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By G. W. Jones

An important activity of the Bureau of Mines is the promotion of safety in mining and industry. As a part of this program, the Bureau determines the explosion hazards of combustible gases, vapors, and solids and investigates means of controlling and preventing explosions. The limits of inflammability (explosive limits) of combustibles are not only of theoretical but also of practical importance, because many industries at one time or another contend with explosive mixtures of combustible gases or vapors in their manufacturing processes. At present many new organic compounds are being manufactured, transported, and used in huge quantities which a few years ago were only laboratory curiosities.

Jan 1, 1941

By Z. G. Song, C. Y. Sun, X. R. Zhang, Y. Yu

In skarn type scheelite deposit, there are calcium minerals with floatability similar to scheelite, such as calcite, fluorite, etc., which are difficult to separate. Heating cleaning method developed by Petrov has been widely applied in processing rough concentrate of scheelite for nearly half a century, but there exists a general lack of full understanding of the interaction between floatation reagent and mineral particles surfaces. The mechanism on separation of scheelite and calcium minerals in heating cleaning process was investigated by mineral flotation experiments, XPS analysis, as well as solution chemistry and crystal chemistry calculations. The results showed that the sequence of minerals floatability using sodium oleate as collector and a large amount of sodium silicate as modifier in heating flotation test was scheelite > calcite > fluorite, which was the same as solution chemistry calculations based on Gibbs free energy vs. pH and also the same as Ca-X intensity order by crystal chemistry analysis. There are two sides about the mechanism of heating cleaning method: one is that the adsorbed collector on calcium minerals surface is desorbed more easily than scheelite, and the other is selective dissolution of calcium ions from the mineral surface because of Ca-X intensity difference in heating and stirring process.

Jan 1, 2014

By F. B. Tough

"INTRODUCTION Organizations formed for the purpose of conducting conservation work in oil fields, in order to conserve and prolong the supply of crude petroleum are rare and novel. Such an organization is the Rocky Mountain Petroleum Association, Denver, Colo, As our production of petroleum can no longer keep with the consumption, the plan of organization, character of work, and results obtained by this association are well worth considering. It is hoped that the results achieved in the Wyoming fields will serve to stimulate similar organizations among operators in the state or other oil fields of the United States, The Rocky Mountain Petroleum Association, Danvers Colo., was formed in May, 1919. It comprises the Midwest Refining Co,. The Ohio Oil Co., and the Continental Oil Co. These three companies entered into a cooperative agree¬ment with the Federal Bureau of Mines whereby $30,000 would be spent under the direction of the bureau, which agreed to furnish competent men, and to furnish the work and expenditure of funds. Although the financial burden for the first year's work, now drawing o a close, was carried by only three companies, they stipulated their desire that the benefit of the work should accrue to the industry, and that the personnel employed should be as zealous to assist one operator as another, without regard to whether ha was contributing to the support of the work or not."

Apr 1, 1920

By W. P. C. Duyvesteyn, J. R. Cutland, J. R. L. Russell

In 1970 it was decided to build a large new plant at the Chingola Division of N.C.C.M., Ltd., to treat concentrator tailings and leach residues with a low copper content by a leach-solvent extraction-electrowinning process. In order to assist in the establishment of the design parameters for the new plant, and to study the interaction of this plant with the existing leach-electrowinning plant, mathematical models, formulated as linear programs, have been developed and used extensively. The paper outlines the metallurgy of the plants and describes briefly the way in which the models have been formulated and used. The formulation involved the use of separable programming to form the products of some variables.

Jan 1, 2014

By S. Jennings

The Red Dog massive sulfide deposit is located in the western Brooks Range of Alaska 100 miles north of the village of Kotzebue. It contains the largest zinc reserve in the world. Reserves were doubled in 1995 with the discovery of the Aqqaluk deposit and significantly increased in 1996, with the discovery of a deep zone of mineralization to the north. At present the global reserve and resource is 143 million tonnes of 16.1 % zinc and 4.3% lead. Red Dog is a silica + sulfide synsedimentary replacement deposit hosted in barite and black shale of the Mississippian Kuna Formation. Red Dog was thrust northward during the late Mesozoic Brookian orogeny. Understanding the setting of the deposit at the time of formation and its subsequent deformation history is critical to current exploration efforts and to future discoveries in the district.

Jan 1, 1998

By Tong Gao, Jingyu Qin, Xiangfa Liu, Zengqiang Li, Yaoxian Zhang

"The recycling of aluminum materials is a green industry while Al–Si–Fe is a typical scrap aluminum alloy. The key point of recycling Al–Si–Fe alloys is to separate Al and Fe. A method by introducing Al–Si–Fe alloy into Mg melt has been investigated in this work. A separation layer with gathered Fe–rich and Al–poor Fe3Al0.7Si0.3particleswereobtained at the bottom of the cooled ingot, indicating that ß–Al5FeSi phase evolves to Fe3Al0.7Si0.3,and quantities of Al are released to the upper Mg matrix simultaneously. However, the evolution of Al3Fe by adding binary Al–Fe alloy into Mg melt is different. It is supposed that element Si plays an important role in the phase evolution procedure, thus affects the performance of this method.INTRODUCTIONThe rapid development of aeronautic, automotive and aerospace technologies strongly depends on the consumption of materials while sustainable development is the future direction. Aluminum is a recyclable material and Fe is one of the most common impurities. Fe can be introduced into Al alloys by adding low–purity alloying materials and by using unprotected ferrous crucible, tools, or equipment (Belov, Eskin, & Avxentieva, 2005; Lu& Dahle, 2005).For instance, wear–resistant rings are usually inserted into piston head when producing Al–Si pistons and an infiltration procedure by putting the cast iron rings into Al melt before casting is always essential. As a result, both the re–melting of pistons and the reuse of Al melt for infiltrating rings lead to the enrichment of Fe element, which can be even high to5 wt.%(Viala, Peronnet, Barbeau, Bosselet, & Bouix, 2002).It is widely known that coarse ß–Al5FeSi particles will form in high Fe–contained Al–Si–Fe alloys which is harmful for the mechanical properties. In the past decades, several methods to eliminate the harmful effect of ß–Al5FeSi have been investigated which can be widely referred (Munson, 1967; Lee, Kawamura, Inoue, Cho, & Masumoto, 1997; Suárez–Peña& Asensio–Lozano, 2006; Eidhed, 2008).These methods can be divided into two kinds. One is to aggregate and remove the Fe–rich phase through the methods of centrifugation, gravity filtration or magnetic separation. The other way is modifing the morphology of flake–like ß–Al5FeSi by overheating the melt or adding neutralized elements. However, these traditional methods are rarely used due to respective disadvantages, while the commonly used method in industries is using primary aluminum for dilution. However, only less than 30wt.% of scrap Al can be added into primary Al melt for each melting work while it also results in the decrease of product quality simultaneously(Zhang, Liu, & Liu, 2016)."

Jan 1, 2018

By Douglas Valentim Fernandes Neves

O aço inoxidável austenítico 316 (316 SS) é um dos materiais metálicos mais utilizados em aplicações médicas devido à combinação de propriedades mecânicas e do baixo custo. No entanto, desgaste e corrosão estimulam mudanças permanentes no tecido humano que podem levar à perda do implante. O desenvolvimento de recobrimentos biocompatíveis e estáveis, que apresentem propriedades mecânicas adequadas, e que não sofram ruptura ou delaminação durante o uso, é uma solução muito promissora para melhorar o desempenho do 316 SS como biomaterial para implantes. Neste trabalho, uma liga intermetálica FeAlCr, que tem apresentado propriedades adequadas para a aplicação como biomaterial, foi utilizada como recobrimento sobre um aço inoxidável 316 de grau médico. O revestimento foi obtido utilizando-se a técnica magnetron sputtering por corrente contínua. Os parâmetros de deposição, como distância substrato - alvo e pressão de gás argônio foram mantidos fixos em 50 mm e 5 mTorr, respectivamente. As amostras foram preparadas com os seguintes valores de potência de sputtering: 50 W, 75W, 100 W e 150 W. A adesão dos filmes foi analisada por teste de scratch, enquanto a espessura e a taxa de deposição foram analisadas por perfilometria ótica. As características estruturais foram analisadas por microscopia eletrônica de varredura com EDS.

Aug 8, 2018

By Gabriel Aguilera, Juan Arismendy

"As a separator machine, the hydrocyclone is one of the most commonly used equipment in different types of industries and particularly in mineral processing, hydrodynamic behavior allows efficient separation, but developing tests to optimize experimental equipment is expensive, therefore Computational Fluid dynamics (CFD) becomes a useful tool for optimizing the geometrical and operational parameters, and allows to analyze and understand the dynamics within the equipment. In the research was developed to simulate of 40 mm hydrocyclone where turbulence model was used Large Eddy Simulation (LES) for the continuous phase, for the generation of the air core and for the interaction of particles at low concentrations was implemented (mixture model), after the simulation was completed validation and comparation was done between simulation values and experimental."

Jan 1, 2014

By J. G. Groppo

A series of performance studies have been conducted using counter-current column flotation to recover a marketable clean coal product from existing preparation plant fine waste streams. The test work was conducted at several preparation plant sites in Kentucky and Virginia and utilized a 0.15m (6 in.) I.D. column that was 5.79m (19 ft.) high. The refuse streams tested included both thickener feed and classifying cyclone overflow with a typical size distribution of 100 mesh X O. The percent solids of the column flotation feed varied from 1.5 to 15% while the ash content ranged from 30-60%. The concentrates produced contained 2-10% ash with BTU recoveries of nearly 90% using 0.12-1.25 kg/ton (0.25-2.5 lbs/ton) fuel oil and 0.12 kg/ton (0.25 lb/ton) MIBC. These results were consistent with or better than results obtained in preliminary laboratory scale column flotation evaluation. Test results from 7 different seams are discussed as well as scale-up relationships utilized to design a full scale installation presently in operation.

Jan 1, 1990

By K. Dzieciol

The paper presents a study about three image correlation methods ?common cross-correlation, mutual information and phase-correlation ? applied to characterize microstructures reconstructed with X-ray tomography. It is shown that phase correlation is not only the fastest, but also the most sensitive method for detection of similar microstructure features, cavities in the present case. A new image correlation indicator is proposed, which takes into account both the phase shift and the amplitude of similar features in compared images. Some preprocessing aspects related to the tomographic reconstruction and filtering out of characteristic noise are also discussed.

Jan 1, 2009

By Bingliang Gao, Junli Xu, Michal Korenko, Jinzhao Guan, Liangxing Li, Zhongning Shi, Zhaowen Wang, Aimin Liu

Al-Si alloy, a precursor of solar grade silicon, was prepared by direct electrolysis in cryolite molten salt at 950 oC using high purity silica as material, liquid aluminum as the cathode and high purity graphite as the anode. The electrochemical behavior of Si(IV) ion was investigated using cyclic voltammetry method. The electrolysis products were characterized by XRD, SEM/EDS and ICP. The results indicate that the reduction process of Si(IV) on tungsten electrode is a two-step process and there is about 0.6 V gap between the two steps. The contents of boron and phosphorus in the aluminum-silicon alloy are 3 ppmw and 8 ppmw, which will make the directional solidification purification effectively and reduce the cost of preparation solar grade silicon from metallurgical grade silicon.

Jan 1, 2015

By Run-bo Wang, Zhe Wang, Fan-yi Meng, Jian-Liang Zhang

The influence of semicharcoal substitution for coke breeze on sintering performance was investigated by pot-grate sintering test. At a fixed fuel ratio, sinter productivity and strength decreased with the substitution increasing from 0 to 100% due to better combustibility. To enhance the utilization efficiency of 100% semicharcoal, sintering parameters (moisture and suction pressure) was adjusted. With the moisture increasing, sinter performance of 100% semicharcoal increased because of the suppression of semicharcoal incomplete combustion. As the moisture further increasing to 9.0%, sinter quality gave rise to a decrease trend. The results also showed that the increase of suction pressure was benefit for the increase of heat transfer rate, leading to the improvement of heat utilization energy. Measures to enhance magnetite oxidation during sintering are discussed based on current understanding of the fundamentals that control the sintering process.

Jan 1, 2015

By Youn-Bae Kang, Jong-Jin Pak, Min-Kyu Paek

The critical evaluation and thermodynamic optimization of Mn-Si-C and its sub-binary systems have been carried out over the whole composition range from room temperature to above the liquidus temperature. The solution properties of the liquid systems have not been clearly described because the liquid solution exhibits a high degree of short-range-ordering. In order to predict the thermodynamics of the liquid solution, the liquid phases were optimized by the modified quasichemical model. The model parameters of the solid phases were also optimized by the compound energy formalism to best reproduce the phase diagram and important thermodynamic properties in Mn-Si-C system. Using the model parameters, various thermodynamic calculations were carried out. The present database will be a part of larger thermodynamic database for the ferromanganese alloy database.

Jan 1, 2014

By Carolina Machado de Castro Amaral

A necessidade de treinamento é uma realidade nas indústrias. A qualificação de operadores é importante para garantir segurança e prevenir perdas econômicas. Nesse contexto, o objetivo desse trabalho é desenvolver e avaliar um simulador de treinamento de operador. O estudo de caso é um moinho vertical, comumente utilizado na indústria de cimento. Nessa direção, passou-se pela construção de um supervisório, pela modelagem e simulação dinâmica de um moinho vertical e, por fim, pela elaboração e execução de um treinamento. Para tal, foram construídos três cenários de situações anormais, além da consideração da operação normal. Ainda em relação à metodologia, treinaram-se dois grupos de alunos com métodos distintos de ensino: o primeiro recebeu apenas um treinamento teórico, através de uma apresentação multimídia; e o segundo, após esse treinamento teórico, recebeu um treinamento prático, ou seja, do tipo aprender fazendo, a partir do contato direto com o simulador de processos. De modo geral, percebeu-se que o contato com a prática possibilitou um maior entendimento da operação do moinho vertical, do grau de dependência entre as variáveis de entrada e de saída, e das variáveis utilizadas para a recuperação do processo à operação normal, contribuindo ainda para uma maior fixação do conhecimento teórico. Esse trabalho é resultado de uma parceria UniversidadeEmpresa, cujas atividades foram desenvolvidas por um grupo de alunos de graduação em Engenharia Química.

Aug 17, 2017

By K Gardner, R Fraval, V Singh

Using new technology to create optimised infill drill programs in underground or open pit settings, it is possible to quantify the value of a drill program. The computer designed programs are optimised to uplift the most amount of resource possible into the specified resource classification, while honouring geological, spatial, equipment and budgetary constraints. When designing ‘by hand’ balancing all these factors is a time-consuming effort with no real way to determine metrics on ‘how good’ a program will be. The optimisation considers many factors allowing geologists to apply critical thinking and domain knowledge to constrain the optimisation, letting the computer do the heavy lifting of determining hole placement. Once programs have been created, they can be integrated into a production schedule. This is a critical step in determining the correct sequencing and balancing of resource availability and seeing how a program will interoperate with other tasks in the mine. For example, if drill drives are a requirement for part of the program, will they be developed in a time frame that is useful for the goals of the program? Do we risk drilling infill holes too late to add value? Do we put production at risk by not classifying parts of the model ahead of time, thus adding to uncertainty? Using software to assist with optimising and scheduling of drilling is a useful technique to save the geologists from the mundanity of manually designing drill programs and puts metrics around the effectiveness of a program and has the potential to add quantifiable value to a program. Examples will be presented that demonstrate the effective use of drill hole optimisation, comparing manual designs with optimised designs, as well as the examples that show the effective use of scheduling.

Mar 22, 2022

By Rick Deschamps

A reoccurring problem with support of excavations in urban areas involves the placement of external support components like anchors or nails in right-a-ways, subway and utility setbacks, in areas occupied by adjacent structures, and within the property of non cooperative neighbors. Such a situation occurred for a project in Arlington, Virginia, which ultimately resulted in the preliminary design of a large footing supported cantilever retaining wall that was extremely costly and impractical to build. An innovative design alternate consisting of a series of vertical concrete elements (VCEs) supported by post tensioned tiedowns was proposed to the General Contractor and accepted by the owner. The VCEs were designed to serve as the main structural elements for both the temporary support of excavation system and the permanent wall. The VCE?s were constructed using single bite diaphragm wall panels oriented perpendicular to the excavation face including a rebar cage and tremie concrete. Threaded inserts were placed within the rebar cage to attach the cast in place exterior wall. Overall stability and lateral movement of the VCEs were controlled by high capacity vertical anchors embedded within the VCE. A detailed instrumentation program was installed to monitor the movements of the VCEs with relation to the excavation depth. The paper present the project case history by discussing the design concepts of the VCE, the construction approaches used to install them, the construction challenges encountered, and the performance of the unique system.

Jan 1, 2008

By Daniel Augusto Godinho de Carvalho

Since the beginning of BOF process, slag formation has been subjected to extensive development. During the initial stages of the blow, fast slag formation is primordial for the process performance. This is mainly to allow oxidizing reactions, and also to protect the refractory. A modeling of BOF process for the purpose of process optimization requires precise knowledge concerning the dissolution of CaO and MgO based materials. Using this knowledge, the optimal process conditions can be ensured by a controlling of the slag formation during the converter steelmaking process. Taking into account an application of large amount of different raw materials, as well as location-specific process conditions, the characterization of the dissolution behavior of different additives is an important key to improve the technological process. Thereby, in the frames of this project, an appropriate model for slag formation is established and compared to operational results for a 330t BOF, operating at ThyssenKrupp CSA, Santa Cruz, Brazil.

Aug 16, 2017

By Yazen Khasawneh, Yao Zhang

Upgrading and maintenance programs were proposed at a power generating plant in Indiana. To perform construction activities associated with the proposed upgrading and maintenance, a LR11350 crawler crane with a dead load of 1,500 ton was required in the vicinity of existing plant structures. The contact pressure from the crane tracks for the heaviest lift, maximum reach and angle (worst loading condition) were estimated by the rigging engineer to be on the order of 84 psi. Several concerns were raised regarding the total and differential settlements while the crane is in operation and the induced stresses on existing underground utilities due to crane loads. Three-dimensional finite element simulations were conducted using hardening soil model for the subsurface soils and elastic model for the other structural elements (underground utilities and crane mats) to optimize the configuration of the proposed crane foundation. It was found 1-foot thick engineered steel mats underlain by a 1.5-foot thick crushed stone pad will provide enough support to the crane. It will also control the settlement to the allowable limit and maintain the stresses in the underground utilities within tolerance. INTRODUCTION A LR11350 heavy lift crawler crane was proposed as part of an upgrade program at an existing power plant in the state of Indiana. The proposed crane will be sitting on an open ground in the vicinity of existing plant facilities, with multiple underground utilities going beneath the proposed footprint of the new crane pad. The existing utilities are of diverse kinds, including sanitary sewer corrugated metal pipes, electrical conduits and variable steel water/oil drain pipes. The safety and functionality of these underground utilities are critical to maintain the proper operation of the power plant. Therefore, the design of the new crane pad foundation system is of essential to control the ground settlement and the imposed stresses to the existing utilities (Davie et al., 1998, Scott 2017). To ensure all utility locations and depths are identified, the proposed footprint was thoroughly surveyed. Information in regard to each identified utility was provided by the owner. Subsurface explorations were conducted using geotechnical soil borings and soundings to evaluate the ground conditions and generate soil profiles. Numerical simulation and analysis utilizing finite element method were performed to design the crane pad foundation system and evaluate the responses of the utilities. This paper summarizes project information, geotechnical conditions and then focuses on the finite element analysis in assisting the design of crane pad and the utilities evaluation.

Jan 1, 2019

By A Smith

Rock masses usually exhibit scale dependent mechanical properties primarily due to presence of discontinuities and their inhomogeneous nature. One of the essential preconditions for selection of appropriate strength and deformation parameters of a rock mass in relation to tunnel design is assessment of the scale of the joint network relative to the scale of excavation. In tunnel design practice, scale effects are estimated indirectly using small-scale unconfined compressive strength (UCS) tests and rock mass classification based empirical correlations. Large-scale UCS tests have the benefit of direct assessment of anisotropic and scale dependent properties of a rock mass.This paper presents results of a large-scale UCS test on a jointed siltstone. A 450 mm diameter sample with inclined bedding planes was cored and tested in uniaxial compression until failure with load and displacement measurements. The aim of the test is to determine strength and deformation parameters and correlate them with results of small-scale UCS tests of the same sample. The relationships between the small-scale and large-scale rock mass parameters were validated against published correlations from the literature.

Mar 8, 2011

By Mizraim Uriel Flores, Elia Guadalupe Palacios, Sayra Ordoñez, Iván Alejandro Reyes, Ister Mireles, Martín Reyes, Francisco Patiño, Hernán Islas, Víctor Hugo Flores

This paper presents the characterization of a sample of mercury jarosite that was synthesized by slowly adding Hg(NO3)2H2O into a Fe2(SO4)3nH2O solution. X-ray diffraction (XRD) analysis performed on the sample confirmed that the compound presents a crystal phase corresponding to mercury jarosite. Analysis through Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM-EDS) determined that the precipitate is composed of mercury, sulfur, iron and oxygen. It is made up of spherical particles with an average size of 38 μm; these particles are made of rhombohedral micro-crystals with sizes ranging between 1 and 2 μm. Chemical characterization was performed through dichromatometry analysis, gravimetry and atomic absorption spectroscopy (AAS), thus obtaining the following composition: 27% Fe3+, 37% SO4 2− 14% Hg2+, 22% OH− + H3O+ + H2O. The following approximate formula of the compound was determined from chemical analysis: [Hg0.39(H3O)0.22]Fe2.71(SO4)2.17(OH)4.79 (H2O)2.09.

Mar 1, 2017