has been introduced to evaluate hot ductility behavior. It is concluded that strain energy is a better measure of hot ductility behaviour than %RA. There is considerable value in the evaluation of the hot stress and strain curves, process metallurgy parameters and their relationship to slab quality instead of just basing hot ductility decisions on simple %RA measurements.

Aug 16, 2017

By Vinicius Cardoso Ottani

Os processos de estampagem de materiais de alta resistência requerem o uso de aços ferramenta de alto desempenho, uma vez que a aplicação de pressões elevadas produz o desgaste acelerado das ferramentas de conformação, e até mesmo a ocorrência de falhas catastróficas e prematuras. Frequentemente, o desgaste de ferramentas é superado pelo aumento da dureza dos punções e matrizes, o que implica na diminuição da tenacidade. Esta estratégia, entretanto, não pode ser aplicada em operações de conformação de alta solicitação em que os componentes devem ser tenazes o suficiente para suportar as cargas elevadas envolvidas. A maior dureza retarda o início das trincas, porém também diminui a tenacidade do material, facilitando sua propagação. Uma dureza mais baixa, por outro lado, propicia maior resistência do material à propagação de trincas pela maior tenacidade, porém facilita sua nucleação. Constata-se então, que a relação dureza e tenacidade em aços ferramenta deve ser aprimorada através de um design microestrutural preciso, no qual ambas as propriedades possam ser melhoradas. O presente estudo buscou avaliar a vida útil de punções e matrizes de aços ferramenta AISI D2 e VF800AT limitada por trincas e lascamentos em processos de estampagem. O VF800AT apresentou resultado satisfatório e contribuiu para um aumento de até cinco vezes da vida útil da ferramenta quando comparada com o aço AISI D2. Os ferramentais empregados nesse trabalho foram também caracterizados em laboratório por meio de microscopia óptica e eletrônica de varredura. O superior desempenho das ferramentas produzidas em aço VF800AT é justificado pela sua superior tenacidade em relação ao AISI D2, devido a uma microestrutura composta de uma matriz de martensita revenida e carbonetos primários em menor fração volumétrica.

Jul 30, 2018

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Dr. Steven G. Jansto

The market demand for reduced fuel consumption and CO2 emissions in the automotive, energy and construction sectors have further increased the demand for new and advanced higher quality microalloyed grades produced via TMCP. The technological integration of the process and physical metallurgical advancements of value-added niobium (Nb) microalloyed thermo-mechanical controlled process (TMCP) steels continue to be developed and is an important element for these more demanding end user requirements and cost-effective steel production. The reheat furnace process step has a profound effect on the TMCP performance, final hot rolled steel quality and mechanical property consistency during the production of hot rolled steels. The uniformity of heating applied across the entire width, thickness and length of the slab or billet is essential in the successful achievement of consistent customer properties regardless of the chemistry. The resultant ferrite grain size in the final hot rolled product is significantly governed by the initial prior austenite grain size. However, the transition from laboratory melted and TMCP hot rolled heats to the production scale is often quite challenging. Aberrations in the reheating process step at the industrial furnace are often the root cause of mechanical property quality issues. These combustion process metallurgy parameters connect directly to the resultant TMCP product quality and is defined as Combustion Metallurgy

Oct 1, 2019

By Franco de Castro Bubani

Cu-base alloys (Cu-Zn-Al, Cu-Al-Be, Cu-Al-Ni), depending on their composition, have martensitic transformations that can be thermally or mechanically induced between a metastable structure called austenite and one or more metastable structures called martensites. In single crystals, depending on the specific composition of the alloy and the crystallographic orientation of the tensile axis, martensite-martensite transformations can be mechanically induced. The hysteresis associated to these martensite-martensite transitions is usually much greater than the one associated to the austenite-martensite transformation. Thus, martensite-martensite transitions are potential candidates for energy dissipation in a mechanical damper. Possible applications that would benefit from high hysteresis include seismic damping devices, dampers for satellites and the aerospace industry, defense and others. We present pseudoelastic cycling results of alloys submitted to different thermal treatments. Our conclusions highlight the fact that, under certain conditions, Cu-base alloys deliver better damping performance than commercially available SMAs and even the new Fe-base SMAs.

Aug 7, 2018

By Piotr Kula

Vacuum carburising with pre-nitriding (PreNitLPC® technology) involves feeding ammonia during the charge heating stage before carburising. The purpose is to restrict the growth of grain in the surface layer of the carburised steel. The article presents the influence of nitrogen on restricting austenite grain growth during vacuum carburising and on mechanical properties (fatigue strength, impact resistance) of layers that underwent such treatment in comparison with traditional carburising methods.

Aug 16, 2017

By Ernesto Gustavo Maffia

En la actualidad, el moldeo por inyección es una tecnología muy utilizada en el procesamiento del plástico pues permite fabricar formas geométricas complejas. Para fabricar los moldes se utiliza ampliamente la aleación C17200 (Cu-2%Be), pero están en desarrollo algunas alternativas con aleaciones base cobre libres de berilio, que tienen valores de dureza por encima de los 30 Rockwell C y buena conductividad. Las aleaciones base de cobre, tipo CuNiSiCr son las más adecuadas como reemplazo. El siguiente trabajo trata del estudio y desarrollo del proceso de fabricación, por fusión, colado y conformado, de una aleación tipo CuNiSiCr de alta dureza y buena conductividad para ser utilizada en la fabricación de moldes de inyección para la industria del plástico. Los resultados preliminares de esta investigación demuestran que a través del aumento sistemático en el contenido de níquel y silicio se consigue un aumento de la dureza (>32 Rockwell C) y una aceptable conductividad eléctrica (˜25%IACS). El fenómeno segregación interfiere fuertemente en los tratamientos termomecánicos, pues se forma una segunda fase interdendrítica, de características frágiles, que genera fracturas en el conformado. Los resultados demuestran que la aplicación del recocido total y control de la temperatura durante la forja minimizan este problema.

Aug 7, 2018

By Cleber Caetano Thomazi

Rotary kilns are continuous process equipment used on calcining of nickel ore. The chemical and physical reactions are created by means of heat up the material to predetermined temperatures. Tertiary air fans are attached to the kiln shell to maintain oxidizing/reduction conditions. Special ducts orientate the air flow inside the kiln. In the present work, two types of failure on distinct tertiary ducts mounted on the same kiln are reported. Chemical analysis, hardness test, metallographic and fractographic examinations were carried out. Fabrication related problems and creep were identified as the root causes of damages.

Oct 30, 2017

By Leandro Rigo Ramos, Marcelo Lucas Pereira Machado, Lumena Gloria de Souza Nunes, Mariana Valinhos Barcelos

The aim of this work was to study the influence of temperature on the grain refining process from severe plastic deformations through the simulation of Accumulative Roll Bonding (ARB) by torsion tests. The assays were performed to simulate the ARB at three different temperatures of 550 ° C, 625 ° C and 700 ° C with 5 torsion cycles with equivalent strain of 0.8 per cycle at a rate of 0.1−1 , totalizing an accumulated deformation of 4.0. Grain refining was obtained with an average size of 2μm, 5μm and 6μm for the temperatures of 550 ° C, 625 ° C and 700 ° C respectively. There was a rise in Vickers hardness by 68%, from 119HV in the annealed sample to 175HV in the deformed sample at 550 ° C. In the deformations at 625 ° C and 700 ° C the value of 130HV E and 150HV respectively was obtained. Based on the obtained results, it can be stated that the severe plastic deformations in microliged steel, carried out at temperatures lower than the end of the austenite-ferrite transformation, produce refined grains of the order of 2μm and, consequently, increase the mechanical strength of the material.

Oct 1, 2019

By Antônio Aldenor Pinheiro Neto, Matheus de Lima Vieira

In mid-2015 the steel industry faced a strong crisis due to the weak performance of the Brazilian economy and the persistent entry of Chinese steel into Brazilian territory. This situation demanded that Brazilian steelmakers seek to develop products to meet new export markets. within the volume of exports possible are the rebars, where its applications are in the construction industry. One of the largest importers is Peru which has a large percentage of this export volume. This market demands as a priority requirement the surface quality of blue condition (low oxidation index) and mechanical properties normative.in order to meet the items required by the customer at a competitive cost, a vanadium microalloyed steel was applied to the hot rolling process without heat treatment after the last rolling pass. Where the great challenge was to achieve a high level of stretching without compromising the minimum limits of tensile strength. Assuming that the steel used is the correct one interventions were made on rolling parameters such as set-point temperature, residence time of pieces in the furnace, linear mass and rolling speed. All the changes made were based on statistical tools and practical tests. Finally, with the execution of actions generated from the statistical analyzes and tests it was possible to reduce process losses by 96%.

Oct 1, 2019

By Sidiney Nascimento Silva

O trabalho descreve os principais resultados dos testes industriais realizados na Usina Presidente Vargas, CSN, Brasil, envolvendo a adição de um catalisador à mistura de carvões, em termos da qualidade do coque e do processo da coqueria. O catalisador em questão é o produto Thermact, que possui partículas nanométricas em sua composição, fornecido pela empresa Abhitech Energycon Limited, Índia. O catalisador foi dosado e adicionado à mistura de carvões via correia transportadora, na proporção, em peso, de 1kg de catalisador para 4.000kg da mistura de carvões. Os resultados dos testes realizados nas Baterias # 1, 4A, 4B e 5 com a adição de um catalisador à mistura de carvões, sinalizaram a viabilidade técnica e financeira da sua aplicação no processo da coqueria. Os principais benefícios decorrentes da adição do catalisador foram: i) aumento potencial da capacidade de produção de coque ao redor de 10% ou, alternativamente, melhoria da qualidade do coque - aumento de 1,4% do valor médio do índice de resistência mecânica a frio do coque, DI150/15, mantendo-se o tempo total padronizado do processo de coqueificação, visando à preservação das Baterias, ou ainda, a utilização de uma mistura de carvões de menor custo, sem prejuízos ao atendimento à especificação do coque para os Altos-Fornos; b) aumento da geração e redução do consumo de gás de coqueria, GCO; iii) aumento na produção de BTX (Benzeno, Tolueno, Xileno) e redução da produção de alcatrão na Planta de Carboquímicos; iv) limpeza do sistema “PROven”, “goosenecks”, tubos de ascensão e paredes dos fornos, sinalizando a sua viabilidade técnica e econômica.

Aug 1, 2018

By Rob van Opbergen, Edo Engel

The highly dynamic economic climate of recent years has tightened the operating envelope for steel producers world-wide. Steel producers continue to experience immense pressure to respond quickly to changing circumstances and the focus has shifted towards efficiency improvement and maximizing flexibility in operations. The ability to safely stop, restart and ramp-up production facilities has become essential. Establishing this level of flexibility, without sacrificing efficiency, requires sound process control, fit-for-purpose process management practices and solid know-how and experience regarding special situations in blast furnace ironmaking operations. The same business environment that demands this increased flexibility has made it increasingly difficult for steel producers to sustain sufficient knowledge about these situations. While many experienced, senior operational staff have retired, a new generation of ironmaking specialists has acquired its hands-on experience over more recent decades, during which these process situations have been much less frequent than before. Over the past 10-15 years, the requirement in the industry for external operational support during e.g. blast furnace blow–downs, salamander tapping and restarts after planned and especially unplanned stops, has become increasingly frequent. This article presents a number of these cases from a process management perspective as well as with regard to project organization and optimized cooperation between internal and external teams of experts.

Oct 1, 2019

By Thomas Höfler, Michael Auinger, Bernhard Linder

Gas-fired pusher furnaces are commonly used to heat steel slabs before hot rolling. Temperatures well above 1000 °C combined with an oxidizing atmosphere containing H2O, CO2 and O2 result in rapid oxidation of most steel grades. The resulting oxide scale and the chemistry of the metal-scale-interface are major determining factors for the occurrence of hot rolling defects. To better understand these phenomena, lab-scale trials were performed with two different steel grades in an electric tube furnace in the temperature range 1000-1250 °C, using an atmosphere of about 20 % H2O, 7 % CO2 and 3 % O2. Humidification of the gas was achieved by evaporation, using a custom thermostat with standard laboratory glassware. The resulting samples were prepared metallographically, using cold mounting under vacuum with taper section angles, and analyzed using light microscopy and SEM/EDS. The scale structure of the Si alloyed steel was highly dependent on the oxidation temperature due to the formation of eutectic liquid phases of FeO, Fe2SiO4 and FeAl2O4. Below the eutectic temperature, the scale of the Si steel appeared to be made up of three distinct areas: The external scale consisting solely of Fe oxides, the internal scale containing Fe2SiO4 and FeAl2O4, and an internal oxidation zone with SiO2 and Al2O3 in a mostly plain Fe matrix. Comparisons of the experimental results with simulations of the internal oxidation showed good qualitative agreement.

Oct 1, 2019

By Marcel Antonio Arcari Bassani

In the mining industry, it is common to have data collected in various formats. In an open pit mining operation, at the early stages of exploration samples are obtained from diamond drillholes. During the production stage, samples are collected from blastholes. The last is more numerous but less precise. From a geostatistical view, this dissimilarity has to be considered to integrate the two sources of information. To combine this different data, three methodologies were investigated: simple kriging with local varying mean, cokriging and ordinary kriging. The exhaustive Walker Lake data set was used and it is considered the source to obtain the true grades. Initially, samples were obtained from the exhaustive data set at a regular spacing grid of 20 x 20 meters. Next, samples were obtained again from the exhaustive dataset at a regular spacing of 5 x 5 meters and a relative error of 25% was added. Then, both data were used to estimate blocks using the three methods mentioned. The grade tonnage curves were compared with the true block grade distribution. Moreover, the block misclassification was evaluated. The results showed that ordinary kriging produced estimates closer to the true block grade distribution and reduced the block misclassification.

Aug 8, 2018

By Jens Kempken

A competitive landscape pressurizes the steel producers business, zero defect requirements from customers forces the operators for additional efforts in process control and quality management. The so called quality related cost, which include also rework, cost for downgrading or even scabbing of material is already a remarkable lever in a plants profitability breakdown. The introduction of advanced state of the art grades in the product portfolio requires already a budgeting for the expenses for R&D and quality management. PQA has been developed as a process and quality management software solution next to existing level 2 or level 3 automation systems. It is focusing on the analysis of process data, equipment information, in line quality measurement devices and trend analysis to obtain an answer whether the process is according to definition and expectation and whether the intermediate or final product can be shipped for further processing as prime material. Advanced analytics which are linked to an expert know how based configuration identifies deficiencies in the production and processing process. An intelligent, state of the art quality rating system evaluates tolerable deviations. PQA comprises the software platform including the database, data configurator and collector from the different sources in the production process and units. The core element of the platform is the knowledge based expert know how package defining process and quality determining fundamentals. The paper describes the structure of the software package, it gives insights on the expert know how package, process and quality evaluation and points out the customer benefits, cost reduction, improvement yield, customer satisfaction increase. The link to recent operational references is given.

Oct 30, 2017

By Daniel Stickel

Current political, economic and ecological guidelines demand the increase of power densities of nearly all machinery parts today. In order to further lower the wear rate towards the ultra-mild sliding wear regime an integral approach is needed, which has to regard contact conditions, surface topography, surface chemistry, as well as sub-surface properties. Still there are no simple parameters to classify the performance of tribosystem. In this study the area and volume affected by tribocontacts are calculated by means of a three dimensional elastic-ideal plastic contact model. The surfaces are generated by means of conventional machining procedures and characterized by scanning white light interferometry. The further input data as to normal and friction forces are derived by ultra-mild sliding wear tests under boundary lubrication conditions of carburized steel against carburized steel and 52100 steel against case-hardened spheroidal cast iron. This contribution will depict the distinct influence of the topography on friction and ultra-mild sliding wear of common Fe-base materials and point on the marked importance of highly localized effects, which govern the acting mechanisms.

Jul 31, 2018

By Leszek Maldzinski

The present concept assumes carrying out the process of controlled nitriding with NH3 alone. This is a simpler process than that using two-component mixes of ammonia diluted with N2 or NH3diss. The regulation of the chemical composition of the atmosphere in the retort, and therefore the regulation of the nitriding potential KN, is obtained through the variation of the inflow rate of NH3 into the retort. What is a completely new things in a relevant process, the inflow of NH3 into the furnace is at times reduced to zero, which widens the range of the gas composition in the retort (and by the same token, of KN). The amount of NH3 introduced into the furnace is regulated (controlled) with the aid of a gas analyzer (for example an infrared analyzer). The gas analyzer opens and closes periodically the NH3 inlet valve with a frequency maintaining a desired gas composition (a desired KN) in the retort. The concept was based on experimental and theoretical investigations in term of thermodynamic and kinetic of gas nitriding. Investigations were carried out in a laboratory furnace with a quartz tube and also in an industrial furnace with a steel retort and a circulating fan. Nitriding was performed using NH3, NH3+H2, NH3+NH3diss. mixtures. In an industrial furnace the supply of NH3 into the retort was periodically closed, though with an operating circulation fan. The studies demonstrated that the growth rate of nitrided layer depends only on the composition of the atmosphere, (or KN), in the retort. It depends neither on a type of atmosphere introduced into furnace (NH3, NH3+NH3diss. or NH3+H2) nor a type of furnace (laboratory with a quartz tube or industrial with steel retort and fan). The results proved also that entirely closing of NH3 supply to the retort does not affect the growth rate of nitrided layer. A detailed analyses of the results was performed in a paper.

Aug 16, 2017

By Jörg Busch

The essential pre-requisite for attaining the high quality of product required from high-speed continuous production processes is the use of new measurement and control technologies. High availability and reproducible measuring results ensure the high level of process stability necessary for full continuous operation. The requirements for the optimisation of quality across the complete production process and for quality analysis systems will be discussed. This report will present examples of basic and new measurement technologies in Cold Rolling Mills and Processing Lines. The following gauging systems will be discussed in detail: Strip tension meter, roll force measurements, weighing systems and shapemeter rolls. The measuring and control systems in this presentation must be seen as high-tech solutions in the field of processing technology. The measuring methods and technologies described are, together with optimised process models and precision control loops and actuators, the main pre-requisites for achieving the quality of product required from high-speed continuous production processes. Interconnected quality management systems enable optimisation across the complete production process.

Jul 30, 2018

By Haruki Inami, Takashi Ishida, Kazuhiro Ohara, Hiroyuki Imanari

The highly competitive business environment of the international metals industry is driving demand for more cost-effective operation of steel making facilities, rolling mills, and strip processing lines. Achieving stable operation is vital if the steel industry is to produce high-quality products constantly and productively. In recent years, advances in computer processing speeds, data acquisition rates, and data storage capacity have rapidly led to greater use of the new technologies of big data, analytics, the IoT, and AI by control system designers and process engineers, and the introduction of industrial applications. The “Smart Rolling Mill” solutions for hot strip mills have been developed by our group with the goal of achieving sophisticated, state of the art, and automated operation in steel rolling mills. The various solution engines improve process stability, increase the performance of mill equipment, and provide improved process control. These solution engines are based on extensive knowledge of the rolling process and the associated control systems. Two solution engines in particular are the diagnosis systems for rolling condition and for product quality that contribute to cost-effective operation and lower yield loss. This paper focuses on the diagnosis systems for rolling condition and for product quality in hot strip mills. Advanced information technologies using big data analytics and machine learning are applied to real-time data collected from the automation system that controls operation and the rolling process. We have developed diagnosis solutions for rolling condition and product quality utilizing predictive and clustering diagnosis. Predictive diagnosis prevents serious problems by detecting changes in the state of the plant or in the rolling condition. Clustering diagnosis classifies patterns of fluctuation in product quality trend charts, providing effective tuning guidance for improving product quality. This paper describes these applications with several examples.

Oct 1, 2019

By Sihai Jiao, Xiaoming Xia, Bo Yan

Checkered plate, which is also known as floor plate, has a raised pattern that provides excellent skid resistance for a wide range of applications, such as flooring, walkways, platforms, stair treads, covers, etc. As one of most common products, carbon steel checkered plate is used in low strength with a large thickness margin for corrosion and costs a lot in corrosion resistance treatment and maintenance. Although austenitic stainless steel checkered plate meets the requirements of general corrosion resistance, it is also hard to provide a highly comprehensive performance for its low yield strength, which mean higher thickness, higher weight, lower stability of structure. Combined the advantages of stainless steel and carbon structural steel, a roll-bonded clad checkered plate with high performance in skid resistance, high strength and corrosion resistant is developed. The metallography shows metallurgically bonded interfaces. Both external and internal bending at room temperature can be done successfully done without any cracks. The yield strength is also significantly improved. Therefore, roll-bonded clad checkered plate is superior in microstructure, strength, ductility and workability. An application case on a pulverized coal injection platform in an iron-making plant, is also introduced to show the way of processing and installation. After two years of installation on the platform, the product still keeps the original appearance. It implies that the developed plate could keep the facilities functions with much less or no maintenance and make them much safer.

Oct 1, 2019