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By W. S. Landers

This report presents a study by the Federal Bureau of Mines of technical factors related to the production of special carbon and tar from selected Wyoming coals. Certain Wyoming high-volatile bituminous and subbituminous coals were processed in bench-scale apparatus to determine potential carbonization yields and in pilot plant retorts to produce sufficient char and tar for testing. These tests have shown that a critical selection of coal is necessary when the coal is processed for a specialized carbon. Generally high yields of tar are obtained from low-temperature carbonization of Wyoming high-volatile bituminous and subbituminous coals, and the yield of tar usually increases with increase in rank within this range of coals. The production and evaluation of industrial carbons from Wyoming coals by using pilot plant and bench-scale techniques is part of the continuous program of upgrading western coals. It has been found that: 1. Most Wyoming coals are nonagglomerating and may be carbonized in fluidized systems. Chars produced in pilot plant retorts at low temperatures contain about 17 to 23 pct, residual volatile matter and are easily ignited. These chars appear suitable as power plant fuel. The tar-plus-light-oil yields range from 14 to 40 gal./ton of raw coal processed. 2. Wyoming high-volatile coals produce a slightly smaller and somewhat weaker coke than currently mined Western United States high-volatile coals used commercially as blending stock in metallurgical coke production.

Jan 1, 1961

By Juan J. Monsalve, Nino Ripepi, Richard Bishop, Jon Baggett

"Terrestrial laser scanning (TLS) is a useful technology for rock mass characterization. A laser scanner produces a massive point cloud of a scanned area, such as an exposed rock surface in an underground tunnel, with millimeter precision. The density of the point cloud depends on several parameters from both the TLS operational conditions and the specifications of the project, such as the resolution and the quality of the laser scan, the section of the tunnel, the distance between scanning stations, and the purpose of the scans. One purpose of the scan can be to characterize the rock mass and statistically analyze the discontinuities that compose it for further discontinuous modeling. In these instances, additional data processing and a detailed analysis should be performed on the point cloud to extract the parameters to define a discrete fracture network (DFN) for each discontinuity set. I-Site Studio is a point cloud processing software that allows users to edit and process laser scans. This software contains a set of geotechnical analysis tools that assist engineers during the structural mapping process, allowing for greater and more representative data regarding the structural information of the rock mass, which may be used for generating DFNs. This paper presents the procedures used during a laser scan for characterizing discontinuities in an underground limestone mine and the results of the scan as applied to the generation of DFNs for further discontinuous modeling.INTRODUCTIONAccording to the Mine Health and Safety Administration (MSHA), between 2006 and 2016, the underground stone mining industry had the highest fatality rate in 4 out of 10 years, compared to any other kind of mining (MSHA, 2016). Additionally, during that same time, 40% of the fatalities were due to ground control issues, such as roof and rib collapses and pillar bursts. The National Institute for Occupational Safety and Health (NIOSH) developed guidelines for designing underground stone mines (Esterhuizen, Dolinar, Ellenberger, and Prosser, 2011). However, these guidelines do not apply to all underground stone mines.Monsalve, Baggett, Bishop, and Ripepi (2018) present a case study of an underground limestone mine experiencing a structurally controlled mode of failure. The authors analyze different methods to study that type of instability. They conclude that the integration of terrestrial laser scanning (TLS) with discrete element modelling (DEM) can be used to prevent rock falls in underground excavations to enhance worker safety. However, an adequate rock mass characterization and structural mapping must be performed in order to generate reliable models that allow the engineer to have a better understanding of the rock mass behavior."

Jan 1, 2018

By P. A. Crane, N. Shirley, Aung Moe, H. M. Nicholson, D. Kan

Kazakhstan’s first commercial copper-leach solvent extraction-electrowinning plant, Central Asia Metals’ Kounrad project, was commissioned in April 2012. Exploiting low grade waste stockpiles produced during Soviet era open pit mining, a 10,000 tpa copper cathode plant was designed, constructed and commissioned within 18 months. Overcoming initial challenges with a workforce unfamiliar with the technology and with extensive periods of sub-zero conditions during winter the project has consistently met targets and produced high quality copper cathodes at cash costs of less than US$1/lb. Challenges encountered during the first two years of operation are described and future plans briefly discussed.

Jan 1, 2014

By A. W. Fahrenwald

"About two years ago the Bureau of Mines, Department of the Interior, and the University of Idaho undertook an investigation of classification in its relation to table concentration of Idaho ores. The cooperation of the management of the Bunker Hill & Sullivan Co. in placing at our disposal their West Mill and facilities as desired, offered an unusual opportunity for studying the field of hindered classification in its practical and economic relation to table concentration.It has been shorn theoretically, and demonstrated experimentally, that ore products are more easily and economically concentrated on tables if the natural feed, consisting of various minerals and of all sizes of particles of each mineral, be classified or grouped into a series of products in which the mineral particles of greatest density are small in diameter relative to the diameter of the mineral particles of lesser density. Products in which the maximum difference in diameter of light and heavy minerals occurs are to be obtained only by true hindered settling classification. To our knowledge there has never been a really good hindered settling classifier used in practice and the present tendency seems to be to by-pass any attempt at such classification.After a careful study of the nature of hindered classification and of the requirements for hindered settling in practice, a classifier has been developed that takes fullest practical advantage of the widely known, but generally only meagerly understood, condition of hindered settling so well analyzed a number of years ago by Dr. Richards.The present paper presents briefly some of the more important practical results accruing through the investigation."

Jun 1, 1924

By Jim Clark

Tunnel boring machine (TBM) tunneling is an ever-increasing prospect for underground construction, and, with each new tunnel bored, there are unknown elements. When boring through the earth, even extensive geotechnical baseline reports can miss fault lines, water inflows, squeezing ground, rock bursting and other types of extreme conditions. This article draws on the consider-able field service experience within Robbins to analyze successful methods of dealing with the most challenging conditions encountered. Many tunnel projects are located in areas with relatively poor access along the tunnel alignment and bored under extremely high overburden. These two factors often result in limited geological information. It would be reason-able to state that the deeper the tunnel, the greater the lev-el of uncertainties. When faced with these uncertainties everyone involved with the project including the owner, the contractor and the machine supplier must be prepared to tackle geological surprises. This article describes the problematic geological conditions and associated difficulties faced on three separate projects and the measures that were taken to overcome these difficulties.

A viable flow sheet of the sorption-flotation technology for gold recovery from low-grade ores and concentrates using powdered activated carbon modified by organic compounds as the sorbent-bearer has been developed. The powdered activated carbon, with high kinetic ability and sufficient specific area, was selected as the all-purpose gold cyanide complex-bearing sorbent which is active during flotation. To improve carbon adsorption capacity and to provide the required floatability its porous structure was filled with a quaternary ammonium compound which can extract gold cyanide complexes and render additional flotation properties to the carbon. To optimise the process and to simplify the layout, adsorption and flotation processes were carried out simultaneously in a mechanical flotation cell. The proposed technology was used for extended and pilot-plant tests of sorption-flotation gold recovery from 0.6 g/t Au final tailings and 2.0 g/t Au gravity tailings. The extended tests were carried out on Taseevskaya (Chita Region) flotation tailings, whereas pilot-plant tests were conducted on Kommunarovskaya (Krasnoyarsk Region) gravity tailings passing to cyanidation, followed by processing with filtration technology. Additional gold recovery from Taseevskaya final flotation tailings was 50.8 per cent. Gold recovery from Kommunarovskaya final gravity tailings was 92.5 per cent. Compared to the complete sludge process conventionally used at the plant, gold recovery was increased by 7.5 per cent due to lower gold losses in the liquid phase and conversion of the refractory non-cyanided metal into a carbon concentrate. This paper presents the experimental results of gold adsorption onto powdered activated carbon modified with quaternary ammonium compounds (sorbent-bearer) as well as sorbent-bearer flotation with various collectors from cyanide solutions and pulps.

Jan 1, 2005

By Robert Boehnke, Bernd Mueller

This contribution presents an innovative, statistically supported method to predict blast vibrations in rock mass. For modelling the processes during and after detonation, a theory is employed which is based on linear momentum (so-called momentum theory), strongly supported by new measurement methods. During the course of the investigations, the following parameters have been found to dominantly influence vibrations: ! charge WB, includes geometrical factors such as borehole length and diameter (kg) ! detonation velocity cd of the explosives used (m/s) ! distance r between the points of emission and immission (m) and the statistically determined negative exponent n ! factor RM or RS of the rock mass which is related to the specific blast momentum and the drilling and blasting technique used and is statistically determined together with the exponent m (mm/kg or mms/kgm)

Jan 1, 2004

By W. K. Gummer

"THE LOCATION of Canada's present aluminum industry is determined by availability of hydroelectric power, and ready access to ocean transport facilities. The chief raw material for the production of the metal is imported by ship over several thousand miles of water. In times of freedom of shipping and uncontested movement this provides the industry with its cheapest method of operation. However, during the early part of the last decade the general conditions of ocean and rail transportation were such that interest in the treatment of materials other than bauxite was greatly stimulated. This was the case not only in Canada, of course, but in most other countries.Canada has no deposits of bauxite and much research was carried out on other aluminous materials, chiefly silicates, in an effort to develop more or less economic and feasible methods of treatment. In the United States, this research was considerably more extensive. Some projects were early shown to be of little or no value, whereas others, including the widely publicized lime-sinter and soda-lime-sinter methods, became important. In North America, however, apart from the application of the sinter method to the hitherto waste-product (red mud) of the normal Bayer plant operation, none of these processes contributed appreciably to the production of aluminum during the war. In certain European countries, on the other hand, largely because of their situation with regard to bauxite deposits, they had a more general application, and Germany, for example, produced alumina from clay, ashes, and slag by at least four methods."

Jan 1, 1952

By S. Deming

Coal is China's main source of energy. In 1988, 76.1% of commercial energy consumption was supplied by coal. To provide a rational utilization of its coal resources, China has paid considerable attention to coal preparation over the last 10 years. In 1980, there were only 105 washeries treating about 100 million tonnes of coal, but by 1988 there were 151 washeries treating 171 million tonnes per year. This paper describes the development of China's coal preparation industry; its growth, the equipment, and the technology. Statistics and information on the current status of the industry are also be presented.

Jan 1, 1991

By J. F. T. Agapito

Stability in Exxon's Colony Pilot Mine in the Piceance Creek Basin, Colorado has been monitored by periodic pillar stress-determinations End roof-to-floor convergence measurements since 1971. Pillar failure has caused marginal stability in some areas of the mine. Measurements taken during the process of failure provided valuable information on the in-situ pillar strength and long-term behavior of the mine structure. Four pillars were reinforced by 32 mm (1-1/4 in) diameter tensioned grouted bolts to increase long-term stability in the northern area of the mine. Stability of this area is necessary because future plans envision its use as an exit/access and ventilation exhaust. Computer analyses were performed to help evaluate the effect of pillar reinforcement on long-term stability. Results indicate that bolting is particularly useful in stabilizing failed pillars, but its effects are significant only in the immediate area of the pillar. The projected significant decrease in deformation of two extensively failed pillars near a main entry indicates that bolting reinforcement will assist the long-term stability of the opening.

Jan 1, 1985

By J. N. Van der Merwe, M. Mathey

"The development and mechanical characterization of coal-crete, a composite material generated from coal fragments and some binder material, is described in this paper. Coal debris was obtained from a colliery in South Africa. The binder used in the study basically consists of cement and water, and further ingredients are added to the mixtures, such as sand, fly ash and polymers, in order to investigate alterations of the mechanical properties of coal-crete.Results from over 220 mechanical tests on coal-cretes with various binder mixtures give consistent trends for the material’s behaviour. Linear relationships are suggested between the uniaxial compressive strength, Young’s Modulus and the indirect tensile strength of the coal-crete.It is shown that mechanical properties comparable to coal can be achieved. Coal-crete is therefore suitable for physical modelling of mining situations in experimental studies and for use as backfill in underground coal mines. The latter application is particularly attractive when refuse coal is used as aggregate material. The indicated trends in this study may be used as a guideline for individual coal-crete design needs. However, some uncertainty remains as to the influence of particle shape, size and gradation, coal rank and age of the coal-crete. These aspects are recommended for further research."

Jan 1, 2015

By L. Becze, B. Pierre, S. Di Carlo, G. P. Demopoulos

From January to June 2007, the autoclave production at the Kidd Metallurgical Site was severely affected as a result of plugged discharge lines and extensive precipitation/crystallization of sulphates that caused massive scaling in different autoclave compartments. Work was performed at McGill University to understand the root causes. The crystallization of zinc and ferrous sulphate salts was investigated in terms of solubility measurements. Scale samples were characterized using chemical and mineralogical-spectroscopic analysis. In this paper, following a description of the Kidd zinc pressure leach operation, highlights from this investigation are presented and solutions used to overcome the problem are outlined.

Jan 1, 2008

By A. E. Isaacson

The U.S. Bureau of Mines is investigating a systems approach to metals recovery from leach liquors produced by in situ leach mining techniques. A successful in situ leaching process requires a thorough under-standing of the complex interrelationships that exist between leaching chemistry and metals recovery. Laboratory research is addressing these interrelationships in the solution mining of a copper oxide deposit. Laboratory tests have been conducted to gather baseline data related to the design and operation of continuous leaching-solvent extraction-electrowinning circuits. This paper addresses the findings of the baseline studies. Specific results include the characterization of simulated in situ leach liquors produced by leaching chrysocolla and chrysocolla-atacamite-bearing copper ores. Metal recovery procedures, utilizing four commercial solvent extraction reagents, are also characterized, and potentially troublesome leach liquor contaminants that may complicate waste management procedures are identified.

Jan 1, 1990

By W. R. Dengler

Dynatec Mining Limited contracted to sink a lS00 metre (4960 ft.) concrete lined shaft for Falconbridge Nickel Mines in Sudbury, Ontario, Canada. The shaft is 6.3 metres (20.S ft.) in diameter inside the concrete lining and is equipped with steel furnishings. Dynatec used the owner supplied 4.6 metre (l5 ft.) diameter double-drum hoist to sink the shaft with 12.S tonne buckets for muck removal and 4 cubic metre concrete buckets for concrete placement. One of the unique features of the shaft sinking operation is the use of a four-boom electric hydraulic drill jumbo permanently mounted in the shaft sinking stage. This paper will describe the performance obtained with the electric hydraulic drilling equipment and the high capacity muck removal and concreting equipment.

Jan 1, 1992

By A. Noble

"A supply of sustainably sourced rare earth elements (REEs) is critical for several high-tech industries, renewable energy technologies, and defense applications. Recent studies have shown that REEs exist in coal and coal combustion byproducts at elevated concentrations and in quantities that could meet domestic demand. Despite these promising findings, declines in rare earth prices, volatile commodity markets, and challenging geo-metallurgical conditions have jeopardized this potentially valuable REE resource. While the dilute REE concentrations inherently necessitate low-cost separation technologies, the ultimately operating cost threshold for economic extraction must be based on commodity price projections and market demand. In this paper, the micro-pricing principle is used to develop a rigorous economic model assessing the inherent value of REEs in coal materials. This model is based upon basket pricing of individual elemental oxides, and elemental distributions of coal samples from various basins. These results may be used to assess the economic viability of potential REE concentration and refining technologies INTRODUCTION Recent efforts by US Department of Energy (DOE) and the National Energy Technology Laboratory (NETL) have suggested that rare earth elements (REEs) may exist in coal and coal byproducts at concentrations suitable for economic extraction and processing. While the knowledge of REE occurrence in coal material dates back over 50 years, recent supply restrictions and material criticality considerations have prompted a national interest to establish a sustainable domestic supply of REEs. REEs are not “rare” in the sense of crustal abundance; however, few natural processes lead to concentrated ore deposits. As a result, the elevated concentrations found in coal material may provide a potentially promising resource for these materials. While the term “rare earths” is often used to describe a singular concept, the 15 rare earth elements actually have varying and sometimes contrasting scarcity and cost profiles. Various authors have proposed classification systems to provide information on REE criticality (e.g. Seredin and Dai, 2012, Zhang et al., 2015). The most straightforward classification is provided on the basis of geochemistry with designations for “light”, “medium” and “heavy” rare earths. Light rare earths (those to the left of the periodic table: Ce, Pr, Nd, and Sm) tend to be more common and less valuable when compared to their medium (Eu, Gd, Tb, Dy, and Y) and heavy (Ho, Er, Tm, Yb, and Lu) counterparts. While light rare earths are often found in traditional ore deposits at economic concentrations, the heavier rare earths are almost exclusively found as ion-absorbed clays (Seredin and Dai, 2012)."

Jan 1, 2016

By I. Westermann, K. Marthinsen, M. S. Remøe

"Al-Mg-Si alloys often add small additions of e.g. Mn or Cr, to form dispersoids, which may act as nucleation sites for Mg2Si particles after homogenization. The purpose is to ensure a high density of uniformly distributed small ?’-particles, which can be dissolved during further processing prior to the final age hardening step. However, their density and spatial distribution are critically dependent on the homogenization procedure. It is therefore important to have a robust and reliable method for assessing their spatial distribution. In the present work an existing methodology for assessing spatial uniformity, the Global Shannon Entropy (GSE), has been implemented and evaluated for different dispersoid structures characterized by scanning electron microscopy. This metric is highly dependent on the parameters used, but by careful selection of adequate parameters, it can be effective in detecting non-uniformity. An important weakness with the GSE was identified, and a modification to improve on the ability to differentiate degrees of non-uniformity is suggested. To evaluate the proposed methodology, the effect of heating rate on dispersoid precipitation behaviour during homogenisation of four Al-Mg-Si alloys with different Mn/Cr-content has been investigated. The metric with the new term has demonstrated promising results, and improved the ability to differentiate degrees of spatial uniformity.INTRODUCTION Al-Mg-Si series alloys are the most common aluminium extrusion alloys and are attractive for applications in a range of sectors (e.g. construction, automotive and recently also in consumer electronics), due to their generally good combination of strength, ductility and corrosion resistance. However, their extrudability and end properties depend critically on the alloy chemistry as well as prior processing conditions. Coarse ß-AlFeSi or Mg2Si-particles typically have a detrimental effect on extrudability, while small dispersoid particles may affect recrystallization, grain growth and precipitation of Mg and Si. The strengthening potential in the final age hardening step depends strongly on the amount of Mg and Si in solid solution after extrusion. The manner in which these particles are spatially distributed will decide whether the final product will exhibit uniform properties, and the number density and sizes will determine the extent of the effect. As such, these are important characteristics."

Jan 1, 2018

By B. Pesic

The recovery of silver and gallium from flue dust with acidified thiourea solutions was examined. The studied parameters were temperature, particle size, thiourea concentration, acid concentration, and the presence of oxidants. The study of the extraction of these two metals was undertaken in sulfuric acid medium. Silver dissolution was dependent on all examined parameters, whereas gallium extraction was only dependent on the initial acid concentration. The experimental results suggest a new very efficient method for recovery of both silver and gallium. Almost complete recovery of silver and gallium can be accomplished within 90 minutes. A technological scheme for recovery of both metals is also proposed.

Jan 1, 1986

By J. A. Mielczarski

An infrared external reflection spectroscopy (ERS) technique has been developed to study the structure of the adsorbed layer of ethyl xanthate formed on copper and natural chalcocite (Cu2S) electrodes. The infrared technique provides information concerning the identity and the orientation of the adsorbed species at monolayer and submonolayer coverages. X-ray photoelectron spectroscopy (XPS) studies have also been conducted to monitor changes at the surface. The results show that the first oxidation peak on the voltammograms for copper and the first and second oxidation peaks on the voltammograms for chalcocite electrodes are not characteristic of a chemisorbed xanthate species, which is contrary to what has been reported by other investigators previously. As evidenced by the XPS spectra, there was an increase in sulfur relative to copper on the copper and chalcocite surfaces over the potential region where these oxidation processes occur. The spectroscopic results (ERS, XPS) indicate that the second and third (on copper) and the third and fourth (on chalcocite) oxidation processes recorded on the voltammograms are due to cuprous ethyl xanthate adsorption. The orientation of the adsorbed molecules of xanthate was observed to change with increasing surface coverage. Therefore, it has been concluded that xanthate can modify the copper and chalcocite surface in two different ways. At lower potentials, xanthate is a source of sulfur for the formation of a sulfur-rich surface. At higher potentials, an adsorption layer of cuprous ethyl xanthate is formed. Contact angle measurements show that both of these processes of xanthate surface modification lead to an increase in the hydrophobicity of the substrates.

Jan 1, 1990

By Kumar M. Lyer

Residence time distribution (RTD) of light and heavy liquids in a pyrometallurgical channel reactor was mathematically modeled by representing the reactor as a combination of ideal reactors. Cold model studies simulated the counter-current flow of slag and matte (or metal) with high-strength bottom gas injection. The experimental variables include flow rates, heights, density and viscosity of the two liquids; gas flow rate; injector diameter; and distance between injectors. The experiments covered a wide range, of the appropriate dimensionless parameter, including conditions in ferrous and nonferrous extractive metallurgy. Dispersion modeling studies were also carried out to determine the degree of backmixing. Results indicate that the degree of backmixing in the channel reactor for various operating conditions corresponds to that for 3-20 perfectly mixed reactors in series.

Jan 1, 1993

By M. Kaya

This paper presents an experimental method to determine the degree of gangue entrainment in mechanical flotation cells and proposes new and inexpensive methods to lessen it. The applicability of froth washing and vibration was studied in laboratory, pilot plant, and plant scales. The effect of wash water on metallurgical performance was tested with various streams from the Falconbridge Strathcona mill at laboratory, pilot, and plant scales, with the 2nd cleaner at the Eastmaque Kirkland Lake mill, and with the 2nd and 3rd zinc and 3rd and 4th copper cleaners at Les Mines Selbaie mill. It was found that gangue recovery was closely related to water recovery in all systems. Wash water at an optimum superficial rate from 0.03 to 0.07 cm/s reduced entrainment by anywhere from 30X to 70X. Wash water can be further assisted by mechanical and ultrasonic vibration of the froth. A further rejection of 10 to 20X becomes possible. As a result of this work, a number of plants in Canada and in the United States have evaluated and/or are now using froth washing.

Jan 1, 1990