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By D. C. Fleck

This report describes a method of using sodium for reducing titanium tetrachloride, developed at Boulder City, Nev., as part of the Federal Bureau of Mines effort to improve the extractive metallurgy of titanium. Finely divided titanium metal, titanium lower chlorides, or a mixture thereof was produced in a continuous operation at temperatures between 105° and 205° C. by the reaction of molten sodium and vaporized titanium tetra-chloride in an agitated bed of finely divided inert solids (powdered sodium chloride or the reaction products). Composition of the product was controlled by varying the relative quantities of sodium and titanium tetrachloride used. A description of the operations and analytical data of the reaction products are given.

Jan 1, 1960

By C. P. Mangelsdorf

This report deals with the efforts to develop a portable device suitable for underground use for the purpose of measuring the frequency of vibration of the horizontal chords of Birmingham roof trusses. Four devices are investigated and evaluated. An approximate emperical expression developed from a mathematical analysis provides a means of converting the frequency into tension. The method appears to be effective in mines with shale roof but requires some modification for other roofs.

Jan 1, 1983

By E. J. Matson

"SUMMARYThe Bureau of Mines has been investigating deposits of critical and essential minerals in the United States since 1939. Projects were set up on only the most promising properties. A preliminary examination of the Rio Grande property was made by Bureau of Mines engineers in July 1942 and the property was examined again in July 1943.The Geophysical Branch of the Bureau undertook a Geophysical survey of the area in November 1943 and was intermittently active in the district until June 1946. The major portion of their work was done from June 191 to November 1945. Favorable areas for exploration were recommended by the Geophysical Branch of the Geological Survey, 3/ and all holes were drilled in them.Two projects were set up by the mining branch in an endeavor to find ore bodies on the strength of the geophysical information."

Sep 1, 1947

By Martin H. Stanczyk

Ultrafine grinding of the industrial minerals mica, pyrophyllite, talc, marble, barite, and fluorite was accomplished using the Bureau-developed and patented attrition-grinding process. The materials, representing minerals of diverse physical characteristics, were batch ground in a 10-inch-diameter machine using statistically designed experimental test programs. The tests were made to determine large effects of variables such as feed pulp density, grinding medium size, and quantity of the electrical energy consumed during grinding on product particle size and bulk density. In designing the test programs, it was assumed that there was no interaction between the variables. Relatively coarse commercial flotation concentrates of mica, barite, and fluorspar and mine-run products of pyrophyllite, talc, and marble were readily ground into subsieve size ranges. Considering the great amount of particle size reduction obtained, the electrical energy requirements for grinding were very low. In general, the test results indicated that the best conditions for particle size reduction were approached when grinding with the coarser fraction of sand grinding media, the higher-sand-to-mineral weight ratio, and the higher feed pulp density.

Jan 1, 1972

By W. P. Diamond, B. M. Bench, C. M. McCulloch

This Bureau of Mines report describes photolineaments obtained from stereoscopic examination of vertical aerial photographs and by the Ronchi grating study of aerial photoindex sheets. The photolineaments are compared with the trends of oriented fracture systems procured by measuring the compass direction of joints in bedrock. The relative reliability of the methods is shown, and the results are presented in graphical, tabular, and written form. Analyses of field measurements of strikes of bedrock joints in the project area indicate for the most part two intersecting sets of major joints oriented N 76° W - N 15° E, and N 57° W - N 27° E. The analyses of lineaments determined by stereoscopic examination of aerial photographs show dominant trends of lineament zones of weakness to be an average of N 65° W - N 20°E. Analysis of lineaments found by Ronchi grid viewing of aerial photoindex sheets indicate dominant trends of N 70° W - N 27° E. The three methods give similar findings and verify the work of previous authors. The Ronchi grid method is a useful guide, but it cannot be substituted for the two more painstaking methods.

Jan 1, 1977

By A. W. Effinger

The Bureau of Mines used regression analysis and applied statistical methods in an effort to rationalize the results of an experiment examining the effects of certain variables on carbon deposition in a reservoir for thermal recovery of petroleum. Although none of the 15 trials of the original experiment resulted in the response of weight-percent of carbon regarded by the experimenter as adequate, values calculated using canonical analysis in two trials yielded responses 33 and 54 percent higher than the minimum acceptable figure. The actual responses differed by less than 3 and 6 percent, respectively, from the predicted responses. Methods are described for defining a path of increasing response based on the minimum point and the response surfaces and for defining a set of values for the parameters in question, which result in increased response, A detailed explanation of the mathematical process used in this analysis is presented in the appendix for ease in computer programing the technique.

Jan 1, 1970

The object of this program was to design and build a self-contained system for remote monitoring of the atmosphere in mines. The system developed uses the mine pager phone line as the primary communication channel and also has the capability of using 208 Hz in the ELF band for wireless transmission through the earth. The depth for through-the-earth trans- mission is expected to be about 80 to 90 meters in high conductivity soil and is limited by the noise level in the ELF band-pass filters. The underground components of the TEM System are energized by mine power through a battery charger - storage battery power supply. In the event of mine power failure the battery capacity is more than sufficient for one week's operation with interrogations every four hours.

By M. M. Tilman

The Bureau of Mines conducted research to evaluate superplastic behavior in commercial magnesium-base alloys AZ6IA, ZK60A, ZW3, AZ3IB, ZWI, and an experimental Mg-12 pct Al alloy. Strain-rate sensitivity indices (m-values), maximum elongations, and effects of superplastic elongation on tensile properties were determined on fine-grained sheet. Inert-gas-pressure hemisphere-forming tests were conducted on selected sheet stock of the five alloys. Formability trials on AZ31B alloy sheet were conducted on industrial equipment for comparison with commercial superplastic forming of Zn-AI alloy. Closed-die-forming tests were performed on extruded ZK60A rod. All alloys exhibited well over 100-pct elongation, indicating superplasticity, at temperatures and strain rates near the maximum m-values. Tensile properties were generally reduced following 100-pct superplastic elongation, but not to an extent that would preclude use of the commercial alloys in the superplastically deformed condition. The potential for industrial superplastic forming of AZ31B sheet was indicated by hemisphere forming in the laboratory and substantiated in industrial forming trials.

Jan 1, 1982

By Thomas J. Fisher, Christopher C. Jobes, Edward F. Fries

This report (Software Safety 2.2) is the third in a nine-part series of recommendations addressing the functional safety of processor-controlled mining equipment. It is part of a risk-based system safety process encompassing hardware, software, humans, and the operating environment for the equipment’s life cycle. Figure 1 shows a safety framework containing these recommendations. The reports in this series address the various life cycle stages of inception, design, approval and certification, commissioning, operation, maintenance, and decommissioning. These recommendations were developed as a joint project between the National Institute for Occupational Safety and Health and the Mine Safety and Health Administration. They are intended or use by mining companies, original equipment manufacturers, and aftermarket suppliers to these mining companies. Users of these reports are expected to consider the set in total during the design cycle. • 1.0 Safety Introduction.—This is an introductory report for the general mining industry. It provides basic system/software safety concepts, discusses the need for mining to address the functional safety of programmable electronics (PE), and includes the benefits of implementing a system/software safety program. • 2.1 System Safety and 2.2 Software Safety.—These reports draw heavily from International Electrotechnical Commission (IEC) standard IEC 61508 [IEC 1998a,b,c,d,e,f,g] and other standards. The scope is “surface and underground safety-related mining systems employing embedded, networked, and non networked programmable electronics.” System safety seeks to design safety into all phases of the entire system. Software is a subsystem; thus, software safety is a part of the system’s safety .• 3.0 Safety File.—This report contains the documentation that demonstrates the level of safety built into the system and identifies limitations for the system’s use and operation. In essence, it is a “proof of safety” that the system and its operation meets the appropriate level of safety for the intended application. It starts from the beginning of the design, is maintained during the full lifecycle of the system, and provides administrative support for the safety program of the full system. • 4.0 Safety Assessment.—The independent assessment of the Safety File is addressed. It establishes consistent methods to determine the completeness and suitability of safety evidence and justifications. This assessment could be conducted by an independent third party. • 5.0 Safety Framework Guidance.—It is intended to supplement the safety framework reports with guidance providing users with additional information. The purpose is to assist users in applying the concepts presented. In other words, the safety framework is what needs to be don and the guidance is the how it can be done. The guidance information reinforces the concepts, describes various methodologies that can be used, and gives examples and references. It also gives information on the benefits and drawbacks of various methodologies. The guidance reports are not intended to promote a single methodology or to be an exhaustive treaty of the subject material. They provide information and references so that the user can more intelligently choose and implement the appropriate methodologies given the user’s application and capabilities. [ ]

Jan 9, 2001

By E. S. Burnett

The temperature entropy (T, S) chart? of thermodynamic properties of nitrogen herewith presented is a complete (1949) revision and a considerable extension of similar charts prepared by the author for use of the helium section of the Bureau of Mines about 25 years previously on the basis of inadequate data then obtaining. During the interval since that early effort, much experimentally determined information on nitrogen properties and behavior has been published, which now permits a more nearly accurate layout and more extensive charting of these relations.

Jan 1, 1950

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Jan 1, 2012

By A. L. Johnson

In this Bureau of Mines report, time-resolved infrared emission spectra and corresponding pressure and temperature histories are reported for large-scale propagations of CH4-air, CH4-air-N2, and CH4-air-CF3Br ignitions in a 12-ft-diam sphere. Absolute spectral radiances were obtained throughout combustion over the 1.6- to 4.8-gym range, and the radiance growth patterns for the H20 (2.5-µm) bands are presented as a function of methane stoichiometry and diluent concentration. Flame temperatures were determined from the C02-band emissions, which approximated unit emissivity shortly after ignition. Burning velocities are also given for some of the test-mixture compositions. Measured flame temperatures were in excellent to fair agreement with theoretical adiabatic values for the CH.-air and CH4-air-N2 mixtures; the best agreement was for the stoichiometric CH4-air mixture. The CH4-air-CF3Br mixtures with =2 pct CF3Br gave poor agreement with theory. The measured temperatures were significantly lower during the early stage of combustion; furthermore, the later stage of combustion was uninhibited and yielded unexpectedly high pressures. Supplemental data from a 2-ft-diam sphere at various initial pressures confirmed that the CF3Br inhibition effectiveness decreases with increased pressure. The possible effects of buoyancy, turbulence, and changing kinetics are discussed.

Jan 1, 1977

By H. V. Makar

A study was conducted by the Bureau of Mines to determine problems associated with the use of ferrous fractions from urban refuse as melting stock for steelmaking and to evaluate the resulting steel products. The study involved 50-pound ingots from laboratory melts and 50-pound ingots from 1-ton electric-arc-furnace melts. The 50 pound ingots from the laboratory melts and the arc-furnace melts were hot rolled to provide material for mechanical and corrosion testing. Results obtained in the study include the following: Most steels rolled successfully and exhibited acceptable surface and edge condition. Tensile strengths of the plain carbon steels were not significantly affected by copper up to concentrations of 0.65 pct and were not affected by tin content up to 0.16 pct. Yield strength increased with increasing copper and tin contents, and impact strength decreased with increasing tin content. Hardness increased slightly with increasing copper content. In general, properties of the steel produced were not measurably affected by charge composition (that is, melting stock), melting practice, or method of scrap preparation.

Jan 1, 1975

By J. D. Hadden

The Bureau of Mines conducted drilling studies in the Pocahontas No. 3, the Pittsburgh, and a western coalbed to establish the gas migration characteristics for each. Gas pressures in the Pittsburgh coalbed were about 260 lb/in2 and in excess of 550 lb/in2 in the Pocahontas No. 3. Caving in drill holes prevented pressure measurements in the western coalbed. The Pittsburgh coalbed contained intersecting "clay veins" which formed gas pressure cells. Although these geological features hamper mining, they can be used to control the flow of methane into a mine working. Methane control techniques are proposed for the Pittsburgh and Pocahontas No. 3 coalbeds.

Jan 1, 1969

By A. C. Fieldner

The Bureau of Mines has recently conducted a study of results obtained in analyzing similar samples of coal and coke by 25 laboratories throughout then country, in comparison with results obtained in the Bureau's coal laboratory at Pittsburgh. The purpose of this work was primarily to obtain a comparison of the methods of coal analysis used by the laboratories of the American Gas Association. Therefore, four standard samples of coal end one of coke ware prepared in the Bureau of Mines coal laboratory at Pittsburgh, and portions sent to each laboratory. At the same time, a like number of standard samples were submitted to 12 commercial laboratories rot affiliated with the Association, for the purpose of comparing their analyses with the results is obtained by the U. S. Bureau of Mines and the American Gas Association. Tire comparison is based on the average of 24 analyses by the Bureau of Mines on each kind of coal, and the accompanying curves show the deviation from this average analysis, together with deviations from the check limits of the American Society for Testing Materials.

Jan 1, 1923

By Henry G. Dorsett

Dust explosion data obtained in laboratory tests by the Bureau of Mines are presented for 73 chemical compounds and mixtures, 29 drugs, 27 dyes, and 46 pesticides. Information is given on ignition temperatures of cloud and layer, minimum igniting energy, minimum explosive concentration, percent of inert dust required to prevent flame propagation, limiting oxygen concentration in the atmosphere to prevent ignition, and pressures and rates of pressure rise at dust concentrations of 0.1, 0.2, 0.5, 1.0, and 2.0 ounces per cubic foot. Explosibility indexes are computed where data are available to permit comparison of the relative explosion hazard. Variations of explosibility parameters with chemical composition are discussed. General means for minimizing the dust explosion hazard are reviewed.

Jan 1, 1968

By Paul W. Jeran

Subsidence was monitored by the U.S. Bureau of Mines over the ends of longwall panels operating in the Pittsburgh, Kittanning, and No. 2 Gas Coalbeds of the northern Appalachian Coal Basin. The final subsidence over the finishing ends of three panels in the Pittsburgh Coalbed are compared with the subsidence measured over the rib at these panels. The characteristics of subsidence are different. At Mine A, data over the start of a longwall panel shows similar characteristics to the subsidence measured over the rib. Subsidence over the fmishing ends of panels in the Kittanning and No.2 Gas Coalbeds are also different from the subsidence over the rib. The use of a subsidence prediction model based on data gathered over the rib of a panel will not yield accurate results if it is applied to the finishing end of a longwall panel. Acceptable results may be obtained along the centerline over the starting end of a panel.

Jan 1, 1991

By C. V. Davis

In the lnvestlg::ìt1on of mAthods for aSS8.7ing platin",. conducted by the Bureau ot MinAs, reoent experiments have d~velopad tha~ with ce..tain orei, especially when thr, quantity Of platinum 1s eonlidarablfl, nit'!le acid w111 not etfßct a iepard-Han of platinum and pa11adium. 'lhe following m;lthod has been found to be accurate and to reiu1 t in a complete S''lun''ation of' th~3:l metals. It is therefo 1" '!eeommei:ed that 1 t ba followed rath::r- than the method of separation with nitrio acid, givèn in Technical Pape'! 270.* At line 22, pagi 14, of that paper, bAglnnlng with ~tarm th,~ metals '.'ith dilute¡ nitrio acid," strikE out the rest of the paragraph, and substttutt~ the pro_t cedure g1 ven below. ?lunder and Thuringer.. have developed mnt¡iods for th"i sflparation of palladium from all the platinum metals exoept platinum bj m ,ans of dlmethy- 19lyoxlme. They state that the~ is no action for several hours if an excess of dimeth¡lglyoxime is added to an aqueous solution of ohloroplatinic acid in the cold, alio that only on boiling is the platinum pTecipi ated ¡~d than only PST't of the platinum i srenoved from the sUut1on. They found that palladium 1s p~ecipi tated quati tat! vely in the oold as (CaH 4N40 Pd) which is insoluble tn water, dilute hydroohlorio acid, dilute acetIc aofd or in 50~ ethyl alcbhol. All of their pT'90ipi tations we~p Carl". ied out ~hile the solutions were being heated. This caused a pal"tia~recipltation of the platinum along wi th the

May 1, 1922

By L. J. Prosser, G. Esterhuizen, A. T. Iannacchione

The potential for roof fails in underground mines remains a clear and present danger for mine workers An investigation of ground conditions in nearly 50 percent of the nation’s underground stone mines fold that the slate of roof stability is primarily determined in a limited and subjective manner. These large-opening mines with roof heights typically 7 m (23 ft) or more, make physical observation difficult. Although some mines use monitoring techniques to gain additional information an roof stability, this practice is usually short term and localized to address ground conditions in a particular section or part of the mine. A roof-fall hazard-assessment techniques was development based on engineering judgment acquired from extensive underground stone mine experience and on exanimation of the related literature. This technique utilizes observational processes to determine roof fall likelihood Case-study scenarios offer a realistic picture of model implementation. Providing the mine level decision-maker with an accurate assessment tool to ascertain the level of ground fall hazards is expected to reduce mint worker injuries and fatalities Moreover; the presences of danger can be overcome with a clear picture of quantified ground conditions.

By John A. Breslin

Three scale models of coal mine entries and mining machines were constructed by the Bureau of Mines to study the effects of ventilation parameters on dust concentrations where mining personnel would be working. A one-fifth-scale model of a coal mine entry with a drum-type continuous-mining machine and a one-sixth-scale model of an entry with a twin-borer-type machine were used as well as a one-fifth-scale model of a longwall face with a double-drum shearer. Methane was used as a tracer gas to simulate respirable dust in the models. The distance of the end of the brattice or tubing from the face was found to be more important than the airflow rate for the drum-type machine. Dust reductions greater than 90 pct were shown to be possible with a secondary ventilation system used with the twin borer and a dust collector mounted on the longwall shearer. Cutting-head speed had a significant effect on concentrations at typical positions of miners with the drum-type machine and longwall shearer but not for the twin borer.

Jan 1, 1976