Refractory Lining Design for Pressure Oxidation Autoclaves

"This paper presents the technique and benefits of the finite element approach for designing the refractory lining in pressure oxidation autoclaves. One-dimensional equations are used to develop an initial refractory design. ANSYS Parametric Design Language (APDL) scripts are then used to build and analyse a more accurate three-dimensional finite element model to verify the refractory thickness, determine weld overlay requirements, and assess mechanical stability. The APDL scripts provide a cost effective means to quickly evaluate various boundary conditions and multiple designs to determine the optimal lining configuration and nozzle layout.INTRODUCTIONNew ore processing facilities demand increased capacity, requiring hydrometallurgy processes that have larger reactor vessels operating at higher pressure and temperature. Many pressure hydrometallurgy operations require vessels with an impermeable membrane and one or more courses of refractory or ceramic brick. The membrane provides corrosion protection for the vessel shell and the brick provides thermal protection for the membrane. Designing a refractory lining with an economic service life as a thermal barrier requires the refractory to be erosion resistant, chemically compatible with the process fluid, and mechanically stable. A fundamental understanding of the factors affecting the lining system is essential as designs move further away from the industry’s experience base.During basic engineering the refractory lining design is developed using one dimensional cylindrical conduction equations for heat transfer and classical hoop stress-strain relationships for determining mechanical stability. The results of the thermal calculations specify the refractory thickness that should prevent the membrane temperature from exceeding the design limit. Mechanical stability of the lining is determined by examining the sensitivity of lining stability with respect to various parameters. There are three criteria that must be satisfied to conclude mechanical lining stability:"