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By Stuart R. Zimmerley, John Gross

"In the study of ball-mill grinding at the Intermountain Experiment Station of the United States Bureau of Mines at Salt Lake City, Utah, it was desirable to measure the work input to a ball mill at the mill itself so that consideration of motor efficiency and transmission losses would be eliminated.The device adopted is essentially that used by Prof. H. E. T. Haultain4 in measuring work input to rolls. The mechanism was changed only so as to adapt it to a ball mill.Figure 1 is a diagrammatic sketch of the apparatus.The pulley which rotates the mill is loose on the mill shaft and is equipped with ball bearings. This pulley is connected by means of three tangential springs to the driving plate, which is solid on the mill shaft. Power applied to the loose pulley is transmitted to the driving plate, and hence to the mill, by the three springs; the greater the resistance of the mill, the greater the spring extension. The extension of the springs is transmitted by the steel extension tape to the differential integrating meter.The integrating meter is operated by two friction wheels in contact with the integrator disk which revolves at a definite ratio of speed to that of the mill. The friction wheels are held in contact with the disk by the spring suspension of the integrator and are connected to a differential gear cage, the revolutions of which are recorded on a counter such as is used in gas meters. Due to the differential gears the c e is stationary when the two friction wheels revolve at the same speed in opposite directions; this condition exists when the integrator is centered on the disk and corresponds to no load or to a zero spring extension. As the lead is applied, the springs extend and move the integrator from the center or zero point, resulting in a difference of speed between the two friction wheels. Due to the revolution of the differential cage this change in. speed is transmitted to the counter. The integrator and extension tape system is kept taut by means of a light spring attached to the integrator, the spring having just enough tension to assure that the integrator returns to zero when the load becomes zero."

Feb 1, 1931

By Raymond B. Ladoo

The uses of talc are many but are not, in general well known or fully developed within the last decade several companies have realized the possibilities of greatly increased use and have intelligently proceeded to develop some of the fields which seemed most promising. This has had a tendency to lift talc from the obscurity in which it had existed for years, but the work is only started and much remains to be done. Considerably more attention has been paid to the technology and utilization of talc in Germany and Austria than in this country, despite the fact that the United States produces 65 of the world's talc and Germany and Austria combined but 5.4%. In the "Bericht,uber die tatigkeit des verbends der talcum-interessenten in Oesterreich-Ungarn" (Proceedings of the Austro-Hungarian Talc Association), for the years 1912 and 1913, many notes upon new uses appeared, together with suggestions as to further development of old uses. Aside from a few notes on the use of tar in paper, little has been published in the English language upon this subject. By recent action of the Talc and Soapstone Producers Association (U.S.A.) funds for research into the properties and uses of talc have been made Available and it is hoped that markets will be materially broadened a a result of this work.

May 1, 1920

By O. W. Terry

The Skene mine, in the Elizabeth District, Illinois, produced lead are from 1901 to 1907. Three exploratory holes drilled just north of the mine were said to have penetrated 40 feet of good zinc are. During the summer of 1944, the Bureau of Mines drilled check holes close to what appeared to be two of the three old holes. They also drilled two holes to the south of the mine and one into the core of the deposit. Results of the investigation are given in this report.

Jan 1, 1948

By Jack E. Fraley

The Bureau of Mines has successfully developed and tested a machine for spraying sealant onto coal mine roof and ribs. Dry material is transported pneumatically to a water-adding nozzle designed to provide dust-free spraying while being nonplugging and self-cleaning. The machine is self-cleaning, 35 inches in height, and capable of applying l/2-inch-thick coatings at over 1,000 ft2/hr.

Jan 1, 1978

By N. F. LeJeune

For a number of years the Bureau of mines has conducted semi-annual surveys to determine the changes in the characteristics of the motor gasoline being sold in the United States. The Bureau of Mines surveys, from April, 1917, to January, 1943, indicated a progressive decrease in the end point range. The survey for July, 1923 showed an interruption in this progressive decrease. This interruption, as shown in Table 1, in the line marked "Difference," was apparently a definite one, for the data obtained in the surveys of July, 19233, January, 19244, and the present one, apparently substantiate it. The figures in Table 1 were obtained by averaging the end points of the least volatile and most volatile samples of gasoline. For example, of 850 samples analyzed in 1919, the 10 per cent (85 samples) having the highest end points and the 10 per cent having the lowest end points were grouped, and the end points of each group averaged. These averages are represented in the table as the "Maximum 10 per cent" and the ?Maximum 10 per cent," respectively. The same scheme was used on the succeeding surveys.

Jan 1, 1924

By W. C. Hudson

"The McLeod sand pits, on the northeast side of the Little Ocmulgee River in Wheeler County, Ga., opposite Lumber City in Telfair Co., were examined by the Bureau of Mines under its war program of Investigation of Critical and Essential Minerals. The pits are about a quarter of a mile above the bridge, which is half a mile above Lumber City. Mrs. A. T. McLeod of Lumber City owns the land, including the pits. The property was inspected by an engineer of the Bureau of nines on March 8, 1945, on recommendation of Capt. Garland Peyton, director, Division of nines, Mining, and Geology of Georgia.The Mcleod pits are at the northwestern extremity of a mile-long series of old pits that were worked from about 1900 until the 1920's. The burning of the spur railroad bridge connecting the pits with the Southern Railway at Lumber City stopped mining operations. The pits on the south-east, or opposite, side of the Glennwood Road from the McLeod pits were first worked by F. L. Hinson and later, in 1921, by Mrs. n. H. Mobley. The glass sand was shipped to Tallapoosa, Ga., and Chattanooga, Tenn., where it was used in the manufacture of bottles for soft drinks. Some of the sand was used as molding and construction material. The sand was mined by hand shoveling it into wheelbarrows, which were unloaded on freight cars. The pits were partly refilled with overburden, so that it is impossible to estimate even roughly the amount of sand excavated.Analyses of samples of glass sand made years age3/ and later in 19404/ roughly check those made by the Bureau of Mines laboratory, except that in the former the iron oxide content usually was greater, attaining a maximum of 0.72 percent.The sand pits are in a valley slightly more than a quarter of a mile wide that lies along the northeast side of the Little Ocmulgee River. The land is either flat or marked by ridges only a few feet high. . A rather thick growth of scrub trees covers most of the valley. The surrounding country consists of gently rolling farm lands. The altitude of the valley is not known, but, judging by its distance from the seashore, it probably is about 200 feet. In addition to the Glennwood highway, which crosses the valley, several old sand roads lead to the pits."

Apr 1, 1946

By Joseph A. DeCarlo

According to the annual survey of beehive-coke plants by the Bureau of Mines, United States Department of the Interior, there were 61 plants with 9,549 ovens in the United States on December 31, 1956, This publication in¬cludes only those for which an annual report was filed with the Bureau of Mines. Not all plants listed were active, however, as nearly one-third of those canvassed were idle all year. A compilation of the returns showed that 44 plants with 6,920 ovens were active part or all year and 17 plants with 2,629 ovens were idle throughout the year. The capacity of beehive ovens has fluctuated between 6 and 14 million tons during the past decade. At the end of 1956, the annual coke capacity of beehive ovens on which reports were received amounted to 5.8 million tons. As noted in table 2, however, not all of this capacity was in operating condition, as 2,093 ovens with a capacity of 1.2 million tons were not operable on [ember] 31, 1956.

Jan 1, 1958

By Glenn C. Reed

"Preliminary examination of the Glass Buttes mercury deposits, Lake County, Oregon, was made in August 1945 at the request of W. S. Lazier, present lessee of the deposit.Most of the prospect openings in the area were inspected. The more significant workings were sampled and napped in detail. This report presents the data obtained from the investigation to date.In its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. noon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metallurgical Branch, R. G. Knickerbocker, chief, analyzes samples and performs beneficiation tests. Both these branches are under the supervision of Dr. P. S. Dean, assistant director.Special acknowledgment is due to S. H. Lorain, chief, Albany Division, Mining Branch and to S. R. Zimmerley, chief, Salt Lake City, Utah, Metallurgical Division, for analyses of the ores.The presence of quicksilver in the Glass Buttes district has been known since about 1930. The area immediately north of Middle Butte has been superficially prospected by numerous test pits, trenches, shafts, and short adits, which revealed a number of opalized zones. Many of these opalized zones contain weak to strong concentrations of cinnabar. The area has not boon explored thoroughly; no mercury has been produced from any of its deposits.A block of 48 full-size claims has been located to cover a large part of the area in sections 34 and 3, Tps. 23 and 24 S.,R. 23 E.,W.M. These claims, held by, location are owned by H. S. Miller, lumberman of Bend, Ore. W. S. Lazier, 10N. W. 20th Avenue, Portland, Ore., currently controls the property under,a nominal leasing agreement. J. W. McDaniel, 44 Lake Place, Bend, Ore., has done much of the underground and surface exploration on the property.The Glass Buttes district is an area of low relief in the Deschutes River drainage system near the northeast corner of Lake County, Ore. (See fig. 1.) The arid climate is marked by extremes of winter and summer temperature. Water for cane use is not available in the immediate area. Well water, however, can be obtained in limited supply on ranch property 5 miles to the south."

Aug 1, 1946

By G. W. Jones

[A survey of the literature relating to ignition temperatures of acetylene-air and acetylene-oxygen mixtures reveals rather wide disagreement in the reported results. In some instances the ignition temperatures of acetylene-air mixtures were reported to be lower then those of acetylene-oxygen mixtures, which is contrary to experience with other combustibles. To clear up some of the reported discrepancies, the authors have investigated the ignition temperatures of acetylene both in air and oxygen, and their results are presented in this report.]

Jan 1, 1941

During 1990-1999, a total of 458 fires occurred in all coal mining categories; 157 of those fires caused 164 injuries and 2 fatalities. The greatest number of fues and fire injuries occurred at surface mines, whch also had the highest risk rate values. A total of 66 fuefighting interventions were required. Of these, there were 25 mine rescue team interventions in underground mines, including 5 mobile equipment firefighting interventions, and 41 fire brigade and fire department interventions at all surface operations, including 19 mobile equipment interventions. In all, 50 fires destroyed or heavily damaged equipment (including 16 pieces of mobile equipment) because of failure of other firefighting methods, late fire detection, undetected fires, or fire size. A total of 1 14 fires were detected late by smoke, and 42 fires were not detected.

By Jeanne A. Zimmer, Brad Smith, Steve Viles, Andrew B. Cecala

A recent report evaluating silica exposure levels in the metal/nonmetal mining industry noted that bag packaging and loading are some of the occupations at the greatest risk. In addition to dust problems, the bag-stacking process is labor intensive, making lost-time injuries common due to back fatigue and strains. During the bag-stacking process, a significant amount of dust can be generated, mainly from product on the outside of the bags and from dust escaping the bag valve upon impact of the bag on the pallet. In an effort to address dust-exposure and back-fatigue issues, Malvern Minerals Co., Hot Springs, Ark., made two major improvements to its ground silica stacking facility. First, the company purchased a semi-automated bag palletizing system (Figure 1). With this system, the bag stacker does not lift the bags, but slides them across a metal table. Small jets of air exit through perforations in the table top (similar to an air hockey game), allowing workers to more easily slide each bag into the proper position. After each layer of bags is completed, the table slides open, and the entire layer of bags is loaded onto an underlying pallet. The table then closes, readying it for another layer of bags. After the entire pallet is loaded, the unit delivers the pallet to a shrink wrap and forklift pick-up area. In addition to this semi-automated palletizing unit, Malvern Minerals purchased an Overhead Air Supply Island System (OASIS) to lower the bag stacker's dust exposure. The OASIS takes outside air, directs it through MEASURING RESPIRABLE DUST The bag stacker's respirable dust exposure was monitored using a RAM-1 instantaneous dust monitor to evaluate the impact of the various changes on the palletizing process and dust-control equipment. The bag stacker wore a vest that held the 10-mm Dorr-Oliver cyclone, which classifies the respirable portion of dust. Flexible tygon tubing was used to connect the cyclone to the RAM-1 dust unit, allowing the bag stacker to perform the palletizing process with minimal interference. The RAM-1 measures respirable dust concentrations by light scattering with a sensing chamber. This device closely simulates gravimetric measurements when calibrated for a specific dust. This instrument is ideal for comparative evaluations, as was the case in this study. Since the RAM-1 is not an MSHA-approved instru¬ment for dust compliance sampling, the dust concen¬trations listed in this article should be used as a com¬parative value of respirable dust concentration and not to determine actual dust concentrations from a com¬pliance standpoint.

By R. L. Hopkins, H. T. Rall

A continuous method has been developed for preparing thiolacetic acid . Acetic anhydride and hydrogen sulfide are passed concurrently over an amine ion- exchange resin , under 20 - psi pressure . The thiolacetic acid , a product of the reaction , is flashed continuously from the crude reaction mixture and is purified by fractional distillation . The yield of thiolacetic acid is in excess of 80 percent based on the acetic anhydride charged . INTRODUCTION In the synthesis of reference compounds needed in the identification of sulfur compounds in petroleum , thiolacetic acid has become an important reagent because of its use in the synthesis of thiols by addition to appropriate olefins : R - CH = CH₂ + CH3 - COSH R- CH2 - CH2 - S - COCH R - CH2 - CH₂ - SH + CH3COONa NaOH (1 ) The commonly used procedures for its preparation , as described by Clark and Hartman (1 )4 and by Ellingboe (2 ) , are based on the batchwise reaction of acetic anhydride with hydrogen sulfide :

Jan 1, 1964

By D. A. Reynolds, L. P. Rockenbach

"The method of analyzing light oil for benzene is fully described by Fieldner and others 4/ and Kester and Kolmes 5/. In this procedure, benzene is determined by shaking 20 cc. of the 79º to 81º C. boiling point cut from the fractionation of the refined light oil with 3 volumes of 98—percent sulfuric acid in an A. S. T. M. separator funnel of the type used for determining water in bitumi¬nous materials. After the mixture has been shaken 5 minutes it is allowed to settle at least half an hour and the acid is drawn off; the residual oil is reported as paraffins and the decrease in volume as benzene. The method has been found satisfactory for light oils from coals carbonized at 5000, 600°, and 7000 C. but does not give accurate, reproducible results for oils from the 800° C. tests.The content of benzene of the 790 to 81° C. cut is high, 90 to 95 percent, for 800° C. light oils, whereas for lower—temperature light oils it is considerably less. Benzene is the most difficult of the aromatics to sulfonate, hence the acid concentration must be maintained above 95 percent to insure complete sulfonation. Sulfuric acid (98 percent) reacts with benzene, but its reaction with paraffins at ordinary temperatures is negligible; however, more concentrated acid will attack paraffins and give erroneous yields of benzene. The reaction between benzene and sulfuric acid forms water that will dilute the acid. The effect of this dilution may be overcome by increasing the acid-to-oil ratio or increasing the strength of the acid. The latter, however, must not be used, because the stronger acid reacts with paraffins."

Mar 1, 1942

By A. W. Deurbrouck

Four samples of Pittsburgh-bed coal, of various size consist and ash content were dewatered in a pilot-size vacuum-disk filter partially enclosed with a steam jacket. Steam fed at 2.5 to 12.5 pounds per minute reduced the moisture content of the filter cakes from 2.8 to 13.8 percentage points more than normal vacuum dewatering. Approximately 1.5 pounds of steam was required to remove 1 pound of water.

Jan 1, 1966

By A. Bartkowiak

The lower flammability limit of methane at 0 p.s.i.g. and ambient temperatures is 5.6 volume percent in chlorine, 5.2 in oxygen, and 5.0 in air. The corresponding upper limit values are 70, 60.5, and 15 volume percent, respectively, so that the range of flammable mixtures is greater in chlorine than in oxygen or air. The lower flammability limit of ethane at 0 p.s.i.g. and ambient temperatures is 6.1 volume percent in chlorine, 3.0 in oxygen, and 2.9 in air. The corresponding upper limits are 58, 66, and 12.5 volume percent, respectively. In this instance the range of flammable mixtures is greater in oxygen than in chlorine or air. Generally, the limits of flammability for both methane-chlorine mixtures and ethane-chlorine mixtures widen with increases in temperature and pressure.

Jan 1, 1960

By E. D. Gardner

"In recent years efficient safety organizations have been considered essential at all well-managed metal mines. Statistics from numerous mines throughout the country show that the expense of operation of these safety departments is repaid many times by the saving due to fewer accidents. Men trained in first aid, mine rescue and fire-fighting are important parts of the safety organization at most mines. It is more desirable, however, to lay stress ma accident prevention and fire precautions rather than on first aid and fire fighting. Both of these phases of safety work have been well developed in the Globe Miami district. The co-operative mine rescue organization* in this district under Orr Woodburn, is one of the best in the country. Mine rescue teams are kept trained at all the mines and the oxygen breathing apparatus is constantly maintained in good condition. Miners are also trained in first aid, and are offered incentives to make themselves proficient both in mine rescue and first-aid work.The Old Dominion Company is among the leaders in the safety movement in the Globe-Miami district. The safety department at this mine was established January 1, 1914, and has been developed to a high degree of efficiency. W. G. McBride, general manager of the company, takes an active part in the safety work and has given Albert Talon the safety inspector, his active support in developing the organization. The success of the department is dos largely to the ability, tact, and personality of the men directing the work.The following description of the establishment and operation of the safety organization at this mine was prepared from information supplied by Mr. Tallon."

Jun 1, 1921

By A. R. Rule

This report describes preliminary studies by the Bureau of Mines to develop a procedure for extracting the fluorine from low-grade fluorspar ores in which the CaF2 particles are finely locked in the calcite matrix. A combination of flotation beneficiation and pyrohydrolysis is applied to recover and to liberate the fluorine. Flotation of a finely locked high-calcite fluorspar ore containing only 11.7 pct CaF2 recovered over 92 pct of the fluorspar at a grade of 51 to 52 pct CaF2. Pyrohydrolysis of the flotation concentrate liberated nearly 90 pct of the fluorine as aqueous HF. By this procedure over 80 pct of the fluorine contained in the original ore was extracted.

Jan 1, 1974

By George S. Rice

There have appeared, from time to time, comparisons of various features of coal mining practice in the United States and Great Britain. A recent, article, appearing in a British journal, points out that the American miner produces 3 1/2 times as much coal per shift as the miner, at one-half the cost, and proceeds to explain the natural industrial, and engineering causes which lead to this result. Amon« he reasons advanced. is that the American coal miner enjoys the advantage of more easily worked seams of coal, due to the fact that the coal mining industry in the United States is of more recent date than in Great Britain. The latter qualification is not correct, because where these advantages exist, they will persist. The coal beds of the United States are not buried deeply, except in the remote parts of the country, as in the Uinta Basin of Utah. The article referred to states that many of our miners are still employed on out seams reached by "adits", (which we term entries), or by vertical shafts of moderate depth. It is probable in fact that the great bulk of the coal of the United States is taken out from a depth of less than 400 feet.

Mar 1, 1920

By M. H. Kline

The Scarlet mine, in Randolph County, N. C., was operated on a small scale at intervals from 1899 to 1915, but no records of the quantity of ore produced are available. J. I. Moore unwatered the mine in March 1948, and Bureau of Mines' engineers examined the underground workings. Several assays checked previous sampling of the mine and indicated a small but comparatively high-grade copper-zinc deposit. The high metal content of the veins and the possibility of developing additional reserves prompted the Bureau of-Mines to drill three holes, totaling 530 feet, at the deposit during March and April 1948. Drilling disclosed that the mineralized vein did not extend over 300 feet along the strike and is probably limited in depth to the contact with the granite mylonite.

Jan 1, 1949

By L. W. Higley

Procedures were developed for reclaiming high-temperature alloy scrap in the form of standard cobalt-base alloy. A cobalt-base, multicomponent, high- temperature alloy, such as S-816, can be successfully melted from scrap, and its specified chemical composition can be retained. Induction furnace melting in a controlled atmosphere was used to obtain ingots that were subsequently fabricated by impact forging to provide specimens for heat treatment and testing. Of the numerous metal elements in S-816 alloy, only small quantities of molybdenum were lost in the melting operation as finally developed. Test results indicated that the scrap material, after melting, forging, and heat treatment, was equivalent in room-temperature tensile strength, in high-temperature creep and stress-rupture properties, and in chemical composition to commercially produced S-816 alloy made from virgin material.

Jan 1, 1963