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By L. G. Marsh

The manufacture of lubricating oils from wax-bearing crude petroleums involves the removal and recovery of the paraffin wax contained in the lubricating distillates. During this process several intermediate products are formed, among them the mixture of waxes and oils known to the refiners as "foots oil." Because of its complex character, foots oil is little understood, and therefore methods of handling it in refineries are often inefficient. The Bureau of Mines is studying the manufacture of lubricating oils, and during the work has investigated the redistillation of foots oil. This report gives in brief the results of the investigation, and recommendations based upon it.

Jan 1, 1926

By Thomas Fraser, H. F. Yancey

BefoRe a new coal-washing plant is installed, or an existing washery is remodelled and improved, considerable experimental work on the coal to be washed should be done. A thorough examination of a coal, to determine whether it can be washed successfully and the best and most economical process for securing a satisfactory grade of washed coal, calls for mine sampling, analytical work, and experimental coal-washing tests which may require several months' time and the expenditure of considerable money. Having collected the required data on the characteristics of the coal and the results secured with different types of machines under different sets of conditions, it is necessary to decide what method of treatment should be used. The interpretation of the experimental data is no small part of the problem. The first step in the investigative work is to determine from the characteristics of the coal and the manner of occurrence of the impurities whether it is possible to separate the dirt from the coal and produce a washed coal of the required quality. Then it is necessary to select the type of washer or the system of treatment that will produce the greatest amount of washed coal of this grade for the least cost. To secure this information, tests may be made at laboratories operated by consulting or contracting engineers, at the testing plants of machinery manufacturers, at commercial washeries, or in an experimental washery erected on the site of the proposed plant. Such tests will produce figures in which every factor, including analyses of raw coal and washed coal and yield of washed coal, may vary widely. To reduce these results to a common basis for comparison is very difficult. A number of plans

Jan 1, 1923

By A. B. Wilder

We study the past Because it is a guide to the present and a promise for the future. The struggle for a better world is strengthened By the hopes, ambitions, and deeds Of those who were before us. As we look backward Our attention is directed forward. ONE hundred years ago, the manufacture of steel from molten pig iron without the use of fuel first began. In the earlier part of the nineteenth century the crucible process was the principal steelmaking method. It was a costly process, producing only a few pounds of steel at a time; so, most of the ferrous metal output was in the form of wrought or pig iron. With the perfection of the converter technique it became possible to produce low cost steel by the ton, thereby completely changing the structure, not only of the ferrous metal industry, but also of industrial production in general. This was the turning point from the Iron Age to the Age of Steel. William Kelly (Fig. 2), Sir Henry Bessemer (Fig. 1), and Joseph G. Martien experimented with the process before 1856. William Kelly began in Eddyville, Ky., in 1847 and has been given credit for first discovering the principle of the pneumatic converter process. Several years later in England Henry Bessemer independently conceived a steelmaking process similar to Kelly's. Bessemer made public his invention at the annual meeting of the British Association for the Advancement of Science held at Cheltenham, England, August 1856. As a result of his paper, "On the Manufacture of Malleable Iron and Steel Without Fuel," and his progressive leadership in the years to follow, the process became permanently identified with the name, Bessemer. Credit for the commercial adaptation of the process must be given two additional persons. Robert Mushet (Fig. 3) in 1856 in England recognized the necessity of deoxidation and recarburization of the converter product and evolved the technique for adding high manganese iron following the blow. In Sweden, in July 1858, G_ F. Göranson [ ]

Jan 1, 1961

Jan 1, 1968

By Hirose K, Itakura K

A new global stiffness matrix evaluates the performance of powered supports by estimating and comparing the global stiffness matrices of ten different types of powered supports with lemniscate linkages, each support having its own deformation characteristics. Expanding the global stiffness matrix allows the implementation of a finite element scheme to analyse the interaction between the powered support and the strata around the coal face.The evaluation of performance by the stiffness matrix method shows that 4-leg chock shields possess both the desirable convergence and shear deformation stiffness properties. The finite element analysis also confirms that 4-leg chock shields present well balanced performance for controlling strata around the coal face.

Jan 1, 1991

By David R. Mitchell, E. A. Reilly, G. R. Gardner, F. P. Lasseter

THE methods that may be applied to the treatment of slurries and water, as these are related to practical coal-preparation problems, are concerned essentially with the movements of solids suspended in water. It is assumed that there are no fundamental differences between the principles involved in the treatment of coal slurries and the phenomena encountered in general mineral-dressing practice, and the latter are-presented in some detail. Basic principles are correlated with present practice for both the anthracite and the bituminous coal fields, and methods are discussed which are designed to utilize best all the material subjected to treatment and suggest a sound approach to the solution of problems relating to the return of clear water to process or to streams. In order to approach the practical phases of the subject with sufficient understanding of the basic principles, it is necessary to discuss two types of phenomena that are applicable. The first is flocculation and the second is sedimentation. Descriptive matter is given covering the various methods and types of equipment employed to conduct these operations, with emphasis on their application to water and coal-slurry treatment. DEFINITION OF TERMS Definitions of terms are consistent with modern developments, and conform, in general, with their usage in mineral-dressing practice. Because of variations in coal-preparation methods, it is impossible to define a rigid upper limit of particle size for a coal slurry or sludge which will apply generally. Limits vary somewhat with the particular treatment method employed at a given plant. For purposes of definition, this limit is chosen as the particle size for which preparation methods such as Chance comes and jigs are usually dispensed with, and other methods, such as the Hydro-tator, tables, and froth flotation, are employed. Generally the limit will be 10 to 6 mesh.

Jan 1, 1950

By Robert Jacob Cefalo, Rio Tinto Kennecott

At the end of 2016, the Mine started a new ore phase in the section of the pit located on the East Wall. The East Wall geological structures required controlled blasting for peak particle velocity (PPV) frequency vibrations to protect the wall. Frequency controlled blasting using linear seed wave superposition modeling was required and implemented to reduce the far-field affects to the wall. This paper covers the work done by the drill and blast engineering group, controls used to protect the mine infrastructure, and the continuation of work-to-date of frequency controlled blasting for wall stability. The narrow width of the layback required the combination of hole sizes to blast large diameter production patterns with smaller diameter trim patterns in the same blast. A single blast had to use different burden & spacing and hole diameters and required the use of different timings throughout the pattern. Electronic detonators were required to limit blast vibrations and accommodate the specific timings needed to reduce low frequencies. The geotechnical group with the help of geotechnical radars worked with the drill and blast group on creating a tracking and reporting of blast performance. The radar readings informed the drill and blast engineers of the performance of the blast as it related to the long term performance of the highwall

Jan 1, 2019

By D. C. Seidel, M. C. Fuerstenau, R. J. Roman

The role of surface charge in soluble salt flotation, which was developed in Part I, is extended to relate the theory to the specific phenomena of KCI-NaC1 separations. Temperature-collector solubility relationships, metal ion activation, and particle size effects are discussed. The initial paper in this series developed and presented the hypothesis that one of the mechanisms of soluble salt flotation may involve electrical attraction between the collector and mineral surface. This hypothesis was developed from a combination of experimental data and free energy calculations, and details of the logic are presented in this first paper.* The studies have indicated that KC1 has a positive surface charge and NaCl a negative charge. KC1 can therefore be floated with sulfonate ion (RSO;) or with an aqueous polar species such as the aqueous amine chloride, RNH3C1(,,). The chloride end of the RNH3C1(,,) molecular dipole is probably negative and will be attracted to the positive surface of the KC1 particles and absorb (actually probably fit into a vacant chloride site) on the mineral surface. The amine end of the collector molecule would extend into the solution phase and provide the air avid surface required for flotation. NaCl particles are floated by such collectors as aqueous molecules of fatty acid salt, RCOONa(,,), in which the positive inorganic end of the dipole is attracted to the negatively charged surface of the NaCl and, in this case, adsorb and probably fit into a vacant sodium site on the surface. The aminium cation, RNH~, should also be a collector for NaC1. For certain collectors, actual precipitates of the collector must be formed before a sufficient amount of the polar aqueous molecule is present to effect flotation. In a system of this type there is a three-way equilibrium between: Aqeous Molecular Solid Precipitate - A of the Collector (Not Dissociated) . Ionic Species (Dissociated). The controlling equilibrium is probably between the precipitated form of the reagent and the aqueous

Jan 1, 1969

By Jerome F. Kuzmick

The use of iron powder during the postwar conversion period has been increasing with great rapidity. This is particularly true in regard to the manufacture of molded mechanical parts such as bushings, gears, cams, small wheels, and the like. Many manufacturers have found it possible to replace machined cast iron and carbon steel with molded iron powder parts, and thereby can not only effect a savings in cost, but can produce a better product as well. As the field of application for iron powder parts widens, greater demands are made upon the powder supplier concerning quality and uniformity characteristics. The following are some of the most important properties parts fabricators desire in the iron powder they use: 1. The powder should have high compressibility so that good density can be obtained without the use of excessive pressures. At the same time, it should show low die wear so that a large number of pieces can be produced from the die. This means that the powder must be of high purity and good softness or plasticity. 2. The powder should produce compacts of high green strength, so that unsintered parts can be handled without breakage or fraying of the edges. 3. The sintering properties should be good so that satisfactory strength is obtained in the sintered piece. 4. Compacts made from the powder should show small but, above all, uniform dimensional changes during the sintering operation so that accurate parts can be produced, and warping and other such bad effects eliminated. 5. The powder should have satisfactory flow properties for automatic molding. 6. It is very important that the powder be uniform in sieve analysis, compressibility, flow, purity, and other qualities, from container to container in any given lot and from shipment to shipment. 7. Price—The fabricators desire all these good properties, but in many instances still do not wish to pay a premium price. There has been considerable discussion as to the importance of price of the powder in relation to the cost of the finished product. It is true that in cases where certain special properties only procured by powder metallurgy are required, price is not a criterion. On the other hand, there have been a number of applications recently made which would not be commercially practical with a powder which commands a premium in price. Iron powder parts are compressed in automatic presses to definite size, shape, and density. The powder is compressed to a density figure dependent upon the function the part is to perform, as well as upon such important considerations as press capacity and die wear. Such parts can be roughly broken down into the following density ranges:

Jan 1, 1949

IN the preceding chapter on thermochemistry and the reactions in and between metal and slag phases and in the following chapter on fuel combustion the main emphasis is placed on the equilibrium or "static" conditions. This equilibrium viewpoint is not concerned with the rate of change in the process or with the mechanisms or paths followed between initial and final states. The questions of just "how it works" and "how fast" belong to the kinetic aspect of any process; their answers are helpful in speeding up or slowing down and thus controlling its operation, and also in understanding its limitations. Any treatment of kinetic factors in the open hearth such as is attempted here and in Chapter 22 must at present be largely qualitative and incomplete. We are only beginning to get quantitative data on rates of reaction and diffusion at high temperatures, as indicated in Chapter 15. Empirical data in the literature on furnace operating rates do not help much to illuminate the details of gas-flow patterns and the complexities of heat flow in the many parts of the furnace system. This chapter is intended to give the reader an introduction to the problems of the flow of gases through the furnace system and the flow of heat in this system. An adequate discussion would require several times the space available here; it is possible here only to outline a few fundamentals and to indicate some of the conditions of heat and gas flow peculiar to the open hearth. Several good general treatments of these subjects may be found in the literature (see references at the end of the chapter). For the designer of open-hearth furnaces, the principles of gas flow are of paramount importance. They are also important to the operation of the process, at least to the extent of a general qualitative picture of the movement of gases in the system. MOTION OF GASES IN FURNACE DUCTS Fluid flow in general can vary between the extremes of laminar or streamline flow with a minimum energy loss, to irregular

Jan 1, 1951

By Don B. Shupe, John K. Berry

The handling and disposal of mine water is a much larger problem than is apparent at first glance. Many more tons of water are removed from underground coal mines in the United States each year than tons of coal. In the old anthracite region of Pennsylvania the average was around 32.7 t (36 st) of water for each ton of coal produced, while bituminous mines average about 4.5 or 5.4 t (5 or 6 st). Water encountered in the mines may come from several different sources. In mines with light cover and without a firm solid roof, rain may seep directly into the workings. This is also true of deeper mines where pillar falls have broken the roof to the surface. The top under creek beds is generally faulty and broken and water comes through the roof at this point. Deeper mines are frequently overlain by water-bearing strata and pillar breaks and faulty top can admit water, while places running to the dip often accumulate water which comes up through the bottom. In all cases, except where passing under a year-round stream, the amount of water made is usually pretty closely connected with the weather-more water during the rainy season, less in the dry, although the deeper a nine is, the longer it is before changes in rainfall are felt. Another source of water, not connected with seasonal changes, is old water, accumulated over a period of time in abandoned workings of the mine, or from flooded adjacent mines. Here the water filters through the coal, the parting, or comes up through cracks in the bottom. Similarly, core holes, drilled to prospect the property, can be a source of unexpected water and modern safety requirements for dust-allaying water at the working faces can turn a pleasant working area into a soggy mess over the weekend if the system is not properly maintained and operated. Why water must be disposed of is obvious. If allowed to accumulate, sooner or later the mine will fill up, or at least it will become "roofed" in low places, blocking ventilation and traffic. It must be controlled long before it reaches this stage. Water standing in the working faces is

Jan 1, 1981

Magnesium-rich olivine is used as an additive in LKABÆs iron ore pellets in order to improve the high-temperature properties of the finished products. Olivine is only added to the pellets that are manufactured for ironmaking in the blast furnace process. The olivine comes from Minelco/LKABÆs mine at Seqi in Greenland. This dunite complex of Archean age contains about 95 - 98 per cent olivine. The grain size is typically 1 - 3 mm but much larger euhedral olivine crystals are common in the porphyritic type. The serpentinisation is absent or weak. The most common minor minerals are chromite, chlorite, talc, phlogopite, amphibole and pyroxene. The crushed olivine is transported to LKABÆs pelletising plants in Northern Sweden. After grinding, small amounts of olivine are mixed with the magnetite concentrate. The concentrate is rolled into green balls, about 10 - 14 mm in diameter. The moist green balls are transferred into the pelletising machine where the maximum temperature is about 1250¦C. The residence time in the pelletising machine is about one hour. Olivine is used in order to get pellets with better high-temperature properties. This paper deals with the olivine alteration during the pelletising process and the behaviour of magnesium following the decomposition of magnetite. The reactions are quite complex in the pellets because the physico-chemical conditions vary considerably in the process from one process step to another, and in the pellet bed from the top to the bottom. Some olivine particles in the finished product show very slight alteration, some particles are completely decomposed. The formation of the iron-rich coronas around the olivine particles is the most typical alteration. In the finished pellets the magnesium is mainly distributed between the following phases: unaltered olivine, coronas, Mg/Fe-ferrite and silicate slag.

Jan 1, 2008

By William B. Beerbower

When full length resin grouted bolts were introduced into U. S. coal mines some 11 years ago, it was assumed that safety would be the primary benefit. There is ample testimony to substantiate the safety factor as an important reason for using resin roof bolts. More recently, it has been determined that many coal operators not only concur with the safety consideration but also benefit economically from the safer working conditions resulting from a reduction in roof falls. IMPROVED SAFETY Some typical roof fall reduction experiences with resin bolting follow: ? Western Kentucky Mine - Resin bolting reduced roof falls by 80%. ? Southern West Virginia Mine - Experienced 141 roof falls between 1971 and 1972. In 1973 with resin bolting, roof falls were reduced 85%. ? Western Pennsylvania Mine - In 1973 had 59 roof falls with mechanical bolts. During the same period of 1974 with resin, only 19 falls were experienced - a reduction of 66%. The overall experience with resin bolted roof support has been an average 50% reduction in roof falls. Long term, this can translate into improved worker morale. As a matter of fact, a general mine foreman at the same Southern West Virginia mine mentioned above commented that improved miner morale was noticeable following the introduction of resin bolting. HOW GREATER SAFETY CAN BE COMBINED WITH INCREASED PRODUCTIVITY IN COAL MINING OPERATIONS Experience has also shown that a reduction of roof falls with resin bolting has resulted in increased production for many coal operators. Some typical examples with mines using resin bolting follow: ? Western Kentucky Mine - Resin bolting contributed to increasing production from 7000 to 11,000 tons per day, due to a 80% reduction in roof falls. This was accomplished in part by a reduction of 50% in timbering requirements and the reassignment of three roof fall cleanup crews to coal production. ? Pennsylvania Mine - Following resin bolting introduction the section showed a 50% increase in production. ? Central West Virginia Mine - Continuous miner production averaged 6 cuts per unit shift prior to resin bolting. Reduction of cleanup time, resulting from improved roof support with resin bolting, increased production to an average of 9 cuts per unit shift. PROPERTIES OF RESIN BOLTING SYSTEMS Several of the important properties of resin bolting systems which contribute to its improved performance are listed below: ? Full length anchored resin bolts and many resin anchored, point anchored bolts provide effective resistance to changing rock strata stresses throughout their length, thereby improving stabilization of rock strata over long periods of time. ? Individual layers of rock are anchored into a single high strength beam providing excellent resistance to vertical and lateral strata movement, the most common cause of roof failure. ? Moisture cannot corrode the fully grouted bolt. ? Has twice the pull strength of mechanical bolts (See Figure 1)

Jan 1, 1982

By John Ward Smith

Oil-yield data are presented for core samples from Colorado Corehole No.1, drilled by the Bureau of Mines and the Atomic Energy Commission in a previously untested oil-shale area near the northern edge of Colorado's Piceance Creek Basin. Continuous oil shale 2068 feet thick, averaging 18.41 gallons of oil per ton of shale and representing 1.8 billion barrels of oil per square mile, occurs at the core site.

Jan 1, 1968

By W. H. Ode

Low-temperature distillation tests at 200°, 350°, and 500° C. were made on a subbituminous coal from Boulder County, Colo., and a subbituminous coal from Weld County, Colo., in connection with a survey of carbonizing properties of American coals and investigations of their chemical and physical properties. The coal represented by the sample from Weld County was reported to give off combustible volatile matter at unusually low temperatures When placed on a fuel bed. The yields of tar and oil and the composition of the gas from this coal, as obtained in the distillation tests, did not confirm this report. These yields and the gas composition of the Weld. County coal differed but little from those obtained from the coal from Boulder County. Both coals yielded tar and gas in amounts considered to be normal for coals of their rank.

Jan 1, 1937

The paper considers the nature of outbursts of coal and firedamp as they occur. t follows the development of methods of working used to try and induce outbursts safely under controlled conditions and details the life support systems used to provide maximum rotection to persons who may be affected by s_lontaneous outbursts. Tilt: NATURE OF OUTBURSTS IN THE UNITED KINGDOM .1y some areas in the coalfields of the ingdom are affected by outbursts of :hal and firedamp. The main area affected is he western end of the Anthracite coalfield r: West Wales. In this area 206 outbursts .eve been recorded resulting in the loss of 8 lives. Anthracite is a high rank coal produced v the geological effects of age, depth and ynamic metamorphism. Outbursts have been xperienced over a wide area of the anthracite field but have been most frequent, and most evere, in the areas where carbon content is its highest and where the coal measures cave been subjected to the highest degree of eulting and overthrusting. Most outbursts ire associated with geological abnormalities ,:id the coal ejected during outbursts is sually of a soft and powdery nature.

Jan 1, 1980

By Morris Steinberg, John Wulff, Robert Kamm

IN powder metallurgy it has often been observed that shrinkage may occur in one direction and growth in another during sintering. Even in long-time sintering experiments the rate of shrinkage may be different in different parts of the compact. In the fabrication of some parts requiring a constant permeability it is even questionable in some cases whether pressing from one direction should be attempted. These observations require for their interpretation a more detailed study of green or pressed density than has heretofore been available. Usually average density measurements of the whole compact are made and in some cases carefully cut sections are measured. A different approach to the problem was first mentioned by Rakowski1 and also used by Balshin.2 Balshin's diagram is reproduced in Fig r and schematically shows the result of pressing three layers of metal powder with fine intervening layers of graphite. The retarding effect of the die walls and a qualitative example of the density distribution is evident. More quantitative information about the distribution of density within a cold-pressed powder compact would be useful in showing the variation in density in compacts as influenced by the type of powder, shape of die, lubrication during the process, and other variables. Furthermore, information about the cracking of cold-pressed compacts may be obtained from an analysis of the stress distribution within a powder compact, and some information about the stress distribution can be obtained in turn from the density and strain distributions. A more detailed report on some of the present experiments appears in reference 3. PRESENT INVESTIGATION In order to ascertain the density gradients in cold-pressed metal powders, a deformable lead grid within the powder was employed. After pressing in cylindrical dies the ejected compact was radiographed, giving a pattern of the deformed grid. From the radiograph density and deformation from point to point is readily measured. From the radiograph strain distribution and stress trajectories were also determined. The latter also permits the determination of the coefficient of friction at the die wall. This technique indicates that the densest part of a compact pressed from one side is at the top outer circumference and the least dense region at the bottom circumference near the stationary plunger. For some heights of compacts the density at the axis is such that the lower density is at the top rather than at the bottom. So irregular a density distribution is due primarily to die-wall friction. As the ratio of diameter to height of compact is increased the die walls play a correspond¬ingly smaller role. More uniform density

Jan 1, 1947

By Sylvan Cromer

The need for a clear understanding of the physical nature of the flow of gas-liquid mixtures in vertical pipes is ever becoming more apparent. This type of flow is encountered when gas and oil are produced from a well; when water is removed from gas wells with siphon lines and when liquids are elevated by means of air or gas lift. Although a number of investigator1-7 have published data on the flow of gas-liquid mixtures, in only a few cases has the experimental setup been devised to permit visual study. In the fields of heat transmission, such as the boiling of liquids and the study of the critical phenomena of the hydrocarbons, researchers have been able to throw additional light on heretofore unexplainable happenings through actual observation in glass apparatus. This investigation was therefore undertaken in order to obtain qualitative as well as quantitative results for air-water flow. Experimental Apparatus and Procedure The flow column used in these tests was made of standard 2-in. pipe and was approximately 98 ft. in height. Pyrex observation sections 2 ft. long having the same internal diameter as the wrought-iron pipe were placed at 14-ft. intervals in the column. The bottom of the tube was cut off square and terminated in the mixing chamber. No perforated nipple or footpiece of any kind was used. To the top of the column was fastened a semicircular return bend having a 4-ft. radius. The flow column was supported by a standard cable-tool drilling derrick (Fig. 1) into which were built observation platforms at each Pyrex section.

Jan 1, 1940

By Christopher Mark

The Bureau of Mines is conducting research to assess the effectiveness of different chain pillar designs in maintaining gate entry stability. The study described in this paper was performed in a 1200 ft long, experimental headgate section which contained three pillar designs: - a three-entry, yield-abutment pillar' system, - a four-entry, yield-yield-abutment pillar system, and - a five-entry, all-yield pillar system. As the longwall mined by the experimental section, Bureau engineers monitored entry convergence, roof sag, and changes in roof quality. The results of the study indicate that the all-yield system performed at least as well as, and probably better than, the two abutment pillar systems.

Jan 1, 1988

By Kennerley P

A significant part of the reserves of the Southern Coalfield lie beneath major water storages and their impounding dam structures. One of the functions of the NSW Government's Dams Safety Committee is to specify the particular mine layouts which can be used beneath the stored waters according to certain guidelines. A study was made of examples of the two different methods of extraction used under the stored waters as proposed by the mining company according to the guidelines and approved by the Dams Safety Committee. Using both pillar monitoring and mathematical modelling approaches it was shown that the recovery of coal from these layouts could be improved while still ensuring the long term stability of both the underground support pillars and the body of the strata. The integrity of the water storages and their impounding structures would therefore not be Affected.

Jan 1, 1986