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By G. B. Shea

The accident experience of the California petroleum industry for 1927 was characterized by a decrease it .the number of fatalities. The year closed with a total of 41 fatal accidents, as compared with a total of 54 for the preceding year. 3 In percentage, the figure for 1927 represents a decrease of 24 per cent from that of 1926 and evidences the promising results of organized safety work, in which the industry in California has taken an absorbing interest. The percentage of decrease for 1927 is the largest recorded in any one year since the compilation of the fatality record in the California petroleum industry was begun. Although good progress has been made during the past few years, much remains to be done to reduce still further the human and economic waste caused by accidents. This review is intended to show the employee, as well as the employer, the proximate and contributing cause of accidents. To increase the value of the report, preventive measures in various instances are suggested, on the theory that accidents of a similar nature will occur unless remedial action in taken to remove the cause.

Jan 1, 1928

By F. S. Crawford

Safety devices and guards are often looked upon as the last word in safety by the men around the shop or large industrial plant . However , thorough knowledge of the details of their jobs and of the dangers attending them are even more important . It should be unnecessary for all men to go through the experience of the first man to meet an unknown danger , but that appears to be about the only way by which many learn . Practically every danger connected with the job around a mine , blast furnace , steel mill , foundry , coke oven , cement mill , or other operation , was encountered for the first time by someone , and if he was fairly fortunate he either got hurt or just missed being injured and lived to tell his " budaies " how it happened; he spread the knowledge of that particular danger . Sometimes , but not often , a man can foresee a danger . If he could always be on guard and remember everything he had ever learned and also know everything that had happened to the other fellow , and then let that knowledge keep him aware of the dangers in his own immediate " job , " so that he would work the safe way for both himself and the other fellow , he would have what safety engineers call " safety consciousness . " Being safety conscious is a fine attribute , as it really means knowing all about one's job . A man who is really safety conscious is one of the best and most efficient workmen in the whole plant . The boss wants men of that kindmen who want to learn and who try to learn every little detail about their jobwhere there is danger of spoiling the heat or getting burned by hot metal in a steel plant or of loading rock instead of coal or ore in a mine . Such men know how to do whatever job they are on easily and with the least amount of hard work and at the same time get it done as quickly as possible with safety . A man who is safety conscious has to nearly all intents and purposes developed eyes in the back of his head , if he is in a big mill where there if something going on all around him . These eyes are not real eyes , but they are what might be termed a sixth sense which he has developed by his experience in the mill as well as in other dangerous work which he may have done before in other plants . There may be occasions when a man's safety consciousness will leave him for just a short time ; this is likely to happen when he is thinking about a quarrel he had with his wife which has not been cleared up happily , or perhaps when he has bought too many things on installment and with sickness at home

Apr 1, 1931

By P. C. Good

Work was done to determine conditions necessary for efficient electrodeposition of aluminum from fused chloride electrolytes. Aluminum was deposited from a molten chloride salt electrolyte over a temperature range of 150° to 750° C. At lower temperatures in a heat-resistant glass cell, aluminum was deposited on stainless steel and on aluminum cathodes. The deposit was recovered in the form of light, feathery dendrites that could not be consolidated. At 750° C, molten aluminum was deposited at cathode current efficiencies as high as 90 to 100 percent on titanium diboride cathodes and in molten aluminum cathodes. Nitride-bonded silicon carbide was the best cell material, although porcelain was also used. The electrolyte consisted of a mixture of sodium and potassium chlorides in 1 to 1 mole ratio, containing aluminum chloride in concentrations ranging from 2 to 30 weight-percent in cells holding up to 1,000 grams of electrolyte. Generally favorable results were attained in studies made at temperatures greater than the melting point of aluminum.

Jan 1, 1966

By T. J. McDonald

The methods used and the results obtained in the application of high-expansion foam on a recent fire in an operating mine in western Pennsylvania were reviewed. This is the first instance where foam has been applied extensively to a fire under actual mining conditions although considerable research has been conducted and experimental fires have been controlled. The Bureau of Mines began investigating the foam-plug technique in 1957 in its experimental coal mine, following reports of successful trials in Eng-land, where the basic methods, using the normal ventilating current, were developed. Early in the research it was apparent that the normal ventilating current in mines in the United States would not provide adequate air pressure to drive a foam plug the distance that might be required. Subsequently, the Bureau of Mines developed a portable high-expansion foam generating unit consisting of a fan having relatively high pressure potential, net, sprays, and metering equipment. To date, foam generators have been constructed by the Bureau, by at least one operating coal company, and by one manufacturer of safety equipment. A number of units from the latter supplier have been adopted by coal-mining companies as an integral part in their firefighting installations.

Jan 1, 1961

By A. Visnapuu

The U.S. Bureau of Mines investigated the oxidation of American Iron and Steel Institute (AISI) Type 304 stainless steel (SS) during annealing in simulated combustion products from several air-CH4 fuel ratios. Atmospheres representing air-CH4 ratios of 14:1 and 18:1 contained free 02, while atmospheres representing 10:1 air-CH, ratio did not. A Cr203 layer formed on SS samples annealed in atmospheres containing free 0, while a Cr-Fe spinel layer formed in atmospheres with no free 02. The Cr203 layer was adherent and presented a protective barrier to metal diffusion, effectively limiting oxidation of the metal substrate. The Cr-Fe spinel was not protective and allowed the diffusion of Fe through the spinel to the gas-oxide interface where it was oxidized to magnetite, which spalled from the surface. This resulted in thick scale layers on samples annealed in atmospheres containing no free 02, as compared to layers formed on samples annealed in atmospheres containing free 02. These results confirmed and explained industrial operators' observations that thick, smoky (fine spalled magnetite) scales form on SS annealed in low free-02 atmospheres, while thin protective oxide layers form on sheets in atmospheres containing free 02.

Jan 1, 2010

By D. Harrington

"While distribution of air currents to working faces is a necessity in coal mines, especially those having explosive gas, advancing faces in metal mines rarely have circulating air other than the ordinarily inadequate amount supplied through the compressed air system. Even where comparatively large quantities of air pass through main mine shafts and levels. whether the circulation is actuated by fans or by natural ventilation, only occasionally can a metal mine be found where any considerable percentage of the ""blind ends"" has circulating air of sufficient velocity to be measured by an anemometer or even be discerned by deflection of flame of candle, or of acetylene lamp; and unfortunately these ""blind ends"" include nearly all of the places from which rock is taken.During several years study of metal-mine ventilation in various mining districts of the United States, it has been found that in some mines many of the workers in ""blind ends"" practically continually breathe air with 0.02 to 0.04 per cent of CO gas from unremoved fumes from explosives; in other mines CO2 chiefly from timber decay and breathing of men, is so high that a candle will not burn though usually the acetylene lamp will, hence oxygen is below 17 per cent but above 12 per cent; in some regions CO2 from strata fills the entire mine forcing cessation of work; in other mines in dead ends, gases such as nitrogen, H2S, SO2, etc., are found under some conditions. In many regions with hot rock or water (especially in deep workings) men in blind ends must work with little or no circulation, in air above SO degrees F. and even above 90 degrees, relative humidity only too frequently being around 100 per cent; in other regions workers in blind ends in practically ""dead"" air must continually breathe enormous quantities of finely divided rock dusts. All of the above conditions are decidedly harmful to health and prevent the worker from delivering anything approaching an adequate quantity of work, and in addition, some of these conditions have direct or indirect effect in bringing about definite increase of accidents; all of the above mentioned bad conditions in ""blind ends"" in metal mines as well as their ill effects, are remediable by providing at those places adequate quantities of fresh circulating air."

Nov 1, 1923

By S. J. Page, W. E. Wallace, P. Bolsaitis, D. Eppelsheimer, M. J. Keane, J. Poston, J. Harrison

"Respirable-sized dust particles from a clay mine and mill were examined for aluminium and silicon content by scanning electron microscopy-energy dispersive X-ray analysis at incident electron energies of 5--20 keV. Most of the high silica content particles, those which had a silicon to silicon plus aluminium signal fraction, measured at 20 ke V, of0.9 or greater, showed a decrease in the silicon fraction of signal with decreasing incident electron energy, down to values of between 0.6 and 0,8 at 5 keV: this decrease was a function of particle size and composition. Simple models for silicon fractiol) of signal vs incident electron voltage suggest this behavour is due to a heterogeneous particle structure in which an aluminosilicate coating occludes the surface of a silica particle core. The coating survives incubation in a major component of pulmonary surfactant.INTRODUCTIONMINING and some other dusty workplace atmospheres are monitored for respirable dust and quartz dust for purposes of occupational health protection, respirable quartz dust being a known cause of pulmonary disease. Respirable quartz exposure data are acquired also for epidemiological research on the correlation of pulmonary disease prevalence with respirable dust composition and concentration. For these purposes quartz content often is measured on collected dust samples by X-ray diffraction or in spectroscopy. Scanning electron microscopy-energy dispersive X-ray analysis spectrometry (SEM-EDX) is also used. The first two methods measure the bulk composition of a multi-particle dust sample; SEM-EDX measures the elemental composition of single ·particles. These methods as typically applied, including SEM-EDX with a 20-30 kilo-electron volt (keV) electron beam accelerating potential, do not distinguish homogeneous distribution of impurities in a particle from possible heterogeneous surface distribution. These measurements of quartz content are not always accurate predictors of the prevalence of dust-induced disease (ROBOCK and BAUER, 1990), which implies that the biologically available quartz surface may not be equivalent to conventionally measured quartz content of respirable dust in some exposure settings. Using a minor modification of conventional scanning electron microscopy-energy dispersive X-ray analysis (SEM-EDX) protocols on samples of settled and airborne dust from a clay mine and mill we have detected heterogeneity with depth for aluminium impurity in high silica content particles, indicating that some of the quartz or 'free silica' respirable particles of the dust are aluminosilicate occluded. Coatings were not removed by incubation of the dust in a surrogate pulmonary hypophase surfactant fluid."

Jan 1, 1990

By John C. Edwards

The Bureau of Mines has developed a time-dependent mathematical model of radiative heating of bulkheads in mines. The model includes both reradiation from the duct (cylindrical) walls and direct radiation from the fire zone. Thermal loss into the wall of the duct and into the bulkhead is included. Both brick and wood bulkheads are considered. It is found that the heating rate of the system scales as the duct length-to-diameter ratio and the flame temperature. In particular, the time required for the irradiated surface of the bulkhead to reach a specified temperature decreases with increasing flame temperature for a fixed length-to-diameter ratio and increases with increasing length-to-diameter ratio for a specified flame temperature. It is also deter-mined that the time, T, for the bulkhead surface temperature to reach a specific value, Tb, for a fixed length-to-diameter ratio less than 4 and for a flame temperature of 1,200 K is approximately linearly dependent on Tb for 500 K < Tb < 700 K, and is nearly exponentially dependent on the length-to-diameter ratio for Tb = 600 and 700 K.

Jan 1, 1979

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Jan 1, 2012

By Will H. Coghill

Recent work on beneficiation of the .Alabama red iron ores and ferruginous sandstones has brought out interesting new facts on particle-size reduction that axe a valuable supplement to what is already known.4/ The work was done by the Southern Experiment Station of the Bureau of Mines in cooperation with-the University of Alabama, University, Ala., on two samples from the Birmingham district. One was an oolitic red iron ore containing about 35 percent iron; the other was a ferruginous sandstone containing about 25 percent iron, particularly attractive because of its low phosphorus content. In both samples rounded quartz (sand) grains were embedded in an oolitic, "onion skin" matrix of hematite. The hematite carries varying amounts of clay, which limits the grade of concentrate that can be made. The clayey hematite is soft, so that the rock crumbles readily under pressure. The sand grains shell out like corn,, and without much exaggeration the mill used for differential grinding might be called a "sheller,"

Jan 1, 1940

By Will H. Coghill

Recent work on beneficiation of the .Alabama red iron ores and ferruginous sandstones has brought out interesting new facts on particle-size reduction that axe a valuable supplement to what is already known.4/ The work was done by the Southern Experiment Station of the Bureau of Mines in cooperation with the University of Alabama, University, Ala., on two samples from the Birmingham district. One was an oolitic red iron ore containing about 35 percent iron; the other was a ferruginous sandstone containing about 25 percent iron, particularly attractive because of its low phosphorus content. In both samples rounded quartz (sand) grains were embedded in an oolitie, "onion skin" matrix of hematite. The hematite carries varying amounts of clay,-which limits the grade of concentrate that can be made. The clayey hematite is soft, so that the rock crumbles readily under pressure. The sand grains shell out like corn,, and without much exaggeration the mill used for differential grinding might be called a "sheller,"

Jan 1, 1940

By R. K. Koch

In seeking substitutes for such critical metals as chromium, cobalt, and nickel, the Bureau of Mines investigated techniques for shape-casting titanium in rammed sand molds. Castings were made in olivine, garnet, chromite, and, for comparison, zircon. It was found that commercial-grade castings up to 31 lb (maximum capacity of furnace) could be made in zircon or olivine molds if a zirconia mold wash was used. Castings up to 4 lb could be made in chromite molds, but heavier castings suffered from some mold-metal reaction. Garnet molds were found to be unsatisfactory for castings of all sizes because of gas blows and rough surfaces. In other tests shell castings of acceptable quality were produced in water-glass-bonded zircon and olivine molds up to weights of 8 lb, but chromite molds were unsatisfactory because rough casting surfaces were caused by mold-metal reaction. Unlike the currently used commercial processes, neither the rammed-sand nor the shell-molding processes developed by the Bureau of Mines generate noxious fumes at any step.

Jan 1, 1980

By H. J. Heinen

The Bureau of Milts studied repetitive batch electrowinning of molybdenum from molybdic oxide ) to determine the effects upon the electrolyte life, purity of metal product , and overall cell performance. The electrolyte consisted of 54.0 weight-percent sodium tetraborate (Na2B407), 23.6 weight-percent sodium chloride (NaC1), 14.9 weight-percent sodium fluoride (NaF), and 7.5 weight-percent Mo03. The feed materials were pure and technical-grade Mo03. Electrolysis was conducted at l,000° C in a graphite cell in an atmosphere of air and carbon oxides. Electrolyte degradation did not occur during repetitive winning of molybdenum from pure Mo03 in an 8-day (5,400-ampere-hour) period of operation. Electrowon metal contained <0.1 percent total impurities. The electrode configuration is a key factor in the direct conversion of technical-grade Mo03 to metal by repetitive cyclic electrolysis. The best configuration found was a cathodic crucible and a central anode. Metal purity of 99.8 percent and a current efficiency of 91 percent were maintained until the combined impurity buildup the electrolyte reached 4.7 percent silicon, l.0 percent aluminum, and 0.6 percent iron. One pound of molybdenum was produced per 1.5 pounds of solvent salts employed. About 25 percent of the initial NaCl and NaF contents of the electrolyte were lost owing to volatilization and crucible penetration.

Jan 1, 1966

By Charles K. Rose

This paper presents some research studies of the rotary drilling of oil shale at the Bureau of Mines Oil-Shale Mine, Rifle, Colo. The experimental procedures and the rotary drill test equipment are described. Theories of rock drillability, rotary bit cutting action, and bit design are presented and discussed. The actions of various bit designs are analyzed and compared with the observed results of actual drilling tests. A cost estimate is made for drilling Colorado oil shale.

Jan 1, 1955

By Fred Kissell

The Bureau of Mines has developed the shearer-clearer--a new type of dust control system for longwall shearers. The system partitions the airflow around the shearer into a clean split and a contaminated split. The dust cloud is confined to the vicinity of the coal face, while the shearer operators remain in the clean split on the gob side of the machine. The shearer-clearer operates on the principle that each water spray moves air like a small fan and can be positioned to direct the dusty air towards the face. The hardware is inexpensive and can be installed in a single shift. It consists of several strategically mounted water sprays and one or more passive barriers. Laboratory testing indicates reductions 1n shearer operator dust exposure as high as 97 pct. Preliminary results from an underground demonstration in one mine also indicate that considerable dust reductions at the shearer may be obtained. In conjunction with the development of the shearer-clearer, dust surveys were conducted in three other mines to determine if some shearer spray systems currently in use partition the flow in a manner similar to the shearer-clearer, and if so, whether this partially accounts for markedly cleaner conditions on some longwalls. Results from these surveys indicate this to be the case. A feature of the cleaner longwalls was a downwind orientation of their water sprays, which is a key element of the shearer-clearer system. The shearer-clearer system described in this report was designed for an Eickhoff EDW 300 shearer working a 7-foot coal seam. The testing to date has concentrated on cutting directions counter to the primary airflow. The development effort continues for different mining equipment and conditions. It is expected that different systems will be required to accommodate the range of conditions occurring underground. Application of the system presented here to conditions different than those described is not likely to produce the same results.

Jan 1, 1981

By Ivan L. Nichols

Tailings dumps at Mercur, Utah, contain about $7 million worth of gold in 3.5 million tons of mill tailings assaying about 0.07 ounce of gold per ton. Commercial mining and milling at Mercur ceased in 1942. To determine whether improved technology was now available that might permit economic reprocessing of the Mercur dumps, the Bureau of Mines probed for a low-cost method that would be applicable to these tailings. A composite sample prepared for laboratory studies assayed 0.062 ounce gold per ton. About 10 percent of the gold occurred as a water-soluble cyanide. Conventional cyanide leaching dissolved 32 percent of the gold, and hot, strong cyanide solution dissolved 42 percent. Results were not improved by pretreatment with acids, bases, or oxidants. After expensive preroasting, gold recovery by cyanidation was increased to 65 percent. The simple procedures were ineffective, and more effective procedures were too costly for economical processing of Mercur tailings.

Jan 1, 1970

By D. J. Bauer, V. E. Shaw

Bastnasite concentrate was processed to recover total rare - earth content and obtain high - purity ceric nitrate . Reaction of the concentrate with 45 percent caustic soda for 1 hour at 180 ° C in stainless steel vessels resulted in 99 - percent conversion to rare - earth hydroxides . A drying step followed by solution in nitric acid produced a tetravalent cerium fraction amenable to extraction with TBP . Single- stage separatory funnel experiments resulted in 90 -percent recovery of ceric nitrate at a purity of 99.9 percent . Fractional extraction in pressure - bubbler columns resulted in 98.5 - percent recovery of 99.5 -percent - pure ceric nitrate .

Jan 1, 1964

By J. E. Murphy

Purification of samarium metal by sublimation and by vaporization from a low-melting metal flux, at the same temperature, were compared. Vaporization proved more effective for removing impurities such as magnesium, calcium, and manganese. Recovery of samarium, however, is more rapid by sublimation because of its constant rate of distillation.

Jan 1, 1970

By Thomas M. Barczak

The Bureau of Mines is conducting research to optimize the capability of mine roof supports so that the selection and design of these supportsare compatible with the conditions in which they are to be employed. This report describes a study that investigates three parameters influencing the load-carrying capability of wood crib supports: height, configuration, and horizontal displacement. Four crib heights, four parallelogram configurations, and three ratlos of horizontal-to-vertical displacements were tested on full-scale wood crib supports in a mine roof simulator. Test results indicated a reduction in load-carrying capability for increases in crib height. Increasing the contact area by changing the intersecting angle between crib blocks to form parallelogram configurations provided a slight increase in load-carrying capability for the first 10 to 12 in of vertical convergence, after which the cribs became more unstable, resulting in significantly less load-carrying capability. Horizontal displacements did not appreciably affect the load-carrying capability of wood crib supports for the range of vertical displacements (less than 10 in) likely to be encountered underground. This report documents these tests and postulates some explanations of failure mechanics for the observed behavior.

Jan 1, 1988

By F. D. DeVaney

An examination of the physical properties of manganese ores is being made at the Mississippi. Valley Station of the United States Bureau of Mines in cooperation with the Missouri School of Mines and Metallurgy, Rolla, Missouri. The object of the study is to find out how much these ores can be beneficiated by such processes as jigging, tabling, magnetic separation, and flotation. Some. of the results were given in an earlier report.4 Eighty samples obtained from various prospects and mines throughout the country have been examined; this is a very small part of those that should be examined before the work can be a definite factor in-the appraisal of manganese ores or the guide in beneficiation which the operators seek. The ore deposits are not expected to reach to great depths vertically, after the manner of copper and gold, but in lateral distribution their greater extent is notable. This applies particularly to the residual and replacement deposits of manganese.

Jan 1, 1929