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By William J. Campbell

The Federal Bureau of Mines provided five test materials--amosite, short-and long-fiber chrysotile, crocidolite, and nonfibrous tremo1ite--to the National Institute of Environmental Health Sciences (NIEHS) for studies on the biological effects of orally ingested asbestos-related materials. An inter-agency agreement between the Bureau and NIEHS made possible this program to characterize these test materials. The Bureau in turn received support through contracts with the Ontario Research Foundation for the milling of amosite and crocidolite, and with the University of Maryland for microscopic measurements. The five test materials, which were supplied in quantities of 960 to 1,200 pounds each, were characterized by chemical-instrumental analysis for elemental composition, surface area, density, X-ray diffraction, infrared spectroscopy, thermogravimetric analysis, mineralogy, and particle size analyses. Particle size distributions were emphasized because of the current theories relating adverse biological effects to length-width characteristics of durable elongated particles.

Jan 1, 1980

By James P. Ulery, Frank E. Chase

Clay veins found in coal mines have caused numerous injuries and fatalities. These structures plague all phases of mining, including entry development, pillar recovery, and panel extraction. Clay veins also increase production costs and may disrupt or halt mining. These detrimental aspects have prompted the Bureau of Mines to investigate the physical characteristics of and roof instability problems associated with clay veins. This was accomplished by observing and mapping clay veins in surface and underground mines. The occurrence and origins of clay veins were also investigated to determine predictive capabilities. The investigators found that clay veins normally occur in more stable, less rapidly subsiding coal basins. Clay veins result when tensile stresses develop fissures which are later infilled. These fissures can be propagated by compactional processes and/or tectonic stresses active during and subsequent to coalification. The Bureau also found that associated faults, fractures, and slicken-side planes commonly parallel clay veins and disrupt the lateral continuity of the immediate and, sometimes, main roof. When clay veins parallel or subparallel the direction of face advance, the roof is segmented into cantilever beams, causing unstable conditions. Consequently, the strata on either side of the clay veins should be bolted and strapped together to form a beam.

Jan 1, 1987

By James Paone

The Bureau of Mines conducted laboratory drillability studies on nine rock types using two mining-type percussive drills. Percussive-bit action was simulated by dropping a known weight on a rock sample to obtain a coefficient of rock strength for each rock drilled. While no single physical property of a rock is completely satisfactory as a predictor of penetration rate, coefficient of rock strength showed a better correlation with penetration rate than did other physical properties. Results also indicate that over the range of energies investigated, energy per unit volume in a given rock is independent of blow energy. A drillability index for the percussive system is proposed that utilizes the coefficient of rock strength test to determine energy per unit volume for a given rock which, along with the work rate of a given drill and the bit diameter, is used to predict the penetration rate as shown in the following equation: [R = 4P pD2 E, where R = penetration rate, in/min, P = work rate, in lb/min, D = bit diameter, in, and Ev = energy required to produce a given volume of rock, in lb/in3.] Laboratory tests indicate this method's potential as a simple and reasonably accurate method of predicting penetration rates with any percussive drill and bit combination.

Jan 1, 1969

By Robert M. Becker

This investigation (in five parts) extends the theory of sample reliability from a sample consisting of a fixed number of items to a sample consisting of a fixed amount of items. Examples of a fixed amount of items per sample are samples consisting of a fixed weight or a fixed volume of unequal size particles. The extension of the theory is confirmed by experimental laboratory sampling using standard procedures. The probability distribution functions (the binomial, hypergeometric, multinomial, generalized hypergeometric, and those here called the compound binomial and compound multimomial functions) are developed from fundamentals. Their distributions are generalized to include some measured characteristic of the items. Infinite population moments are derived from moment-generating functions, and finite population moments are developed from corresponding infinite population moments using a newly defined mathematical operation. The first three experimental moments in laboratory sampling to given weights of particles are compared with the theoretical moments of their corresponding compound mult.inomial distributions. The agreement is striking. The study is divided into five parts. Part 1 deals with probability or random sampling to n items and with all sampling to n items per sample from some one probability distribution. This is the area of sampling covered by well-known theory. Accordingly, the procedures may be different but many of the results are well known.

Dec 1, 1964

By Walter E. Pittman

This Bureau of Mines study surveys the current state of technology and the various research efforts that have been undertaken to dewater the dilute phosphatic clays generated in the production of phosphate rock. The research described includes early dewatering experiments, fundamental studies of clays and of flocculation, and minor dewatering techniques such as freeze-thaw methods, the ANDCO process, moving screens, sand wick, crust development, and overburden pumping. Some methods that are currently being evaluated are described. They include the Estech sand-clay mix process using the Enviro-Clear thickener, sand-clay sandwiching, dredge mix, dredge process, and the sand-spray process. Developing technology for dewatering phosphatic clays also is described, including the Bureau of Mines rotary trommel method and the Gardinier process.

Jan 1, 1984

By H. O. McDonald

The Bureau of Mines reviewed the chemical vapor deposition (CVD) literature on the nonmetal binary and ternary compounds of the group IVB, VB, and VIB elements, with emphasis directed to the following nonmetals: B, C, N, O, and Si. This review examines each of these binary and selected ternary compounds of the group IVB, VB, and VIB elements as coatings and gives some of their preparative methods, uses, and properties. A total of 259 references were found for these compounds of the nine elements. This review was utilized in the Bureau's research to provide abrasion-, erosion-, and corrosion-resistant coatings in order to conserve critical metals and protect various metallic surfaces in metallurgical, mining, and energy conversion systems.

Jan 1, 1983

By Roy L. Soderberg

Ground support for metal, nonmetal, and coal mines was examined through fill placement with a pneumatic stower to increase extraction, reduce ground pressures, and improve general mine safety. Several pneumatically stowed stope-fill products were tested to determine the effects of specific gravity, gradation, moisture, and impact velocity on the in-place density of the stowed fill. Hydraulic sand filling has now served the mining industry for several decades but because of the low density does not always provide ample support to the hanging wall; therefore, the sill and crown pillars sometimes build up excessive stresses that are detrimental to mining. Cementation of a dense fill adjacent to a pillar to allow 100-pct extraction of the pillar, or a fill that can be placed without the use of water and where water is a detriment to rubber-tired mining equipment, was found to be a possible use of pneumatic fill. Placing of coal mine washery products into abandoned underground workings is another possibility in order to completely eliminate surface impoundments.

Jan 1, 1976

By W. W. Adams, E. E. Getzin, T. D. Lawrence

"The thirteenth annual accident-prevention competition conducted by the Bureau of Mines during the calendar year 1937 was completed with 318 mines and quarries participating. This contest, known as the National Safety Competition, is open to all minas and, quarries employing 25 or more men underground or in the quarry or open pit. The entries are divided into five groups to obtain as nearly as possible uniformity of operating conditions and hazards. The five divisions are: (1) Underground anthracite mines, (2) underground bituminous-coal mines, (3) underground metal mines, (4) underground nonmetal mines, (5) quarries and open-pit mines. A bronze trophy, known as Sentinels of Safety, provided by the Explosives Engineer magazine, is awarded to the winner of each group. The trophy is kept by the winning company 1 year and then transferred to the winner of the succeeding year's contest. Certificates of Honorable Mention are given to plants ranking second, third, fourth, and fifth in each group and to all plants operating without a lost-time accident provided the period of exposure to hazard was not less than 30,000 man-hours. Relative standing in the contest is determined by the contestant's accident-severity rate, which represents the total number of days of employee disability from accidents per thousand man-hours worked by all employees.The 1937 contest was outstanding in that the accident-frequency rate for the contest group as a, whole was the lowest on record. Moreover, with one exception 1934, the accident-severity rate was the lowest ever attained: For frequency, 3S.0 accidents per million man-hours worked; and for severity, 8.2 days lost from accidents per thousand man-hours worked. The rates represent a decline of 62 percent in accident frequency since 1925, the first year of the contest, a remarkable accomplishment both for the contest group and for the purpose of the contest because a majority of the contestants have not only participated during the past year but have been enrolled several years, some enrollments even dating back to 1925."

Aug 1, 1938

By Joseph A. DeCarlo

This publication presents a tabulation of oven-and beehive-coke plants in the United States as well as pertinent statistical data on the number, capacity, kind, and condition of the ovens. Coke is an essential raw material in pig-iron production and the coal-chemical materials produced during the coking process are used to manufacture fertilizers, paints, plastics, synthetic rubber, explosives, detergents, nylon, pharmaceuticals; dyes, and many other products necessary to the high standard of living in this country. In table 1 the oven-coke plants in the United States on December 31, 1959, are listed. This shows the name and address of the company, location of the plant, classification or type of ownership, number and type of ovens, annual coke capacity, and the coal-chemical materials produced. The "furnace" plants I are those owned by iron and steel companies and most of them are integrated with blast furnaces to facilitate transportation of raw materials for steel making. Furnace plants represented 87 percent of the total coking capacity and their average annual capacity was 1. 3 million tons. The "merchant" plants are those associated with chemical companies, gas utilities, as well as those that produce metallurgical, industrial, and residential-heating grades of coke and coal-chemical materials for sale on the open market. These coke plants are smaller than furnace plants and in 1959 their average coke capacity was only 520 thousand tons annually. On December 3l, 1959, there were 54 furnace and 20 merchant oven-coke plants in existence in the United States.

Jan 1, 1960

By Henry G. Dorsett

Dust explosion data obtained in laboratory tests by the Bureau of Mines are presented for 73 chemical compounds and mixtures, 29 drugs, 27 dyes, and 46 pesticides. Information is given on ignition temperatures of cloud and layer, minimum igniting energy, minimum explosive concentration, percent of inert dust required to prevent flame propagation, limiting oxygen concentration in the atmosphere to prevent ignition, and pressures and rates of pressure rise at dust concentrations of 0.1, 0.2, 0.5, 1.0, and 2.0 ounces per cubic foot. Explosibility indexes are computed where data are available to permit comparison of the relative explosion hazard. Variations of explosibility parameters with chemical composition are discussed. General means for minimizing the dust explosion hazard are reviewed.

Jan 1, 1968

By M. M. Tilman

The Federal Bureau of Mines developed a rolling method that improves creep resistance and yield strengths of lead alloys containing up to 5 wt-pct Sb. The 0.69-inch-thick slab-cast alloys were breakdown-rolled to 0.226 inch and finish-rolled to 0.063 inch at 5-or 20-pct reduction per pass. Rolling was at room temperature to simulate conventional cold rolling, and at 75°, 125°, and 175° C. Two alternative methods evaluated consisted of (1) a single cold final pass followed by annealing and (2) a single hot final pass. Two additional processing methods involving percipitation strengthening were included for comparison. Compared with conventional cold rolling, hot rolling at 125° and 175° C with multiple light passes vastly improves creep resistance and raises yield strengths. Tensile strengths are less affected. The other treatments also improve creep resistance significantly and generally improve tensile properties; magnitudes vary with treatment and composition.

Jan 1, 1975

By Noel N. Moebs

Coal mine roof failure is categorized according to character, trend, or pattern of occurrence. Two principal categories of failure are proposed--geology related and stress related. Geology-related failure includes both lithology and structure. Each of several subcategories reflects the probable cause of failure and thereby provides a basis for the selection of appropriate techniques for reducing the incidence of failure. These control techniques, depending on local conditions, may include supplementary support, destressing, reduction of mine air humidity, or a change in the customary support methods.

Jan 1, 1986

By Thomas M. Garland

Reports that set forth the pertinent facts of existing secondary-recovery operations are an integral part of the work of the Bureau of Mines in promoting conservation and efficient utilization of the petroleum resources of the Nation. Knowledge of the success or failure of waterflood projects in an area is very useful to other operators. Although projects will not have identical results, information concerning the flood performance, method of operation, and difficulties encountered on one project will help operators to determine the feasibility of flooding a similar sand and to select the methods of operation most likely to prove successful. The increasing cost of discovering and developing new oil reserves, as well as the unending effort to reduce operating costs and increase ultimate oil recovery from known petroleum reservoirs, has required the petroleum industry to evaluate continuously the performances of various secondary-recovery methods. Waterflooding was recognized early by the petroleum industry as a possible means of increasing oil recovery. From the early accidental floods in Pennsylvania and through many haphazard attempts to inject eater into oil-bearing formations, waterflooding emerged as one of the more important methods of oil recovery. Waterflooding is important not only to the oil industry but also to the economy of the area concerned.

Jan 1, 1962

By Philip G. Freeman

The growth-promoting properties of coal-derived humus were tested by a variety of bioassay methods. Humate materials used included leonardite, a form of naturally oxidized lignite, and humic acids extracted from leonardite. It was found that the greatest effects were evident when water-soluble humic acid was applied to excised root tips. No significant short-term effect was noted when water-soluble humic acid was applied to stem or coleoptile sections. Root initiation was promoted in bean stems when high concentrations of coal-derived humate were applied. Gross weight of tomato plants was increased by up to 40 percent when coal-derived humates were added in concentrations of 101 to 104 ppm to the nutrient in a hydroponic growth test of 6 weeks' duration. It is concluded that coal-derived humate promotes the uptake of minerals, specifically iron, by serving as a metal chelate.

Jan 1, 1968

By Arnold M. Lansche

Domestic Production.-Domestic production of white arsenic, AS,03, was derived entirely as a byproduct of smelting arsenic-containing copper ores by The Anaconda Company at Anaconda, Mont., and American Smelting and Refining Company at Tacoma, Wash. The Anaconda Company discontinued production of white arsenic in 1965. Arsenic metal was not produced. Consumption and Uses.-Most of the white arsenic produced in 1965 was consumed in manufacturing lead and calcium arsenate insecticides.

Jan 1, 1966

By B. D. Sartwell

The formation of alloyed regions near the surface of metals using ion implantation is being investigated by the Bureau of Mines as a means of providing corrosion resistance using much smaller amounts of the strategic alloying metals. Two ion implantation systems that can implant low-energy chromium, nickel, or aluminum ions into low-cost substrate materials such as iron or carbon steel have been designed and constructed. The development of the ion source, ion beam acceleration stage, mass analysis system, and target chamber are described in detail. The ion-implanted alloys have been characterized using proton-induced x-ray emission to give the total number of atoms implanted and to determine the extent of any surface contamination introduced by the ion implantation process. Research conducted at other laboratories on metallurgical applications of ion implantation is given.

Jan 1, 1980

By S. P. Polack

"INTRODUCTION The purpose of this circular is to correlate the information obtained during personal investigations at the sites of four rock tunnels in the process of construction and information obtained from the records and personal views of the constructors of two other tunnels that were not visited during the, excavation phase of construction and to present this information for the benefit of those who contemplate future construction of rock tunnels.Modern mechanized coal mining requires better, safer, properly alined haulageways and beltways; consequently, better understanding of tunneling methods by coal-mining men will be necessary. The possibility of future high-speed haulage systems utilizing rock tunnels in the more solid rock strata above or below the coal beds must not be discounted. In the past, tunnels have been driven for use in draining and unwatering inundated coal mines. At present, the need for such tunnels is very evident in some parts of the coal-mining regions, notably in the Pennsylvania anthracite fields, and studies along these lines are in progress. The average coal-mining man has little time or opportunity to visit tunnels while they are being exca-vated; therefore, it is hoped that this information will assist him in constructing tunnels safely if he is required to do so in the future.The tunnels described herein differ in size, shape, usage, and, in many instances, in their geological aspects. Full-face, heading and bench, and pilot-tunnel, and enlargement methods of excavation were utilized.The roof-support methods show diverse designs and materials of construction to suit each purpose and condition. The superiority of steel roof support over wood is demonstrated beyond doubt and is shown clearly in the photographs included in this circular.The illustrations (photographs taken by the U. S. Bureau of Mines, the U. S. Corps of Engineers, and others) show many of the necessary steps taken during the excavation and the erection of roof support in tunnels under construction."

May 1, 1950

By James E. Hill

In the course of exploratory drilling during World War II by the Bureau of Mines under the Strategic and Critical Minerals investigations Program, a problem arose as to the ultimate disposal of the drill core resulting from that program. The difficulties experienced in obtaining factual information to evaluate mineral deposits examined (during that program) influenced the Bureau in a decision to catalog and store the drill cores for future reference. Initially, the drill cores were stored at the nearest Bureau of Mines station that had space available for the purpose. Recently the Bureau stations at Minneapolis, Minn., and Denver, Colo., were designated as the locations of permanent drill-core storage facilities. Drill cores that are retained from Bureau of Mines mineral-exploration projects are stored at these two locations and are given preference in selecting cores for storage. Drill cores are accepted also for storage from other Government agencies, State agencies, private companies, or individuals on the basis of available facilities and consistent with the significance of the core in relation to Bureau of Mines objectives and national interest. Selection and acceptance of such drill core are determined by the Bureau of Mines. The drill cores stored at the two locations are available for inspection by any person having a legitimate interest in the mineral deposits represented by the cores. Approximately 1,850,000 feet of drill core can be stared in the facilities now available to the Bureau of Mines. Approximately 475,000 feet of drill care is stored or scheduled for storage at Minneapolis, Minn., and 240,000 feet of core stored or scheduled for storage at Denver, Colo. A list of drill core now in storage at the Bureau of Mines core-storage facilities at Denver and Minneapolis is included as appendix A.

Jan 1, 1957

By J. J. Taber

This is the final report on Grant No. G0144067. The report presents the results of a number of laboratory studies carried cut in several different ways to determine the effectiveness of foam for blocking the flow of gas in coal. The effectiveness; (of foam for retarding or blocking the flow gas in various porous media has been observed by many investigators1-4 but we are not aware of similar detailed studies in coal. Because of the diversity of our experiments, the key findings and general conclusions are presented very briefly in Section II. As a convenience to the reader a complete table of cements is included to enable the reader to find those experiments and studies of greatest interest.

Jan 1, 1976

By Edward F. Divers

This Bureau of Mines report describes the results of a program to develop small, rugged scrubbers with high dust collection efficiency for use in under-ground coal mines. The Bureau's Pittsburgh (Pa.) Research Center has developed and assisted in the development of several types of improved scrubbers that are especially suitable for various underground mining applications. Research efforts concentrated on reducing the size, power, and water consumption of these scrubbers, while optimizing their dust collection efficiency. Fractional dust collection efficiency, air volumetric range, size, power, water consumption, and application guidelines for each type are described. Air pressure differentials ranged between 2-and 3D-inches water column (wc). The dust collection efficiency of six scrubbers--a venturi, two flooded-fibrous-bed, a venturi-impaction plate, a wetted-fan, and a rotating flooded-bed--were compared. The rotating flooded-fibrous-bed and the stationary flooded-fibrous-bed scrubbers showed the highest coal dust collection efficiency. Test results show that these scrubbers can generally achieve respirable size coal dust collection efficiencies in the high 90-pct range required to reduce both long-(8-hour) and short-term coal mine dust concentrations below Federal requirements.

Jan 1, 1979