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By Ananda Moreira Vaz Ourique de Avila

Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells (SOFC) interconnects, replacing the ceramic materials. However, at high temperatures, on the order of 700-850 0C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the SOFC. Thus, the knowledge on kinetics of oxidation/corrosion of these steels and their relationship with the microstructural transformations are of great importance. In this study, samples of ferritic stainless steels AISI 430, AISI 441 and Crofer22APU® were tested for oxidation at high temperature (800 0C) for long periods of time (up to 3,600 hours) and mass gains were monitored allowing the determination of the oxidation behaviors of these steels. Additionally, the microstructural characteristics of the samples before aging (corrosion-oxidation test) and after various oxidation times were evaluated by optical (OM) and scanning electron microscopy (SEM), as well as by micro chemical elemental analysis (EDS) and X-ray diffraction (XRD) phase analysis. Electrical characterization allowed determination of electrical area-specific resistances (ASR) characteristics of the systems studied, thus relating the electrical and oxidative behaviors of steels evaluated.

Aug 7, 2018

By Otaviano Donizeti Valadão de Freitas

Ruídos elétricos afetam os circuitos lógicos e conseqüentemente podem comprometer a confiabilidade nos controles de processos, e para minimizar as influências desses ruídos, algumas medidas básicas foram tomadas, com instalações adequadas de todo o sistema, como padronização do aterramento, encaminhamento de cabos, etc. Depois que as medidas foram implementadas, o resultado foi um sistema mais confiável. Se apenas um fio for encaminhado de forma incorreta ou se o aterramento estiver inadequado, pode ser suficiente para causar problemas. A experiência mostra que é muito difícil que todas as medidas sejam aplicadas integralmente, mas se não forem tomadas pelo menos as medidas básicas, o sistema ficará suscetível.

Sep 25, 2017

By Rudolf Hubmer

In October 2013 JSW Steel decided to place an order to Primetals Technologies Austria (former Siemens VAI Metals Technologies) for the installation of a comprehensive Level 2 process optimization system for more than 20 existing production facilities of various suppliers. For SMS-I new L2 systems are provided for two hot metal pretreatment stations, three hot metal desulphurization stations, three ladle furnaces, two 1-strand slab casters, a ladle tracking system as well as a shop supervisory system. Additionally the existing L2 system for one 1-strand slab caster is being upgraded in the course of the project. In SMS-II new L2 systems for the 7 hot metal desulphurization stations, 4 ladle furnaces, 1 new RH vacuum degasser, ladle tracking system and a shop supervisory system are supplied. Despite of the challenging time schedule the commissioning of the single facilities started within less than 12 month after contract effectiveness. The installed Level 2 process optimization systems together with the achieved results are described in this paper.

Aug 16, 2017

By Michael Windhager

UltimaTM rolls have been designed for intermediate and finishing stands of rod and bar and small and medium section mills. The rolls and rings are spun cast, with a highly alloyed working layer and a tough nodular iron core. Microstructure and hardness level can be adjusted over a wide range, which allows us to adapt the rolls to differing rolling conditions. After introducing the UltimaTM concept, this paper will describe the results of UltimaTM rolls achieved in various mill applications, like finish rolling of rebar, and slitting. Special emphasis is given to performance gains when using UltimaTM rolls, compared to standard rolls. This paper also examines the impact of UltimaTM rolls on mill and roll shop productivity.

Jul 30, 2018

By Raúl Daniel López

Ternium-Siderar steelmaking has been focused in permanent improvements and process optimization. At present the Slab Continuous Caster N°1 has been totally transformed after 20 years of uninterrupted work. The authors of this paper summarize and comment on aspects which were the main changes and place emphasis largely on those technological developments in which they have been active during that period. Productivity and quality have been our goals during the last 20 years; it has led us to improve process and to achieve better control tools. In the development of this presentation, the authors will put special emphasis on the explanation of those works that were made following their own experiences through the technical personnel who belong to the staff of the company.

Jul 30, 2018

By Gilberto Álvares da Silva

New elements have been inserted in NiTi lately, resulting in ternary alloys with specific characteristics beyond Shape Memory Effect and Superelasticity. Among all others alloying elements, the Ag additions itself gives potential antibacterial activity to that smart material. So on, the elaboration procedures of ternary NiTiAg alloys was studied in order to obtain a melting procedure to ensure further studies on this alloy. Microstructural and thermal analyses were used to evaluate the VAR-remelting production of NiTiAg with 4.0% wt silver content. The microstructure is composed by a NiTi matrix, pure Ag precipitates, and, scarcely, TiC inclusions. Heat treatments at high temperature could not dilute those Ag particles, but could lead to the precipitation of new ones. The silver element reduces the temperature of the martensitic transformation, yielding a material with superelastic behavior, beyond induces the R-phase on cooling stage of this alloy.

Aug 8, 2018

By Dilermando Nagle Travessa

High strength-light weight materials are very attractive for the transportation sector, particularly to the aerospace industry. High strength-age hardenable aluminium alloys are widely used in airframes due to their unique combination of strength, density, toughness, corrosion resistance, cost and easy processing. However, the hardening capacity of such alloys is somehow saturated due to thermodynamic issues related to the conventional processing. The production of aluminum-matrix composites is a promising strategy to overcome this limitation, resulting in strength levels that cannot be reached by actual commercial aluminum alloys. In the present work, multiwall carbon nanotubes were used to reinforce the AA6061 aluminium alloy. 1 and 2% weight percent of MWCNT were mixed to the alloy powder by high-energy ball-milling process. The blended powder was consolidated by hot extrusion. The obtained composite bars were submitted to heat treatment for the T6 condition in order to combine both CNT dispersion and precipitation hardening effects. Optical and scanning electron microscopy, as well as hardeness testing, was used to characterize the bars. Typical wrought microstructure, free of defects, was observed on the extruded bars. Hardness of the composites was observed to increase by 20, 28 and 68% for 1% MWCNT 6 h milling, 2% MWCNT 6 h milling and 2% MWCNT 10 h milling, respectively, in the as-extruded condition. The better performance for the composites blended at higher milling time was attributed to a better nanotubes dispersion. Subsequent heat treatment to the T6 condition did not result in additional hardening.

Aug 8, 2018

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the ex-service condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 52 to 224 MPa producing rupture times varying from 5 to about 3950h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results obtained on a similar plate of the same material in the virgin condition.

Aug 16, 2017

By Francisco Morganti

This report gives in the first part the metallurgical basics for the production of AHSS grades in integrated steel plants starting at the melt shop and ending at the annealing lines of the cold mill. The corresponding process and plant technologies in each production step with its specifics and rules are explained. In the second part by way of example the practical requirements for TRIP 780 steel grade are highlighted like a recipe for process control in the steel plant, hot and cold rolling mill, annealing line and finally skin pass mill. Measuring of mechanical technological properties on samples shows that the specifications according to DIN EN 10268 are fulfilled.

Oct 30, 2017

By Humberto Tronconi Coelho

The use of friction dampers are wide proposed for a variety of mechanical systems for which it is not possible to apply viscoelastic materials, fluid based dampers or others viscous dampers. An important example is the application of friction dampers in aircraft engines to reduce the blades vibration amplitudes. In most cases, friction dampers have been studied in a passive way, however, a significant improvement can be achieved by controlling the normal force in the contact region. The aim of this paper is to study four control strategies for friction dampers based on three different hysteresis cycles. The first control strategy maximizes the energy removal in each harmonic oscillation cycle, by calculating the optimum normal force based on the last displacement peak. The second control strategy combines the first one with the maximum energy removal strategy used in the smart spring devices. Finally, is presented the strategy which homogenously modulates the friction force. Numerical studies were performed with these four strategies defining the performance metrics. The best control strategy was applied experimentally. The experimental test rig was fully identified and its parameters were used for numerical simulations. The obtained results have shown the good performance for the friction damper and selected strategy, also, the agreement between numerical and experimental results.

Jul 31, 2018

By Mühlböck Marlene

Increasingly stringent global environmental regulations are forcing steel producers to continually improve the efficiency of sinter waste gas treatment. With the Selective Waste Gas Recirculation (SWGR) system from Primetals Technologies, lower production costs can be achieved and the size of downstream waste gas cleaning units can be reduced for investment savings. SWGR features the extraction and reuse of hot sinter off gas from selected wind boxes along the sinter strand, which contributes to improved energy efficiency and off gas treatment in the sintering process. With the next generation of SWGR, Primetals Technologies can provide an energy optimized, emission optimized and environmentally friendly solution that meet customer requirements and country specific regulations. This paper demonstrates the latest developments in selective waste gas recirculation, especially results from pot grate tests and comparison from lab to real plant data. Furthermore theoretical finding and mathematical modelling is presented.

Aug 16, 2017

By Mingyu Ma, Lingling Liu, Liqing Chen, Houlong Liu

In this article, a 444-type heat-resistant ferritic stainless steel containing 0.05wt% Ce and 2wt% (Mo+W) was used as an experimental material and a study was carried out on the effect of rolling processes on the microstructures and texture evolution as well as on the mechanical properties and formability. The rolling processes contain hot rolling at different hot rolling finish temperatures, annealing after hot rolling, cold rolling and subsequent annealing. As for the hot rolling process, two hot rolling finish temperatures, 860 C and 770 C, were adopted, and their influence on the microstructures and mechanical properties was comparatively studied. The results showed that the microstructures after hot rolling and subsequent annealing could be refined by lowering the hot rolling finish temperature. The resultant microstructures after cold rolling and annealing were hereditarily refined. Lowering the hot rolling finish temperature can weaken the -fiber texture in hot rolled or cold rolled ferritic stainless steel strip. However, the -fiber texture was homogeneously strengthened by annealing the cold rolled ferritic stainless steel strip. Enhanced mechanical property and formability in terms of strength and average plastic strain ratio could be obtained by lowering the hot rolling finish temperature of ferritic stainless steel.

Oct 1, 2019

By Carlos Gonzalez-Rivera

An alternative cooling curve analysis method focused on the experimental determination of the latent heat of phase changes and phase transformation kinetics is proposed in this work. The method analyses the cooling process of a metallic sample, initially liquid that is contained into a cylindrical metallic mold, both of known weight, thermally isolated at its top and bottom. The method is based on an energy balance associated with the experimental measurement of the temperature change of the sample and the mold during their cooling process. From the numerical processing of the cooling curves, are obtained approximate values of the acting global heat transfer coefficient as a function of temperature in order to describe quantitatively the energy exchange of the metal/mold system with its surroundings. These relationships and other experimental data are used to process the cooling curve of the sample and the mold during solidification, in order to obtain the latent heat of solidification.The method was applied experimentally to zinc and tin of commercial purity, initially liquids and contained into stainless steel molds in order to determine its ability to measure the latent heat of solidification. The obtained results suggests that this method shows a good potential to characterize the solidification of metals.

Oct 30, 2017

By Torben Ulisses da Silva Carvalho

A têmpera é um dos tratamentos térmicos mais utilizados nos aços, visando o aumento de sua dureza a partir de mudanças drásticas em sua microestrutura. A fim de aliviar as tensões provindas desse tratamento, realiza-se o revenido, fazendo com que o aço obtenha propriedades mecânicas viáveis ao uso. Este trabalho teve como objetivo realizar os tratamentos térmicos de têmpera em água, salmoura e óleo e, posteriormente, o revenido no aço SAE-4140 fornecido pela SINOBRAS, uma siderúrgica de Marabá-PA. Foi realizada a caracterização microscópica das amostras antes e depois dos tratamentos, sendo possível visualizar as mudanças na microestrutura do material, além da confirmação do aumento de resistência mecânica através do ensaio de dureza.

Aug 16, 2017

By Ana Carolina Fernandes Reis

O objetivo do trabalho foi investigar a recuperação metalúrgica da flotação de sulfeto de ouro utilizando diferentes tamanhos de partículas, a partir de ensaios de moagem e flotação em bancada, visando analisar o melhor desempenho e seletividade do processo. O minério em estudo apresenta um teor médio de ouro de 5,28 ppm e 0,59% de S. Nos testes verificou-se uma correlação diretamente proporcional entre a recuperação mássica e metalúrgica, ambas mostraram-se inversamente proporcional a seletividade no concentrado. A granulometria com 90% passante na malha de 0,053mm obteve o melhor resultado de recuperação tanto do ouro como de sulfetos, em contra partida, apresentou o menor grau de seletividade.

Aug 16, 2017

By Caroline Gomes de Oliveira

Os impactos causados pela exploração dos recursos naturais pelo homem geram uma crescente inquietação em relação futuro do planeta a longo prazo. Assim, as fibras naturais vegetais ganham destaque como material de reforço por suas boas propriedades mecânicas, baixo custo e por serem biodegradáveis. Umas das fibras que mais ganhou destaque nas últimas décadas é a fibra de rami, objeto de inúmeros estudos. Neste trabalho, analisou-se o efeitodo tecido produzido com a fibra de rami como reforço para a matriz epóxi sob esforços de impacto Charpy e Izod. A metodologia utilizada foi a produção de placas laminadas sob afeito de vácuo. Os resultados mostram notável diferença na resistência ao impacto do compósito comparado à matriz sem reforço.

Oct 30, 2017

By André de Albuquerque Vicente

Observou-se porosidade de Kirkendall em juntas soldadas dissimilares de liga Fe-Cr-Al do tipo 23Cr-7Al, e aço inoxidável austenítico AISI 310 (25Cr-20Ni). Utilizou-se como consumível de soldagem a própria liga Fe-Cr-Al. O processo de soldagem utilizado foi o GTAW. Caracterizaram-se 3 conjuntos de corpos de prova soldados com diferentes energias de soldagem, antes e após o tratamento isotérmico a 1150oC por 936 horas ao ar. Nos corpos de prova tratados termicamente, observou-se a formação de poros bem como significativas variações dos teores de Al nos metais depositados e formação de camada protetora de alumina nas superfícies oxidadas.

Oct 30, 2017

By Lidia Rangel Roveta

O processo de aciaria da ArcelorMittal Aços Planos América do Sul tem um abastecimento de diário de Cal em torno de 420 ton. O processo de abastecimento deste produto, que consiste da programação, liberação de portaria e descarregamento não estava satisfatório, considerando o tempo de permanência de caminhões na portaria aguardando liberação e consequentemente custos com diárias e alimentação. Visando otimizar este processo, a partir do resultado da analise dos procedimentos de descarga, utilizado atualmente, foi implementado como plano de ação um sistema automatizado de agendamento de descarga de Cal que, após 15 dias de implantação resultou na redução de 66% no custo de pagamento de diária, além de previsão de ganho futuro em frete.

Aug 16, 2017

By Andressa Pereira dos Reis Croucillo

O desenvolvimento de impressoras 3D permitiu uma maior produção de peças e próteses médicas provenientes de polímeros termoplásticos como PLA e ABS, para produção de filamentos. Este trabalho avaliou as características mecânicas de próteses impressas, em determinada temperatura, de filamento PLA. Foram impressos diversos corpos de provas, para a realização de testes de tração, verificando que a configuração com densidade 100%, espessura de 0,4 mm e direção de impressão de 45° e 135° apresentou melhor resultado de resistência mecânica. Realizaram-se também, simulações matemáticas para análise de resistência à queda e flambagem. O conjunto de testes físicos e matemáticos determinou que o PLA não atendeu os requisitos para aplicação deste como próteses.

Oct 30, 2017

By Rodrigo Alberto Moreira Gomes

São apresentados os resultados da instalação de uma câmara de combustão compacta para a substituição de óleo combustível por coque de petróleo, em um sistema de secagem e moagem de minério de níquel denominado Usina Sul, instalado na Unidade de Niquelândia – GO, da Votorantim Metais. Esta nova câmara de combustão, desenvolvida em parceria com a Dynamis Engenharia e Comércio, atingiu eficiências de queima acima de 95% (comprovada por medições realizadas em Planta Piloto). Além de elevada eficiência de combustão, esta câmara compacta possibilitou que se atingisse o patamar de 100% de substituição de óleo por coque de petróleo, representando ganhos significativos no custo da Unidade. Ganhos também foram observados na vida do refratário da câmara existente, denominada câmara VMN.

Jul 31, 2018