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By Z. Zborovszky

The feasibility of using the nucleation properties of combustion generated particulates for the identification of their sources was investigated, using the Cloud Condensation Nuclei (CCN) Spectrometer. The Investigated materials included coal, wood, belt materials, electrical insulation, brattice cloth, and diesel exhaust. The materials were heated In an oven using filtered air flow, and their time, temperature, and the critical supersaturation spectrum of condensation nuclei (also referred to as the CCN spectrum) produced by the combusting material were recorded. Some data was obtained on a typical metal-mine background containing blasting products. The data was processed and analyzed In an attempt to specify parameters and limits that would allow the identification of the combustion sources. It appears that under controlled test conditions It Is possible to Identify the source on the basis of data derived from the CCN spectrum. More general use of the Idea for fire detection under uncontrolled practical circumstances in an actual mining environment does have potential but would require further research.

Jan 1, 1978

By Chris Uys, Johan Labuschagne

Sishen Iron Ore Mine, located in the Northern Cape, is an open cast mine excavating approximately 100 million tons rock to produce 25 million tons of high grade haematite ore per annum. The size of the pit is approximately 12 km ‘1.5 km ‘150 metres. The final depth is planned to be around 350 metres. It is hard rock mining operation employing the conventional truck and shovel method. Mining benches are twelve and a half metres in height and are divided into blasting blocks, each consisting of approximately 300 000 tons of material.

Jan 1, 1997

The safety of personnel is the most important matter during a mine fire. However, there is not enough research on a case when a fire occurs near a shaft and the behavior of the fire gas is not well understood. Therefore, a series of experimental study using a scaled ventilation circuit model was carried out. The behavior of ventilation air during a mine fire near a shaft was investigated. The model consists of two vertical shafts, three horizontal ducts connecting the shafts and an exhaust fan from the shaft bottom. The cross section of the shaft and duct is a square of 200×200mm. The height of the shafts is 3400mm. The length of the ducts is 1540mm. The lower duct is set at the same level as the shaft bottom. The middle and upper duct are set at 750mm and 1760mm above the shaft bottom respectively. The airflow rates through the ducts can be adjusted by regulators installed in each duct. The behavior of the fire gas was measured by anemometer, thermometer, and visualized using laser light .The air was ventilated downward in both shafts before the initiation of the fire. Some amount of fire gas of high temperature rose upward gradually along the shaft wall regardless of the downward ventilation after the initiation of the fire. Then the direction of main ventilation air suddenly reversed upward in the shaft. The direction of ventilation reversed in many places in the model and the fire gas reached even the part not anticipated.

Jan 1, 2009

By David Rahal, Des Erasmus, Ken Major

"Over the past twenty years there has been an increased emphasis on fine grinding in the minerals industry. This spurred the development of a range of new fine grinding equipment in the 1990s. At that time, the Knelson-Deswik mill was developed in South Africa for the pigments industry.Knelson Milling Solutions currently offers a wide range of laboratory, pilot and production scale mills. These mills bridge the gap between traditional low speed vertical mills and the high speed horizontal mills (tip speed < 3 and > 15 m/s respectively). They are designed to run at tip speeds between 10 and 12 m/s and are capable of operating with very dense grinding media. The result is a power intensity that is higher than the low speed mills and overlaps that of the high speed mills. This allows the mill to be customized for a wide range of grinding applications.A case study at Aquarius Platinum’s Kroondal Mine shows that the Knelson-Deswik technology can produce a consistent product size despite feed variations. It also shows that the throughput was proportional to the slurry density at Kroondal. The case study identified increasing the slurry density as a process change that can increase throughput and reduce the specific energy consumption.INTRODUCTIONThe increasing complexity and finer grain sizes of modern ore bodies have increased the importance of effective mineral liberation in obtaining acceptable grades and recoveries (Jankovic, Valery and La Rosa, 2003; Lichter and Davey, 2006; Napier-Munn, Morell, Morrison and Kojovic, 1996). This trend has increased the significance of fine grinding technology because the input energy increases exponentially as the required product size decreases from 100 to 10 microns (Gao and Weller, 1993a).The US Department of Energy recently provided the context for the potential energy savings in the US Mining Industry (BCS, 2007). They reported that grinding consumes approximately 494 TBtu/year. This was over double the consumption of the second highest equipment category, diesel materials handling systems (211 TBtu/yr). The proportion of grinding energy allocated to fine grinding can only be expected to increase as finer ore deposits are mined. It is therefore critical that fine grinding efficiency continue to improve through the selection of appropriate equipment and the development of best practices for existing applications."

Jan 1, 2011

By Jan E. Nesset, Antonio DiFeo, James A. Finch, Jose Hernandez-Aguilar, Cesar O. Gomez

"The gas dispersion measurement sensors and methodology developed by the mineral processing group at McGill University have to-date been employed at a number of plants in Canada, Australia, the U.S., South Africa and South America. In some cases the measurements have been directly linked with metallurgical performance while in others the gas dispersion surveys on their own have proved very useful in understanding the behaviour of the flotation cells. In addition to reviewing the current state of the gas dispersion measurement technology, the paper will present a series of case studies from the various plants and will show how this technology brings a remarkable new level of understanding to flotation behaviour. The influence of the bubble size distribution on recovery and grade are emphasized in the paper.INTRODUCTIONBackgroundThe advent of new sensors to characterize gas dispersion parameters in flotation cells is a development that is long overdue. While the chemistry of flotation has been studied since the early 1900’s, it is only now that the significance of bubble size distribution, gas rate and gas holdup can be meaningfully measured in-plant with robust and precise sensors. Early researchers, like T.A. Rickard (1916) recognized the importance of understanding the role of air and bubbles in flotation when he wrote in 1916 “we know that the key to the flotation process is to be found not in the oil, the acid, or the apparatus, but in the bubbles. The man who understands the mystery of a soap bubble has mastered the chief mystery of flotation”. In his 1999 review paper on The Froth Flotation Century D.W. Fuerstenau laments the fact that due to their “inert nature”, bubbles have never received their due attention from researchers who tended to focus on the chemical, physical, surface and colloidal aspects, rather than the physics of the process. It is perhaps fitting that now, 100 years after the inception of industrial flotation practice at Broken Hill, Australia, researchers and industry have turned their attention toward the importance of truly understanding the role of bubbles in flotation."

Jan 1, 2005

By Floyd D. Varley, C. M. K. Boldt

Toolbox training is often described as short, informal training conducted at a worksite by technically competent persons for the benefit of a work team. The key feature of toolbox training is the focus on a work team and what is important to that group in its workplace. Toolbox training conducted by peers can connect miners and establish the feeling that the hazard is a real threat to them. This feeling can bridge the gap between delivery of a safety message and behavioral changes that can prevent an accident. Toolbox training is a popular form of "maintenance" training that should not be used to teach a new skill. The 10- or 15-minute toolbox session is simply too short a time to teach or learn a new skill and test for skill development. However, the toolbox format is an excellent way to inform workers of changes in workplace rules, conditions, or hazards by bringing the discussion of change to the level of the work group and suggesting how a change will affect the way workers perform their jobs. Toolbox training should be structured to address a very specific hazard. That is, the hazard source should be identified and the effect of the hazard on the worker described. The temptation to discuss a safety subject in broad terms will result in an equally vague result. For instance, discussing "equipment guards" is inappropriate for a 15-minute training session. There simply is not enough time to cover all the hazards and their remedies. A more appropriate topic would be "placing guards on a conveyor return roller" or "hazards of cleaning a conveyor return roller." Each topic is concise enough to allow the trainer time to define a particular threat to the safety of miners and discuss ways to defend against that threat. The clearest way to a safe workplace is to identify hazards methodically and eliminate them. This cannot be done with sweeping, generalized training. Some best practices that will protect a worker from the hazard should be presented, and the hazard should be located at the specific worksite. Toolbox training is an opportunity for the work team to participate in learning and share experiences and knowledge, often through storytelling. Storytelling is an ancient form of passing along information in an entertaining way. It is entertaining because it draws the listener in with imagination and creativity. Stories told within work groups are a way for miners to exchange experiences in which they made mistakes that resulted in an accident or a near-miss and learned a valuable lesson. Thus, co-workers can learn from others without the pain or fear that accompanied the storyteller&apos;s learning path. To encourage these shared experiences, the people in the group must be comfortable with one another. Participation doesn&apos;t stop with listening to a near-miss story or informing the group of an unsafe work practice. Participation by sharing experiences, knowledge, and skills should lead toward action in changing the unsafe tool, practice, or machine (Wallerstein, 1992). This power to change is called empowerment. Empowered workers use toolbox training sessions to discuss a problem; direct their own knowledge, experience, and talents in the context of their work environment to solve the problem; and put into practice what they have learned by sharing (Baker, 1992). A worker is much more likely to implement changes they have contributed to creating than changes forced upon them. Toolbox training functions best when the group size is small (under 20) and composed of workers with similar job functions. While combining all workers on a shift or multiple shifts may be convenient, the level of participation will drop dramatically as group size increases and participants are less connected. Similarly, when the work group participants are from different job functions, keeping the materials relevant to the individual becomes more difficult. The role of management in the toolbox training system is to communicate among various groups so that all groups at a mine site are hearing the same message. In very small operations, combining work groups can be productive if the trainer can promote open discussions and lead the group to solutions that address the needs of all and not let one group or individual dominate the discussion. WHY USE NARRATIVE METHODS An effective communications tool is to use stories as a means of describing a hazard and its consequences. Historically, using stories to transfer knowledge between individuals of the same and different generations is well established. All good stories share the same elements required to communicate safety principles. Stories require a setting (the part of the workplace), a plot (the circumstances that lead to a hazard), the solution (best practices), the lesson (what can happen), and the result (what will be done to prevent the hazard) (Dennehy, 1999).

Jan 1, 2002

By J. Eric Nylund

"Intensive mechanization and automation in the LKAB, Kiruna Mine in Sweden have resulted in substantial rise in productivity and decrease in production cost. Capital investment in a modern mine today averages a considerable amount per miner and costs increase with requirements for more efficient methods and equipment. Equipment reliability becomes more and more important. Equipment maintenance requirements are directly proportional to equipment reliability and grade of availability. Weaknesses in the equipment result in unnecessary costs with regard to maintenance which can add up considerably per year, but of more importance are the costs caused by equipment breakdown. These breakdowns disturb or interrupt the production and often cause damage to other parts of the system. This paper discusses the important parameters involved in mine car wheel wear and the design principles of wheels, axle suspension and track.IntroductionTrains operating in an underground mine do not follow the same standard of performance as trains operating on surface railways. The differences in speed, curve radius and environment require different methods of calculation for underground train systems, and when judging the parameters involved one must keep in mind these differences at all times.While surface railway technology was given all possible attention over the last century no one was seriously looking into underground rail haulage in the sense of rail vehicles performance on the track until LKAB in 1975 started to question the methods of calculations used. Even though LKAB by then attained mine car maintenance cost that was 1/6 to 1/10 of other mining companies they were not pleased with the situation. The objective for the ensuing engineering work was to derive the reasons for wear and breakdowns. Once those reasons were established, the design of a completely new generation of mine cars could start. The result of these efforts were beyond all expectations. The maintenance cost on mine cars had been reduced to 1/15 of prior car generation which already had comparatively low cost.The most significant cost savings were made on wheel maintenance, which earlier represented 50% to 55% of car maintenance. Wheel life was increased from an average of 3 to 30 years or more.The LKAB theories around wheel wear are described in the following report."

Jan 1, 1987

By Olli Aulio, Outokumpu Oy

"GENERALThe Outokumpu Company is today an important European producer of metals from its own mines: copper nickel cobalt, ferro chrome and zinc being the main products. In 1972 about 4 million tons of ore was hoisted from eleven mines.Outokumpu Oy has gained experiences on the various aspects of on line computer control since 1968. This knowledge has been combined to develop a standard computer control package for concentrator control. Before the development of computer control package was started Outokumpu Oy had three large computer control systems. The first system was at the Pyhasalmi Concentrator, thee second at the LokkolaPlant, and the installation of the third system at the Vuonos Concentrator was just started.The characteristics of general computer software packages - both control and executive ones - were thus well-known as well as the practical usage of control theory. Furthermore Outokumpu had developed the Courier analyzer which included a so-called minicomputer. This project had given experience both 1n totally self made real tire executives and in computer hardware and peripheral d=vices. The instrumentation of the Outokumpu concentrators was designed and installed traditionally by the engineers of Outokumpu themselves."

Jan 1, 1973

By C. Larsen, E. Goodwin, E. Konigsmann

"This paper describes the development of an innovative effluent treatment process for cyanide and heavy metal removal from tailings wastewaters at Hemlo Gold Mines Inc. Golden Giant operation.The importance of minimizing dissolution of contaminants in the gold leaching circuit is discussed, as well as using recycled water in milling circuits to the fullest extent possible. Finally, a brief description of the role of natural cyanide degradation in the tailings pond is provided.Emphasis is placed on the need for overall water quality management to ensure minimum effluent treatment process costs and complexity while producing excellent quality effluents.1.0 INTRODUCTIONHemlo Gold Mines Inc. owns and operates its Golden Giant Mine located forty kilometres east of Marathon, Ontario. The Golden Giant mine is one of three gold operations exploiting the large gold orebody located in the Hemlo area. The milling facilities include two stage secondary crushing, three stage, closed circuit ball mill grinding with no reagents, thickening, cyanide leaching and carbon in pulp gold recovery unit operations. The average throughput is 3000 tonnes per day of 10 grammes per tonne gold ore. Figure 1.1 shows a schematic flowsheet of the operation."

Jan 1, 1989

By G C. Bolton

Experiments were conducted to access the feasibility of removing zinc from lead slag by sulfation or chlorination or both. Gaseous sulfation with sulfur dioxide and oxygen released only 50 per cent of zinc even under the most severe conditions. Sulfation with concentrated sulfuric acid by a fast-leach process released 95 per cent of zinc while pug-roasting released a maximum of 78 per cent of zinc. Chloridization with NaCl in the presence of sulfating gas released 50 per cent of zinc, while direct chlorination with chlorine gas and oxygen released 85 per cent of zinc and 100 per cent of lead in a chloride condensate containing little impurities.

Jan 1, 1980

By José A. Rios, José A. Vidalôn

The case study of a highland area in the Central Andes of Peru, where many abandoned polymetallic mines are found, is presented. Some of these mines generate metal leaching and acid rock drainage (ML/ARD) or have potentially ARD generating (PAG) tailings/waste rock storage. Effluents are discharged into the first of two lakes in line, which act as reservoirs for irrigating an important valley in the desert coastal region. Drainage fees, their relationship with the deposit and the solid-wastes mineralogy are discussed, as well as variations in water and sediments composition, the benthos, and the aquatic/riparian flora/fauna in these lakes.

Jan 1, 2000

By T. J. Lynch

A new class of polymeric dispersants for industrial minerals has been synthesized and evaluated. Currently available dispersants give initial low viscosities at high mineral loadings, however slurry viscosities can rapidly double or triple on standing over the first several days. The new dispersants give low initial viscosities that are more stable and maintain a lower viscosity for at least one month. The new dispersants are made possible by controlling the polymer molecular weight distributions during their manufacture such that essentially all of the dispersant is adsorbed onto the mineral surface, preventing depletion flocculation.

Jan 1, 2012

By Carlos Lam, Joram M. Amir, Erez I. Amir

"Abstract The modulus of elasticity of pile material (E) is an important parameter for the interpretation of both static and dynamic loading tests on piles. This value is commonly assumed to be constant with depth though it may not be true for deep bored piles due to the chosen casting method and/or selfweight consolidation. To provide evidence to support this proposition, the results of compressive strength tests on core samples taken from four different studies have been presented. The results show a marked increase in the strength and stiffness values with depth. The results of crosshole ultrasonic tests conducted at another site also confirm the same pattern. It is therefore recommended that before load testing a pile the distribution of the E values along the pile axis should be investigated. This will ensure the use of a realistic elastic modulus value and hence the correct interpretation of thedistribution between the shaft and end resistances.IntroductionThe modulus of elasticity of pile material (E) is an important parameter for the interpretation of both static and dynamic load tests on piles. Multiplying E by the strain measured by either strain gauges (e.g. ASTM D4945) or tell-tales (e.g. Geffen and Amir, 1971) gives the stresses acting at a given pile section. Typically, in the absence of better information, the value of E is derived from laboratory tests on concrete cubes or cylinder specimens taken on site and is assumed to be constant along the pile. While this may be correct for pre-fabricated concrete piles that are cast in horizontal molds, it may not be true for cast-in-place piles that are produced in the vertical position.There are at least two factors that may contribute to the change in concrete properties with depth in a bored pile. First, the casting methods may be by free fall in dry holes (e.g. Kiefer and Baker, 1994) or by using a tremie tube if support fluids are used. In the former case, the earlier batches reach the bottom of the pile bore at a higher velocity and are thus compacted under higher energy. Second, regardless of the casting method, the fresh concrete in the pile bore will always consolidate at least partially under its own self weight. The materials in the lower parts of the pile will therefore experience a higher consolidating pressure. This can reduce the pore volume and the water content in the wet concrete, thus changing the properties of the hardened concrete. Recent research by Justs et al. (2011) has shown that even a relatively small pressure can have a significant positive effect on concrete properties such as compressive strength and stiffness. However, the possible change of concrete properties with depth is commonly ignored by foundation engineers in the current design practice."

Jan 1, 2014

By S. P. Singh

Drifts are an integral component of underground mining. They provide access for men and material, means for transporting ore and rock and serve as air passageways. In view of their importance on the overall safety, economy and productivity of mines, empirical guidelines for controlled blasting design in drifts have been developed in this study. The application of the proposed concept was described by generating blast hole patterns for a mine with the help of a computer program. The mechanism of blast damage and the need for controlled blasting to alleviate ground control problems in underground mines have been outlined in this paper. The economic analysis between normal-and controlled blasting was performed based on the information from an operating mine. In addition, the review of drift blasting practices and problems in Canadian mines was also carried out in this study.

Jan 1, 1990

By Jewel Andrew Gomes

Arsenic is considered as one of the toxic materials being controlled by Environmental Protection Agencies in several developed and developing countries. It is found in the nature as constituents of the soil, minerals and also in various organic forms. It enters the air, water, and land from wind-blown dust and gets into water from runoff, leaching, soil erosion and anthropogenically from chemicals used for wood preservation, insecticides, medicine, military purpose, pigments, and electronic circuitries. There are several techniques available for removal of Arsenic, such as coagulation/filtration, lime softening, ion exchange, reverse osmosis, nanofiltration, wet chemical, and electrochemical. Electrocoagulation has been found as one of the most efficient techniques to remove inorganic arsenic with more than 99% efficiency. In this paper, we present our work on electrochemical treatment of both the inorganic and organic arsenic from water using various sacrificial electrode materials, i.e., iron, aluminum, copper, and combination of them. The floc produced by this method has been also characterized using XRD, SEM/EDS, FTIR, and cyclic voltammetry.

Jan 1, 2010

To George Orwell the year of 1984 was the inspiration for a book. To most New Zealanders it was the year that the fourth Labour Government was elected to power. It was also the year that the review of mining legislation commenced. While Orwell&apos;s book and the election of Labour are clearly events of some historic note, one could be excused for classifying the review of minerals legislation somewhat differently in terms of its present achievements! Since the review began it has led a tortuous path through a rapidly evolving policy environment to a point three years hence where no major policies have been determined.

Jan 1, 1987

By K. H. Brandt

A standard planning system for the development of roadways was adopted for German coal mines based on the results of geotechnical and rockmechanical investigations. Its goal is to provide for sufficient support systems under conditions of multiple seam mining at great depth. The report points out the required determination of geotechnical parameters and the basis for achieving a high level of planning reliability and resulting high performance in roadway development and longwall mining. The instrumentation and the planning procedure for selecting the support design most appropriate for the geotechnical conditions are described and demonstrated by examples.

Jan 1, 2004

By Randolph R. Dreher, Michael L. Schreder

"In recent years, FFE Minerals has designed, installed and commissioned several large grinding mill circuits. This paper discusses the issues related to the erection and commissioning of large grinding mill circuits. The three circuits discussed are Collahuasi in Chile, Minera Los Pelambres in Chile, and Century Zinc in Australia. These circuits include large SAG and ball mills with both gear and gearless drive arrangements, as well as, both trunnion and shell supported mills. Aspects of these features are discussed with respect to their impact on installation and commissioning. While the normal challenges of mill erection and start-up were experienced, there were also a few unexpected challenges encountered partly due to the large scale of the equipment. An overview of the equipment and design ratings of these circuits is also provided.COLLAHUASIOverviewThe Collahuasi mills were started-up in November of 1998. The site is located in the Andes Mountains at an elevation of 4300 meters. The grinding circuit includes two lines featuring one SAG mill and one ball mill for each line. The circuit features a recycle conveyor around the SAG mills with provision for adding a pebble crusher in the future. The design tonnage of the grinding plant is 60,000 MTPD with an ore BWI of 10.5 kWh/MT.The SAG mills are 32’ x 15’ (1 3’ EGL) with 10,800 HP drives. The drive arrangements are dual pinion through pneumatic clutches. The mills are driven by low speed synchronous motors with CCV variable speed drives. The SAG mills are trunnion supported and use hydrostatic lubrication. Feed to the SAG mills is via a rock-box type feed chute on a cart. The mills discharge on to trommel screens with a bucket wheel to remove the oversize.The ball mills are 22’ x 36.5’ (36’ EGL) with 12,500 HP drives. The drive arrangements are dual pinion through pneumatic clutches. The fixed speed mills are driven by low speed synchronous motors with GE Quadramatic load sharing drives. The ball mills are shell-supported and feature multi-pad bearings with hydrodynamic lubrication. The mills are fed via a rubber lined sump box with feed spout on a cart. The ball mills also discharge on to trommel screens. Twenty-six inch (26”) diameter hydrocyclones are in closed circuit with the ball mills."

Jan 1, 2001

By J. R. Thoenen, J. L. Vallely, M. C. Malamphy

"SUMMARYMagnetic and gravimetric surveys wore conducted over an area of ap¬proximately 1,400 square miles in the bauxite district of central Arkansas. The primary purpose of these surveys was to discover any possible buried and hitherto unknown syenite masses favorable for the occurrence of bauxite and to determine the approximate position of the buried flanks of the known syenite masses which might offer conditions favorable for the discovery of new ore bodies.Those surveys indicated that the various syenite outcrops were domes or bosses on a large batholith and that ether similar domes occurred on the batholith but did net outcrop.Drilling on the local geophysical anomalies proved the presence of 10 buried domes, but only 2 of them were found to project above the upper surface of the Midway clays, a requisite of conditions favorable for the occurrence of bauxite ore bodies. The geophysical data indicated the approximate configuration of the buried flanks of the known syenite coutcrops, and the portions of these flanks that project above the Midway have now been outlined more accurately by drilling.The geophysical surveys have produced evidence permitting the elimi¬nation of a large area as unfavorable for the occurrence of bauxite.Magnetic surveys extending along the Midway-Wilcox contact from Gurdon, in Clark County, on the southwest to Searcy, in White County, on the northwest have proved the improbability of the existence of other syenite masses similar to those found in Pulaski and Saline Counties. A detailed magnetic survey of the Magnet Cove area in Hot Spring County has proved that the syenite mass exposed in that locality is an isolated intrusion and entirely unrelated to those of Pulaski and Saline Counties. This syenite mass does not occur under conditions believed to be favorable for the occurrence of bauxite."

Feb 1, 1945

By John Wilson

"The Rietveld numerical method was used to calculate the relative abundances of phases in both synthetic binary mixtures and synthetic and natural ores, using X-ray diffraction data. The results were compared with those of image analysis and a chemical method. The ranges of the relative errors were estimated. The Rietveld method is found to be acceptable for determining the abundances of major and minor phases and the amorphous component of partially crystalline samples. In complex mixtures, where there are several trace phases (~<2 wt%) present, the technique becomes less accurate. It is most useful as an alternative technique to image analysis when sample preparation is problematic or sample particle sizes are sub-micron. It is a manual method which requires user input during the fitting process, but is both simpler and faster than image analysis due to the reduced set up time and sample preparation required. It is now implemented at CANMET as a technique for quantitative analysis.INTRODUCTIONUntil recently, the Applied Mineralogy group at CANMET used only image analysis and chemical techniques to determine phase quantities. An effort to develop quantitative X-ray diffraction (XRD) has been on-going for several years. Initially, the reference intensity ratio (RIR) method with external standards was tried with some success (Szymanski and Petruk, 1989). The main difficulty with this technique was finding adequate standard material for each phase present in the sample. This shortcoming made the method ultimately impractical, given the wide variety of materials which come to the laboratory for analysis.The Rietveld refinement method of quantitative XRD (Hill et al 1993, Mumme et al 1996), in contrast, requires no standards and requires minimal sample preparation and therefore a more rapid turnaround compared to image analysis. The Rietveld method also has advantages over image analysis in that it can identify and quantify polymorphs, ultra fine materials and many types of hydroxide products. As well, it is useful for analyzing materials such as bauxite or talc, which do not polish well enough for making mounts of the quality required for image analysis. To quantify amorphous material and phases which are present in amounts below the detection limit of XRD, the addition of a standard material is still required. However, in such cases only one standard is needed, which is alumina."

Jan 1, 2003