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By Raymond J. Isherwood

The U. S. Bureau of Mines has investigated the domestic primary and secondary lead smelting and refining industries to determine the economic impacts of existing and proposed environmental, health, and safety regulations. The impacts are assessed in terms of capital and operating costs for existing and alternative smelting/ refining technologies. Industry response to regulatory implementation is estimated and quantified in terms of import value from lost lead production. For the primary lead industry, regulatory compliance may add up to 1.15 ¢/lb refined lead to operating cost for rehabilitated plants. Alternative smelting/refining methods could reduce net operating costs by as much as 4.36 ¢/lb refined lead. Capital expenditures would vary from $750 to $1,000 per annual mt of smelter capacity. Secondary lead smelter operating costs would increase about 3.8 ¢/lb refined lead to comply with existing regulations. Capital expenditures would average about $124 per annual mt of smelter capacity. Implementation and enforcement of proposed regulations would result in closure of the primary lead industry and additional expenditures for compliance by the secondary lead industry. Enforcement of the most extreme proposed regulations would force the secondary lead industry to close.

Jan 1, 1988

By S. K. Vidyarthi

Most wastewater clean-up processes suffer from a fundamental lack of specificity in that a Reverse Osmosis process removes all dissolved solids, an Electrodialysis Reversal process removes all ions, wanted or unwanted, etc. Most techniques require the use of a membrane or contact surfaces that are prone to foul-up and are ineffective in situations where solids may be present. A photochemical process for the metallurgical industry on the other hand has the ability to operate specifically on targets that can range from one selected ion to an entire group of homologous species such as all biologically active species. Processes can be designed to change the oxidation states of a target altering the environmental impact. Several processes are currently in operation ranging from Cyanide removal to disposal of radiation wastes. This paper describes applicable photochemical processes with the help of certain key model examples.

Jan 1, 1988

By Torrance AC

A joint research programme conducted by BHP Central Research Laboratories and Du Pont Wesfarmers Pty Ltd examined the effect of the size of cast primers on the run up and steady state detonation veloci- ties of ammonium nitrate based explosives as a function of blasthole diameter. Both continuous and point to point velocity of detonation meas- urement techniques were used. The field trials examined a number of the Du Pont HDP series of primers in conjunction with ANFO, emulsion and watergel explosives. Results indicate that the run up velocity of 187mm diameter ANFO charges is negligible using cast primers as small as 150g. owever, emulsion and watergel explosives did exhibit run up in both 187 and 311mm diameter blastholes, independent of the size of primer. This could last from 7 to 10 blasthole diameters.

Jan 1, 1988

By R. Harris, M. Misra

Column flotation technology has a demonstrated potential for recovering clean coal from high-ash waste fines. The effect of different variables such as air flow rate, frother addition, depressant addition, percent solids and particle size on the quality of separation are discussed. Results indicate that air flow rate and depressant addition are the important variables which control the selectivity in the flotation of fine coal in a column cell. Separation efficiency achieved with column cells is significantly better than that with conventional flotation cells. Under appropriate experimental conditions with a deep column, more than 80 percent coal can be recovered in the concentrate containing 10 percent ash from waste fines containing over 60 percent ash.

Jan 1, 1988

By R. Frenette, A. W. Mo, H. A. Hamza

Fine particles present major technical and economic problems to those who deal with solid/liquid separation processes. In the coal industry the problem is compounded by the large amounts of produced fines such as those present in Western Canadian coals. Flocculants in the form of high molecular weight water soluble polymers are commonly considered an effective solution for the enhancement of the separation process. These reagents are relatively expensive especially when considering a low-price commodity such as coal. Optimization of the use of these reagents is therefore an operational necessity. Six polymers were evaluated as to their effectiveness in flocculating a fine coal tailing. Results were compared with those for a reference flocculant, in-use at that time in the washery. It was shown that, in general, flocculants significantly improve the solid/liquid separation process. The ranking of the flocculants as to their effectiveness in settling and filtration indicated that the best flocculants for settling were not necessarily the most effective for filtration. Flocculants that showed the best filtration improvement were generally cationic and those best for settling were anionic.

Jan 1, 1988

By Bowdler RJ, Lowson RT, Sarbutt JV

There have been few long-term studies of sulphide oxidation under controlled conditions. The object of this study was to investigate the oxidation and leaching characteristics of pyritic mine material under conditions that were commensurate with field conditions but which could be controlled and monitored on a long term basis. The test material - overburden from Woodlawn Mines Pty Ltd - was packed into a 300 cm high column and leached with water at an infiltration rate of 256 mm y-1 for 5 years. Chemical conditions within the column were continuously monitored by sensors embedded in the overburden and leachate from the base of the column was analysed weekly. The study examined the relationships between heavy metal release and gas, moisture, and chemical conditions in the column.

Jan 1, 1988

By Minchinton A

CPeX is a non-ideal explosive performance prediction model. The model takes into account the rate of energy release, the extent of chemical reac- tion and the effect of confinement on energy release. The model resolves the explosive energy into `shock' and `heave' com- ponents as a function of explosive type, hole diameter and rock type. The predictions of the model are compared for a bulk emulsion, and a prill-doped bulk emulsion in soft rock. The predictions, based on calibra- tion of the model with simple unconfined detonation velocity measure- ments, show the significant effect of non-ideality on explosive Performance.

Jan 1, 1988

By Derk G. E. Kerfoot

The extractive metallurgy of nickel and cobalt has proved to be a particularly fruitful area for innovation in hydrometallurgy and electrometallurgy ever since the development of the Hybinette process for nickel in the early 1900's. In current practice, nickel concentrates are generally smelted to high grade mattes which are then refined to metal by a combination of hydrometallurgy and electrometallurgy, although low grade copper-nickel concentrates are refined directly by the ammonia pressure leach process. Matte refining processes in commercial operation include the direct electrolysis of matte, the ammonia pressure leach, sulphuric acid leaching using air or oxygen at elevated pressure, or at ambient pressure, and chlorine or chloride leaching. Refined nickel is recovered either as electrolytic cathode, or as metal powder by hydrogen, reduction. Hydrometallurgy has also found application in the treatment of nickel laterite ores, both in the reduction roast ammonia-ammonium carbonate leach process, pioneered by Caron and in the Moa Bay acid leach process. Cobalt is recovered as a co-product of copper in central Africa, and as a byproduct of hydrometallurgical nickel refining elsewhere. In the African plants, the copper-cobalt concentrates are roasted and leached in sulphuric acid solution, and copper and cobalt are recovered separately from the leach solution by direct electrowinning. A variety of hydrometallurgical techniques are used for the separation of cobalt from nickel, including selective precipitation and crystallization, solvent extraction, and ion exchange. Like nickel, refined cobalt is recovered either as electrolytic cathode or as metal powder by hydrogen reduction.

Jan 1, 1988

By S. K. Kawatra, K. A. O, DeLa&apos

On-line sensors and process controls are important for efficient operation of coal preparation plants. The objective of this paper is to describe the current practice in on-line measurement of composition, density, moisture, level, flow and weight. This paper also discusses how on-line sensors can be implemented in process control, and how sensors which are currently being developed can be utilized.

Jan 1, 1988

By M. Fiset, D. Belley

"In a country with a cold climate like Canada, the cost of replacing worn parts of snowplow equipment such as blades, is enormous. A great number of these blades, with different mechanical properties, are available, but few studies have been made to facilitate their selection according to the optimum ratio of wear resistance to cost. To attain this objective, laboratory tests have been developed to correlate test results with those obtained from various road service conditions. The test materials, 1080steel in different states, 1090steel and D2 tool steel were chosen to cover a large range of hardness as well as different microstructures. Comparison of the wear resistance of the test materials relative to a standard revealed, in general, a good correlation between the results of laboratory cement wheel tests and those from the road tests. Scanning electron microscope wear scars of laboratory and road test specimens were compared to determine if similar removal material mechanisms were active. IntroductionThe correlation between wear tests in service and those performed with the aid of laboratory equipment is of considerable interest. As a matter of fact, when correlation exists, it allows one to evaluate the performance of a material more easily and at a lesser cost.Several authors have been interested in simulating various wear circumstances, especially abrasive wear. In particular, the simulation of wear on implements working the soil, has been tried by several researchers. The test using the rubber wheel seems to be the one giving the best correlation if the soil is rather sandy and its moisture content is low.However, little work has been done concerning wear on the plates, skids and blades attached to trucks used for levelling and snowplowing; such equipment being used to keep roads clear in northern countries. Now each year, companies introduce new steels by claiming that the y are superior in performance to their predecessor s and invariably they demand a higher cost. The study presented here was undertaken with the goal of making a more judicious choice of these steels by simulating their behaviour in the laboratory. Moreover, the examination of abraded surfaces in situ and in the laboratory have also allowed us to compare the respective wear mechanisms."

Jan 1, 1988

By Michael P. Moore, Christopher J. Rise

"Over the past twenty years, there have been numerous studies which have attempted to correlate the prevalence of Coal Workers' Pneumoconiosis (CWP) with different characteristics of the coal seam. Some investigators have tried to find a relationship, or the lack of a relationship, between the rank of coal seams and the incidence of CWP. Others have attempted to show that there is a positive correlation between the mean mass of respirable dust in the mine atmosphere and the prevalence of CWP. Still others have tried to determine the influence of the quartz content of respirable dust on the incidence of CWP. Unfortunately, many of these different investigations have conflicting conclusions.One area of research with conflicting conclusions deals with the relationship between the rank of the coal and the incidence of CWP. For example, an inves¬tigation conducted in Pennsylvania and West Virginia coal mines concluded that the prevalence of CWP increases with an increase in coal rank (1). A study in Great Britain also observed a close relationship between the rank of coal and the prevalence of CWP (2). However, another study involving 312 Appalachian coal miners concluded that the association between coal rank and CWP might be fortuitous and that other factors may be more important (3). In addition, an investigation involving 2,600 miners during a period of twenty years in Great Britain established that there is only a weak correlation between the prevalence of CWP and the rank of the coal (4). Consequently, it appears that there is still uncertainty as to whether or not the rank of the coal seam has an influence on the development of CWP.Another area of investigation concerns the relationship between the mean mass of respirable dust present in the mine atmosphere and the prevalence of CWP. A study involving 4,122 miners over a period of ten years in Great Britain noted a high correlation between the mean mass of respirable dust and the incidence of CWP (5). Another investigation involving 3,154 British face workers con¬cluded that the overall mass of respirable dust is the factor most closely related to the ten-year attack rate of CWP (6). However, a study conducted in thirty-one mines in the United States concluded that it is doubtful that the quantity of respirable dust alone is responsible for the difference in the prevalence of CWP (7). Even though there are conflicting conclusions, there are many more investigators who confirm, rather than deny, the relationship between the mean mass of respirable dust and the development of CWP.The third subject of investigation is the role of quartz in the incidence of CWP. For example, two studies in Great Britain concluded that the quartz content in coal mine dust has no relationship to the prevalence of CWP (8,9). But a study involving 312 Appalachian coal miners revealed that the level of exposure to free silica plays an important role in the development of CWP (10). Once again, the conclusions reached by different researchers are conflicting.Probably the most important factor in the discrepancy among the studies is the variability among different coal mines. A mine operating in an inherently ""dusty"" seam may have a low concentration of respirable dust while a mine operating in a less dusty seam may have a high concentration of respirable dust. This discrepancy is a result of variables such as the effectiveness of ventilation or the efficiency of the water sprays. Consequently, it is very difficult to compare the dustiness of different coal seams by in-mine measurements of the respirable dust concentration. A laboratory test would more accurately characterize a coal seam according to its respirable dust production."

Jan 1, 1988

By Brigden J. F, Birrell

A regional geochemical exploration programme commenced in July 1983, based upon low-density sampling of lateritic duricrust over parts of the Yilgarn Block of Western Australia. This resulted in recognition of an area significantly anomalous in chalcophile elements that progressively led to the discovery of the Johnston Range gold deposits in 1985. The deposits, on the Barlee 1:250,000 map sheet, occur in four mineralized zones, and production is expected to commence during 1988. The programme leading to the Johnston Range discoveries was a collaborative research/ applications study between the AGE Joint Venture (Greenbushes Ltd., St. Joe Minerals, and from 1985, Sons of Gwalia NL) and the CSIRO Laterite Geochemistry Research Group (Smith, 1987). It built upon a precursor project sponsored by Greenbushes Tin Ltd that commenced in 1980 and arose from an orientation laterite research project in the Greenbushes rare metal pegmatite district (Smith et at., 1987). Both were multi-commodity programmes and included the search for gold deposits. Basic methodologies for sampling and data interpretation have been described by Smith and Perdrix (1983) and Smith et at. (1984). Continuous geochemical coverage of designated parts of greenstone belts was sought using a triangular grid of 3-km or 1-km spacing, depending upon the expected prospectivity of the areas and the size and characteristics of the ore deposit targets. First-pass sampling, that resulted in the Johnston Range discoveries, was at 3-km spacing and several samples within a 30-km by 5-km area were

Jan 1, 1988

By Hang G, Hongtian X

In this paper, it is briefly introduced that China's Ordovician limestone confined-water menaces coal mining and Ordovician water is prevented and cured to secure the safety of coal mining. The theory of "Down-Three-Zones" is presented on the basis of research and practice in recent ten years. The concept of "Down-Three-Zones" of floor water-eruption is described clearly. Finally, the principle and method of applying the theory of "Down-Three-Zones" are discussed. 1. An Introduction of Damage: China is rich in coal resources. The conditions of coal field geology are quite complicated. There is an area of two million square kilometre of Karst limestone in nine million six thousand square kilometres of territory. The resources of underground water are rather plentiful, but this menaces coal exploration. Sixty percent of coal mines in China are damaged by limestone confined-water in different scales, particularly coal mines located the Carboniferous-Permian coal fields of the Ordovician limestone distribution area of Northern China. Because there is the 500-800 metre thickness of Ordovocian limestone and the well developed Karst containsl plentiful water, Karst water can have more than 100 Kg/cm pressure. Limestone aquifers have only distances of several metres or several decade metres to coal seam, Karst water can enter the aquituge and even the coal seam, large eruptions often occur. For example, a mine of 3 million ton production capacity had an eruption of 2053 cubic metres per minute. This is the largest confined-water eruption which has brought enormous economic damage and threatened the safe production of coal mining. Therefore, the prevention and cure of Ordovician water has immense advantage to the development of the coal industry. There are several decades experience in the prevention of Ordovician water-eruption in China. The prevention of Ordovician water-eruption has two kinds of plans. 1) dewatering and depression: it refers to dewatering of aquifers as roofs of seam and depression of aquifers as floors of seam in mining areas. 2) comprehensive prevention under the condition of having water pressure in aquiters. Due to enormous water, electricity, equipment and lots of other factors, the former isn't used extensively, the latter tits to China's actual conditions and is used widely. So-called comprehensive prevention under the condition of

Jan 1, 1988

By Neil Schofield

"The Pine Creek gold mineralization is associated with saddle reefs and quartz and quartz sulphide veining within the Enterprise Anticline. The anticlinal structure is complex and the mineralization was considered prior to development to be dominantly strata controlled. Gold grades vary up to 160 gin 1.5 m core samples with coefficients of variation in excess of three.The estimation of ore reserves for such a deposit must account for both the geological complexity and the extreme variability of gold grade.This paper describes the structural and variogram analysis of the gold grades and demonstrates the importance of incorporating the geological model in such an analysis. Variogram interpretation is greatly improved and greater insights into the finer geological structure areprovided. Part 2ofthis work presents the application of multigaussian kriging to reserve estimation for deposits with highly variable grade and which consequently demand highly selective mining operations. IntroductionThe Enterprise Gold Mine is situated some 220 km southeast of Darwin in Australia's tropical north. Gold is believed to have been discovered there in 1869 during the construction of the overland telegraph line.From 1894to 1915, some 75 000 ounces of gold were produced from 121 000 tonnes mined mainly by Chinese leaseholders. From 1906 to 1915, government-sponsored drilling led to the sinking of the Enterprise Shaft to 79 m and several drives were developed. Mining ceased because of war.Since late 1980, Goldfields Exploration Pty. Ltd. had explored on several mining tenements near Pine Creek under joint venture with the title holders, Enterprise Mines NL. This work culminated in the development of the current mine which opened on October 29, 1985.Feasibility studies to determine the economic viability of mining were based on ore reserves generated by project geologists using a sectional polygonal approach tuned to the interpreted geological control of the mineralization.The study motivating this two-part paper covers are-estimation of the recoverable reserve s using the geostatistical approach of multigaussian kriging developed at Stanford University, (Verly, 1984)."

Jan 1, 1988

By Dickson B. L

Groundwater geochemistry is controlled by chemical interactions with aquifer rocks, and offers a powerful geochemical exploration technique for locating concealed mineral- isation. Techniques are applied for identifying constituents of aquifers using the compositions of their groundwaters, collected from the surface through drill holes, water bores or springs. Even slowly moving groundwaters have passed through large volumes of rocks which surround any sample site. Products from these rock-water contacts modify the groundwater. By relating water composition to the minerals from which the dissolved species may have been derived, geochemical exploration information is obtained for a significantly larger zone than is represented by drill hole rock samples. In this paper we describe some solution chemical tech- niques we are applying in mineral exploration, particularly in areas of Australia where ground- waters are highly saline and contain enhanced concentrations of trace metals. EQUILIBRIUM MODELS FOR SALINE GROUNDWATERS Central to our technique is the assumption that in low rainfall regions, aquifer rocks and contained groundwaters are in chemical equili- brium. Solubility calculations then allow us to predict upper limits to the soluble products of groundwater interaction with aquifer rocks and to identify minerals with which the groundwater is saturated. Whilst equilibrium calculations require input of concentrations of all dissolved species, they are actually based on "activity" of dissolved species rather than the analysed concentrations. Unless waters have very low ionic strengths (a measure of total dissolved solids), activity of a solute is not equal to its analytical concentration but equals concentration multiplied by an "activity coefficent". Several methods exist for calculating mineral solubilities. The ion-association model, commonly used in programs such as WATEQ (Truesdell and Jones, 1974) and later deriv- atives such as MINTEQ, assume the formation of complex ions such as MgSO4(0), CaCl+, which are described by formation constants. Activity coefficients are obtained by the extended Debye

Jan 1, 1988

By N. S. Dalal, X. Shi, V. Vallyathan

"Correlated spectroscopic and cytotoxicity measurements were made on newly crushed silica to find whether the fracture-induced, silicon related (Si-0· or Si· type) free radicals play a direct role in the mechanism of hemolysis by silica particles. The free radical content of the silica particles was controlled through the radical decay, thermal annealing, and boiling processes, and was followed with electron spin resonance spectroscopy. Portions of the same sample were evaluated for their hemolytic potential, employing sheep erthyrocyte and optical absorption techniques. The results indicate little, if any, correlation between the amount of the silicon-based radicals and the hemolytic potential of the fresh dusts, but these or related radical sites might be contributors to silica cytoxicity and fibrogenicity via peroxidative pathways .INTRODUCTIONIn an earlier convnunication (1.) from our laboratory it was reported that mechanical crushing of coal and quartz under normal air atmosphere generates free rad;cals on the particle surfaces, and that these radicals decay with time, hence pointing to a higher toxicity of fresh dusts in relationship to pneumoconiosis and silicosis. More recently Fubin; et al.(2) have also reported the detection by electron spin resonance (ESR) of the formation of SiO· and Si·-type of radicals from quartz particles crushed under atmospheric conditions. In agreement with earlier ESR studies on single crystals of quartz crushed under high vacuum (10-10 torr) (3) and subsequent exposure to air (3), and to other gases (4), these radicals were identified (2) as being formed by the hemolytic cleavage of the Si-0-Si bonds and the reactions of the Si· and SiO· ,radical with atmosphere. Fubin; et al. (2) also suggested that these radicals might be involved in the mechanism of the fibrotic action by silica, either by transforming the particle surface into a selective oxidating agent or as an initiator of a sequence of reactions leading to fibrosis. Earlier Gabor and Anea (5) had reported that lipid peroxidation caused by free radicals on the silica surface might be involved in the red blood cell membrane damage. Thus far, however, no parallel cytotoxicity, fibrogenicity, and free radical studies on a given Quartz dust sample have been reported, except for some earlier work from our laboratory (1,6,7). We now present more recent results obtained from parallel cytotoxicity, fibrogenicity, and free radical measurements on a freshly made quartz dust. The dust’s free radical content was measured using ESR spectroscopy while its cytotoxicity poteni1al was estimated via hemolysis. Hemolysis was employed as the tox1c1ty test because it 1s a widely used method for estimating the potential of a dust for disrupting the cell membrane (8). The f1brotic potential was followed.by measuring the dust-induced lipid perox1dat1on. us1ng linole1c ac1d as a model lipid. As discussed below, the results obtained suggest new clues.to the mechanism of the Quartz-related cytotoxicity and fibrogenicity."

Jan 1, 1988

By Adrian Brown

Groundwater inflow and impacts have become major aspects in the permitting and operation of many gold mines. First, the hydrothermal or placer genesis of many of the orebodies being investigated or produced today almost guarantees that mines will be "wet", involving groundwater control as part of operations. Second, the style of ore deposition a1 so often involves a1teration of the host rock, resulting in relatively weak, low permeabi1ity materials that require extensive groundwater pressure control for stable mining. Third, the location of many mines in arid areas guarantees that impacts on water resources will be matters of key focus during permitting and operation. However, groundwater control and protection is a technically difficult area and often involves managerial decisions and activities that do not fit comfortably into traditional mining. In an attempt to overcome some of these difficulties, this paper provides a guide to mine managers and hydrologists as to appropriate strategies for designing, setting up, operating, and evaluating groundwater programs at gold mines that get the job done and are cost effective.

Jan 1, 1988

By Culshaw MG, Deaves AP, Bell FG

The accurate prediction both of the water ingress into sub-surface excavations and the nearby groundwater pressures is of fundamental importance to the control of the stability and flooding of tunnels or mines constructed below the water table. Predic- tions are usually based on laboratory and in situ permeability determinations together with observations of groundwater conditions in boreholes. Although established theoretical methods provide a basis for prediction, the actual ingress depends on many factors. The objective of this paper is to explore the geological controls on groundwater conditions, and the available methods of prediction of both groundwater flow and pressure are outlined. Salient points are emphasised by reference to a case history involving the construc- tion of a tunnel in a faulted and mixed sequence of sandstones, siltstones, shales and coals. Water ingress quantities have been monitored for a variety geological and geotechnical conditions including heavily faulted and mine disturbed ground. The overall results are discussed with reference to the relevant hydrological and geologi- cal conditions in terms of the geological structure, lithology and rockmass condition as well as the construction methods.

Jan 1, 1988

By G. J. Desroches

"In order to improve zinc plant productivity, areas of low efficiency were identified. As a result, solution purification was improved, additional dust precipitator capacity was made available and a new zinc casting plant was installed. The effects of these and other changes are discussed and the expenditure and benefits reviewed. HistoryThe operation of the Flin Flon metallurgical complex including an electrolytic zinc plant commenced in October 1930. The design of the zinc plant was based on that of the Commonwealth Mining and Smelting Company at Trail, British Columbia, the Anaconda Great Falls Montana Plant and the Electrolytic Zinc Company plant at Risdon, Tasmania.The plant began with a design capacity of 60 tons per day and currently produces 255 tons per day. Since plant start-up, approximately 3.5 million ton s of zinc metal have been produced, most of it exceeding special high-grade specifications.IntroductionThe facility incorporates the basic process steps of roasting, leaching, purification, electrowinning and casting. Figure I details the flowsheet. During the late 1970s, management recognized that in order for the zinc plant to continue operating, it was necessary to introduce cost-effective practices.Study groups, consisting of design engineers and operations personnel, were formed to investigate the details of plant revisions.The objectives were to improve productivity by reducing manual labour, reducing energy usage, increasing zinc recovery, increasing metal output and reducing costs.This paper details the changes made during the period 1979to 1986 and shows how these changes have affected the productivity and economics of the zinc plant operation."

Jan 1, 1988

By Jong-Jip Kim, J. G. Byrne, W. Kim, In-Ok Shim, John E. Flinn

"Two rapid solidification processes for 304 stainless steel were studied: centrifugal atomization (CA) in a helium atmosphere and atomization by exposing argon-containing melt to vacuum (VGA). Positron annihilation and x-ray line broadening measurements of explosively consolidated monoliths were used to clarify microhardness measurements as a function of annealing temperature. Interesting differences in positron response between CA and VGA materials are ascribed to more carbide formation in the CA material than in the VGA material in the 600 0C range. In addition, hot isostatic pressing of the CA material was examined as to the relations between mechanical behavior, pore shape, and relative density. A variable stress concentration factor is introduced into the theory to allow for changing pore shape as relative density increases.IntroductionThere are many potential advantages of rapid solidification processing (RSP), such as a high degree of matrix supersaturation, finely dispersed microstructures, improved chemical homogeneity, and retention of metastable phases, which have been studied extensively. To consolidate rapidly solidified material which is in powder form into useful shapes often requires subjecting the material to elevated temperature for extended periods of time under mechanical forces, as in hot isostatic pressing or hot extrusion. In such cases, some of the characteristics of the rapid-cooling step can be strongly affected. An alternative is dynamic consolidation (1), for example by explosive forming, where the time frame at least is extremely short.In the present work, effects of the consolidation processes of hot isostatic pressing (HIP) and explosive forming in a die are examined. The particular material is 304 stainless steel. The characteristics of both RS and VGA 304 stainless-steel powders were described by Wright, Flinn, and Korth (2) earlier."

Jan 1, 1988