Sample preparation, the key to successfully use x-ray techniques in exploration and mining environment

X-ray systems for elemental and phase determination have become more expensive and easier to use. In this sense, although the new systems offer more functions in the software for matrix correction, preconfigured optimized measurement parameters as well as wizards for method development, they will not perform for the applications if not used with the right sample preparation technique. Experience in this sector is not widely shared since it is a more empirical trial and error approach unique to the sample preparation equipment used. This paper outlined 3 case studies, where the sample preparation was crucial in the adaptation of the X-ray technique and it also illustrated that an analytical solution is not complete without the sample preparation, which ultimately governs the accuracy of reference materials and unknowns used. Comparing the necessary sample for XRF with the one used for ICP analysis clearly shows the time and cost savings.